CN114621823A - Multifunctional cleaning disinfectant and preparation method thereof - Google Patents

Multifunctional cleaning disinfectant and preparation method thereof Download PDF

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Publication number
CN114621823A
CN114621823A CN202210326483.9A CN202210326483A CN114621823A CN 114621823 A CN114621823 A CN 114621823A CN 202210326483 A CN202210326483 A CN 202210326483A CN 114621823 A CN114621823 A CN 114621823A
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China
Prior art keywords
parts
multifunctional cleaning
disinfectant
cleaning
biosurfactant
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Pending
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CN202210326483.9A
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Chinese (zh)
Inventor
张勇斌
李星炎
齐元胜
梁荣华
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Nanjing Junke Chaocai Technology Co ltd
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Nanjing Junke Chaocai Technology Co ltd
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Priority to CN202210326483.9A priority Critical patent/CN114621823A/en
Publication of CN114621823A publication Critical patent/CN114621823A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C11D1/06—Ether- or thioether carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38618—Protease or amylase in liquid compositions only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/10—Objects to be cleaned
    • C11D2111/14—Hard surfaces

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to the technical field of disinfectant preparation, in particular to a multifunctional cleaning disinfectant and a preparation method thereof. The multifunctional cleaning disinfectant is prepared from the following components in parts by mass: 0.1-5 parts of biosurfactant, 0.1-3 parts of biological enzyme, 0.1-3 parts of cosolvent, 0.1-6 parts of bactericide, 0.1-3 parts of auxiliary agent and 50-100 parts of water. According to the invention, through the addition of various components such as biosurfactant, biostatic enzyme, modern high-efficiency nano silver ions and the like, the technical effects of high-efficiency cleaning, quick sterilization, green, convenience, harmless residue, safety and environmental protection are achieved, and the sanitation, safety and normal logistics supply of outdoor food of troops can be effectively guaranteed.

Description

Multifunctional cleaning disinfectant and preparation method thereof
Technical Field
The invention relates to the technical field of disinfectant preparation, in particular to a multifunctional cleaning disinfectant and a preparation method thereof.
Background
The cleaning disinfectant is widely applied to different places such as restaurants, hospitals, schools and the like, and has very positive and effective effects on human health and sanitation. The cleaning and disinfecting liquid is roughly divided into the following parts by distinguishing from the disinfecting components: oxygenates, aldehydes, phenols, alcohols, bases, salts, halogens, surfactants; generally, the cleaning agent is classified into three main types, i.e., an aqueous cleaning agent, a semi-aqueous cleaning agent and a non-aqueous cleaning agent. Most of the cleaning disinfectant used in daily life belongs to a water-based cleaning agent, and an ideal cleaning disinfectant needs to have strong decontamination capability and is environment-friendly, convenient to use for cleaning and disinfection and harmless to human health, and a cleaned water body is easy to purify and meets the safety and environment-friendly standard.
The common chemical disinfectant utilizes chemical drugs to permeate into the body of bacteria, so that mycoprotein coagulates and denaturates, the activity of bacterial enzyme is interfered, the metabolism and growth of the bacteria are inhibited or the structure of a bacterial membrane is damaged, the permeability of the bacteria is changed, the physiological function of the bacteria is damaged, and the like, thereby achieving the purposes of disinfection and sterilization. However, the use effect of many chemical disinfectants is poor due to the problems of safety and health, environmental residual pollution and microbial drug resistance caused by chemicals, and the chemical disinfectants cause damage to the environment, so that people often have a lot of concerns and dissatisfaction when using the disinfectants.
Therefore, the technical problem that needs to be solved by the technical staff in the field is how to provide a disinfectant solution with good sterilizing effect and no harm to human body and environment so as to solve the technical problems of high residue of chemical disinfectants and damage to human environment in the prior art.
Disclosure of Invention
The invention aims to provide a multifunctional cleaning disinfectant and a preparation method thereof, and the multifunctional cleaning disinfectant achieves the technical effects of efficient cleaning, rapid sterilization, green, convenience, no harm to residue, safety and environmental protection by adding various components such as biological surface active factors, biological antibacterial enzymes, modern efficient nano silver ions and the like, and can effectively guarantee the food sanitation safety and the normal logistics supply of personnel in the field.
In order to achieve the above object, the present invention provides the following technical solutions:
the invention provides a multifunctional cleaning disinfectant, which is prepared from the following components in parts by mass: 0.1-5 parts of biosurfactant, 0.1-3 parts of biological enzyme, 0.1-3 parts of cosolvent, 0.1-6 parts of bactericide, 0.1-3 parts of auxiliary agent and 50-100 parts of water.
Preferably, the biosurfactant is one or more of rhamnolipid, sophorolipid, algal glycolipid and sucrose ester.
Preferably, the biological enzyme is one or more of lipase, protease and lysozyme.
Preferably, the dissolution promoter is one or more of N-alkyl glucamide, fatty alcohol polyoxyethylene ether, alkyl glycoside, polyoxypropylene block polymer and polyoxyethylene sorbitan monooleate.
Preferably, the bactericide is one or more of nano silver ions, hydrogen peroxide, 8-hydroxyquinoline and dodecylamine ethyl glycine.
Preferably, the adjuvant is one or more of lactic acid, acetic acid, sodium gluconate, sodium citrate, ethylene diamine tetraacetic acid and cyclodextrin.
The invention also provides a preparation method of the multifunctional cleaning disinfectant, which mixes the biosurfactant, the biological enzyme, the cosolvent, the bactericide, the auxiliary agent and water.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, the biological enzyme, the biological surfactant and the bactericide are compounded, so that the synergistic effect is achieved, the cleaning permeability of the cleaning agent and the disinfection and sterilization effects of the bactericide can be effectively enhanced, and the purposes of efficient cleaning and sterilization, environmental protection, health, safety, convenience and harmlessness are achieved.
2. The invention can be used for quickly cleaning and disinfecting the surfaces of tableware, kitchen supplies, a plurality of daily office supplies and the like, and the sterilization rate reaches 99.9 percent; the cleaning agent can also be used for simple cleaning and disinfection of fruits and vegetables, can effectively remove microorganisms and residual pesticides on the surfaces of the fruits and the vegetables, prolongs the preservation and the preservation, and avoids the pollution of harmful microorganisms and toxins thereof. The device has six advantages of high efficiency, cleanness, rapid sterilization, energy and water conservation, greenness, convenience, harmless residue, safety and environmental protection, and can effectively guarantee the dietary sanitation safety and the normal logistics supply of personnel in the field. Meanwhile, the problem of white pollution to the environment caused by using a large amount of disposable tableware is also avoided.
3. The cleaning disinfectant has a washing-free function, tableware, utensils and the like can be cleaned by directly using the cleaning disinfectant, and meanwhile, the cleaning and disinfection of the utensils are completed, so that the cleaning efficiency is greatly improved, and the waste of domestic water is reduced. The food such as fruits and the like can be directly eaten after being cleaned, and the problems that the outdoor clean water source is difficult to find, the electric heating disinfection consumes time, the chemical cleaning wastes energy and water, the cleaning sewage is discharged and polluted and the like are effectively solved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the provided drawings without creative efforts.
Fig. 1 to 9 show the test report of the multi-functional cleaning and disinfecting solution spectral density (the entrusted unit is the unit because the Beijing Anxinhaoder cleaning company is the parent company of the Nanjing military science and technology company and is responsible for the earlier-stage research of the cleaning agent product of the Nanjing military science and technology company).
Detailed Description
The invention provides a multifunctional cleaning disinfectant, which is prepared from the following components in parts by mass: 0.1-5 parts of a biosurfactant, 0.1-3 parts of a biological enzyme, 0.1-3 parts of a cosolvent, 0.1-6 parts of a bactericide, 0.1-3 parts of an auxiliary agent and 50-100 parts of water; the compound is preferably prepared from the following components in parts by mass: 1-4 parts of a biological surfactant, 1-2 parts of a biological enzyme, 1-2 parts of a dissolving promoter, 1-5 parts of a bactericide, 1-2 parts of an auxiliary agent and 60-90 parts of water; the composite material is further preferably prepared from the following components in parts by mass: 2-3 parts of a biological surfactant, 1.5 parts of a biological enzyme, 1.5 parts of a cosolvent, 2-4 parts of a bactericide, 1.5 parts of an auxiliary agent and 70-80 parts of water; more preferably, the composition is prepared from the following components in parts by mass: 2.5 parts of biosurfactant, 1.5 parts of biological enzyme, 1.5 parts of cosolvent, 2-4 parts of bactericide, 1.5 parts of auxiliary agent and 75 parts of water.
In the present invention, the biosurfactant is one or more of rhamnolipid, sophorolipid, algal glycolipid and sucrose ester; preferably sophorolipid and sucrose ester, the mass ratio of sophorolipid to sucrose ester is 2: 1.
In the present invention, the biological enzyme is one or more of lipase, protease and lysozyme; preferably lipases and lysozymes; the mass ratio of the lipase to the lysozyme is 1: 1.
In the invention, the dissolution promoter is one or more of N-alkyl glucamide, fatty alcohol polyoxyethylene ether, alkyl glycoside, polyoxypropylene block polymer and polyoxyethylene sorbitan monooleate; preferably N-alkyl glucamide, alkyl glycoside and fatty alcohol-polyoxyethylene ether; the proportion of the N-alkyl glucosamide, the alkyl glycoside and the fatty alcohol-polyoxyethylene ether is 1: 1.
In the invention, the bactericide is one or more of nano silver ions, hydrogen peroxide, 8-hydroxyquinoline and dodecylamine ethyl glycine; preferably nano silver ions, hydrogen peroxide and dodecylamine ethyl glycine; the ratio of the nano silver ions, the hydrogen peroxide and the dodecylamine ethyl glycine is 2: 10: 15.
In the invention, the auxiliary agent is one or more of lactic acid, acetic acid, sodium gluconate, sodium citrate, ethylene diamine tetraacetic acid and cyclodextrin; preferably lactic acid, sodium gluconate, ethylene diamine tetraacetic acid and cyclodextrin; the ratio of the lactic acid to the sodium gluconate to the ethylene diamine tetraacetic acid to the cyclodextrin is 2: 3: 1.
The invention also provides a preparation method of the multifunctional cleaning disinfectant, which mixes the biosurfactant, the biological enzyme, the cosolvent, the bactericide, the auxiliary agent and water.
The technical solutions provided by the present invention are described in detail below with reference to examples, but they should not be construed as limiting the scope of the present invention.
Example 1
A multifunctional cleaning disinfectant is prepared from the following components in parts by mass:
1 part of sophorolipid, 0.5 part of sucrose ester, 0.5 part of lipase, 0.5 part of lysozyme, 0.5 part of N-alkyl glucose fatty amide, 0.5 part of fatty alcohol-polyoxyethylene ether, 0.5 part of alkyl glycoside, 0.2 part of nano silver ion, 1 part of hydrogen peroxide, 1.5 parts of dodecylamine ethyl glycine, 0.2 part of lactic acid, 0.3 part of sodium gluconate, 0.1 part of ethylene diamine tetraacetic acid, 0.1 part of cyclodextrin and 100 parts of water;
the preparation method of the multifunctional cleaning disinfectant comprises the following steps: mixing the above components.
Example 2
A multifunctional cleaning disinfectant is prepared from the following components in parts by mass:
3 parts of rhamnolipid, 2 parts of sucrose ester, 0.1 part of lipase, 0.2 part of protease, 0.1 part of lysozyme, 1 part of N-alkyl glucose fatty amide, 1 part of fatty alcohol-polyoxyethylene ether, 1 part of alkyl glycoside, 0.4 part of nano silver ions, 1.6 parts of hydrogen peroxide, 0.3 part of lactic acid, 0.3 part of acetic acid, 2.1 parts of sodium gluconate, 0.1 part of ethylene diamine tetraacetic acid, 0.2 part of cyclodextrin and 100 parts of water;
the preparation method of the multifunctional cleaning disinfectant comprises the following steps: mixing the above components.
Example 3
A multifunctional cleaning disinfectant is prepared from the following components in parts by mass:
0.1 part of algal glycolipid, 0.1 part of sophorolipid, 0.1 part of lipase, 0.05 part of fatty alcohol-polyoxyethylene ether, 0.05 part of alkyl glycoside, 0.02 part of nano silver ion, 0.06 part of hydrogen peroxide, 0.02 part of 8-hydroxyquinoline, 0.05 part of lactic acid, 0.05 part of sodium gluconate and 100 parts of water;
the preparation method of the multifunctional cleaning disinfectant comprises the following steps: mixing the above components.
Example 4
A multifunctional cleaning disinfectant is prepared from the following components in parts by mass:
0.2 part of algal glycolipid, 0.3 part of sucrose ester, 0.4 part of protease, 0.1 part of lysozyme, 0.4 part of N-alkyl glucamide, 0.5 part of alkyl glycoside, 0.2 part of polyoxyethylene sorbitan monooleate, 0.5 part of 8-hydroxyquinoline, 0.5 part of dodecylamine ethyl glycine, 0.2 part of acetic acid, 0.2 part of sodium citrate, 0.1 part of ethylene diamine tetraacetic acid and 100 parts of water;
the preparation method of the multifunctional cleaning disinfectant comprises the following steps: mixing the above components.
Example 5
The multifunctional cleaning disinfectant obtained in example 1 was subjected to a sterilization experiment. The experimental indicator bacteria comprise staphylococcus aureus (ATCC 6538) and escherichia coli (8099), which are provided by the institute of microorganisms of Chinese academy of sciences.
The sterilization experiment is carried out according to a quantitative suspension sterilization test method in 'sterilization technical specification' issued by the national ministry of health. And inoculating a single colony of each test bacterium to a common nutrient agar culture medium slant, and culturing for 24 hours at 37 ℃. Collecting fresh slant culture of each test bacteria, washing off thallus Porphyrae on the slant with tryptone-containing diluent (TPS), diluting with sterile water to obtain test bacterial suspension with concentration of 1 × 106～5×106cfu/ml。
The cleaning disinfectant obtained in example 1 was diluted 20 times with distilled water to prepare a 5% solution, which was then kept at 20 ℃ for further use. Respectively sucking 0.5ml of test bacterial suspension, respectively adding into test tubes containing 4.5ml of diluted cleaning disinfectant, rapidly mixing, acting for 5min, respectively adding neutralizer, and performing serial 10-fold dilution for plate coating. A parallel experiment was performed using the sterile water diluent instead of the cleaning disinfectant, as a positive control. And (4) culturing the bacterial trophosome test sample in an incubator at 37 ℃ for 48 hours, observing the final result and respectively calculating the sterilization rate.
The bactericidal ratio was [ (average viable count of control group-average viable count of test group)/average count of control group ] × 100%
Average number of viable bacteria on plate Control group Disinfectant set Rate of sterilization
Escherichia coli 103 0 100％
Staphylococcus aureus 389 0 100％
According to the experimental data, the cleaning and disinfecting liquid disclosed by the invention has good sterilization and bacteriostasis effects on escherichia coli and staphylococcus aureus, and the cleaning and disinfecting liquid is an excellent sterilization product.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.

Claims (7)

1. The multifunctional cleaning disinfectant is characterized by being prepared from the following components in parts by mass: 0.1-5 parts of biosurfactant, 0.1-3 parts of biological enzyme, 0.1-3 parts of cosolvent, 0.1-6 parts of bactericide, 0.1-3 parts of auxiliary agent and 50-100 parts of water.
2. The multifunctional cleaning and disinfecting solution of claim 1, wherein the biosurfactant is one or more of rhamnolipid, sophorolipid, algal glycolipid and sucrose ester.
3. The multifunctional cleaning disinfectant as claimed in claim 1, wherein said biological enzyme is one or more of lipase, protease and lysozyme.
4. The multifunctional cleaning and disinfecting solution of claim 1, wherein the dissolution promoter is one or more of N-alkyl glucamide, fatty alcohol-polyoxyethylene ether, alkyl glycoside, polyoxypropylene block polymer and polyoxyethylene sorbitan monooleate.
5. The multifunctional cleaning and disinfecting solution of claim 1, wherein the disinfectant is one or more of nano silver ions, hydrogen peroxide, 8-hydroxyquinoline and dodecylamine ethyl glycine.
6. The multifunctional cleaning and disinfecting liquid as claimed in claim 1, wherein the auxiliary agent is one or more of lactic acid, acetic acid, sodium gluconate, sodium citrate, ethylenediamine tetraacetic acid and cyclodextrin.
7. The method for preparing a multifunctional cleaning and disinfecting solution as claimed in any one of claims 1 to 6, wherein the biosurfactant, the biological enzyme, the cosolvent, the bactericide, the adjuvant and water are mixed.
CN202210326483.9A 2022-03-30 2022-03-30 Multifunctional cleaning disinfectant and preparation method thereof Pending CN114621823A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115975747A (en) * 2022-11-07 2023-04-18 杭州西子卫生消毒药械有限公司 Enzyme cleaning solution and use method thereof
CN116509827A (en) * 2023-04-28 2023-08-01 天津大学 Clean skin disinfectant and application thereof
EP4361238A1 (en) * 2022-10-26 2024-05-01 ChemTEK UG (haftungsbeschränkt) Compositions comprising glycamines

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106591013A (en) * 2016-11-30 2017-04-26 大连百奥泰科技有限公司 Biological detergent composition
US20170128605A1 (en) * 2015-11-10 2017-05-11 American Sterilizer Company Cleaning and disinfecting composition
CN113930295A (en) * 2021-11-10 2022-01-14 广州市爱家有方日用品有限公司 Cleaning composition containing biological enzyme and preparation method thereof
CN114149871A (en) * 2021-12-20 2022-03-08 南京军科超材科技有限公司 Biological environment-friendly oil stain cleaning agent with fire extinguishing function and preparation method and application thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20170128605A1 (en) * 2015-11-10 2017-05-11 American Sterilizer Company Cleaning and disinfecting composition
CN106591013A (en) * 2016-11-30 2017-04-26 大连百奥泰科技有限公司 Biological detergent composition
CN113930295A (en) * 2021-11-10 2022-01-14 广州市爱家有方日用品有限公司 Cleaning composition containing biological enzyme and preparation method thereof
CN114149871A (en) * 2021-12-20 2022-03-08 南京军科超材科技有限公司 Biological environment-friendly oil stain cleaning agent with fire extinguishing function and preparation method and application thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4361238A1 (en) * 2022-10-26 2024-05-01 ChemTEK UG (haftungsbeschränkt) Compositions comprising glycamines
CN115975747A (en) * 2022-11-07 2023-04-18 杭州西子卫生消毒药械有限公司 Enzyme cleaning solution and use method thereof
CN116509827A (en) * 2023-04-28 2023-08-01 天津大学 Clean skin disinfectant and application thereof

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