CN114575164A - 一种耐久天然抗菌防蚊香味整理剂的应用工艺 - Google Patents
一种耐久天然抗菌防蚊香味整理剂的应用工艺 Download PDFInfo
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Abstract
本发明公开一种耐久天然抗菌防蚊香味整理剂的应用工艺，使用水蒸气蒸馏法，从艾草中的茎、叶中提取艾草精油，将提取的精油与包覆壁材进行均质乳化，再通过升温聚合作用，将精油包覆在壁材之中，从而形成稳定、易分散的微胶囊乳液，开稀后的乳液采用浸渍、浸轧或喷淋的方式整理到织物上，通过焙烘，交联并反应到织物上。经本发明整理后的织物，具有缓慢释放香味以及高效、持久抗菌防蚊的功能，生产的成品可用于服装、蚊帐、毛巾被、睡衣、枕套等，可直接与人体皮肤接触，无刺激性。
Description
技术领域
本发明涉及纺织品整理技术领域，具体涉及一种耐久天然抗菌防蚊香味整理剂的应用工艺。
背景技术
纺织品的抗菌和防蚊整理为两种不同的功能性整理：
1)抗菌整理常常使用抗菌剂，分为非天然和天然两种类型，非天然一般有重金属离子(银离子、锌离子等)、双胍、季铵盐等种类，天然抗菌剂主要为甲壳素抗菌剂、植物精油等；
2)防蚊整理剂一般为氯菊酯类产品，驱避蚊虫。一般抗菌剂不具有防蚊效果，防蚊剂不具有抗菌效果。同时非天然类的抗菌剂和防蚊剂一般都有异味，且可能对人体有一定的危害。
发明内容
本发明目的是开发一种耐久天然抗菌防蚊香味整理剂的应用工艺，打破抗菌、防蚊的技术壁垒，将抗菌、防蚊统一应用于纺织品上，并带来清新宜人的香味，在保护人体健康的同时，提供宜人的香味，舒缓身心。通过该整理剂整理后的织物，具有缓慢释放香味以及高效、持久抗菌防蚊的功能，生产的成品可用于服装、蚊帐、毛巾被、睡衣、枕套等，可直接与人体皮肤接触，无刺激性，以克服现有技术的不足。
本发明所采用的技术方案如下：
一种耐久天然抗菌防蚊香味整理剂的应用工艺，包括以下步骤：1)使用水蒸气蒸馏法，从艾草中的茎、叶中提取艾草精油；2)将艾草精油与包覆壁材进行均质乳化；3)通过升温聚合作用，将精油包覆在壁材之中，从而形成稳定、易分散的微胶囊乳液；4)开稀后的乳液采用浸渍、浸轧或喷淋的方式整理到织物上，然后焙烘，使其交联并反应到织物上。
步骤4)采用定形机加工，加工工艺是一浸一轧，压力2.0kg/cm2，车速 20m/min，140℃定形。
均质乳化工艺：将精油和壁材按一定的比例及少量乳化剂进行搅拌，混合均匀；在40℃恒温水浴中，以6000r/min的速度高剪切均质乳化处理，得到均一的水包油乳液。
升温聚合工艺：升温聚合工艺是在3000r/min的机械搅拌条件下，以40℃开始，以1℃/min速度升温后保温持续搅拌，然后迅速降温凝集成微胶囊乳液。
本发明的有益效果是：
(1)对人体环保、友好：防蚊剂和抗菌剂一般为化学合成制剂，对人体具有一定的刺激性，而艾草防蚊整理剂是从草本植物中进行原料采集而来的，因此对人体皮肤友好。
(2)抗菌防蚊效果优异：经整理剂整理后的纺织品，通过第三方检测机构测试：1)蚊虫的驱避率高达80％，达到了GBT30126防蚊评价的A级；2)抗菌效果达到FZ/T73023的AAA抗菌要求。
(3)织物舒适性好：经本产品整理后的织物具有持久的天然艾草香味，增加了纺织品的服用性能。
(4)加工工艺合理、易实现产业化：本发明抗菌防蚊整理的加工工艺简易，可以通过浸渍和浸轧两种方式进行处理。通过调整用量满足不同的市场需求，产业化加工操作简易。
具体实施方式
下面详细描述本发明的实施例，仅用于解释本发明，而不能理解为对本发明的限制。
本发明通过使用具有特殊反应型结构的抗紫外线整理剂进行加工，使织物获得优异的抗紫外效果，从而满足各种市场需求。
艾草是一种具有极高药用价值的草本植物，而被记录于《尔雅》、《本草纲目》等中药典籍之中，有消炎、止血、祛湿、抗过敏等诸多功效。本发明首先通过使用水蒸气蒸馏法，从艾草中的茎、叶中提取艾草精油，但精油具有不稳定性且不溶于水，不能直接作用于纺织品；须将提取的精油、特殊的包覆壁材进行均质乳化，再通过升温聚合作用，将精油包覆在壁材之中，从而形成稳定、易分散的微胶囊乳液。均质乳化工艺：将精油和壁材按一定的比例及少量乳化剂进行搅拌，混合均匀；在40℃恒温水浴中，以6000r/min的速度高剪切均质乳化处理，得到均一的水包油乳液。升温聚合工艺：升温聚合工艺是在 3000r/min的机械搅拌条件下，以40℃开始，以1℃/min速度升温后保温持续搅拌，然后迅速降温凝集成微胶囊乳液。
开稀后的乳液(即工作液)，采用浸渍、浸轧或喷淋的方式整理到织物上，通过一定的温度焙烘，可以交联并反应到织物上，因此具有良好的耐洗性能；织物经过摩擦、拍打、揉搓等作用，使得微胶囊壁材局部破裂，芯材缓慢释放，从而具有长效的抗菌、防蚊效果。
实施例一：
加工织物：无纺布
助剂用量：30g/L
加工方式：定形机加工
加工工艺：一浸一轧(压力2.0kg/cm2，车速20m/min)，140℃定形。
整理后织物对白纹伊蚊驱避率80.77％，达到GBT30126防蚊评价的A级。
实施例二：
加工织物：绉纱印花布
助剂用量：50g/L
加工方式：定形机加工
加工工艺：一浸一轧(压力2.0kg/cm2，车速20m/min)，140℃定形。
整理后织物对白纹伊蚊驱避率69.52％，达到GBT30126防蚊评价的B级。
实施例三：
加工织物：棉针织布
助剂用量：30g/L
加工方式：定形机加工
加工工艺：一浸一轧(压力2.0kg/cm2，车速20m/min)，140℃定形。
整理后的棉针织布满足FZ/T73023的AAA抗菌要求(洗涤50次)。
尽管已经示出和描述了本发明的实施例，本领域的普通技术人员应当理解：在不脱离本发明的原理和宗旨的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由权利要求及其等同替换所限定，在未经创造性劳动所作的改进等，均应包含在本发明的保护范围之内。
Claims (4)
1.一种耐久天然抗菌防蚊香味整理剂的应用工艺，其特征在于包括以下步骤：1)使用水蒸气蒸馏法，从艾草中的茎、叶中提取艾草精油；2)将艾草精油与包覆壁材进行均质乳化；3)通过升温聚合作用，将精油包覆在壁材之中，从而形成稳定、易分散的微胶囊乳液；4)开稀后的乳液采用浸渍、浸轧或喷淋的方式整理到织物上，然后焙烘，使其交联并反应到织物上。
2.根据权利要求1所述的耐久天然抗菌防蚊香味整理剂的应用工艺，其特征在于：步骤4)采用定形机加工，加工工艺是一浸一轧，压力2.0kg/cm2，车速20m/min，140℃定形。
3.根据权利要求1或2所述的耐久天然抗菌防蚊香味整理剂的应用工艺，其特征在于：在步骤2)中，均质乳化工艺是将精油和壁材一起搅拌，混合均匀；在40℃恒温水浴中，以6000r/min的速度高剪切均质乳化处理，得到均一的水包油乳液。
4.根据权利要求4所述的耐久天然抗菌防蚊香味整理剂的应用工艺，其特征在于：在步骤3)中，升温聚合工艺是在3000r/min的机械搅拌条件下，以40℃开始，以1℃/min速度升温后保温持续搅拌，然后迅速降温凝集成微胶囊乳液。
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