CN114504117A - Preparation method of heating non-combustible fuming base material - Google Patents
Preparation method of heating non-combustible fuming base material Download PDFInfo
- Publication number
- CN114504117A CN114504117A CN202210134124.3A CN202210134124A CN114504117A CN 114504117 A CN114504117 A CN 114504117A CN 202210134124 A CN202210134124 A CN 202210134124A CN 114504117 A CN114504117 A CN 114504117A
- Authority
- CN
- China
- Prior art keywords
- powder
- smoking
- plant
- preparation
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/285—Treatment of tobacco products or tobacco substitutes by chemical substances characterised by structural features, e.g. particle shape or size
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/42—Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention relates to a preparation method of a heating non-combustible fuming base material. The non-combustible heating fuming base material has the characteristics of sufficient smoke quantity, soft smoke, good delicate sense, sufficient aroma quantity, good smoke richness and obviously weakened miscellaneous gas, and has good sensory quality; meanwhile, in the preparation method, the water content is controlled to be not 15-40%, the long-time heating in the drying and forming process is reduced, and the volatilization loss of the fragrance components of the base material is reduced.
Description
[ technical field ] A
The invention belongs to the technical field of heating non-combustible products. More particularly, the present invention relates to a method of making a heated non-combustible smoking substrate.
[ background of the invention ]
In recent years, the global smoke control environment is becoming more and more severe, consumers pay more and more attention to health, and meanwhile, health is also paid more and more attention, so that novel tobacco products which greatly reduce the release amount of harmful components of tobacco are rapidly becoming the development focus of tobacco industries of all countries in the world, and the market share is gradually increased. At present, tobacco industry enterprises are faced with the contradiction of paying attention to the health of consumers, reducing the release amount of harmful substances in cigarettes and improving economic benefits, so that the research and development of novel low-harm tobacco become an important subject and an innovative development direction of the tobacco industry.
The heating non-combustible cigarette is one of the novel tobacco product types, and is mainly characterized in that a heat source is used for heating and baking a tobacco material at a lower temperature (300-. At present, the base material is manufactured by the traditional paper making method, the rolling method and the thick pulp method mainly through heating the non-burning tobacco, and then a certain amount of essence and spice is added on the basis of the base material, so that the aroma and the flavor of the non-burning tobacco are enriched. However, due to the limitation of the processing technology, the problems of insufficient smoke adsorption capacity and peculiar smell generated in the smoking process due to the fact that the existing base material is low in adsorption performance or low in adhesive consumption exist, and meanwhile, the problems of insufficient smoke amount, insufficient aroma amount, firewood smell, miscellaneous gas and the like generally exist in the existing commercially available non-burning heating smoke bomb, and the sensory experience of consumers is poor.
Therefore, the present inventors have completed the present invention by a large number of experimental studies and analyses for overcoming the technical defects of the prior art.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide a preparation method of a heating non-combustion fuming base material.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a preparation method of a heating non-combustion fuming base material.
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Uniformly mixing the spice plant powder, the fuming material powder, the forming auxiliary agent and the additive by using mixing equipment to obtain a mixed material;
B. adding water
Adding water accounting for 15-40% of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a paste or colloid mixed material;
C. press forming
And D, processing the paste or colloid mixed material obtained in the step B into a strip or sheet mixed material by adopting a spiral roller extrusion method or a rolling method, and then heating and drying in drying equipment to obtain the strip or sheet heating non-combustion fuming base material.
According to a preferred embodiment of the present invention, in step a, the weight ratio of the perfume plant powder, the smoking material powder, the forming aid and the additive is 50 to 80: 10-20: 5-15: 0 to 5.
According to another preferred embodiment of the present invention, in the step a, the aromatic plant powder is one or more aromatic plant powders selected from tea powder, tea stalk powder, areca nut powder, coffee powder, barley tea powder, mint powder, lotus leaf powder, Compositae plant powder, Rosaceae plant powder or orchid plant powder;
wherein the Compositae plant is flos Chrysanthemi, Bellis Perennis, Severum cinerascens or Tagetes Erecta; the Rosaceae plant is flos Rosae Rugosae, flos Rosae Multiflorae, flos Rosae chinensis or flos persicae; the orchid family plant is orchid, dendrobium, gastrodia elata or butterfly orchid.
According to another preferred embodiment of the present invention, in step a, the particle size of the spice plant powder or the smoking material powder is 100 to 160 mesh.
According to another preferred embodiment of the invention, in step a, the smoking material is one or more smoking materials selected from the group consisting of glycerol, medium chain triglycerides or propylene glycol.
According to another preferred embodiment of the present invention, in step a, the forming aid is one or more forming aids selected from sodium carboxymethylcellulose, sodium polyacrylate, pectin, guar gum or sodium alginate.
According to another preferred embodiment of the present invention, in step a, the additive is one or more additives selected from the group consisting of flavors, calcium salts, sweeteners or cooling agents.
According to another preferred embodiment of the present invention, the aroma flavor is one or more aroma flavors selected from floral, fruity, tobacco or plant extracts; the calcium salt is one or more calcium salts selected from calcium carbonate, calcium bicarbonate or calcium chloride; the sweetener is one or more selected from sucralose, aspartame, neotame or saccharin; the cooling agent is one or more cooling agents selected from WS-23, WS-3 or menthol.
According to another preferred embodiment of the invention, in the step C, the strip-shaped or sheet-shaped mixed material obtained in the step B is dried by heating at 90-120 ℃ for 8-10 min in a drying device selected from electrothermal blowing drying, microwave drying or infrared drying.
According to another preferred embodiment of the invention, the rod-or sheet-shaped heated non-burning smoking substrate obtained in step C has a water content of 10% by weight or less.
The present invention will be described in more detail below.
The invention relates to a preparation method of a heating non-combustible fuming base material.
According to the present invention, a heated non-combustible smoking substrate is understood to be a smoking material of the type which heats a non-combustible sheet.
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Uniformly mixing the spice plant powder, the fuming material powder, the forming auxiliary agent and the additive by using mixing equipment to obtain a mixed material;
according to the present invention, the essential role of the perfume plant in heating a non-burning smoking substrate is primarily to provide the aroma component to the heating of the non-burning smoking substrate.
The spice plant powder used in the invention is one or more spice plant powders selected from tea powder, tea stalk powder, areca nut powder, coffee powder, barley tea powder, mint powder, lotus leaf powder, compositae plant powder, rosaceae plant powder or orchidaceae plant powder;
wherein the tea powder is one or more selected from green tea, black tea, pulverized YINZI, and pulverized YINZICHUN tea; the tea stalk powder is one or more tea stalk powder selected from green tea, black tea, white tea or yellow tea stalk, and in the invention, the tea stalk is understood to be the tender branch stem of green tea, black tea, crushed silverweed or crushed silverweed tea plant; the areca powder is one or more areca powders selected from Chinese olive areca, black nut areca, Hainan variety or heat ground No. 1 variety areca; the coffee powder is one or more coffee powders selected from coffee of the varieties of blue mountain coffee, black coffee, Yunnan arabica coffee or Vietnam coffee; the barley tea powder is one or more selected from Korean barley tea, oil-cut barley tea, domestic barley tea or high-confidence organic barley tea; the mint powder is one or more mint powder selected from apple mint, spearmint, pineapple mint or lemon perfume mint; the lotus leaf powder is one or more lotus leaves selected from Weishan lake lotus leaves, Yihongtang lotus leaves or Qingmajie lotus leaves; the Compositae plant is flos Chrysanthemi, Bellis Perennis, flos Chrysanthemi or flos Tagetis Erectae; the Rosaceae plant is flos Rosae Rugosae, flos Rosae Multiflorae, flos Rosae chinensis or flos persicae; the orchid family plant is orchid, dendrobium, gastrodia elata or butterfly orchid.
The spice plant powder used in the present invention is a powder made of products currently marketed, such as green tea sold under the trade name dehydrated green tea powder by Jiangsu Jinjie food Co., Ltd, mint powder sold under the trade name mint powder by Kangdu pharmaceutical Co., Ltd, lotus leaf powder sold under the trade name food-grade lotus leaf powder by Tanzhou Wangpio food Co., Ltd, chrysanthemum sold under the trade name chrysanthemum tea by Huangshan Hua food trade Co., Ltd, rose sold under the trade name Yunnan red flower by Jingning Hongheng trade company, and dendrobium sold under the trade name dendrobium huoshan by the Ministry of medical science in Liu Tian Hua of the Ming city.
In accordance with the present invention, the primary function of the smoking material in heating a non-burning smoking substrate is to provide the smoking amount to the smoking substrate.
The smoking material used in the present invention is one or more smoking materials selected from glycerol, medium chain triglycerides or propylene glycol, all of which are currently marketed products, such as medium chain triglycerides sold under the trade name food grade MCT oil by shanghai kooqing bio.
According to the invention, the particle size of the spice plant powder or the smoking material powder is 100-160 meshes. If they are less than 100 mesh in size, the surface of the smoking material may be uneven, affecting its flatness and hence its performance; if their particle size is larger than 160 mesh, they will affect the carrying ability of the smoking material, and thus affect the aroma of the smoking material; therefore, they are suitable in the particle size of 100 to 160 mesh.
According to the invention, the forming auxiliary agent mainly plays a role in preparing the heating non-combustible smoking base material in bonding various raw materials for preparing the smoking base material together, thereby being beneficial to forming.
The forming aid used in the present invention is one or more forming aids selected from sodium carboxymethylcellulose, sodium polyacrylate, pectin, guar gum or sodium alginate, which are currently marketed products such as sodium carboxymethylcellulose sold under the trade name food grade sodium carboxymethylcellulose by the howa spain food additives limited, and guar gum sold under the trade name guar gum by the bei bai seiko biotechnology limited, of shandong.
According to the invention, the additive has a primary function in heating the non-combustible smoking substrate to supplement the fragrance of the smoking substrate.
The additive used in the present invention is one or more additives selected from flavors, calcium salts, sweeteners or cooling agents.
Wherein, the essence and spice additive basically plays a role in supplementing or adjusting the aroma of the smoking material.
The essence is one or more of flower essence, fruit essence, tobacco essence or plant extract.
The floral fragrances used in the present invention are, for example, one or more fragrances selected from jasmine essence, clove essence, rose essence or orange flower, which are all products currently marketed, for example, by the Guangzhou Siweda perfumery company under the trade name Rose essence; the fruity flavor used in the present invention is, for example, one or more flavors selected from blueberry flavor, hami melon flavor, watermelon flavor, or grapefruit flavor, which are currently marketed products, such as flavors sold under the trade name blueberry flavor by Hangzhou Bairui flavor spices Limited; the essence having a tobacco flavor used in the present invention is, for example, one or more essence selected from ethyl maltol, vanillin, maple essence, or aromatic tobacco flavor essence, which are currently commercially available products, such as those sold under the trade name maple essence by Guangzhou Siwed perfumery Co., Ltd; the plant extract used in the present invention is, for example, one or more flavors and fragrances selected from the group consisting of rose extract, emblic leafflower fruit extract, olive extract or puerarin tea extract, which are currently commercially available products, such as flavors and fragrances sold under the trade name olive extract by the company riwise biotechnology limited;
the basic function of the calcium salt additive is to function as a leavening agent, an acid-base regulator or a curing agent.
The calcium salt used in the present invention is one or more calcium salts selected from calcium carbonate, calcium bicarbonate or calcium chloride, which are currently commercially available products;
the primary function of the sweetener additive is to provide a sweet taste to the smoking substrate or to suppress a portion of the off-flavor of the smoking substrate.
The sweetener used in the present invention is one or more selected from sucralose, aspartame, neotame, and saccharin, which are currently commercially available products, such as aspartame sold under the trade name food grade aspartame by tiger ti trade, inc. of suzhou, neotame sold under the trade name neotame by Jiangsuo Nuojia food ingredients, inc;
the primary function of the cooling agent additive is to provide a cooling sensation to the smoking substrate.
The cooling agent used in the present invention is one or more cooling agents selected from WS-23, WS-3 or menthol, which are currently commercially available products, such as WS-23 cooling agent sold under the trade name cooling agent WS-23 by KANCHEN SANKANG, Inc., and WS-3 cooling agent sold under the trade name menthane amide WS-3 cooling agent by KANCHENWANGNANXIANG NATURAL PERFUME, Inc.
According to the invention, the weight ratio of the spice plant powder, the fuming material powder, the forming auxiliary agent and the additive is 50-80: 10-20: 5-15: 0 to 5.
In the present invention, when the amounts of the smoking material powder, the forming aid and the additive are within the above ranges, if the amount of the spice plant powder is less than 50, the aroma persistence and aroma effect of the smoking material are reduced; if the amount of the spice plant powder is more than 80, the aroma stability of the smoking material is poor and the miscellaneous gas is heavy; therefore, the amount of the spice plant powder is 50 to 80, preferably 58 to 72;
when the amounts of the spice plant powder, the forming aid and the additive are within the above ranges, if the amount of the smoking material powder is less than 10, the smoking amount of the smoking material is insufficient; if the using amount of the smoking material powder is more than 20, the surface of the smoking material is wet, the smoking material is inconvenient to store, and the smoking effect is influenced; therefore, the amount of the smoking material powder is suitably 10 to 20, preferably 12 to 18;
when the amounts of the spice plant powder, the smoking material powder and the additive are in the range, if the amount of the forming aid is less than 5, the forming effect of the smoking material is poor, and the mechanical property of the smoking material is unstable; if the amount of forming aid is greater than 15, the smoking substrate will be stiffer and will also increase cost; therefore, the amount of the forming aid is 5 to 15, preferably 7 to 12;
when the amounts of the plant spice powder, the smoke generating material powder and the forming aid are within the ranges, the amount of the additive can be 0 under the condition that the plant spice powder has sufficient fragrance and high quality; if the amount of the additive is more than 5, the aroma components of the smoking substrate are mixed, and the smoking experience is affected; therefore, the amount of the additive is suitably 0 to 5, preferably 1 to 4;
preferably, the weight ratio of the spice plant powder, the smoking material powder, the forming aid and the additive is 58-72: 12-18: 7-12: 1 to 4.
B. Adding water
Adding water accounting for 15-40% of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a paste or colloid mixed material;
according to the invention, the main purpose of adding water into the mixed material obtained in the step A is to uniformly mix the components of the smoking material and simultaneously facilitate the formation of the subsequent smoking material.
If the water content in the mixed material obtained in the step A is lower than 15%, the material is too dispersed and is not easy to form, and the phenomena of powder falling and the like are probably generated after forming; if the water addition amount in the mixed material obtained in the step A is higher than 40%, the material is wet, and the subsequent forming is difficult; therefore, the amount of water added into the mixed material obtained in the step A is preferably 15-40%;
C. press forming
And D, processing the paste or colloid mixed material obtained in the step B into a strip or sheet mixed material by adopting a spiral roller extrusion method or a rolling method, and then heating and drying in drying equipment to obtain the strip or sheet heating non-combustion fuming base material.
The details of the screw roll extrusion method can be found in CN1107314A, the name of the invention "a high-efficiency automatic rolling tobacco sheet production line". Details of the rolling process can be found in the literature: the author, institute of science and technology for tobacco and beet industry, Henan province, entitled "test report for manufacturing tobacco sheet by rolling method", Nicotiana tabacum scientific Commission, 1976, 02.
According to the invention, the strip-shaped or sheet-shaped mixed material is dried by heating at 90-120 ℃ for 8-10 min in a drying device selected from electrothermal forced air drying, microwave drying or infrared drying.
The electrothermal blowing drying apparatus, the microwave drying apparatus, and the infrared drying apparatus used in the present invention are commercially available products, for example, an electrothermal blowing drying apparatus sold under the trade name of electrothermal blowing drying oven by Changzhoulong and instruments manufacturing Co., Ltd, a microwave drying apparatus sold under the trade name of box-type microwave drying apparatus by Shandongpeng mechanical apparatus Co., Ltd, and an infrared drying apparatus sold under the trade name of belt drying oven by Yono mechanical Co., Ltd, of the department of the city.
The rod or sheet form heated non-combustible smoking substrate obtained in step C has a water content of less than 10% by weight as measured according to standard YC/T28.8-1996.
The control of the water content of the rod or sheet-like heated non-combustible smoking substrate to below 10% is because the smoking substrate is easy to store when the water content is below 10% and also is not prone to off-flavour.
According to YC/T138-1998 tobacco and tobacco product sensory evaluation standards, a panel of 15 panel experts was examined on a bar-shaped or sheet-shaped heat-not-burn smoking substrate, and the examination results are shown in Table 1 below.
Meanwhile, the conventional rod-shaped or sheet-shaped non-combustible heated smoking substrate described in CN110477438A, entitled "smoking article not combustible by heating and method for manufacturing the same" was also evaluated as a control sample, and the evaluation results are also shown in table 1 below.
[ advantageous effects ]
The invention has the beneficial effects that:
the non-combustible heating fuming base material has the characteristics of sufficient smoke quantity, soft smoke, good delicate sense, sufficient aroma quantity, good smoke richness and obviously weakened miscellaneous gas, and has good sensory quality; meanwhile, in the preparation process of the fuming base material, the moisture is controlled to be 15-40% by weight, the long-time heating in the drying and forming process is reduced, and the volatilization loss of the aroma components of the base material is reduced. In addition, the invention can adjust and supplement the aroma of the fuming base material by performing secondary perfuming on the base material.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: preparation of the inventive heated non-combustible smoking substrate
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh tea powder spice plant powder, a glycerol fuming material, a 100-160-mesh pectin forming aid and a blueberry fruity flavor essence and calcium bicarbonate mixture (weight ratio 1: 1) additive by using mixing equipment according to a weight ratio of 68: 14: 13: 2, uniformly mixing to obtain a mixed material;
B. adding water
Adding water accounting for 15% of the total weight of the mixture into the mixture obtained in the step A, and fully mixing to obtain a pasty mixture;
C. press forming
And (3) processing the pasty mixed material obtained in the step (B) into a strip-shaped or sheet-shaped mixed material by adopting a screw roll extrusion method, and then heating and drying the mixed material in an electrothermal blowing drying device sold under the trade name of an electrothermal blowing drying box by Changzhoulong and apparatus manufacturing limited at the temperature of 102 ℃ for 10min to obtain the strip-shaped heating non-combustible fuming base material.
The resulting heated non-burning smoking substrate strip had a water content of 9.8% by weight, measured according to the method described in the specification.
The strip-shaped heat non-combustible smoking substrate prepared in this example was subjected to smoking according to the method described in the specification of the present application, and the results of smoking thereof are shown in table 1 below.
Meanwhile, a conventional stick-or sheet-shaped, non-combustible heated smoking substrate described in CN110477438A, entitled "a smoking article not combustible by heating and a method for producing the same" was also evaluated as a control sample K2, and the evaluation results are also shown in table 1 below.
Example 2: preparation of a non-combustible heated smoking substrate according to the invention
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh mint powder, medium-chain triglyceride smoking material, 100-160-mesh guar gum forming aid and maple tobacco flavor and aspartame sweetener mixture (weight ratio is 1: 1) additive according to a weight ratio of 74: 16: 15: 3, uniformly mixing to obtain a mixed material;
B. adding water
Adding 21% of water by weight of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a colloidal mixed material;
C. press forming
And C, processing the colloidal mixed material obtained in the step B into a sheet-shaped mixed material by adopting a rolling method, and then heating and drying for 8min at the temperature of 108 ℃ in a microwave drying device sold by Shandong Popp mechanical equipment Co.
The resulting heated non-burning smoking substrate had a water content of 9.6% by weight, measured according to the method described in the specification.
The sheet-like, heat-not-burn smoking substrate prepared in this example was evaluated according to the method described in the present specification, and the evaluation results are shown in table 1 below.
Example 3: preparation of the inventive heated non-combustible smoking substrate
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh lotus leaf powder spice plant powder, a propylene glycol smoking material, a 100-160-mesh sodium carboxymethylcellulose forming aid, an emblic leafflower fruit extract, a neotame sweetener and a menthol cooling agent mixture (weight ratio is 2: 1: 1) and additives in a weight ratio of 50: 10: 5: 0, uniformly mixing to obtain a mixed material;
B. adding water
Adding water accounting for 35 percent of the total weight of the mixture into the mixture obtained in the step A, and fully mixing to obtain a pasty mixture;
C. press forming
And C, processing the paste mixed material obtained in the step B into a strip-shaped mixed material by adopting a screw roll extrusion method, and then heating and drying for 9min at the temperature of 114 ℃ in an infrared drying device sold by Mino mechanical company of China under the trade name of a belt drying box to obtain the strip-shaped heating non-combustible fuming base material.
The resulting heated non-burning smoking substrate strip had a water content of 9.0% by weight, measured according to the method described in the specification.
The strip-shaped heat non-combustible smoking substrate prepared in this example was subjected to smoking according to the method described in the specification of the present application, and the results of smoking thereof are shown in table 1 below.
Example 4: preparation of the inventive heated non-combustible smoking substrate
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh chrysanthemum perfume plant powder, a smoking material of a mixture of glycerol and medium-chain triglyceride (the weight ratio is 3: 1), a 100-160-mesh sodium polyacrylate forming aid, a clove fragrance type essence, calcium carbonate, a sucralose cooling agent and a WS-23 cooling agent mixture (the weight ratio is 1: 3: 1: 2) additive according to the weight ratio of 62: 20: 7: 1, uniformly mixing to obtain a mixed material;
B. adding water
Adding water accounting for 40 percent of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a colloidal mixed material;
C. press forming
And (c) processing the colloidal mixed material obtained in the step (B) into a sheet-like mixed material by a roll pressing method, and then heating and drying the sheet-like mixed material at 90 ℃ for 10 minutes in an electric hot air drying apparatus sold under the trade name of an electric hot air drying oven by Changzhoulong and Instrument manufacturing Co., Ltd to obtain a sheet-like heating non-combustible fuming substrate.
The resulting heated non-burning smoking substrate had a water content of 9.9% by weight, measured according to the method described in the specification.
The rod-shaped or sheet-shaped heat non-combustible smoking substrate prepared in this example was evaluated according to the method described in the present specification, and the evaluation results are shown in table 1 below.
Example 5: preparation of the inventive heated non-combustible smoking substrate
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh rose spice plant powder, a fuming material of a mixture (weight ratio is 1: 1) of glycerol and propylene glycol, a 100-160-mesh sodium alginate forming auxiliary agent and an additive of a mixture (weight ratio is 2: 1) of calcium carbonate and aspartame sweetening agent according to the weight ratio of 56: 12: 9: 4, uniformly mixing to obtain a mixed material;
B. adding water
B, adding water accounting for 26% of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a colloidal mixed material;
C. press forming
And D, processing the colloidal mixed material obtained in the step B into a strip-shaped mixed material by adopting a screw roll extrusion method, and then heating and drying for 9min at the temperature of 96 ℃ in a microwave drying device sold by Shandong Popp mechanical equipment Limited under the trade name of box-type microwave drying equipment to obtain the strip-shaped heating non-combustible fuming base material.
The resulting heated non-burning smoking substrate in strip or sheet form had a water content of 9.2% by weight, measured according to the method described in the specification.
The rod-shaped or sheet-shaped heat non-combustible smoking substrate prepared in this example was evaluated according to the method described in the present specification, and the evaluation results are shown in table 1 below.
Example 6: preparation of the inventive heated non-combustible smoking substrate
The preparation method comprises the following preparation steps:
A. preparation of the mixture
Mixing 100-160-mesh dendrobium spice plant powder, glycerol, a mixture (weight ratio of 3: 1: 2) of medium-chain triglyceride and propylene glycol, 100-160-mesh pectin, a mixture (weight ratio of 2: 1: 1) of guar gum and sodium polyacrylate, a forming aid, a mixture (weight ratio of 1: 1: 1) of calcium bicarbonate, a saccharin sweetener and a menthol cooling agent, and additives in a weight ratio of 80: 18: 11: 5, uniformly mixing to obtain a mixed material;
B. adding water
B, adding water accounting for 30% of the total weight of the mixture into the mixture obtained in the step A, and fully mixing to obtain a pasty mixture;
C. press forming
And (C) processing the pasty mixed material obtained in the step (B) into a strip-shaped mixed material by adopting a spiral roller extrusion method, and then heating and drying for 8min at the temperature of 120 ℃ in an infrared drying device sold by Mino mechanical company of all cities under the trade name of a belt drying box to obtain the strip-shaped or sheet-shaped heating non-combustion fuming base material.
The resulting heated non-burning smoking substrate in strip or sheet form had a water content of 9.6% by weight, measured according to the method described in the specification.
The rod-shaped or sheet-shaped heat non-combustible smoking substrate prepared in this example was evaluated according to the method described in the present specification, and the evaluation results are shown in table 1 below.
Table 1: smoking evaluation result of heating non-combustion fuming base material prepared by the invention
| Sample(s) | Smoking amount (5X) | Aroma (32) | Coordination (6) | Miscellaneous gas (12) | Irritation (20) | Aftertaste (25) | Is totaled |
| Example 1 | 4.5 | 32 | 6 | 10 | 15 | 25 | 92.5 |
| Example 2 | 4 | 28 | 5 | 11 | 15.5 | 25 | 88.5 |
| Example 3 | 4.6 | 29 | 5.5 | 10 | 15 | 24.5 | 88.6 |
| Example 4 | 4.7 | 28 | 5.7 | 12 | 16 | 25 | 91.4 |
| Example 5 | 4.5 | 31 | 5.9 | 11 | 15 | 25 | 92.4 |
| Example 6 | 4.2 | 24 | 4 | 8 | 15 | 21 | 76.2 |
| Control sample K2 | 3.9 | 25 | 4.5 | 8.5 | 15 | 20 | 76.9 |
Indicates the primary improved smoking substrate performance of the present invention.
The results listed in table 1 clearly show that, compared with the control sample, the non-combustible smoking substrate of the invention has sufficient smoking amount, good smoke stability, outstanding aroma, good harmony, soft smoke, basically no miscellaneous gas, small irritation, comfortable aftertaste and good sensory experience for smokers.
Claims (10)
1. A preparation method of a heating non-combustible fuming base material is characterized by comprising the following preparation steps:
A. preparation of the mixture
Uniformly mixing the spice plant powder, the fuming material powder, the forming aid and the additive by using mixing equipment to obtain a mixed material;
B. adding water
Adding water accounting for 15-40% of the total weight of the mixed materials into the mixed materials obtained in the step A, and fully mixing to obtain a paste or colloid mixed material;
C. press forming
And D, processing the paste or colloid mixed material obtained in the step B into a strip or sheet mixed material by adopting a spiral roller extrusion method or a rolling method, and then heating and drying in drying equipment to obtain the strip or sheet heating non-combustion fuming base material.
2. The preparation according to claim 1, wherein in step a, the weight ratio of the spice plant powder, the smoking material powder, the forming aid and the additive is 50-80: 10-20: 5-15: 0 to 5.
3. The method according to claim 1 or 2, wherein in the step a, the spice plant powder is one or more spice plant powders selected from tea powder, tea stalk powder, areca nut powder, coffee powder, barley tea powder, mint powder, lotus leaf powder, Compositae plant powder, Rosaceae plant powder, or orchid plant powder;
wherein the Compositae plant is flos Chrysanthemi, Bellis Perennis, Severum cinerascens or Tagetes Erecta; the Rosaceae plant is flos Rosae Rugosae, flos Rosae Multiflorae, flos Rosae chinensis or flos persicae; the orchid family plant is orchid, dendrobium, gastrodia elata or butterfly orchid.
4. The method according to claim 1 or 2, wherein in step a, the particle size of the powder of the spice plants or the smoking material is 100 to 160 mesh.
5. The method of claim 1 or 2, wherein in step a, the smoking material is one or more selected from the group consisting of glycerin, medium chain triglycerides, and propylene glycol.
6. The method according to claim 1 or 2, wherein in step a, the forming aid is one or more forming aids selected from sodium carboxymethylcellulose, sodium polyacrylate, pectin, guar gum, or sodium alginate.
7. The method according to claim 1 or 2, wherein in step A, the additive is one or more additives selected from the group consisting of flavors and fragrances, calcium salts, sweeteners, and cooling agents.
8. The method according to claim 7, wherein the aroma chemicals are one or more aroma chemicals selected from the group consisting of floral, fruity, tobacco or plant extracts; the calcium salt is one or more calcium salts selected from calcium carbonate, calcium bicarbonate or calcium chloride; the sweetener is one or more selected from sucralose, aspartame, neotame or saccharin; the cooling agent is one or more cooling agents selected from WS-23, WS-3 or menthol.
9. The preparation method according to claim 1, wherein in the step C, the strip-shaped or sheet-shaped mixed material obtained in the step B is dried by heating at 90-120 ℃ for 8-10 min in a drying device selected from electrothermal forced air drying, microwave drying or infrared drying.
10. The method according to claim 1, wherein the water content of the heated non-combustible smoking substrate in the form of a rod or sheet obtained in step C is 10% by weight or less.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210134124.3A CN114504117A (en) | 2022-02-14 | 2022-02-14 | Preparation method of heating non-combustible fuming base material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210134124.3A CN114504117A (en) | 2022-02-14 | 2022-02-14 | Preparation method of heating non-combustible fuming base material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114504117A true CN114504117A (en) | 2022-05-17 |
Family
ID=81551986
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210134124.3A Pending CN114504117A (en) | 2022-02-14 | 2022-02-14 | Preparation method of heating non-combustible fuming base material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114504117A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415612A (en) * | 2011-11-22 | 2012-04-18 | 吉林烟草工业有限责任公司 | Agilawood slice fragrant silks and preparation method thereof |
| CN107319628A (en) * | 2017-05-27 | 2017-11-07 | 浙江中烟工业有限责任公司 | One kind is applied to heat incombustible tobacco matrixes and preparation method thereof |
| CN108576912A (en) * | 2018-06-08 | 2018-09-28 | 湖北中烟工业有限责任公司 | The reconstituted tobacoo and its production technology of a kind of metal-containing powders applied to low temperature cigarette |
| CN109393543A (en) * | 2018-12-21 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of ultra-micro powder plantflakesare and preparation method thereof |
| JP2019076077A (en) * | 2017-10-23 | 2019-05-23 | 株式会社 東亜産業 | Manufacturing method of filling material for electronic tobacco cartridge using non-tobacco plant |
| CN112155247A (en) * | 2020-09-04 | 2021-01-01 | 安徽集友广誉科技有限公司 | Plant slice, preparation method and cigarette substitute |
| CN112273707A (en) * | 2020-11-19 | 2021-01-29 | 云南纯旭生物科技有限公司 | Atomized smoking material for heating non-combustible product |
-
2022
- 2022-02-14 CN CN202210134124.3A patent/CN114504117A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102415612A (en) * | 2011-11-22 | 2012-04-18 | 吉林烟草工业有限责任公司 | Agilawood slice fragrant silks and preparation method thereof |
| CN107319628A (en) * | 2017-05-27 | 2017-11-07 | 浙江中烟工业有限责任公司 | One kind is applied to heat incombustible tobacco matrixes and preparation method thereof |
| JP2019076077A (en) * | 2017-10-23 | 2019-05-23 | 株式会社 東亜産業 | Manufacturing method of filling material for electronic tobacco cartridge using non-tobacco plant |
| CN108576912A (en) * | 2018-06-08 | 2018-09-28 | 湖北中烟工业有限责任公司 | The reconstituted tobacoo and its production technology of a kind of metal-containing powders applied to low temperature cigarette |
| CN109393543A (en) * | 2018-12-21 | 2019-03-01 | 云南巴菰生物科技有限公司 | A kind of ultra-micro powder plantflakesare and preparation method thereof |
| CN112155247A (en) * | 2020-09-04 | 2021-01-01 | 安徽集友广誉科技有限公司 | Plant slice, preparation method and cigarette substitute |
| CN112273707A (en) * | 2020-11-19 | 2021-01-29 | 云南纯旭生物科技有限公司 | Atomized smoking material for heating non-combustible product |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108077992B (en) | It is a kind of to heat do not burn cigarette suction particle and manufacturing method | |
| CN106987314B (en) | Citrus reticulata flavor essence for bead blasting of cigarettes and application of citrus reticulata flavor essence in cigarettes | |
| WO2019100545A1 (en) | Low-temperature cigarette and preparation method therefor | |
| CN110169606B (en) | Heating non-combustible fuming particle and preparation method and application thereof | |
| JP7440123B2 (en) | Smoke-generating substrate for tobacco sticks in electronic cigarettes and method for producing the same | |
| CN106235376A (en) | A kind of reconstituted tobacco being applicable to heat non-combustion-type Medicated cigarette | |
| CN108523206B (en) | Preparation method of cigar flavor cooling and flavoring section and heating non-combustion cigarette base rod | |
| CN108576931B (en) | Raw material formula of flue-cured tobacco flavor cooling and blending section, preparation method thereof and base rod of cigarette without burning during heating | |
| CN108576932B (en) | Raw material formula of mixed type flavor cooling and blending section, preparation method thereof and base rod of cigarette without burning during heating | |
| CN108576912A (en) | The reconstituted tobacoo and its production technology of a kind of metal-containing powders applied to low temperature cigarette | |
| CN110584214B (en) | Composite fragrant essence for low-temperature cigarettes and application thereof | |
| CN110714367A (en) | Cool and sweet gloss oil, preparation method and tipping paper for cigarettes | |
| CN110150716A (en) | It is a kind of for heating the Alevaire and application thereof for the cigarette that do not burn | |
| CN108926030A (en) | A kind of tobacco style leaf composition for multiple heating mode cigarette, multiple heating mode cigarette and preparation method thereof | |
| CN110226775A (en) | It is a kind of to add in the flavoring tow stick and preparation method thereof heated in the cigarette filter rod that do not burn | |
| CN106947597B (en) | Pine pollen essence for cigarette bead blasting and application of pine pollen essence in cigarettes | |
| CN107022415B (en) | Semen Scaphii Lychnophori essence for cigarette bead blasting and application thereof in cigarette | |
| CN109156888A (en) | A kind of 3D printing cigarette and preparation method thereof | |
| CN107549870A (en) | A kind of Novel buccal cigarette product processing method containing black tea extract | |
| CN108542000B (en) | Raw material formula of tobacco shred flavor cooling and flavoring section, preparation method thereof and heating non-combustion cigarette base rod | |
| CN114504117A (en) | Preparation method of heating non-combustible fuming base material | |
| CN107418730B (en) | Kumquat flavor essence for bead blasting of cigarettes and application of kumquat flavor essence in cigarettes | |
| CN114009826B (en) | Heating cigarette core material and preparation method thereof | |
| CN112931920A (en) | Non-tobacco heating non-combustion sheet and preparation method thereof | |
| CN114680363A (en) | Processing method of flavor type reconstituted tobacco |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |