CN114469828A - Amber congee and preparation method thereof - Google Patents

Amber congee and preparation method thereof Download PDF

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Publication number
CN114469828A
CN114469828A CN202210143895.9A CN202210143895A CN114469828A CN 114469828 A CN114469828 A CN 114469828A CN 202210143895 A CN202210143895 A CN 202210143895A CN 114469828 A CN114469828 A CN 114469828A
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phase
parts
extract
amber
stirring
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肖军
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Guangzhou Hezhong Nonwoven Cosmetics Group Co ltd
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Guangzhou Hezhong Nonwoven Cosmetics Group Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention discloses amber coagulated fat and a preparation method thereof, wherein the amber coagulated fat is prepared from the following raw materials: deionized water, dipropylene glycol, butanediol, glyceryl polyether-26, carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin, carboxymethyl beta-dextran sodium, beta-glucan, p-hydroxyacetophenone, arginine, saccharide isomerate, cactus extract, radix ophiopogonis extract, radix scutellariae extract, oat bran extract, polysorbate-20, caprylyl hydroximic acid and essence. The amber congee prepared by adopting the special dosage for matching has better relieving and repairing effects, has good stability and is suitable for the general population.

Description

Amber congee and preparation method thereof
Technical Field
The invention relates to the technical field of daily cosmetics, in particular to amber congelation and a preparation method thereof.
Background
In daily life, human skin directly contacts with the external environment, and pollutants such as dust, particles, harmful gas and various bacteria exist in the air, so that the pollutants can damage the human skin (especially the facial skin) through contact, damage is caused to the skin, and skin problems such as inflammation, aging, allergy, dryness and the like are caused. The demand of Chinese people on safe and high-quality skin care products is huge, but in the skin care product industry at present, a large number of products containing antibiotics and hormones exist, and after long-term use, the skin is converted into allergic skin and is irreversible, so that the skin care products can seriously affect the daily life, work and study, and even the psychological health of people.
Therefore, a safe and reliable repair type skin care product which can relieve the skin problem, can penetrate into the skin bottom, promotes the regeneration and repair of skin tissues, reduces the recurrence is urgently needed in the market.
Disclosure of Invention
In order to solve the technical problems, the invention provides the amber grease and the preparation method thereof, and the amber powder is compounded with various plant extracts, so that the problem of skin can be relieved, and the amber powder can penetrate into the bottom of the skin to promote the regeneration and repair of skin tissues.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the invention provides amber coagulated fat which comprises the following raw materials in parts by weight:
phase A: 80-90 parts of deionized water, 2-5 parts of dipropylene glycol, 1-4 parts of butanediol, 261-3 parts of glyceryl polyether, 0.1-0.3 part of carbomer, 0.1-0.2 part of amber powder, 0.05-0.25 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.05-0.2 part of allantoin, 0.02-0.1 part of carboxymethyl beta-dextran sodium, 0.001-0.002 part of beta-glucan and 0.2-0.4 part of p-hydroxyacetophenone;
phase B: 0.1-0.5 part of arginine;
and C phase: 0.1-0.6 part of saccharide isomerate, 0.01-0.04 part of cactus extract, 0.01-0.04 part of radix ophiopogonis extract, 0.001-0.01 part of radix scutellariae extract and 0.01-0.02 part of oat bran extract;
phase D: polysorbate-200.01-0.02 parts;
phase E: 0.02-0.08 parts of caprylyl hydroximic acid;
and (3) phase F: 0.001-0.004 parts of essence.
In some specific embodiments, the amber congelation comprises the following raw materials in parts by weight:
phase A: 87.436 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.2 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
In some specific embodiments, the amber congelation comprises the following raw materials in parts by weight:
phase A: 87.486 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.15 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
e phase: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
In some specific embodiments, the amber congelation comprises the following raw materials in parts by weight:
phase A: 87.536 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.1 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
e phase: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
In a second aspect, the present invention provides a method for preparing the above-mentioned amber coagulated fat, comprising the following steps:
s1, adding accurately weighed deionized water into a vacuum emulsifying pot, heating to 95-100 ℃, and keeping the temperature for 30 minutes;
s2, uniformly dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and carboxymethyl beta-dextran sodium by using dipropylene glycol, butanediol and glyceryl polyether-26, and putting into a vacuum emulsifying pot; then, sequentially adding other materials in the phase A, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz to be completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then cooling, wherein the stirring speed is frequency-modulated at 18-20 Hz;
s3, adding the B-phase material, uniformly stirring at a stirring speed of 20-25 Hz, and then cooling, wherein the stirring speed is 20-25 Hz when cooling;
s4, sequentially feeding the C-phase materials at 40-45 ℃ and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, adding the D-phase material, and uniformly stirring the D-phase material at a stirring speed of 20-25 Hz through frequency modulation;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, then adding and uniformly stirring at a frequency modulation speed of 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, then adding the F-phase material, uniformly stirring the F-phase material at a stirring speed of frequency modulation 20-25 Hz, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, inspecting, stopping the machine, filtering the material after the inspection is qualified, and thus obtaining the material.
In some specific embodiments, in step S2, the homogenization rate is 2400-3000 r/min, and the homogenization time is 3 min.
In some specific embodiments, in step S2, the cooling rate is 2 deg.C/min.
In some specific embodiments, in step S3, the cooling rate is 1 deg.C/min.
In some embodiments, in step S7, the filtering operation is filtering with a 100 mesh screen.
Compared with the prior art, the invention provides the amber coagulated fat and the preparation method thereof, and the amber coagulated fat has the following beneficial effects:
in the invention, dipropylene glycol, butanediol, glyceryl polyether-26, saccharide isomerate, allantoin, radix ophiopogonis extract and arginine play a role in moisturizing; carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer plays a thickening role; the amber powder has the function of conditioning the skin; the carboxymethyl beta-glucan sodium and the beta-glucan play a role in repairing; the cactus extract has anti-allergy effect; the radix Scutellariae extract and oat bran extract have antiaging effect; the p-hydroxyacetophenone and the caprylyl hydroximic acid play a role in preserving; the polysorbate-20 plays a role in solubilization; the essence plays a role of fragrance.
The amber congee prepared by adopting the special dosage for matching has better relieving and repairing effects, has good stability and is suitable for the general population.
Detailed Description
The technical solutions of the present invention will be described clearly and completely below, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides amber coagulated fat which comprises the following raw materials in parts by weight:
phase A: 80-90 parts of deionized water, 2-5 parts of dipropylene glycol, 1-4 parts of butanediol, 261-3 parts of glyceryl polyether, 0.1-0.3 part of carbomer, 0.1-0.2 part of amber powder, 0.05-0.25 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.05-0.2 part of allantoin, 0.02-0.1 part of carboxymethyl beta-dextran sodium, 0.001-0.002 part of beta-glucan and 0.2-0.4 part of p-hydroxyacetophenone;
phase B: 0.1-0.5 part of arginine;
and C phase: 0.1-0.6 part of saccharide isomerate, 0.01-0.04 part of cactus extract, 0.01-0.04 part of radix ophiopogonis extract, 0.001-0.01 part of radix scutellariae extract and 0.01-0.02 part of oat bran extract;
phase D: polysorbate-200.01-0.02 parts;
phase E: 0.02-0.08 parts of caprylyl hydroximic acid;
and (3) phase F: 0.001-0.004 parts of essence.
The preparation method of the amber congelation comprises the following steps:
s1, adding accurately weighed deionized water into a vacuum emulsifying pot, heating to 95-100 ℃, and keeping the temperature for 30 minutes;
s2, uniformly dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and carboxymethyl beta-dextran sodium by using dipropylene glycol, butanediol and glyceryl polyether-26, and putting into a vacuum emulsifying pot; then, sequentially adding other materials in the phase A, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz to be completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then cooling, wherein the stirring speed is frequency-modulated at 18-20 Hz;
s3, adding the B-phase material, uniformly stirring at a stirring speed of 20-25 Hz, and then cooling, wherein the stirring speed is 20-25 Hz when cooling;
s4, sequentially feeding the C-phase materials at 40-45 ℃ and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, adding the D-phase material, and uniformly stirring the D-phase material at a stirring speed of 20-25 Hz through frequency modulation;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, then adding and uniformly stirring at a frequency modulation speed of 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, then adding the F-phase material, uniformly stirring the F-phase material at a stirring speed of frequency modulation 20-25 Hz, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, inspecting, stopping the machine, filtering the material after the inspection is qualified, and thus obtaining the material.
In a preferred embodiment, in step S2, the homogenization rate is 2400 to 3000r/min, and the homogenization time is 3 min.
In a preferred embodiment, in step S2, the temperature decrease rate is 2 ℃/min.
In step S3, the temperature decrease rate is preferably 1 ℃/min.
In a preferred embodiment, in step S7, the filtering operation is filtering with a 100 mesh screen.
The present invention is described in further detail below by means of detailed examples.
The starting materials used in the following examples are all commercially available.
Example 1
The embodiment provides amber coagulated fat which comprises the following raw materials in parts by weight:
phase A: 87.436 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.2 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
The preparation method of the amber congealing fat comprises the following steps:
s1, cleaning and disinfecting production equipment and tools, checking whether all valves of the vacuum emulsifying pot are closed, then adding accurately weighed deionized water into the vacuum emulsifying pot, heating to 95-100 ℃, and preserving heat for 30 minutes;
s2, starting a homogenizer, homogenizing and dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and sodium carboxymethyl beta-dextran uniformly by using dipropylene glycol, butanediol and glyceryl polyether-26, and then putting into a vacuum emulsifying pot, wherein the homogenizing rate is 2400-3000 r/min, and the homogenizing time is 3 min; then sequentially putting other materials in the phase A into a vacuum emulsifying pot, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz until the materials are completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then starting cooling water to cool, wherein the cooling speed is 2 ℃/min, and the stirring speed is frequency modulated to 18-20 Hz when the temperature is lowered;
s3, putting the B-phase material into a vacuum emulsifying pot at the temperature of 60-65 ℃, uniformly stirring at the stirring speed of frequency modulation 20-25 Hz, and then starting cooling water to cool, wherein the cooling speed is 1 ℃/min, and the stirring speed is frequency modulation 20-25 Hz when cooling;
s4, sequentially putting the C-phase materials into a vacuum emulsifying pot at the temperature of 40-45 ℃, and uniformly stirring at the stirring speed of frequency modulation of 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, putting the D-phase material into a vacuum emulsifying pot, and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, putting into a vacuum emulsifying pot, and uniformly stirring at a frequency modulation speed of 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, putting the F-phase material into a vacuum emulsification pot, uniformly stirring at a frequency modulation stirring speed of 20-25 Hz, then starting cooling water, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, checking, stopping the machine, and filtering and discharging by using a 100-mesh filter screen after various physicochemical indexes (viscosity, appearance, smell, PH and skin feel) are checked to be qualified.
Example 2
The embodiment provides amber coagulated fat which comprises the following raw materials in parts by weight:
phase A: 87.486 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.15 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
The preparation method of the amber congelation comprises the following steps:
s1, cleaning and disinfecting production equipment and tools, checking whether all valves of the vacuum emulsifying pot are closed, then adding accurately weighed deionized water into the vacuum emulsifying pot, heating to 95-100 ℃, and preserving heat for 30 minutes;
s2, starting a homogenizer, homogenizing and dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and sodium carboxymethyl beta-dextran uniformly by using dipropylene glycol, butanediol and glyceryl polyether-26, and then putting into a vacuum emulsifying pot, wherein the homogenizing rate is 2400-3000 r/min, and the homogenizing time is 3 min; then sequentially putting other materials in the phase A into a vacuum emulsifying pot, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz until the materials are completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then starting cooling water to cool, wherein the cooling speed is 2 ℃/min, and the stirring speed is frequency modulated to 18-20 Hz when the temperature is lowered;
s3, putting the B-phase material into a vacuum emulsifying pot at the temperature of 60-65 ℃, uniformly stirring at the stirring speed of frequency modulation 20-25 Hz, and then starting cooling water to cool, wherein the cooling speed is 1 ℃/min, and the stirring speed is frequency modulation 20-25 Hz when cooling;
s4, sequentially putting the C-phase materials into a vacuum emulsifying pot at the temperature of 40-45 ℃, and uniformly stirring at the stirring speed of frequency modulation of 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, putting the D-phase material into a vacuum emulsifying pot, and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, putting into a vacuum emulsifying pot, and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, putting the F-phase material into a vacuum emulsification pot, uniformly stirring at a frequency modulation stirring speed of 20-25 Hz, then starting cooling water, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, checking, stopping the machine, and filtering and discharging by using a 100-mesh filter screen after various physicochemical indexes (viscosity, appearance, smell, PH and skin feel) are checked to be qualified.
Example 3
The embodiment provides amber coagulated fat which comprises the following raw materials in parts by weight:
phase A: 87.536 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.1 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
The preparation method of the amber congelation comprises the following steps:
s1, cleaning and disinfecting production equipment and tools, checking whether all valves of the vacuum emulsifying pot are closed, then adding accurately weighed deionized water into the vacuum emulsifying pot, heating to 95-100 ℃, and preserving heat for 30 minutes;
s2, starting a homogenizer, homogenizing and dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and sodium carboxymethyl beta-dextran uniformly by using dipropylene glycol, butanediol and glyceryl polyether-26, and then putting into a vacuum emulsifying pot, wherein the homogenizing rate is 2400-3000 r/min, and the homogenizing time is 3 min; then sequentially putting other materials in the phase A into a vacuum emulsifying pot, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz until the materials are completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then starting cooling water to cool, wherein the cooling speed is 2 ℃/min, and the stirring speed is frequency modulated to 18-20 Hz when the temperature is lowered;
s3, putting the B-phase material into a vacuum emulsifying pot at the temperature of 60-65 ℃, uniformly stirring at the stirring speed of frequency modulation 20-25 Hz, and then starting cooling water to cool, wherein the cooling speed is 1 ℃/min, and the stirring speed is frequency modulation 20-25 Hz when cooling;
s4, sequentially putting the C-phase materials into a vacuum emulsifying pot at the temperature of 40-45 ℃, and uniformly stirring at the stirring speed of frequency modulation of 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, putting the D-phase material into a vacuum emulsifying pot, and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, putting into a vacuum emulsifying pot, and uniformly stirring at a frequency modulation speed of 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, putting the F-phase material into a vacuum emulsification pot, uniformly stirring at a frequency modulation stirring speed of 20-25 Hz, then starting cooling water, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, checking, stopping the machine, and filtering and discharging by using a 100-mesh filter screen after various physicochemical indexes (viscosity, appearance, smell, PH and skin feel) are checked to be qualified.
To verify the beneficial effects of the present invention, the following tests were performed.
First, stability test
30g of the amber congealed fat prepared in examples 1 to 3 were respectively put into 30ml PET bottles, 3 bottles were respectively put in an environment of room temperature, heat resistance (48 + -1) DEG C and cold resistance (-18 + -2) DEG C for 1D, 3D, 1W, 2W, 1M, 3M, 5M and 6M, and the state of the product was observed and evaluated, and the test results are shown in Table 1.
Table 1 product stability test results
Figure BDA0003507897470000131
Figure BDA0003507897470000141
As can be seen from the results of Table 1 above, the amber congeal prepared by the present invention has good stability.
Second, testing the usage effect
50 subjects with dry skin and eczema (except for subjects with healthy body) were tested for the effects of moisturizing, moisture retention, allergic reaction, etc. using the amber congee prepared in examples 1-3, wherein 40 adult women and 10 infants within 3 years old were used. The results are shown in Table 2.
The moistening test method comprises the following steps: the efficacy was evaluated after 0.5 hour of smearing on the inner side of the arm, behind the ear, and on the face of the subject.
Moisture retention test method: efficacy was evaluated after applying to the inner arm, behind the ear, and on the face of the subject for 8 hours.
Allergic reaction test method: the test subjects were applied to the inner side of the arm, behind the ear and on the face, and heat sensation evaluation was performed after 1 hour, itching evaluation was performed after 8 hours, and erythema evaluation was performed after 24 hours.
Skin dryness recovery test method: the skin drying part of the subject is smeared once every 8 hours, and the skin drying recovery evaluation is carried out after 48 hours.
Eczema recovery test method: the test piece is smeared on the skin eczema part of a test subject once every 8 hours, and the recovery evaluation of the skin eczema is carried out after the test piece is continuously used for 7 days.
The eczema recurrence test method comprises the following steps: smearing on the skin eczema part of a subject once every 8 hours, continuously using for 7 days, stopping using for 7 days, and evaluating the recurrence of the skin eczema.
TABLE 2 comparison table for use effect test in examples 1 to 3
Figure BDA0003507897470000151
The results of the usage effect test in table 2 show that: the amber gel meets the technical standard requirements of products, the product efficacy test meets the product regulation requirements, and the product meets the regulation requirements of cosmetic safety technical specification (2015 edition), and the amber gel can help the skin to eliminate inflammation symptoms such as red swelling, pain and itch caused by dryness, strengthen the skin, supplement a sebum membrane, moisten the skin, promote the regeneration of skin tissues, reduce the recurrence of eczema, and has good effect of relieving and repairing.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (9)

1. The amber coagulated fat is characterized by comprising the following raw materials in parts by weight:
phase A: 80-90 parts of deionized water, 2-5 parts of dipropylene glycol, 1-4 parts of butanediol, 261-3 parts of glyceryl polyether, 0.1-0.3 part of carbomer, 0.1-0.2 part of amber powder, 0.05-0.25 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.05-0.2 part of allantoin, 0.02-0.1 part of carboxymethyl beta-dextran sodium, 0.001-0.002 part of beta-glucan and 0.2-0.4 part of p-hydroxyacetophenone;
phase B: 0.1-0.5 part of arginine;
and C phase: 0.1-0.6 part of saccharide isomerate, 0.01-0.04 part of cactus extract, 0.01-0.04 part of radix ophiopogonis extract, 0.001-0.01 part of radix scutellariae extract and 0.01-0.02 part of oat bran extract;
phase D: polysorbate-200.01-0.02 parts;
phase E: 0.02-0.08 parts of caprylyl hydroximic acid;
and (3) phase F: 0.001-0.004 parts of essence.
2. The amber grease as claimed in claim 1, which is prepared from the following raw materials in parts by weight:
phase A: 87.436 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.2 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: 200.0167 parts of polysorbate-water;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
3. The amber grease as claimed in claim 1, which is prepared from the following raw materials in parts by weight:
phase A: 87.486 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.15 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
4. The amber grease as claimed in claim 1, which is prepared from the following raw materials in parts by weight:
phase A: 87.536 parts of deionized water, 5 parts of dipropylene glycol, 3 parts of butanediol, 262.5 parts of glycerol polyether, 0.2 part of carbomer, 0.1 part of amber powder, 0.15 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of allantoin, 0.05 part of carboxymethyl beta-dextran sodium, 0.002 part of beta-glucan and 0.4 part of p-hydroxyacetophenone;
phase B: 0.35 part of arginine;
and C phase: 0.5 part of saccharide isomer, 0.01 part of cactus extract, 0.015 part of radix ophiopogonis extract, 0.002 part of radix scutellariae extract and 0.015 part of oat bran extract;
phase D: polysorbate-200.0167 parts;
phase E: 0.05 part of caprylyl hydroximic acid;
and (3) phase F: 0.0033 parts of essence.
5. The method for producing amber curds according to any one of claims 1 to 4, comprising the following steps:
s1, adding accurately weighed deionized water into a vacuum emulsifying pot, heating to 95-100 ℃, and keeping the temperature for 30 minutes;
s2, uniformly dispersing carbomer, amber powder, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin and carboxymethyl beta-dextran sodium by using dipropylene glycol, butanediol and glyceryl polyether-26, and putting into a vacuum emulsifying pot; then, sequentially adding other materials in the phase A, and stirring the materials at a stirring speed of frequency modulation 18-20 Hz to be completely dissolved; after the materials are completely dissolved, keeping the stirring speed unchanged, keeping the temperature and stirring for 30min, and then cooling, wherein the stirring speed is frequency-modulated at 18-20 Hz;
s3, adding the B-phase material, uniformly stirring at a stirring speed of 20-25 Hz, and then cooling, wherein the stirring speed is 20-25 Hz when cooling;
s4, sequentially feeding the C-phase materials at 40-45 ℃ and uniformly stirring at a stirring speed of frequency modulation 20-25 Hz;
s5, completely dissolving the D-phase material at 40-45 ℃, adding the D-phase material, and uniformly stirring the D-phase material at a stirring speed of 20-25 Hz through frequency modulation;
s6, heating the E-phase material to 70 ℃ at 40-45 ℃, completely dissolving, cooling to 45 ℃, then adding and uniformly stirring at a frequency modulation speed of 20-25 Hz;
s7, completely dissolving the F-phase material at 40-45 ℃, then adding the F-phase material, uniformly stirring the F-phase material at a stirring speed of frequency modulation 20-25 Hz, cooling to 38 ℃ at a cooling speed of 1 ℃/min, taking the material, inspecting, stopping the machine, filtering the material after the inspection is qualified, and thus obtaining the material.
6. The method of claim 5, wherein: in step S2, the homogenization rate is 2400-3000 r/min, and the homogenization time is 3 min.
7. The method of claim 1, wherein: in step S2, the cooling rate is 2 ℃/min.
8. The method of claim 1, wherein: in step S3, the cooling rate is 1 deg.C/min.
9. The method of claim 1, wherein: in step S7, the filtering operation is filtering with a 100 mesh screen.
CN202210143895.9A 2022-02-17 2022-02-17 Amber congee and preparation method thereof Pending CN114469828A (en)

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