CN114796060A - White-to-black essence and preparation method thereof - Google Patents

White-to-black essence and preparation method thereof Download PDF

Info

Publication number
CN114796060A
CN114796060A CN202210599936.5A CN202210599936A CN114796060A CN 114796060 A CN114796060 A CN 114796060A CN 202210599936 A CN202210599936 A CN 202210599936A CN 114796060 A CN114796060 A CN 114796060A
Authority
CN
China
Prior art keywords
extract
hair
black
white
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202210599936.5A
Other languages
Chinese (zh)
Inventor
刘惠安
刘勇
郭凯文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuxiang Biotechnology Shanghai Co ltd
Original Assignee
Fuxiang Biotechnology Shanghai Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuxiang Biotechnology Shanghai Co ltd filed Critical Fuxiang Biotechnology Shanghai Co ltd
Priority to CN202210599936.5A priority Critical patent/CN114796060A/en
Publication of CN114796060A publication Critical patent/CN114796060A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • A61K8/9761Cupressaceae [Cypress family], e.g. juniper or cypress
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The application relates to the field of cosmetics, and particularly relates to a white-to-black essence and a preparation method thereof. The white-to-black essence comprises the following raw materials in parts by weight: polygonum multiflorum root extract, ganoderma atrum extract, black mulberry extract, pseudo-ginseng root extract, black sesame extract, artemisia angustifolia leaf/stem extract, saposhnikovia divaricata root extract, artemisia argyi leaf extract, cnidium monnieri seed extract, rosemary extract, biota orientalis leaf extract, ginger root extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract. It can effectively improve white hair, hair combing performance, hair glossiness, and hair care. The preparation method is simple, and the prepared essence has high content of effective components.

Description

White-to-black essence and preparation method thereof
Technical Field
The application relates to the field of cosmetics, and particularly relates to a white-to-black essence and a preparation method thereof.
Background
White hair refers to hair that is totally or partially whitened. Under normal conditions, the inside of the hair papilla is rich in blood vessels, so that sufficient nutrition is provided for the hair papilla and hair bulb, and melanin granules are smoothly synthesized. When melanin granules are inhibited from forming on papillae or hair bulb, or formed, they are not transported into hair by some factor, and melanin granules in medulla and cortex of hair are reduced or eliminated, white hair appears. Wherein the reduction of the amount of tyrosinase is one of the pathological mechanisms of white hair.
Although white hair does not threaten life, the external appearance is greatly influenced, particularly, at present, the work and life pressure of people is great, people with early white hair are increased, and the mental pressure and the psychological burden of the people are increased.
White hair can be dyed black through the hair dye, but the hair dye contains benzene compounds, so that the hair quality can be damaged after long-term hair dyeing, certain influence can be caused to the body, and the hair dye can treat the symptoms and the root causes.
Disclosure of Invention
The application aims to provide a white-to-black essence which can effectively improve white hair and protect and nourish hair.
Another object of the present application is to provide a method for preparing the essence for turning white into black, which is simple and has high content of effective components.
The technical problem to be solved by the application is solved by adopting the following technical scheme.
On one hand, the embodiment of the application provides a white-to-black essence which comprises the following raw materials in parts by weight: 0.05-5 parts of polygonum multiflorum root extract, 0.1-3 parts of ganoderma atrum extract, 0.1-1 part of black mulberry fruit extract, 0.05-1.5 parts of pseudo-ginseng root extract, 0.01-1.0 part of black sesame extract, 0.05-0.5 part of southernwood leaf/stem extract, 0.05-0.5 part of divaricate saposhnikovia root extract, 0.05-1.0 part of argy wormwood leaf extract, 0.01-0.5 part of cnidium monnieri seed extract, 0.05-5 parts of rosemary extract, 0.05-2 parts of biota orientalis leaf extract, 0.05-2.0 parts of ginger root extract, 0.001-0.3 part of cinnamon bark extract, 0.001-0.5 part of sophora flavescens root extract, 0.001-1.0 part of licorice root extract and 0.001-1.0 part of grapefruit peel extract.
On the other hand, the embodiment of the application provides a preparation method of a white-to-black essence, which comprises the following steps: step S1, feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing; step S2, raw material dissolution: starting steam, heating to 90 +/-2 ℃, keeping the stirring speed at 15-25RPM, and keeping the temperature for 25-35 min; step S3, cooling to 48-52 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract; stirring; step S4, cooling to 42-45 ℃, adding capryl hydroximic acid and preservative, and stirring; and step S5, cooling to 38-40 ℃, filtering and discharging.
Compared with the prior art, the embodiment of the application has at least the following advantages or beneficial effects:
1. the application provides a white-to-black essence which comprises a plurality of plant extracts beneficial to hair, wherein the polygonum multiflorum root extract, the black mulberry extract, the folium artemisiae argyi extract, the rosemary extract, the ginger root extract, the cinnamon extract and the grapefruit fruit extract can improve the blood circulation of scalp, prevent alopecia and grow hair; the ganoderma atrum extract, pseudo-ginseng root extract, black sesame extract and radix sileris extract can activate tyrosinase activity, promote melanin generation, resist oxidation, remove free radicals and resist aging; the southernwood leaf/stem extract, the cnidium monnieri seed extract, the rosemary extract, the sophora flavescens root extract and the licorice root extract can relieve the scalp, relieve itching and sterilize; the folium Platycladi extract can improve scalp oil secretion, repair hair follicle, and improve hair loss. The plant extracts can fully exert respective drug effects, and can effectively promote scalp blood circulation, promote melanogenesis and promote white hair to turn black. In addition, the hair care shampoo can resist oxidation, inflammation and aging, effectively improve the hair combing performance and the hair glossiness, care the hair and nourish the hair, and has good long-term use effect.
2. The application also provides a preparation method of the white-to-black essence, the preparation method is simple, and the prepared essence is high in effective component content.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings that are required to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present application and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained from the drawings without inventive effort.
Fig. 1 is a hair wet combing curve detection result of white-to-black essence provided in experimental example 2 of the present application.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present application clearer, the technical solutions of the embodiments of the present application will be clearly and completely described below. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
It should be noted that the embodiments and features of the embodiments in the present application may be combined with each other without conflict. The present application will be described in detail below with reference to specific examples.
The white-to-black essence comprises the following raw materials in parts by weight: 0.05-5 parts of polygonum multiflorum root extract, 0.1-3 parts of ganoderma atrum extract, 0.1-1 part of black mulberry fruit extract, 0.05-1.5 parts of pseudo-ginseng root extract, 0.01-1.0 part of black sesame extract, 0.05-0.5 part of southernwood leaf/stem extract, 0.05-0.5 part of divaricate saposhnikovia root extract, 0.05-1.0 part of argy wormwood leaf extract, 0.01-0.5 part of cnidium monnieri seed extract, 0.05-5 parts of rosemary extract, 0.05-2 parts of biota orientalis leaf extract, 0.05-2.0 parts of ginger root extract, 0.001-0.3 part of cinnamon bark extract, 0.001-0.5 part of kushen root extract, 0.001-1.0 part of licorice root extract and 0.001-1.0 part of grapefruit peel extract.
The polygonum multiflorum root extract has the effects of tonifying essence and blood, blackening beard and hair, strengthening bones and muscles and tonifying liver and kidney, has a good hematopoietic function, can promote blood circulation, can supplement nutrition for hair follicles of scalp so as to nourish hair, enables the hair to be tough and not easy to break, is rich in luster, can promote hair growth, and can increase hair density.
Pharmacological research shows that ganoderma lucidum polysaccharide can play a role in growing hair by promoting DNA synthesis of skin and accessory tissues thereof. Ganoderma has effects of resisting oxidation, scavenging free radicals, and delaying aging. Alopecia and white hair are all manifestations of aging, so the effects of ganoderma lucidum on promoting hair growth, alleviating alopecia caused by aging and blackening white hair are probably related to the effects of ganoderma lucidum on resisting oxidation and scavenging free radicals.
The mulberry extract has the effects of increasing blood supply of skin (including scalp) and improving blood circulation, and has certain nutrition and health care effects on hair. The black mulberry can effectively improve scalp blood circulation, prevent alopecia and promote hair growth.
Notoginseng radix extract contains saponins, small amount of flavonoid glycoside, and alkaloid, and has hemostatic, tonic, and immunity enhancing effects. The notoginsenoside can reduce the formation of free radicals, inhibit lipid peroxidation in vivo and activate SOD activity, thereby accelerating the removal of free radicals and having anti-aging effect.
The black sesame extract contains sesamin, which can remarkably enhance the melanogenesis in B16 melanoma cells, activate cell proliferation, melanogenesis and tyrosinase activity, and promote the transcription of melanogenesis-related genes. The black sesame can increase hair luster, promote hair growth and regrowth, and has effects of resisting dandruff, resisting dryness, and deeply regulating.
The southernwood leaf/stem extract has obvious effect of relieving skin, and can also rapidly relieve itching and red swelling. Effectively inhibit fungi on the surface layer of the skin and regulate the immunity of the skin.
The radix Saposhnikoviae extract has effects in resisting aging, relieving exterior syndrome, dispelling cold, eliminating dampness, and relieving pain. Ledebouriella root contains many coumarin compounds and chromone compounds. Has effects in scavenging free radicals, and can be used as antioxidant; it also has antibacterial and anti-inflammatory effects.
The folium Artemisiae Argyi extract is a dark brown powdery substance obtained by extracting herba Artemisiae Scopariae with ethanol as extraction solvent under reflux and heating for several times, and removing residue and water. The folium Artemisiae Argyi extract contains various natural medicinal components, and can be absorbed by human body to enhance antiallergic ability, reduce various allergic diseases, and resist bacteria and virus. The folium Artemisiae Argyi extract contains volatile oil of natural chemical components, and also contains flavonoid or natural polysaccharide, and can promote scalp metabolism after being absorbed by scalp.
The cnidium monnieri (L.) kurz seed extract is derived from fruit of cnidium monnieri (L.) kurz belonging to Umbelliferae. The fructus Cnidii contains several coumarins as main effective components, and has high osthole content. Cnidium fruit is warm in nature, pungent and bitter in flavor and slightly toxic. Externally used for eliminating dampness, killing parasites and relieving itching, internally taken for warming kidney and strengthening yang, dispelling wind and eliminating dampness.
The rosemary extract mainly comprises rosmanol, carnosol and carnosic acid, has strong antioxidant activity, has strong astringent effect, and can promote scalp blood circulation, condition greasy skin, improve alopecia and reduce dandruff. The rosmarinic acid also has strong anti-inflammatory activity, and can protect skin, strengthen skin, and promote skin function.
The folium Platycladi extract has effects of cooling blood, stopping bleeding, promoting hair growth, and blackening hair. Is helpful for improving the exuberant secretion of grease, avoiding the reproduction and breeding of bacteria, preventing hair follicle necrosis, repairing hair follicle, improving hair loss and preventing alopecia.
The effective component of the ginger root extract is gingerol, which can enhance the activity of skin and activate skin, and has the functions of oxidation resistance and anti-aging; can also promote hair growth, and can be used as hair promoter; it also has moisture keeping and odor inhibiting effects.
The cinnamon extract can promote blood circulation, repair easily-injured capillary vessels, and improve the flow of the capillary vessels, so that the activity of hair follicle cells is promoted, more nutrition is provided for the scalp, and hair growth is promoted.
The extract of the root of Sophora flavescens Aiton has the main active ingredients of various alkaloids, has the effects of resisting bacteria, diminishing inflammation, relieving itching and regulating water and oil balance, and can be used as an antibacterial agent, an anti-inflammatory agent, a skin anti-aging agent, a weight-losing agent and a humectant.
The licorice root extract can improve dryness, reduce desquamation and restore skin softness, and also has anti-irritant, anti-inflammatory and skin soothing effects.
The grapefruit fruit extract mainly serves as an odor inhibitor and a skin conditioner in cosmetics and skin care products, has a good inhibitory effect on uricase and has a broad-spectrum antibacterial property; has strong eliminating effect on free radicals, and has antiaging and antioxidant effects; has the effects of activating luciferase and resisting inflammation; it has effects in promoting cholesterol secretion, and increasing skin softness; has effect in promoting hyaluronic acid secretion, and can be used as humectant.
In conclusion, the application provides a white-to-black essence which comprises a plurality of plant extracts beneficial to hair, wherein the polygonum multiflorum root extract, the black mulberry fruit extract, the artemisia leaf extract, the rosemary extract, the ginger root extract, the cinnamon extract and the grapefruit fruit extract can improve the blood circulation of scalp, prevent alopecia and promote hair growth; the ganoderma atrum extract, pseudo-ginseng root extract, black sesame extract and radix sileris extract can activate tyrosinase activity, promote melanin generation, resist oxidation, remove free radicals and resist aging; the southernwood leaf/stem extract, the cnidium monnieri seed extract, the rosemary extract, the sophora flavescens root extract and the licorice root extract can relieve the scalp, relieve itching and sterilize; the folium Platycladi extract can improve scalp oil secretion, repair hair follicle, and improve hair loss. The plant extract has reasonable formula, can effectively promote scalp blood circulation, promote melanin generation, improve white hair, resist oxidation, inflammation and aging, effectively prevent alopecia and promote hair growth, and has good curative effect after long-term use.
In some embodiments of the present application, the essence further comprises 0.01 to 2.0 parts by weight of caprylyl hydroximic acid, 0.01 to 0.15 parts by weight of disodium EDTA, 1 to 11 parts by weight of a humectant, 0.1 to 2 parts by weight of a preservative, and 48.05 to 98.145 parts by weight of water.
The caprylyl hydroximic acid mainly has the effects of an antibacterial agent and a chelating agent in cosmetics and skin care products, is safe, can be used safely, has no influence on pregnant women, and has no pox-causing property. Is an ideal bacteriostatic organic acid. Has high-efficiency and selective chelating capacity for ferrous ions and ferric ions, and has limited growth of mould in an environment with limited ferric ions. And has the optimal carbon chain length capable of promoting the degradation of the cell membrane structure. Therefore, the antibacterial agent has stronger antibacterial capability and is a novel substitute substance for the preservative.
Disodium EDTA is mainly used as chelating agent and has stabilizing effect in cosmetics, and mineral chelating agent has synergistic antiseptic effect. And has a certain synergistic effect on an anticorrosion system and an antioxidant system.
The moisturizer is a substance with strong hygroscopicity, and can nourish scalp, prevent dry scalp and dandruff.
The preservative of the cosmetics refers to natural or synthetic components which are added into the cosmetics to prevent or delay the growth of microorganisms and prevent the cosmetics from rotting and deteriorating. Without preservatives, microorganisms will invade and multiply, causing turbidity, precipitation, foaming, color or taste changes in the cosmetic, and the emulsion will mildew, break emulsions, clump, and cause spoilage of the product. The preservative is effective in prolonging the life of the product. Also, the prescribed amount of preservative is safe.
In some embodiments of the present application, the humectant is one or more of propylene glycol, butylene glycol, 1, 2-hexanediol, glycerin, 1, 3-propanediol, and sodium hyaluronate.
In some embodiments of the present application, the humectant includes the following materials in parts by weight: 0.1 to 3 portions of propylene glycol, 0.3 to 4.0 portions of butanediol, 0.1 to 0.8 portion of 1, 2-hexanediol, 0.5 to 3 portions of glycerol, 0.1 to 1.0 portion of 1, 3-propylene glycol and 0.001 to 0.3 portion of sodium hyaluronate.
In some embodiments of the present application, the preservative is one or more of phenoxyethanol, ethylhexyl glycerol, and p-hydroxyacetophenone.
In some embodiments of the present application, the preservative is a mixture of phenoxyethanol and ethylhexyl glycerin, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerin is (9-10): (1-2).
On the other hand, the application provides a preparation method of the white-to-black essence, which comprises the following steps:
step S1, feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing;
step S2, raw material dissolution: starting steam, heating to 90 +/-2 ℃, keeping the stirring speed at 15-25RPM, and keeping the temperature for 25-35 min;
step S3, cooling to 48-52 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract; stirring;
step S4, cooling to 42-45 ℃, adding capryl hydroximic acid and preservative, and stirring;
and step S5, cooling to 38-40 ℃, filtering and discharging.
The plant extract is added after the temperature is reduced, so that the inactivation of the active ingredients in the plant extract can be effectively avoided.
In some embodiments of the present application, in the step S3, the stirring speed is 10-20 RPM.
In some embodiments of the present application, in the step S4, the stirring speed is 10-20 RPM.
In some embodiments of the present application, a 450-. Under the conditions, the prepared essence is fresh and cool and is beneficial to absorption.
The features and properties of the present application are described in further detail below with reference to examples.
Examples
The respective raw materials were prepared according to table 1.
TABLE 1 proportions (g) of the components of examples 1 to 4
Figure BDA0003667694720000101
The above plant extracts are all purchased from Shanghai; Biotech limited.
The preparation method of example 1 is as follows: feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing; raw material dissolution: starting steam, heating to 90 ℃, keeping the stirring speed at 20RPM, and keeping the temperature for 30 min; cooling to 50 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract, and stirring at the rotation speed of 15 RPM; cooling to 45 ℃, adding capryl hydroximic acid and a preservative, and stirring at the rotation speed of 15 RPM; cooling to 40 deg.C, filtering with 400-mesh double-layer filter cloth, and discharging. And after the inspection is qualified, filling and warehousing.
The preparation method of the embodiment 2 comprises the following steps: feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing; raw material dissolution: starting steam, heating to 92 ℃, keeping the stirring speed at 15RPM, and keeping the temperature for 35 min; cooling to 48 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract, and stirring at the rotation speed of 10 RPM; cooling to 42 ℃, adding the octanoyl hydroximic acid and the preservative, and stirring at the rotation speed of 10 RPM; cooling to 38 deg.C, filtering with 450 mesh double-layer filter cloth, and discharging. And after the inspection is qualified, filling and warehousing.
The preparation method of examples 3-4 was: feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing; raw material dissolution: starting steam, heating to 88 ℃, keeping the stirring speed at 25RPM, and keeping the temperature for 20 min; cooling to 52 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract, and stirring at the rotation speed of 15 RPM; cooling to 44 ℃, adding the octanoyl hydroximic acid and the preservative, and stirring at the rotation speed of 15 RPM; cooling to 39 deg.C, filtering with 550-mesh double-layer filter cloth, and discharging. And after the inspection is qualified, filling and warehousing.
Experimental example 1
In order to verify the effect of the white-to-black essence prepared by the embodiment of the application, a curative effect observation experiment is carried out on part of people.
The application method and the dosage of the white-to-black essence provided by the embodiment 3 of the application are as follows: when the hair is washed, the essence prepared in the embodiment is adopted for washing, and the scalp is massaged and washed clean. Washing every 2-3 days. The dosage is 15-20g for male, and 25-30g for female. The observation target is the population under 50 years old, 60 patients are selected for treatment, 3 months are 1 course of treatment, and 4 courses of treatment are continuously observed. Observations were made at the end of treatment 1 and treatment 4.
And (3) evaluating the curative effect:
the root of the white hair grows black hair, or the white hair is pulled out to show that the hair follicle of the hair root turns black;
the grey yellow root of the white hair is regarded as the obvious effect;
the white hair root is still white and is not effective.
TABLE 2 test results
Figure BDA0003667694720000121
As can be seen from table 2, the white-to-black essence provided in example 3 of the present application can effectively convert white hair into black hair.
Experimental example 2
In order to verify the hair care efficacy of the white to black essence provided in example 3, the white to black essence prepared in example 3 was sent to underwell research service (shanghai) ltd for testing.
1. Purpose of the test
The corresponding groups of hair bundles treated by the blank control and the samples are tested by an instrument, and the hair combing performance and the glossiness of the blank control group and the sample group are subjected to data statistical analysis, so that the hair combing performance and the glossiness after the product is used are evaluated, and a basis is provided for product efficacy declaration.
2. Test method and principle
2.1 Hair combing Performance test
The combing property of the hair is an important index for testing the care effect of the hair washing and caring product, which means that the resistance when the hair is combed by a comb is large, the damage of the hair quality can increase the friction and the curling degree between hair fibers, so that the hair is more difficult to comb, and the friction force between the hair can be reduced by using the hair washing and caring product, so that the hair can be combed more easily.
2.2 Hair gloss measurement
The glossiness of hair is the important parameter that the cosmetic embodiment of hair appearance embodies, and it is mainly influenced by the clean and damaged degree on hair surface, and the hair tegument unit of healthy hair is regular arrangement like the scale, and when hair received the light irradiation, partly light can get into inside the hair fibre, and another part light can take place to reflect or refract at hair tegument surface, leads to the bundle of hair to be the hi-lite through the reflection light. The care efficacy of the wash care product can be evaluated by measuring the gloss of the hair.
3. Sample properties: brown transparent liquid
4. Preparation before testing
Hair test tresses: 20 healthy black hair tresses: 15cm 1.5cm 2 g.
5 protocol
5.1 design of solution
20 identical flat healthy black hair tresses (15cm x 1.5cm x 2g) were selected and divided into 2 groups, 10 for the sample group and 10 for the blank control group.
Gloss test time points: before and after sample treatment.
Testing parameters: hair wet combing force, wet combing total work, hair gloss.
5.2 test time
04/08/2022 to 04/08/2022
5.3 environmental conditions
In the test process, the links such as instrument test and the like are carried out under the environmental conditions that the temperature is 21.0 +/-1.0 ℃ and the relative humidity is 50.0 +/-10.0% RH.
5.5 sample processing method
The action site: and (3) hair.
The treatment method comprises the following steps: after the hair is moistened by water, a proper amount of sample is uniformly coated on the moistened hair, and the moistened hair is washed clean by water after being massaged for 3 minutes.
6. Test method
6.1 Hair pretreatment
Preparing 20 hair bundles, dividing into 2 groups, preparing 10 hair bundles in a sample group, preparing 10 hair bundles in a blank control group, wetting the hair bundles at the water temperature of 37.0 +/-2.0 ℃, uniformly smearing 1mL of 10% SLES, gently kneading until the foam is rich for 1min, removing oil stains on the hair surface and the hair surface, washing at a constant flow rate, hanging the hair bundles in a constant-temperature and constant-humidity chamber for balancing after the hair bundles are washed clean, and naturally drying. The gloss parameter value (before treatment) for each bouquet of chinese character was measured using an instrument and recorded.
6.2 Hair combing Performance test
6.2.1 Wet comb test
Blank control group test: taking 10 bundles of hair, washing the hair with water at the temperature of 37.0 +/-2.0 ℃ at a constant flow rate, and slightly wiping the hair with hands after the hair is washed clean.
The sample group test comprises wetting hair bundle with 10 hair bundles at 37.0 + -2.0 deg.C, uniformly smearing appropriate amount of sample, gently kneading for 3min, and adding water at constant flow rate.
And (4) washing, and lightly wiping by hands after the washing is clean.
The hair bundles are installed on an instrument and fixed well for wet combing test, each hair bundle is tested for 1 time, the parameters of the instrument are adjusted, the displacement is 150mm, the combing speed is 101mm/min, and data are recorded.
6.3 Hair gloss measurement
After the hair combing performance test, the hair was combed 10 times on both sides using a flat narrow-toothed comb, and then subjected to a hair glossiness test. The gloss parameter values (after treatment) were measured using an instrument for the blank and the sample, about imperial, and recorded.
6.4 test apparatus
6.4.1XJ801 Hair comb, Shanghai Xiangjie Instrument science and technology, Inc., China, calibrated half a year according to the method provided by the instrument manufacturers.
1) Hair combing test
The hair wet combing test was performed with an XJ801 Hair comb.
6.4.2 probes Skin-Glossynnetere GL200, CK, Germany, all were hand-held test probes for direct contact with hair, supplied by the instrument manufacturer half a year
The method performs the calibration.
Hair gloss measurement the gloss of each strand was measured separately using a probe Skin-GlossymeterGL 200.
7. Evaluation of results
After the samples are treated, the instrument tests the change results of the respective parameters of the hair care, the sample group is obviously improved compared with a blank control group (P is less than 0.05), and the test product is determined to have the hair care effect.
8. Data analysis
Statistical analysis of the data was performed using SPSS. The test data were subjected to normal distribution test with progressive significance (bilateral) P >0.05 and the metrology data expressed as mean to standard deviation. If the test data obey normal distribution, the self front-back comparison in the group adopts paired t test, and the comparison between the groups adopts independent sample t test: and if the test data is in abnormal distribution, performing statistical analysis by adopting a rank sum test method.
9. Test results
9.1 Hair combing test results
TABLE 3 Hair combing test results
Figure BDA0003667694720000171
Figure BDA0003667694720000172
Note: p <0.05, and the samples have significant difference after treatment compared with a blank control group.
The smaller the total work of combing the dry and wet hair, the better the hair combing performance. As can be seen from table 3 and fig. 1, the hair wet combing force was reduced and the difference was significant, and the total hair wet combing work was reduced and the difference was significant after the sample treatment, as compared to the blank control group.
9.2 Hair gloss test results
TABLE 4 Hair gloss measurement results
Figure BDA0003667694720000173
Figure BDA0003667694720000174
Note: p <0.05, and the samples have significant difference after treatment compared with a blank control group.
The larger the test value, the higher the glossiness of the hair. The results are shown in table 4, where the sample treated the hair gloss level increased and the difference was significant compared to the blank control.
10. Conclusion of the experiment
Compared with a blank control group, the hair wet combing force and the wet combing total work are respectively and obviously reduced by 49.50 percent and 53.85 percent after the sample treatment, which shows that the combing degree of hair bundles treated by the sample is superior to that of Chinese imperial. The glossiness of the hair is remarkably improved by 45.51 percent, which shows that the glossiness of the hair bundle treated by the sample is better than that of the hair sample of the blank control group, and the effect of improving the glossiness of the hair is achieved.
And (4) conclusion: the sample can improve hair combing performance and hair gloss.
In summary, the present application provides a white-to-black essence, which includes a plurality of plant extracts beneficial to hair, wherein the polygonum multiflorum root extract, the black mulberry fruit extract, the artemisia leaf extract, the rosemary extract, the ginger root extract, the cinnamon extract and the grapefruit fruit extract can improve blood circulation of scalp, prevent alopecia and promote hair growth; the ganoderma atrum extract, the pseudo-ginseng root extract, the black sesame seed extract and the divaricate saposhnikovia root extract can activate tyrosinase activity, promote melanin generation, resist oxidation, remove free radicals and resist aging; the southernwood leaf/stem extract, the cnidium monnieri seed extract, the rosemary extract, the sophora flavescens root extract and the licorice root extract can relieve the scalp, relieve itching and sterilize; the folium Platycladi extract can improve scalp oil secretion, repair hair follicle, and improve hair loss. The plant extracts can fully exert respective drug effects, and can effectively promote scalp blood circulation, promote melanogenesis and promote white hair to turn black. In addition, the hair care shampoo can resist oxidation, inflammation and aging, effectively improve the hair combing performance and the hair glossiness, and has good long-term use effect.
The application also provides a preparation method of the white-to-black essence, the preparation method is simple, and the prepared essence is high in effective component content.
The embodiments described above are some, but not all embodiments of the present application. The detailed description of the embodiments of the present application is not intended to limit the scope of the claimed application, but is merely representative of selected embodiments of the application. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.

Claims (10)

1. The white-to-black essence is characterized by comprising the following raw materials in parts by weight: 0.05-5 parts of polygonum multiflorum root extract, 0.1-3 parts of ganoderma atrum extract, 0.1-1 part of black mulberry fruit extract, 0.05-1.5 parts of pseudo-ginseng root extract, 0.01-1.0 part of black sesame extract, 0.05-0.5 part of southernwood leaf/stem extract, 0.05-0.5 part of divaricate saposhnikovia root extract, 0.05-1.0 part of argy wormwood leaf extract, 0.01-0.5 part of cnidium monnieri seed extract, 0.05-5 parts of rosemary extract, 0.05-2 parts of biota orientalis leaf extract, 0.05-2.0 parts of ginger root extract, 0.001-0.3 part of cinnamon bark extract, 0.001-0.5 part of kushen root extract, 0.001-1.0 part of licorice root extract and 0.001-1.0 part of grapefruit peel extract.
2. The whitening-blackening essence according to claim 1, further comprising 0.01-2.0 parts by weight of caprylhydroxamic acid, 0.01-0.15 part by weight of disodium EDTA, 1-11 parts by weight of a humectant, 0.1-2 parts by weight of a preservative and 48.05-98.145 parts by weight of water.
3. The white-to-black essence according to claim 2, wherein the humectant is one or more of propylene glycol, butylene glycol, 1, 2-hexanediol, glycerin, 1, 3-propanediol, and sodium hyaluronate.
4. The white-to-black essence according to claim 2, wherein the humectant comprises the following raw materials in parts by weight: 0.1 to 3 portions of propylene glycol, 0.3 to 4.0 portions of butanediol, 0.1 to 0.8 portion of 1, 2-hexanediol, 0.5 to 3 portions of glycerol, 0.1 to 1.0 portion of 1, 3-propylene glycol and 0.001 to 0.3 portion of sodium hyaluronate.
5. The white-to-black essence according to claim 4, wherein the preservative is one or more of phenoxyethanol, ethylhexyl glycerol and p-hydroxyacetophenone.
6. The white-to-black essence according to claim 2, wherein the preservative is a mixture of phenoxyethanol and ethylhexyl glycerin, and the mass ratio of the phenoxyethanol to the ethylhexyl glycerin is (9-10): (1-2).
7. A method for preparing the white-to-black essence according to any one of claims 1 to 6, comprising:
step S1, feeding and dispersing: adding EDTA disodium, a humectant and part of water into an emulsifying pot, and uniformly dispersing;
step S2, raw material dissolution: starting steam, heating to 90 +/-2 ℃, keeping the stirring speed at 15-25RPM, and keeping the temperature for 25-35 min;
step S3, cooling to 48-52 ℃, adding ginger root extract, rosemary extract, cacumen biotae extract, pseudo-ginseng root extract, black mulberry extract, polygonum multiflorum root extract, southernwood leaf/stem extract, divaricate saposhnikovia root extract, folium artemisiae argyi extract, cnidium monnieri seed extract, ganoderma atrum extract, black sesame seed extract, cinnamon bark extract, sophora flavescens root extract, licorice root extract and grapefruit peel extract, and stirring;
step S4, cooling to 42-45 ℃, adding caprylyl hydroximic acid and preservative, and stirring;
and step S5, cooling to 38-40 ℃, filtering and discharging.
8. The method of claim 7, wherein the stirring speed in step S3 is 10-20 RPM.
9. The method of claim 7, wherein the stirring speed in step S4 is 10-20 RPM.
10. The method for preparing white-to-black essence according to claim 7, wherein in step S5, the filtration is performed by using 450-mesh 550-mesh double-layer filter cloth.
CN202210599936.5A 2022-05-28 2022-05-28 White-to-black essence and preparation method thereof Pending CN114796060A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210599936.5A CN114796060A (en) 2022-05-28 2022-05-28 White-to-black essence and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210599936.5A CN114796060A (en) 2022-05-28 2022-05-28 White-to-black essence and preparation method thereof

Publications (1)

Publication Number Publication Date
CN114796060A true CN114796060A (en) 2022-07-29

Family

ID=82520064

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202210599936.5A Pending CN114796060A (en) 2022-05-28 2022-05-28 White-to-black essence and preparation method thereof

Country Status (1)

Country Link
CN (1) CN114796060A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115212153A (en) * 2022-08-05 2022-10-21 广州姿采化妆品厂 Polygonum multiflorum nutrient solution and preparation method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108403504A (en) * 2018-04-24 2018-08-17 安徽安之酸化妆品有限公司 A kind of hair scalp care essence breast containing chlorophyll and qinghaosu
CN111529436A (en) * 2020-04-23 2020-08-14 深圳市熙雨中医药研究有限公司 White hair blackening, hair nourishing and protecting, hair loss preventing and hair growing essence and preparation method thereof
CN111700841A (en) * 2020-06-11 2020-09-25 梧州市华夏医药科技有限公司 Hair loss preventing and hair growing shampoo containing ganoderma atrum plant extract essence and preparation method thereof
CN111803426A (en) * 2020-07-17 2020-10-23 广州市逸轩精细化工有限公司 Anti-hair loss and hair-fixing nutrient solution and preparation method thereof
CN112569169A (en) * 2021-02-04 2021-03-30 杭州千唯健康科技有限公司 White-to-black essence
CN113081935A (en) * 2021-04-28 2021-07-09 惠州市肌缘生物科技股份有限公司 Amino acid oil-control fluffy moisturizing hair conditioner and preparation process thereof
CN114533624A (en) * 2022-02-25 2022-05-27 广东省安信药业有限公司 White hair blackening liquid and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108403504A (en) * 2018-04-24 2018-08-17 安徽安之酸化妆品有限公司 A kind of hair scalp care essence breast containing chlorophyll and qinghaosu
CN111529436A (en) * 2020-04-23 2020-08-14 深圳市熙雨中医药研究有限公司 White hair blackening, hair nourishing and protecting, hair loss preventing and hair growing essence and preparation method thereof
CN111700841A (en) * 2020-06-11 2020-09-25 梧州市华夏医药科技有限公司 Hair loss preventing and hair growing shampoo containing ganoderma atrum plant extract essence and preparation method thereof
CN111803426A (en) * 2020-07-17 2020-10-23 广州市逸轩精细化工有限公司 Anti-hair loss and hair-fixing nutrient solution and preparation method thereof
CN112569169A (en) * 2021-02-04 2021-03-30 杭州千唯健康科技有限公司 White-to-black essence
CN113081935A (en) * 2021-04-28 2021-07-09 惠州市肌缘生物科技股份有限公司 Amino acid oil-control fluffy moisturizing hair conditioner and preparation process thereof
CN114533624A (en) * 2022-02-25 2022-05-27 广东省安信药业有限公司 White hair blackening liquid and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
产品运营: "植观洗发水怎么样 世界十大防脱洗发露", Retrieved from the Internet <URL:https://article.autotimes.com.cn/article/92600.html> *
广州市博倩精细化工有限公司: "苗寨印像润发洗发露", Retrieved from the Internet <URL:https://hzpba.nmpa.gov.cn/gccx/chakan.html?prodId=875450510570684416&gb=G> *
广州振业医药科技有限公司: "发轻松头皮调理液", Retrieved from the Internet <URL:https://hzpba.nmpa.gov.cn/gccx/chakan.html?prodId=952950616202674176&gb=G> *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115212153A (en) * 2022-08-05 2022-10-21 广州姿采化妆品厂 Polygonum multiflorum nutrient solution and preparation method thereof
CN115212153B (en) * 2022-08-05 2023-08-15 广州姿采化妆品厂 Polygonum multiflorum nutrient solution and preparation method thereof

Similar Documents

Publication Publication Date Title
CN105726391B (en) A kind of dendrobium candidum shower cream
CN108498408B (en) Whitening essence
CN106265385A (en) A kind of submissive glossy shampoo composite and application thereof
CN109106677B (en) Composition with whitening function and application thereof
CN105381007A (en) Externally-applied traditional Chinese medicine composition with effect on whitening skin, preparation as well as preparation method and application thereof
CN113908091B (en) Anti-hair-loss hair-growing composition and preparation method and application thereof
CN111529413A (en) Nicotinamide capsule mask and preparation and use methods thereof
CN111529477A (en) Composition for caring hair, and preparation and application thereof
KR101853743B1 (en) External composition for skin containing Kalopanax pictus (Thunb.) Nakai extract
KR101997177B1 (en) Shampoo composition for improving state of scalp and hair
CN114796060A (en) White-to-black essence and preparation method thereof
CN105853293A (en) Cosmetic composition with whitening effect and hand cream with whitening effect
KR101639578B1 (en) Cosmetic composition containing Ocimum basilicum seed extract
CN111166707B (en) Facial anti-aging repairing and nursing composition and preparation method and application thereof
KR20080077762A (en) The herb medicine composition which has a dehairing prevention and a hair growth promotion effect
KR100778662B1 (en) Cleansing composition containing natural oriental plant extracts
CN115054566B (en) Scalp aging resisting composition and preparation method thereof
KR100930688B1 (en) Oriental composition for reinforcement of hair-roots and cleanness of scalp and its preparation method
KR101459742B1 (en) Cosmetic composition for improving acne containing extracts of natural substance
CN110613663A (en) Skin repairing composition, skin care product and preparation method thereof
CN115869233A (en) Whitening and anti-wrinkle essence and preparation method thereof
CN110101648B (en) Beauty-care concealer air cushion BB cream
KR100738434B1 (en) Cosmetic composition containing pyrrolidinyl diaminopyrimidine oxide
CN113368003A (en) Composition with overnight muscle repairing effect and preparation method and application thereof
KR20130092260A (en) Composition for anti-dandruff

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20220729