CN114767583A - Pure natural plant blackhead removing composition and preparation method and application thereof - Google Patents
Pure natural plant blackhead removing composition and preparation method and application thereof Download PDFInfo
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- CN114767583A CN114767583A CN202111286880.XA CN202111286880A CN114767583A CN 114767583 A CN114767583 A CN 114767583A CN 202111286880 A CN202111286880 A CN 202111286880A CN 114767583 A CN114767583 A CN 114767583A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention discloses a pure natural plant blackhead removing composition which comprises the following preparation raw materials in parts by weight: 10-30 parts of witch hazel plant extract, 1-5 parts of Lythraceae plant extract, 5-20 parts of Labiatae plant extract, 0.1-1 part of fruit acid, 5-20 parts of lactobacillus/algae extract fermentation product and 55-65 parts of solvent. The combination of the hamamelis virginiana extract, the fermentation product of the lactobacillus/algae extract and the pomegranate fruit extract can dissolve blackheads in pores, so that the effect of removing the blackheads is achieved, the pore reducing effect is achieved, the blackhead regeneration is reduced, the permeation of acidic substances can be relieved by adopting the synergistic compounding effect of lactobionic acid and mint leaf hydrolat, the irritation effect of the composition on skin is reduced, the moisturizing effect of the composition is increased, and the skin is smooth and tender.
Description
Technical Field
The invention relates to a pure natural plant blackhead removing composition, relates to A61K, and particularly relates to the field of cosmetics.
Background
Blackheads are a common skin problem, particularly in a T-shaped area of facial skin, have the problem of large blackhead pores while producing heavy oil, and are formed by exposing a sebum surface layer blocking the pores to air and turning black after contacting with dust and angstrom and oxidizing. Common blackhead removing methods include tearing, adsorption, acid brushing and the like, the tearing, the adsorption and the like easily cause large pores, dust is easy to deposit blackheads and relapse, the cleaning effect is not thorough, and the acid brushing method has high irritation to the skin, is sensitive to the skin and is not suitable for people with thin horny layers.
Chinese patent CN202011312785.8 discloses a blackhead removing essence, which is prepared by adding salicylic acid to adjust grease, dissolving blackheads to inhibit blackhead growth, but salicylic acid substances have strong irritation to skin and are not suitable for many sensitive skin types. Chinese patent CN201610553492.6 discloses a propolis blackhead removing nose mask, wherein a 3D net-drawing type structure is formed by adding a plant formula to relieve pore expansion pressure and repair pore elasticity, but after the nose mask is torn off, the nose mask lacks convergence repair on pores, dust in the environment is more easily accumulated at pore openings, blackheads are continuously regenerated, and the eradication effect cannot be realized.
Disclosure of Invention
In order to improve the blackhead removing effect of the composition and reduce the irritation to the skin, the invention provides a pure natural plant blackhead removing composition, which is prepared from the following raw materials in parts by weight: 10-30 parts of witch hazel plant extract, 1-5 parts of Lythraceae plant extract, 5-20 parts of Labiatae plant extract, 0.1-1 part of fruit acid, 5-20 parts of lactobacillus/algae extract fermentation product and 55-65 parts of solvent.
As a preferred embodiment, the preparation raw materials comprise, in parts by weight: 13-20 parts of witch hazel plant extract, 1-3 parts of lythraceae plant extract, 8-15 parts of labiate plant extract, 0.3-0.9 part of fruit acid, 8-15 parts of lactobacillus/algae extract fermentation product and 60-63 parts of solvent.
As a preferred embodiment, the preparation raw materials comprise, in parts by weight: 15 parts of hamamelidaceae plant extract, 2 parts of lythraceae plant extract, 10 parts of labiatae plant extract, 0.8 part of fruit acid, 10 parts of lactobacillus/algae extract fermentation product and 62.2 parts of solvent.
As a preferred embodiment, the witch hazel extract is selected from the group consisting of an extract of a plant of the genus liquidambar, an extract of a plant of the genus muscardine, an extract of a plant of the genus semiliquidambar, an extract of a plant of the genus hamamelis, an extract of a plant of the genus hydrangea, and a combination of any one or more of these.
As a preferred embodiment, the Hamamelis plant extract is one or more selected from the group consisting of Hamamelis virginiana extract, Hamamelis minor extract, Hamamelis virginiana extract, and Hamamelis virginiana extract.
As a preferred embodiment, the witch hazel extract is a witch hazel extract.
As a preferred embodiment, the extract of the lythraceae plant is selected from one or more of the group consisting of an extract of a lagerstroemia plant, an extract of a lythraceae plant, and an extract of a pomegranate plant.
As a preferred embodiment, the extract of the pomegranate plant is an extract of pomegranate, and preferably, the extract of pomegranate is one or more selected from an extract of pomegranate leaves, an extract of pomegranate bark, an extract of pomegranate flowers, and an extract of pomegranate fruits.
As a preferred embodiment, the extract of the plant of the family lythraceae is an extract of pomegranate fruit.
As a preferred embodiment, the weight ratio of the witch hazel extract, the lythraceae extract and the lactobacillus/algae extract fermentation product is (10-30): (1-5): (5-20).
As a preferred embodiment, the weight ratio of the witch hazel extract, the lythraceae extract and the lactobacillus/algae extract fermentation product is (13-20): (1-3): (8-15).
As a preferred embodiment, the weight ratio of the witch hazel extract, the lythraceae extract to the lactobacillus/algae extract fermentation product is 15: 2: 10.
the applicant finds in the experimental process that the combination of hamamelis virginiana extract, lactobacillus/algae extract fermentation product and pomegranate fruit extract has a good blackhead removing effect and is less irritating to the skin, and guesses that the possible reason is that: the main component of the fermentation product of the lactobacillus/algae extract is lactic acid which is ester-soluble acid with large molecular weight, can soften cutin, enters pores along sebaceous glands secreting oil, dissolves oil and fat substances causing pore blockage, promotes epithelial cells to metabolize and accelerate the dissolution and discharge of blackheads, but high-content lactic acid can stimulate the dermis layer of the skin to cause red swelling, the mashup contained in the witch hazel extract and the pomegranate polyphenol in the pomegranate fruit extract have synergistic effect, can react with the protein of the skin to reduce the irritation of the lactic acid to the dermis skin and can astringe the skin, the pores can be timely reduced after the blackheads are discharged, the dust is prevented from being accumulated on the surface of the pores again, and the mashup contained in the witch hazel extract also has the function of regulating the secretion of the skin oil and fat, can regulate water and oil balance of skin and improve skin state. Applicants further found that the weight ratio of witch hazel extract, pomegranate fruit extract and lactobacillus/algae extract fermentation product was 15: 10: 2, has a long-term removing effect on blackheads, has a remarkable removing effect on blackheads after long-term use of the composition, and can reduce the regeneration of the blackheads.
As a preferred embodiment, the labiatae plant extract is selected from one or more of lavender plant extract, mentha plant extract, basil plant extract, origanum plant extract, rosmarinus plant extract and caryophyllum plant extract.
As a preferred embodiment, the mentha plant extract is at least one selected from the group consisting of peppermint extract, spearmint extract, peppermint extract, and spearmint extract, and preferably, the peppermint extract is peppermint leaf hydrosol.
In a preferred embodiment, the extract of the labiatae plant is peppermint leaf hydrosol.
As a preferred embodiment, the fruit acid is selected from one or a combination of glycolic acid, lactic acid, tartaric acid and lactobionic acid.
As a preferred embodiment, the fruit acid is lactobionic acid.
In a preferred embodiment said lactobionic acid is present in an amount of 10-30% by weight, more preferably said lactobionic acid is present in an amount of 10% by weight.
The applicant finds that the synergistic compounding of lactobionic acid and peppermint leaf hydrolat can enable the skin to have a good moisturizing effect and enable the skin to be fine and smooth, and the possible reasons are guessed that lactobionic acid acts on the surface of the skin to reduce the polymerization force among corneocytes, accelerate the falling of aged corneocytes, unblock pores and effectively prevent the pores from being blocked.
The solvent is not limited in kind, and preferably, deionized water.
The second aspect of the invention provides a preparation method of a pure natural plant blackhead removing composition, which comprises the following steps: mixing Hamamelidaceae plant extract, Lythraceae plant extract, Labiatae plant extract, fruit acid, and lactobacillus/algae extract fermentation product, stirring at 40-50 deg.C for 30-40min, and removing foam.
The third aspect of the invention provides application of the pure natural plant blackhead removing composition in water, milk, cream, gel and gel cosmetics.
Compared with the prior art, the invention has the following beneficial effects:
(1) the pure natural plant blackhead removing composition disclosed by the invention can dissolve blackheads in pores by adopting the combination of the hamamelis virginiana extract, the lactobacillus/algae extract fermentation product and the pomegranate fruit extract, so that the blackhead removing effect is achieved, and meanwhile, the effect of reducing the pores is achieved, and the regeneration of the blackheads is reduced.
(2) The pure natural plant blackhead removing composition disclosed by the invention can alleviate the permeation of acidic substances, reduce the irritation of the composition to the skin, increase the moisturizing effect of the composition and enable the skin to be smooth and tender by adopting the synergistic compounding effect of lactobionic acid and peppermint leaf hydrolat.
(3) The pure natural plant blackhead removing composition adopts a Hamamelis virginiana extract, a fermentation product of a lactobacillus/algae extract fermentation product and a pomegranate fruit extract 15: 10: 2, a long-term blackhead removing effect is achieved, and the regeneration of the blackheads can be reduced by using the composition for a long time.
Detailed Description
The present invention will be specifically described below by way of examples. It should be noted that the following examples are only for illustrating the present invention and should not be construed as limiting the scope of the present invention, and that the insubstantial modifications and adaptations of the present invention by those skilled in the art based on the above disclosure are still within the scope of the present invention.
In addition, the starting materials used are all commercially available, unless otherwise specified.
Examples
A pure natural plant blackhead removing composition is prepared from Hamamelidaceae plant extract, Lythraceae plant extract, Labiatae plant extract, fruit acid, lactobacillus/algae extract fermentation product, and solvent, and is shown in Table 1.
The Hamamelidaceae plant extract is Hamamelis virginiana extract, and is purchased from ballad brocade chemical industry Co.
The extract of the Lythraceae plant is pomegranate fruit extract, and is available from limited Huzhou Jiamei biochemicals.
The Labiatae plant extract is peppermint leaf hydrolat, available from Guangzhou Rose Fu trade company, Inc.
The fruit acid is lactobionic acid with the mass fraction of 10 percent and is purchased from Hangzhou union chemical engineering Co.
The lactobacillus/algae extract fermentation products were purchased from branded korea.
The solvent is deionized water.
A method for preparing a pure natural plant blackhead removing composition comprises the following steps: mixing Hamamelidaceae plant extract, Lythraceae plant extract, Labiatae plant extract, fruit acid, and lactobacillus/algae extract fermentation product, stirring at 45 deg.C for 30min, and defoaming.
TABLE 1
Performance test
1. And (3) safety testing: according to standard SN/T2329-2009 test for cosmetic irritancy of chick embryo chorioallantoic membrane: eggs hatched to 9 days old are peeled off with tweezers from their air cell ends, the inner membrane is infiltrated with 0.9% physiological saline, the egg membrane is carefully peeled off from the edge, and the chorioallantoic membrane leaks out. 0.3mL of the blackhead-removed composition of examples 1 to 9 was taken by a pipette and dropped on the membrane, and after 3 minutes, the change of blood vessels in the chorioallantoic membrane was observed. Each sample was tested in parallel 6 times.
The chick embryo score is the average value of the scores of single chick embryos in 6 experiments, wherein the single chick embryo score is the sum of the bleeding degree, the blood coagulation degree and the blood vessel melting degree observed by each chick embryo, and the result retains the last two decimal points.
The scoring standard is as follows: ES is less than or equal to 12: no/mild irritation; 12 < ES < 16: moderate irritation; ES is more than or equal to 16 and has strong irritation. The test results are shown in table 2.
2. And (3) black head removing effect test: 1) the testing principle is as follows: the invention adopts VISIA skin detector to analyze the black head removing effect. The VISIA skin detector uses advanced optical imaging, RBX and software technologies to detect and analyze skin spots, pores, wrinkles and skin texture, as well as subcutaneous blood vessels and pigmented lesions such as porphyrins (lipids), brown spots, erythema, etc. due to uv irradiation. 2) And (3) testing process: screening healthy subjects with the age of 20-45 years, wherein the skin is oily, the two sides of the nose have obvious blackheads, and each group contains 15 people, and the total number of the groups is 9; the subjects rested for 20 minutes between constant temperature and humidity after using the cleansing product, the subjects' facial condition was evaluated by the panelists, and photographed using VISIA 7, and the skin condition before using the sample was recorded. The instant blackhead removal effect of the samples was analyzed by again taking a photograph of the subject's facial condition after 15 minutes of subsequent use of the product under the direction of the experimenter. And the facial condition of the subjects was again assessed on day 7 of sample use and analyzed by imaging with VISIA 7. The samples were evaluated for long-term blackhead removal.
3) Test results and analysis: the formula for calculating the effect of removing the blackheads is as follows: a ═ A2-A1)/A1 × 100%
Note: a is the blackhead change rate; a2 is the number of blackheads after use of the sample; a1 is the number of blackheads before using the sample. The results are shown in Table 3.
TABLE 2
| Chick embryo Scoring | Irritation property | |
| Example 1 | 0 | Has no irritation |
| Example 2 | 0 | Has no irritation |
| Example 3 | 0 | Has no irritation |
| Example 4 | 0 | Has no irritation |
| Example 5 | 0 | Has no irritation |
| Example 6 | 0 | Has no irritation |
| Example 7 | 0.67 | Has no irritation |
| Example 8 | 0 | Has no irritation |
| Example 9 | 0 | Has no irritation |
TABLE 3
Claims (10)
1. The pure natural plant blackhead removing composition is characterized by comprising the following raw materials in parts by weight: 10-30 parts of witch hazel plant extract, 1-5 parts of Lythraceae plant extract, 5-20 parts of Labiatae plant extract, 0.1-1 part of fruit acid, 5-20 parts of lactobacillus/algae extract fermentation product and 55-65 parts of solvent.
2. The pure natural plant blackhead removing composition as claimed in claim 1, wherein the hamamelidaceae plant extract is selected from the group consisting of a liquidambar extract, a muscarine extract, a semiliquidambar extract, a hamamelidaceae plant extract, a bungarus extract, and a petunia plant extract.
3. The pure natural plant blackhead removing composition as claimed in claim 2, wherein the hamamelis plant extract is selected from one or more of hamamelis virginiana extract, hamamelis minor extract, hamamelis japonica extract, and hamamelis virginiana extract.
4. The pure natural plant blackhead removing composition according to claim 1 or 2, wherein the extract of the lythraceae plant is one or more selected from the group consisting of an extract of a lagerstroemia plant, an extract of a lythraceae plant, and an extract of a punica plant.
5. The pure natural plant blackhead removing composition according to claim 4, wherein the extract of the punica is an extract of punica granatum, and preferably, the extract of punica granatum is one or more selected from an extract of punica granatum leaves, an extract of punica granatum peel, an extract of punica granatum flowers, and an extract of punica granatum fruits.
6. The pure natural plant blackhead removing composition as claimed in claim 1 or 2, wherein the Labiatae plant extract is selected from one or more of Lavandula plant extract, Mentha plant extract, Ocimum plant extract, Oregano plant extract, Rosmarinus plant extract, and Mentha plant extract.
7. The pure natural plant blackhead removing composition according to claim 6, wherein the Mentha plant extract is at least one selected from the group consisting of Mentha piperita extract, Mentha viridans extract, Mentha piperita extract, and Mentha rotundifolia extract, and preferably, the Mentha piperita extract is Mentha piperita leaf hydrosol.
8. The pure natural plant blackhead removing composition as claimed in claim 1 or 2, wherein the fruit acid is selected from one or more of glycolic acid, lactic acid, tartaric acid, and lactobionic acid.
9. A method for preparing the pure natural plant blackhead removing composition according to any one of claims 1 to 8, comprising the steps of: mixing Hamamelidaceae plant extract, Lythraceae plant extract, Labiatae plant extract, fruit acid, and lactobacillus/algae extract fermentation product, stirring at 40-50 deg.C for 30-40min, and defoaming.
10. The use of the pure natural plant blackhead removal composition according to any one of claims 1 to 8, wherein the composition is applied to water, milk, cream, gel, or gel cosmetics.
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Cited By (2)
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| CN115337243A (en) * | 2022-09-14 | 2022-11-15 | 上海臻臣化妆品有限公司 | Blackhead removing composition and cosmetic |
| CN118021691A (en) * | 2024-04-09 | 2024-05-14 | 广州天玺生物科技有限公司 | Cosmetic composition for deep water supplementing and preparation method thereof |
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| CN118021691A (en) * | 2024-04-09 | 2024-05-14 | 广州天玺生物科技有限公司 | Cosmetic composition for deep water supplementing and preparation method thereof |
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