CN114699350A - Hair dye with pomegranate peel extract as raw material and preparation method thereof - Google Patents
Hair dye with pomegranate peel extract as raw material and preparation method thereof Download PDFInfo
- Publication number
- CN114699350A CN114699350A CN202210367538.0A CN202210367538A CN114699350A CN 114699350 A CN114699350 A CN 114699350A CN 202210367538 A CN202210367538 A CN 202210367538A CN 114699350 A CN114699350 A CN 114699350A
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- parts
- hair
- hair dye
- raw material
- extract
- Prior art date
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- 239000000118 hair dye Substances 0.000 title claims abstract description 61
- 239000002994 raw material Substances 0.000 title claims abstract description 48
- 239000001575 punica granatum l. bark extract Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 48
- 241000219991 Lythraceae Species 0.000 claims abstract description 23
- 235000014360 Punica granatum Nutrition 0.000 claims abstract description 23
- 241000283690 Bos taurus Species 0.000 claims abstract description 22
- 235000018553 tannin Nutrition 0.000 claims abstract description 13
- 239000001648 tannin Substances 0.000 claims abstract description 13
- 229920001864 tannin Polymers 0.000 claims abstract description 13
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- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 9
- 244000269722 Thea sinensis Species 0.000 claims abstract description 9
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- 150000007949 saponins Chemical class 0.000 claims abstract description 9
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 9
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 9
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- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 8
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Landscapes
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- General Health & Medical Sciences (AREA)
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- Biotechnology (AREA)
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- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of hair dyes, and particularly relates to a hair dye taking a pomegranate rind extract as a raw material and a preparation method thereof, wherein the hair dye is prepared from the following raw materials in parts by weight: 10-30 parts of pomegranate bark extract, 5-20 parts of tannin, 5-20 parts of FeCl3.6H2O2.5-20 parts, 1-5 parts of sodium hyaluronate, 5-20 parts of aloe polysaccharide, 2.5-10 parts of tea saponin, 2.5-10 parts of NaOH2.5-10 parts and 85-130 parts of water. The pomegranate rind is used as the raw material, can nourish hair, inhibit bacteria and diminish inflammation, has no toxic or side effect, has good hair blackening effect, has natural and bright color of the hair after use, and can well care and nourish the hair, wherein the hair is blackened and bright by complexing plant-derived tannin and ferric ions, the water content of the hair is increased and moistened by hyaluronic acid and aloe polysaccharide, and the hair dye is endowed with the function of gel water.
Description
Technical Field
The invention relates to the technical field of hair dyes, in particular to a hair dye taking a pomegranate rind extract as a raw material and a preparation method thereof.
Background
The coloring component of the chemical hair dye mainly comprises aniline compounds, such as p-phenylenediamine and the like, and the p-phenylenediamine is an internationally recognized carcinogenic substance, so that the harm to human bodies is widely accepted at home and abroad. Foreign studies have shown that the incidence of breast cancer, skin cancer, leukemia, bladder cancer in people who often have hair dyes is increased.
According to the detection of hundreds of hair dyes by related departments, nearly 90 percent of hair dyes contain toxic chemical substances such as nitrobenzene, aniline and the like, and are easily absorbed by the skin, so that some people generate acute hair dye allergy. The specific clinical symptoms are: after the hair-care product is used, scalp itch, hair withering, scalp reddish eruption, scalp suppuration and the like are caused, and the worst result after the hair-care product is used for a long time is cancer.
The basic ones currently used in retail markets and professional hair salons are chemical hair dyes, the main components of which are toxic chemicals such as aniline, phenols and the like, e.g., p-phenylenediamine, p-aminophenol, m-aminophenol, toluene 2, 5-diamine, resorcinol, p-methylaminophenol, 2, 4-diaminophenoxyethanol hydrochloride, N-bis (2-hydroxyethyl) -p-phenylenediamine sulfate, 4-amino-2-hydroxytoluene, 2-methylresorcinol, hydroxyethyl-p-phenylenediamine sulfate, 1, 5-naphthalenediol, 4-chlororesorcinol and the like. After long-term use of the chemical hair dye, as long as 1% of the chemical hair dye is absorbed into human body, poisoning is accumulated, wherein chemical substances are combined with certain cells, deoxyribonucleic acid in cell nucleus is damaged, cell mutation is caused, and skin cancer, bladder cancer, leukemia and the like are induced, and experts warn the people to ' warn ' the disease from the beginning '.
Compared with chemical hair dye, the coloring molecules adopted by the real plant hair dye product are all extracted from plants. According to the prior art, plant coloring molecules which can meet the specification of hair scales comprise black mulberry, black bean peel, black medlar, gallnut, polygonum multiflorum, black walnut and the like. The pure natural plant hair dye is not added with aniline and derivatives thereof.
In the years, the aim is to search for a safe and nontoxic natural hair dye with better hair blackening effect which can replace a chemical hair dye from natural plants, and the inventor finds that the pomegranate bark extract can well meet the requirements, is prepared by taking pomegranate bark as a raw material and adopting a proper solvent for extraction and refining, can blacken the hair and nourish the hair, can effectively dilate blood vessels, improves microcirculation, and has stronger oxidation resistance, free radical scavenging capacity, anti-inflammation, anti-allergy, hair fungus inhibition and other effects.
Therefore, we propose a hair dye using pomegranate rind extract as a raw material and a preparation method thereof to solve the above problems.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a hair dye taking pomegranate rind extract as a raw material and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a hair dye taking a pomegranate rind extract as a raw material is prepared from the following raw materials in parts by weight: 10-30 parts of pomegranate bark extract, 5-20 parts of tannin, 2.5-20 parts of FeCl3.6H2O, 1-5 parts of sodium hyaluronate, 5-20 parts of aloe polysaccharide, 2.5-10 parts of tea saponin, 2.5-10 parts of NaOH and 85-130 parts of water.
In the hair dye taking the pomegranate bark extract as the raw material, the pomegranate bark extract is prepared by the following steps:
s1, taking fresh pomegranate rind, drying and crushing to 10-30 meshes;
s2, weighing, adding 50-95% ethanol (S/v) in an amount which is 6-7 times that of the raw materials, carrying out reflux extraction for 3 hours at the water bath temperature of 90 ℃, and filtering;
s3, adding 5 times of 50-95% ethanol into filter residue, reflux-extracting for 2.5 hours, filtering, and combining the filtrates;
s4, concentrating under reduced pressure to obtain an extract, adding purified water twice the weight of the raw materials into the extract to dissolve the extract, cooling, and centrifuging to obtain insoluble substances A and a centrifugate B;
s5, passing the centrifugate through a macroporous adsorption resin column, wherein the ratio of the volume of a column bed to the raw material is 1/1 (v/S);
s6, removing impurities by washing with water with the volume twice that of the column bed, eluting with 80% ethanol with the volume three times that of the column bed, mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to be paste-like, and drying in vacuum to obtain the pomegranate bark extract.
In the hair dye taking the pomegranate bark extract as the raw material, the hair dye raw material also comprises 0.5 part of mint essential oil and 0.5 part of potassium sorbate.
A preparation method of a hair dye taking pomegranate rind extract as a raw material comprises the following steps:
s1, weighing 2.5-20 parts of FeCl3.6H2O, and adding 2.5-20 parts of water for dissolving;
s2, weighing 2.5-10 parts of NaOH, and adding 2.5-20 parts of water for dissolving;
s3, weighing 1-5 parts of sodium hyaluronate and 0.5 part of potassium sorbate, adding 50-64 parts of water, heating to dissolve, adding 5-20 parts of aloe polysaccharide and 2.5-10 parts of tea saponin, and uniformly stirring;
s4, weighing 10-30 parts of pomegranate bark extract, 5-20 parts of tannin, adding 30-50 parts of water, and heating for dissolving;
s5, adding the mixture obtained in the step S4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step S5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step S6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step S7, and stirring;
s9, processing the mixed system diameter colloid mill obtained in the step S8 to obtain a homogeneous system, namely the natural hair dye taking the pomegranate bark extract as the raw material
In the method for preparing the hair dye by using the pomegranate bark extract as the raw material, the pomegranate bark extract is rich in various nutritional ingredients including anthocyanin and various amino acids such as tannin, wax, mannitol, mucilage, gallic acid, malic acid, pectin, gum, isoquercitrin, cyanidin-3-glucoside, cyanidin-3, 5-diglucoside, crying-geraniin-3-glucoside, crying-geraniin-3, 5-diglucoside and the like.
In the preparation method of the hair dye using the pomegranate bark extract as the raw material, the hair dye obtained in the step S9 is used by wetting hair with hands in the early morning, dipping a little pasty hair dye by a toothbrush, uniformly coating the hair dye on white hair, and rubbing the hair dye back and forth for a moment, so that the hair dye is dyed into black, does not need to be washed immediately, and is washed before sleeping at night.
Compared with the prior art, the hair dye taking the pomegranate bark extract as the raw material and the preparation method thereof have the advantages that:
1. the invention aims at the potential risks of allergy, carcinogenesis and the like of chemical hair dyes, and provides a natural hair dye which is healthy, safe, convenient to use and free of toxic and side effects and takes pomegranate bark extract as a raw material.
2. The pomegranate rind is used as the raw material, can nourish hair, inhibit bacteria and diminish inflammation, has no toxic or side effect, has good hair blackening effect, has natural and bright color of the hair after use, and can well care and nourish the hair, wherein the hair is blackened and bright by complexing plant-derived tannin and ferric ions, the water content of the hair is increased and moistened by hyaluronic acid and aloe polysaccharide, and the hair dye is endowed with the function of gel water.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Example 1
Preparation method of pomegranate bark extract
Taking fresh pomegranate rind, drying, and crushing to 10-30 meshes; weighing, adding 80% ethanol (s/v) in an amount which is 6 times that of the raw materials, performing reflux extraction at the water bath temperature of 90 ℃ for 3 hours, and filtering; extracting the residue with 5 times of 80% ethanol under reflux for 2.5 hr, filtering, and mixing filtrates; concentrating under reduced pressure to obtain extract, dissolving the extract in purified water twice the weight of the raw materials, cooling, and centrifuging to obtain insoluble substance A and centrifugate B; passing the centrifugate through macroporous adsorbent resin column, wherein the ratio of the volume of the column bed to the raw material is 1/1 (v/s); washing with water twice the volume of the column bed to remove impurities, eluting with 80% ethanol 3 times the volume of the column bed, mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to obtain an extract, and vacuum drying to obtain the pericarpium Granati extract.
Second, hair dye formula
Third, the preparation method
S1, weighing 5 parts of FeCl3.6H2O, and adding 5 parts of water for dissolving;
s2, weighing 4 parts of NaOH, and adding 5 parts of water for dissolving;
s3, weighing 1 part of sodium hyaluronate and 0.5 part of potassium sorbate, adding 50 parts of water, heating to dissolve, adding 10 parts of aloe polysaccharide and 2.5 parts of tea saponin, and uniformly stirring;
s4, weighing 20 parts of pomegranate bark extract, 10 parts of tannin, adding 40 parts of water, and heating for dissolving;
s5, adding the mixture obtained in the step 3 into the step 4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step 5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step 2 into the step 6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step 7, stirring,
and S9, treating the mixed system obtained in the step 8 by using a colloid mill to obtain a uniform system, namely the natural hair dye taking the pomegranate rind extract as the raw material.
Example 2
Preparation method of pomegranate bark extract
Taking fresh pomegranate rind, drying, crushing to 10-30 meshes, and weighing; adding 7 times of 95% ethanol (s/v), extracting under reflux at 90 deg.C for 3 hr, and filtering; extracting the residue with 5 times of 95% ethanol under reflux for 2.5 hr, filtering, and mixing filtrates. Concentrating under reduced pressure to obtain extract, dissolving the extract in purified water twice the weight of the raw materials, cooling, and centrifuging to obtain insoluble substance A and centrifugate B; passing the centrifugate through macroporous adsorbent resin column, wherein the ratio of the volume of the column bed to the raw material is 1/1 (v/s); washing with water twice the volume of the bed to remove impurities, and eluting with 90% ethanol 3 times the volume of the bed; mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to obtain an extract, and vacuum drying to obtain the pomegranate bark extract.
Second, hair dye formula
Third, the preparation method
S1, weighing 20 parts of FeCl3.6H2O, and adding 20 parts of water for dissolving;
s2, weighing 10 parts of NaOH, and adding 10 parts of water for dissolving;
s3, weighing 2 parts of sodium hyaluronate and 0.5 part of potassium sorbate, adding 50 parts of water, heating to dissolve, adding 20 parts of aloe polysaccharide and 10 parts of tea saponin, and uniformly stirring;
s4, weighing 30 parts of pomegranate bark extract and 20 parts of tannin, adding 50 parts of water, and heating to dissolve;
s5, adding the mixture obtained in the step 3 into the step 4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step 5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step 2 into the step 6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step 7, stirring,
and S9, treating the mixed system obtained in the step 8 by using a colloid mill to obtain a uniform system, namely the natural hair dye taking the pomegranate rind extract as the raw material.
Example 3
Preparation method of pomegranate bark extract
Taking fresh pomegranate rind, drying, crushing to 10-30 meshes, and weighing; adding 6 times of 50% ethanol (s/v), extracting under reflux at 90 deg.C for 3 hr, and filtering; extracting the residue with 5 times of 50% ethanol under reflux for 2.5 hr, filtering, and mixing filtrates; concentrating under reduced pressure to obtain extract, dissolving the extract in purified water twice the weight of the raw materials, cooling, and centrifuging to obtain insoluble substance A and centrifugate B; passing the centrifugate through macroporous adsorbent resin column, wherein the ratio of the volume of the column bed to the raw material is 1/1 (v/s); washing with water twice the volume of the bed to remove impurities, and eluting with 50% ethanol 3 times the volume of the bed; mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to obtain an extract, and performing vacuum drying to obtain the pomegranate bark extract.
Second, hair dye formula
Third, the preparation method
S1, weighing 2.5 parts of FeCl3.6H2O, and adding 2.5 parts of water for dissolving;
s2, weighing 2.5 parts of NaOH, and adding 2.5 parts of water for dissolving;
s3, weighing 5 parts of sodium hyaluronate and 0.5 part of potassium sorbate, adding 50 parts of water, heating to dissolve, adding 5 parts of aloe polysaccharide and 5 parts of tea saponin, and uniformly stirring;
s4, weighing 15 parts of pomegranate bark extract and 15 parts of tannin, adding 30 parts of water, and heating for dissolving;
s5, adding the mixture obtained in the step 3 into the step 4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step 5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step 2 into the step 6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step 7, and stirring;
s9, processing the mixed system obtained in the step 9 by a colloid mill to obtain a uniform system, namely the natural hair dye taking the pomegranate bark extract as the raw material.
Example four
Preparation method of pomegranate rind extract
Taking fresh pomegranate rind, drying, crushing to 10-30 meshes, and weighing; adding 7 times of 70% ethanol (s/v), extracting under reflux at 90 deg.C for 3 hr, and filtering; extracting the residue with 5 times of 70% ethanol under reflux for 2.5 hr, filtering, and mixing filtrates; concentrating under reduced pressure to obtain extract, dissolving the extract in purified water twice the weight of the raw materials, cooling, and centrifuging to obtain insoluble substance A and centrifugate B; passing the centrifugate through macroporous adsorbent resin column, wherein the ratio of the volume of the column bed to the raw material is 1/1 (v/s); washing with water twice the volume of the bed to remove impurities, and eluting with 70% ethanol 3 times the volume of the bed; mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to obtain an extract, and vacuum drying to obtain the pomegranate bark extract.
Second, hair dye formula
Third, the preparation method
S1, weighing 10 parts of FeCl3.6H2O, and adding 10 parts of water for dissolving;
s2, weighing 6 parts of NaOH, and adding 6 parts of water for dissolving;
s3, weighing 3 parts of sodium hyaluronate and 0.5 part of potassium sorbate, adding 64 parts of water, heating to dissolve, adding 10 parts of aloe polysaccharide and 2.5 parts of tea saponin, and uniformly stirring;
s4, weighing 10 parts of pomegranate bark extract, 5 parts of tannin, adding 30 parts of water, and heating for dissolving;
s5, adding the mixture obtained in the step 3 into the step 4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step 5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step 2 into the step 6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step 7, and stirring;
s9, processing the mixed system obtained in the step 9 by a colloid mill to obtain a uniform system, namely the natural hair dye taking the pomegranate bark extract as the raw material.
The use method of the natural hair dye comprises the following steps:
the hair is moistened by hands every morning, a little pasty hair dye is dipped by a toothbrush and evenly smeared on white hair, and the white hair is rubbed back and forth for a moment, so that the hair is dyed into black. The water does not need to be washed immediately, and the water can be washed before sleeping at night.
The four groups of the examples correspond to the hair dyeing effect of natural hair dye:
| examples | 1 | 2 | 3 | 4 |
| Before dyeing hair | White colour (Bai) | White colour (Bai) | White colour (Bai) | White colour (Bai) |
| After dyeing hair | Black (black) | Black (black) | Black colour | Black colour |
| Discomfort feeling | Is free of | Is free of | Is free of | Is composed of |
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. The hair dye taking the pomegranate bark extract as the raw material is characterized by being prepared from the following raw materials in parts by weight: 10-30 parts of pomegranate bark extract, 5-20 parts of tannin, 2.5-20 parts of FeCl3.6H2O, 1-5 parts of sodium hyaluronate, 5-20 parts of aloe polysaccharide, 2.5-10 parts of tea saponin, 2.5-10 parts of NaOH and 85-130 parts of water.
2. The hair dye taking the pomegranate rind extract as the raw material as claimed in claim 1, wherein the pomegranate rind extract is prepared by the following steps:
s1, taking fresh pomegranate rind, drying and crushing to 10-30 meshes;
s2, weighing, adding 50-95% ethanol (S/v) in an amount which is 6-7 times that of the raw materials, carrying out reflux extraction for 3 hours at the water bath temperature of 90 ℃, and filtering;
s3, adding 5 times of 50-95% ethanol into filter residue, reflux-extracting for 2.5 hours, filtering, and combining the filtrates;
s4, concentrating under reduced pressure to obtain extract, dissolving the extract in purified water twice the weight of the raw materials, cooling, and centrifuging to obtain insoluble substance A and centrifugate B;
s5, passing the centrifugate through a macroporous adsorption resin column, wherein the ratio of the volume of a column bed to the raw material is 1/1 (v/S);
s6, removing impurities by washing with water with the volume twice that of the column bed, eluting with 80% ethanol with the volume three times that of the column bed, mixing and dissolving the centrifugal insoluble substance A and the eluent, concentrating to be paste-like, and drying in vacuum to obtain the pomegranate bark extract.
3. The hair dye taking the pomegranate rind extract as the raw material as claimed in claim 1, wherein the hair dye raw material further comprises 0.5 part of mint essential oil and 0.5 part of potassium sorbate.
4. A preparation method of a hair dye taking a pomegranate bark extract as a raw material is characterized by comprising the following steps:
s1, weighing 2.5-20 parts of FeCl3.6H2O, and adding 2.5-20 parts of water for dissolving;
s2, weighing 2.5-10 parts of NaOH, and adding 2.5-20 parts of water for dissolving;
s3, weighing 1-5 parts of sodium hyaluronate and 0.5 part of potassium sorbate, adding 50-64 parts of water, heating to dissolve, adding 5-20 parts of aloe polysaccharide and 2.5-10 parts of tea saponin, and uniformly stirring;
s4, weighing 10-30 parts of pomegranate bark extract, 5-20 parts of tannin, adding 30-50 parts of water, and heating for dissolving;
s5, adding the mixture obtained in the step S4, and uniformly stirring;
s6, adding the ferric trichloride solution obtained in the step 1 into the step S5, and uniformly stirring;
s7, adding the sodium hydroxide solution obtained in the step 2 into the step S6, and uniformly stirring;
s8, adding 0.5 part of mint essential oil into the step S7, and stirring;
s9, processing the mixed system obtained in the step S8 by a colloid mill to obtain a uniform system, namely the natural hair dye taking the pomegranate rind extract as the raw material.
5. The method of claim 4, wherein the pomegranate bark extract is rich in a plurality of nutrients including tannin, wax, mannitol, mucilage, gallic acid, malic acid, pectin, gum, isoquercitrin, cyanidin-3-glucoside, cyanidin-3, 5-diglucose, crying-geraniin-3-glucoside, anthocyanins such as crying-geranium-3, 5-diglucose, and amino acids.
6. The method for preparing the hair dye using the pomegranate rind extract as a raw material according to claim 4, wherein the hair dye obtained in the step S9 is used by wetting the hair with hands in the morning, dipping a little pasty hair dye with a toothbrush, uniformly applying the pasty hair dye on the white hair, and rubbing the hair back and forth for a moment, so that the hair is dyed into black, and the hair is washed before sleeping at night without being washed immediately.
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