CN114804627A - Reduction-sintering phase-separation-induced palace yellow croaker seed crystal glaze and preparation method thereof - Google Patents
Reduction-sintering phase-separation-induced palace yellow croaker seed crystal glaze and preparation method thereof Download PDFInfo
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- 239000013078 crystal Substances 0.000 title claims abstract description 65
- 238000005191 phase separation Methods 0.000 title claims abstract description 33
- 241001596950 Larimichthys crocea Species 0.000 title claims abstract description 20
- 238000005245 sintering Methods 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 238000010304 firing Methods 0.000 claims abstract description 24
- 239000000919 ceramic Substances 0.000 claims abstract description 17
- 239000008139 complexing agent Substances 0.000 claims abstract description 16
- 239000007791 liquid phase Substances 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims description 20
- 238000000498 ball milling Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 13
- 238000004040 coloring Methods 0.000 claims description 12
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000010453 quartz Substances 0.000 claims description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 5
- 230000002829 reductive effect Effects 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 229910015902 Bi 2 O 3 Inorganic materials 0.000 claims description 4
- 229910021532 Calcite Inorganic materials 0.000 claims description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000001506 calcium phosphate Substances 0.000 claims description 4
- 229910000389 calcium phosphate Inorganic materials 0.000 claims description 4
- 235000011010 calcium phosphates Nutrition 0.000 claims description 4
- 239000011363 dried mixture Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 239000010433 feldspar Substances 0.000 claims description 4
- 230000001939 inductive effect Effects 0.000 claims description 4
- 229910052742 iron Inorganic materials 0.000 claims description 4
- 229910052744 lithium Inorganic materials 0.000 claims description 4
- 239000002689 soil Substances 0.000 claims description 4
- 239000000454 talc Substances 0.000 claims description 4
- 229910052623 talc Inorganic materials 0.000 claims description 4
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 2
- 230000006698 induction Effects 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 238000003786 synthesis reaction Methods 0.000 claims description 2
- 241000251468 Actinopterygii Species 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 21
- 238000002425 crystallisation Methods 0.000 abstract description 6
- 230000008025 crystallization Effects 0.000 abstract description 6
- 239000011521 glass Substances 0.000 abstract description 6
- 239000007788 liquid Substances 0.000 abstract description 4
- 238000000926 separation method Methods 0.000 abstract description 4
- 230000006641 stabilisation Effects 0.000 abstract description 3
- 238000011105 stabilization Methods 0.000 abstract description 3
- 229910052723 transition metal Inorganic materials 0.000 abstract description 3
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 238000005034 decoration Methods 0.000 description 4
- 239000006103 coloring component Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000006722 reduction reaction Methods 0.000 description 1
- OJYBUGUSFDKJEX-UHFFFAOYSA-N tungsten zirconium Chemical compound [Zr].[W].[W] OJYBUGUSFDKJEX-UHFFFAOYSA-N 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention relates to a ceramic glaze, in particular to a reduction-sintering phase-separation-induced palace yellow croaker crystal fancy glaze and a preparation method thereof. A reduction-sintering phase-separation-induced palace yellow croaker seed crystal fancy glaze comprises 15% -25% of a color generation crystal nucleus complexing agent and 75% -85% of a liquid phase separation functional environment group. The invention provides a reduction-firing phase-separation-induced palace yellow piscicultural crystal fancy glaze, which is characterized in that the compound stabilization preset treatment of a color generation crystal nucleus of a transition metal element and the selective enrichment effect of a glaze glass liquid separation isolated relative crystallization color generation component are adopted, so that the stable and controllable realization of a glazed palace yellow piscicultural stereoscopic crystal fancy effect under the reduction firing condition is realized, and a novel crystal artistic glaze which can be fired under the conventional reduction condition is obtained.
Description
Technical Field
The invention relates to a ceramic glaze, in particular to a reduction-sintering phase-separation-induced palace yellow croaker crystal fancy glaze and a preparation method thereof.
Background
According to the search, at present, no related technical content report of reduction, sintering and phase separation induced palace yellow croaker seed crystal fancy glaze exists at home and abroad. As an adjacent crystal glaze technology, the appearance effect of the crystal glaze is realized by a harsh process of quenching and long-time heat preservation in the sintering process, and even if the appearance effect is realized by the harsh process, the controllability of the decoration effect is still poor, so that the crystal glaze can not be applied to the stable production of mass products. Further, the desired effect cannot be obtained under the severe atmosphere conditions of the reduction firing.
For example, the crystal grain and phase-splitting precursor crystal fancy glaze disclosed in chinese patent CN102887729B, although the crystal grain effect becomes controllable and easy to realize by applying the dual precursor function of the crystal grain presetting and the phase-splitting technology of the base glaze, and the harsh firing requirement is largely avoided, the crystal grain shape and color generation effect peculiar to the royal yellow piscicultural crystal are not present in the appearance effect, and the fancy glaze cannot be fired under the reducing condition. Therefore, the existing ceramic glaze technology is essentially different from the reduction firing phase separation induction palace yellow croaker crystal fancy glaze of the invention in both artistic effect and formation mechanism. So far, under the condition of reduction firing, no ideal crystal flower artistic glaze exists, and further development of reduction firing artistic ceramic products is restricted.
Disclosure of Invention
In order to solve the problems, the invention provides a method for stably pre-treating the coloring crystal nucleus of a transition element in an integrated and stable manner, separating two glaze glass liquids, isolating, relatively crystallizing and selectively enriching coloring components, so that the palace yellow roe-shaped three-dimensional crystal flower effect of a glaze surface can be stably and controllably realized under the condition of reduction firing, a novel crystal artistic glaze effect which can be fired under the conventional reduction condition is obtained, and the appearance of the glaze is noble and honorable. The artistic space and the added value of the ceramic product are expanded to a greater extent. The specific technical scheme is as follows:
a reduction-sintering phase-separation-induced palace yellow croaker seed crystal fancy glaze comprises 15% -25% of a color generation crystal nucleus complexing agent and 75% -85% of a liquid phase separation functional environment group.
Preferably, the color generation crystal nucleus complexing agent consists of the following raw materials in parts by weight: WO 3 ：18-22％、Bi 2 O 3 ：10-13％、TiO 2 ：20-30％、Fe 2 O 3 ：12-18％、MgCO 3 ：8-12％、ZrO 2 : 10-15%, quartz: 7 to 10 percent.
Preferably, the liquid phase separation functional environment group consists ofThe raw materials comprise by weight: lithium feldspar: 38-44%, quartz: 10-14%, Suzhou soil: 6-10% of BaCO 3 ：2-6％、SrCO 3 : 5-6%, calcium phosphate: 6-10% of TiO 2 : 3-5%, calcite: 5-8%, talc: 10 to 16 percent.
A preparation method of a reduction-firing phase-separation-induced palace yellow croaker seed crystal fancy glaze comprises the following steps:
preparation of a coloring crystal nucleus complexing agent: respectively weighing the raw materials of the color-developing crystal nucleus complexing agent, adding the raw materials into a ball mill, performing ball milling and mixing according to the proportion of 1:0.8 of material water, sieving the mixture by a 60-mesh sieve, drying the mixture, calcining the dried mixture in a kiln at 1100 ℃, performing stable synthesis, and performing ball milling on the mixture by a 80-mesh sieve for later use.
Preparing a liquid phase separation functional environment group and finished glaze: respectively weighing the raw materials of the liquid phase separation functional environment groups, adding the raw materials into a ball mill, carrying out ball milling with the ratio of material water to be 1:0.8, adding the coloring crystal nucleus complexing agent in proportion 2 hours before ball discharging, carrying out ball milling, sieving with a 100-mesh sieve, and adjusting the concentration to be 50-55 Baume for later use.
A firing method for reducing, firing and phase-separating and inducing palace yellow croaker crystal glaze adopts a glaze dipping or glaze spraying method to decorate the reducing, firing and phase-separating and inducing palace yellow croaker crystal glaze on the surface of a ceramic blank, and after drying, reducing and firing at 1260 degrees and 1280 degrees.
Compared with the prior art, the invention has the following beneficial effects:
the invention provides a reduction-firing phase-separation-induced palace yellow piscicultural crystal fancy glaze, which is characterized in that the compound stabilization preset treatment of a color generation crystal nucleus of a transition metal element and the selective enrichment effect of a glaze glass liquid separation isolated relative crystallization color generation component are adopted, so that the stable and controllable realization of a glazed palace yellow piscicultural stereoscopic crystal fancy effect under the reduction firing condition is realized, and a novel crystal artistic glaze which can be fired under the conventional reduction condition is obtained.
The mechanism is as follows: the coloring and crystal nucleus components of the transition metal elements are preset in a composite stable state through the tungsten-zirconium crystal, so that the coloring and crystal seeding components can also play a role stably and controllably under the common reduction sintering condition, and the bottleneck interference problem of the reduction atmosphere on crystallization and coloring is fundamentally solved; the unique glaze glass composition enables the two-liquid separation zone to be isolated and relatively generate color and generate a selective enrichment effect on the crystallization group components, thereby enabling the glaze surface to have a unique palace yellow roe-shaped three-dimensional crystal pattern effect, highlighting the noble and honorable smell of emperor and filling the blank of reducing and sintering the high-grade crystal glaze.
The product of the invention is a high-grade novel artistic glaze for ceramic decoration. When in use, the finished glaze can be decorated on the surface of a ceramic blank by adopting a glaze dipping or glaze spraying method, and is reduced and sintered at 1260 and 1280 ℃ in a shuttle-type gas kiln after being dried. The product of the invention has conventional preparation process, is suitable for decoration of high-grade artistic ceramics and daily ceramics, has novel and unique decorative effect, and is a novel artistic glaze material for ceramic decoration with a special formation mechanism.
Drawings
FIG. 1 is a schematic illustration of reduction firing phase separation induced firing of palatine yellow croaker seeded fancy glaze to orange;
FIG. 2 is a schematic view of reduction firing phase separation induced firing of palatine yellow croaker seed crystal glaze into golden yellow.
Detailed Description
The invention will now be further described with reference to the accompanying drawings.
The invention provides a method for realizing the integration, stabilization, presetting treatment, isolation, relative crystallization and selective enrichment effect of coloring components of a glaze glass by adopting transition element coloring crystal nucleus, and the separation, isolation, relative crystallization and selective enrichment effect of coloring components of glaze glass, so that the palace yellow roe-shaped three-dimensional crystal flower effect of a glaze surface can be stably and controllably realized under the condition of reduction firing, a novel crystal artistic glaze effect which can be fired under the conventional reduction condition is obtained, and the appearance of the glaze is noble and honorable. The artistic space and the added value of the ceramic product are expanded to a greater extent. The invention of the ceramic artistic glaze opens up a new way for the development of high-grade ceramic artistic glaze, and has the significance of methodology.
Example one
As shown in fig. 1, the reduction firing phase separation induces the palatine yellow croaker seed crystal glaze, wherein the color is a yellow color (orange) with a warm color system:
content of the coloring crystal nucleus complexing agent:
liquid phase separation functional environment group and finished product glaze content:
color generation crystal nucleus complexing agent: WO 3 ：22％、Bi 2 O 3 ：13％、TiO 2 ：21％、Fe 2 O 3 ：18％、MgCO 3 ：8％、ZrO 2 : 9% and 9% of quartz.
The raw materials are respectively weighed and then added into a ball mill, the raw materials and water are mixed in a ball milling mode according to the proportion of 1:0.8, the mixture is sieved by a 60-mesh sieve, the dried mixture is calcined in a kiln at 1100 ℃, the mixture is synthesized in a stable state, and the mixture is ball-milled by 80 meshes for later use.
Liquid phase separation of functional environment groups and finished glaze: lithium feldspar: 38%, quartz: 12%, suzhou soil: 6% of BaCO 3 ：5％、SrCO 3 : 6 percent of calcium phosphate, 8 percent of TiO 2 : 3% of calcite: 8%, talc: 14 percent. The raw materials are respectively weighed and then added into a ball mill, the ball milling is carried out by using feed water in a ratio of 1:0.8, and the weight ratio of the raw materials to the feed water is 75: adding a coloring crystal nucleus complexing agent in a proportion of 25, ball-milling, sieving with a 100-mesh sieve, and adjusting the concentration to 50-55 Baume degrees for later use.
The finished glaze is decorated on the surface of a ceramic body by adopting a glaze dipping or spraying method, and is reduced and sintered at 1260 plus 1280 ℃ in a shuttle gas kiln after being dried.
Example two
As shown in fig. 2, the reduction firing phase separation induces the palatine yellow croaker seed crystal glaze, wherein the color is a yellow color (golden yellow) with a cool tone:
color generation crystal nucleus complexing agent:
WO 3 ：18％、Bi 2 O 3 ：10％、TiO 2 ：28％、Fe 2 O 3 ：12％、MgCO 3 ：11％、ZrO 2 : 11% and 10% of quartz. The raw materials are respectively weighed and then added into a ball mill, the raw materials are mixed in a ball mill according to the ratio of 1:0.8, the mixture is sieved by a 60-mesh sieve, the dried mixture is calcined in a kiln at 1100 ℃, the mixture is synthesized in a stable state, and the mixture is ball-milled by a 80-mesh sieve for later use.
Liquid phase separation of functional environment groups and finished glaze: lithium feldspar: 44. quartz: 14%, suzhou soil: 8% of BaCO 3 ：2％、SrCO 3 : 5%, calcium phosphate: 6% TiO 2 : 5%, calcite: 5%, talc: 11 percent.
Respectively weighing the raw materials, adding the raw materials into a ball mill, carrying out ball milling with the material water in a ratio of 1:0.8, and carrying out ball milling 2 hours before ball discharging according to a ratio of 86: adding a coloring crystal nucleus complexing agent in a proportion of 14, ball-milling, sieving by a 100-mesh sieve, and adjusting the concentration to be 50-55 Baume degrees for later use.
The finished glaze is decorated on the surface of a ceramic body by adopting a glaze dipping or spraying method, and is reduced and sintered at 1260 plus 1280 ℃ in a shuttle gas kiln after being dried.
The technical principle of the present invention is described above in connection with specific embodiments. The description is made for the purpose of illustrating the principles of the invention and should not be construed in any way as limiting the scope of the invention. Based on the explanations herein, those skilled in the art will be able to conceive of other embodiments of the present invention without inventive step, which shall fall within the scope of the appended claims.
Claims (5)
1. A reduction-sintering phase-separation-induced palace yellow croaker seed crystal fancy glaze is characterized by comprising 15% -25% of a color generation crystal nucleus complexing agent and 75% -85% of a liquid phase separation functional environment group.
2. The reductive sintering phase separation inducing palace yellow croaker seed crystal fancy glaze according to claim 1, wherein:
the color generation crystal nucleus complexing agent consists of the following raw materials in parts by weight:
WO 3 ：18-22％、Bi 2 O 3 ：10-13％、TiO 2 ：20-30％、Fe 2 O 3 ：12-18％、MgCO 3 ：8-12％、ZrO 2 : 10-15%, quartz: 7 to 10 percent.
3. The reductive sintering phase separation inducing palace yellow croaker seed crystal fancy glaze according to claim 1, wherein:
the liquid phase separation functional environment group is composed of the following raw materials by weight:
lithium feldspar: 38 to 44 percentQuartz: 10-14%, Suzhou soil: 6-10% of BaCO 3 ：2-6％、SrCO 3 : 5-6%, calcium phosphate: 6-10% of TiO 2 : 3-5%, calcite: 5-8%, talc: 10 to 16 percent.
4. A preparation method of a reduction-sintering phase-separation-induced palace yellow croaker seed crystal fancy glaze is characterized by comprising the following steps:
preparation of a coloring crystal nucleus complexing agent: respectively weighing the raw materials of the color-developing crystal nucleus complexing agent, adding the raw materials into a ball mill, performing ball milling and mixing according to the proportion of 1:0.8 of material water, sieving the mixture by a 60-mesh sieve, drying the mixture, calcining the dried mixture in a kiln at 1100 ℃, performing stable synthesis, and performing ball milling on the mixture by a 80-mesh sieve for later use.
Preparing a liquid phase separation functional environment group and finished glaze: respectively weighing the raw materials of the liquid phase separation functional environment groups, adding the raw materials into a ball mill, carrying out ball milling with the ratio of material water to be 1:0.8, adding the coloring crystal nucleus complexing agent in proportion 2 hours before ball discharging, carrying out ball milling, sieving with a 100-mesh sieve, and adjusting the concentration to be 50-55 Baume for later use.
5. A method for sintering grain crystal glaze of palace yellow croaker by reduction sintering and phase separation induction is characterized in that,
adopting a glaze dipping or glaze spraying method to decorate the phase separation induced palace yellow fish crystal fancy glaze on the surface of the ceramic body by reduction firing, drying and reducing firing at 1260-1280 ℃.
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