CN114403494A - Electronic cigarette oil without nicotine and preparation method thereof - Google Patents
Electronic cigarette oil without nicotine and preparation method thereof Download PDFInfo
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- CN114403494A CN114403494A CN202210159331.4A CN202210159331A CN114403494A CN 114403494 A CN114403494 A CN 114403494A CN 202210159331 A CN202210159331 A CN 202210159331A CN 114403494 A CN114403494 A CN 114403494A
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- parts
- throat
- propylene glycol
- nicotine
- essence
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- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 43
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 title claims abstract description 33
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 229960002715 nicotine Drugs 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 240
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 193
- 239000002269 analeptic agent Substances 0.000 claims abstract description 71
- 235000013599 spices Nutrition 0.000 claims abstract description 41
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 235000011187 glycerol Nutrition 0.000 claims description 75
- 239000000796 flavoring agent Substances 0.000 claims description 41
- 235000019634 flavors Nutrition 0.000 claims description 40
- 239000000203 mixture Substances 0.000 claims description 28
- 238000003756 stirring Methods 0.000 claims description 28
- 238000002156 mixing Methods 0.000 claims description 22
- 239000003205 fragrance Substances 0.000 claims description 17
- 239000002304 perfume Substances 0.000 claims description 8
- SWNIAVIKMKSDBJ-UHFFFAOYSA-N 2-methyl-5-(1-methylpyrrolidin-2-yl)pyridine Chemical compound CN1CCCC1C1=CC=C(C)N=C1 SWNIAVIKMKSDBJ-UHFFFAOYSA-N 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 230000001953 sensory effect Effects 0.000 abstract description 14
- 235000019504 cigarettes Nutrition 0.000 abstract description 7
- 239000000853 adhesive Substances 0.000 abstract 1
- 230000001070 adhesive effect Effects 0.000 abstract 1
- 235000013772 propylene glycol Nutrition 0.000 description 69
- 239000000686 essence Substances 0.000 description 65
- 239000003921 oil Substances 0.000 description 21
- 235000019198 oils Nutrition 0.000 description 21
- 241000208125 Nicotiana Species 0.000 description 18
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 18
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 15
- 238000012360 testing method Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 7
- 239000012258 stirred mixture Substances 0.000 description 7
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 6
- 235000019439 ethyl acetate Nutrition 0.000 description 6
- NUJGJRNETVAIRJ-UHFFFAOYSA-N octanal Chemical compound CCCCCCCC=O NUJGJRNETVAIRJ-UHFFFAOYSA-N 0.000 description 6
- 240000005385 Jasminum sambac Species 0.000 description 5
- 239000003973 paint Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 description 4
- 235000010254 Jasminum officinale Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 229940093503 ethyl maltol Drugs 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 3
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 235000019719 rose oil Nutrition 0.000 description 3
- 239000010666 rose oil Substances 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 241000220317 Rosa Species 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- HJJPJSXJAXAIPN-UHFFFAOYSA-N arecoline Chemical compound COC(=O)C1=CCCN(C)C1 HJJPJSXJAXAIPN-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 235000019264 food flavour enhancer Nutrition 0.000 description 2
- 239000008369 fruit flavor Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009965 odorless effect Effects 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 description 1
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- 240000007154 Coffea arabica Species 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 244000147568 Laurus nobilis Species 0.000 description 1
- 235000017858 Laurus nobilis Nutrition 0.000 description 1
- 240000008790 Musa x paradisiaca Species 0.000 description 1
- 235000018290 Musa x paradisiaca Nutrition 0.000 description 1
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- 244000290333 Vanilla fragrans Species 0.000 description 1
- 235000009499 Vanilla fragrans Nutrition 0.000 description 1
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000019606 astringent taste Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 235000013736 caramel Nutrition 0.000 description 1
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000016213 coffee Nutrition 0.000 description 1
- 235000013353 coffee beverage Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 150000001954 decanoic acid esters Chemical class 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000013401 experimental design Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 235000019990 fruit wine Nutrition 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000021147 sweet food Nutrition 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/10—Devices using liquid inhalable precursors
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention relates to the technical field of adhesive dispensing, in particular to nicotine-free electronic cigarette oil and a preparation method thereof, wherein the nicotine-free electronic cigarette oil comprises the following components in parts by weight: glycerol: 40-60 parts; essence and spice: 20-30 parts of a solvent; propylene glycol: 5-39 parts; and throat-stimulating agents: 1-5 parts. The electronic cigarette liquid without nicotine disclosed by the invention can reduce the harm of the cigarette liquid to human bodies and can obtain the same sensory experience as nicotine by substituting the throat stimulating agent for nicotine.
Description
Technical Field
The invention relates to the technical field of electronic cigarette oil, in particular to nicotine-free electronic cigarette oil and a preparation method thereof.
Background
The electronic cigarette liquid is a novel tobacco product produced by imitating the traditional tobacco, in order to have the throat-hitting feeling and the physiological satisfaction brought by the nicotine in the traditional tobacco, a certain concentration of nicotine is added into the electronic cigarette liquid, and the nicotine is a toxic and addictive plant alkali and often brings harm to the human body in the process of using the electronic cigarette.
Disclosure of Invention
In order to overcome the above-mentioned drawbacks of the prior art, the present invention provides a nicotine-free electronic cigarette liquid to solve the above-mentioned problems of the background art.
The technical scheme adopted by the invention for solving the problems in the prior art is as follows: the electronic cigarette liquid without nicotine comprises the following components in parts by weight:
glycerol: 40-60 parts;
essence and spice: 20-30 parts of a solvent;
propylene glycol: 5-39 parts; and
throat-stimulating agent: 1-5 parts.
It can be seen that the essence, the perfume, the propylene glycol, the throat stimulating agent and the glycerol are mixed, and the propylene glycol has good solubility, so that all the components can be well dissolved, and the atomized steam has the sensory experience similar to nicotine after being sucked by a human body. According to the invention, the throat stimulating agent is used for replacing nicotine, so that the harm of tobacco tar to human bodies can be reduced, and the same sensory experience as nicotine can be obtained.
As a preferable scheme of the invention, the throat stimulating agent has a chemical formula as follows: 2-methyl-5- (1-methyl-2-pyrrolidinyl) pyridine.
As a preferred scheme of the invention, the paint comprises the following components in parts by weight:
glycerol: 50 parts of a mixture;
essence and spice: 20 parts of (1);
propylene glycol: 29 parts; and
throat-stimulating agent: 1 part.
As a preferred scheme of the invention, the paint comprises the following components in parts by weight:
glycerol: 50 parts of a mixture;
essence and spice: 25 parts of (1);
propylene glycol: 23 parts; and
throat-stimulating agent: and 2 parts.
As a preferred scheme of the invention, the paint comprises the following components in parts by weight:
glycerol: 40 parts of a mixture;
essence and spice: 30 parts of (1);
propylene glycol: 27 parts of (1); and
throat-stimulating agent: and 3 parts.
As a preferable scheme of the invention, the paint comprises the following components in parts by weight:
glycerol: 60 parts;
essence and spice: 20 parts of (1);
propylene glycol: 16 parts of a mixture; and
throat-stimulating agent: 4 parts.
As a preferred scheme of the invention, the paint comprises the following components in parts by weight:
glycerol: 60 parts;
essence and spice: 25 parts of (1);
propylene glycol: 10 parts of (A); and
throat-stimulating agent: 5 parts of the raw materials.
A preparation method of electronic cigarette oil without nicotine comprises the following steps:
respectively taking out 40-60 parts of glycerol, 20-30 parts of essence and spice, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent in corresponding containers for later use;
pouring the essence, the perfume, the propylene glycol, the throat stimulating agent and the glycerol into a mixing container in sequence for stirring treatment; and
taking out and standing to obtain the product.
As a preferred embodiment of the present invention, the process of sequentially pouring the flavors and fragrances, propylene glycol, throat stimulating agent and glycerin into a mixing container for stirring treatment further comprises:
the stirring speed is 300-500 rpm.
As a preferred embodiment of the present invention, the process of sequentially pouring the flavors and fragrances, propylene glycol, throat stimulating agent and glycerin into a mixing container for stirring treatment further comprises:
and stirring the essence, the spice, the propylene glycol, the throat stimulating agent and the glycerin at normal temperature and normal pressure.
Drawings
Fig. 1 is a flow chart of a method for preparing nicotine-free electronic cigarette liquid according to an embodiment of the present invention.
Detailed Description
The following further describes embodiments of the present invention with reference to the drawings. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto.
In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
According to the embodiment of the invention, the essence and the spice, the propylene glycol, the throat stimulating agent and the glycerin are mixed, and the propylene glycol has good dissolubility, so that all the components can be well dissolved, and are uniform and stable, and after the atomized steam is sucked by a human body, the nicotine-like sensory experience is realized. According to the invention, the throat stimulating agent is used for replacing nicotine, so that the harm of tobacco tar to human bodies can be reduced, and the same sensory experience as nicotine can be obtained.
The technical solution and the technical effect of the present invention will be further described by specific examples.
Example one
The invention provides nicotine-free electronic cigarette oil which comprises the following components in parts by weight:
glycerol: 40-60 parts; essence and spice: 20-30 parts of a solvent; propylene glycol: 5-39 parts; and throat-stimulating agents: 1-5 parts.
The invention is characterized in that the health and safety level of the essence and the spice is edible level, and the essence and the spice are water-soluble and oil-soluble, and are suitable for all flavors of edible essence. For example, fruit flavors, coffee, vanilla, chocolate, jasmine, rose, and the like may be used.
The propylene glycol has a chemical formula of C3H8O2, is colorless viscous liquid at normal state, is nearly odorless, and smells slightly sweet.
Glycerol is also glycerol, is colorless, odorless, sweet, clear, viscous and liquid in appearance, and is an organic substance. Glycerol, which absorbs moisture from the air, also absorbs hydrogen sulfide, hydrogen cyanide and sulfur dioxide. Insoluble in benzene, chloroform, carbon tetrachloride, carbon disulfide, petroleum ether and oils.
The throat-stimulating agent has the chemical formula: 2-methyl-5- (1-methyl-2-pyrrolidinyl) pyridine; cas number of acute larynx agent is: 101540-79-8. The throat stimulant can replace nicotine, and can achieve the sensory effect similar to nicotine.
Specifically, 40-60 parts of glycerin, 20-30 parts of essence and flavor, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent are respectively taken out and put into corresponding containers for standby application, and 40-60 parts of glycerin, 20-30 parts of essence and flavor, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent are added into a specified mixing container for stirring treatment, so that the mixture of essence and flavor, propylene glycol, throat stimulating agent and glycerin is uniformly mixed. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained. Because the propylene glycol has good solubility, all the components can be well dissolved, the propylene glycol is uniform and stable, and after the atomized steam is absorbed by a human body, the atomized steam has sensory experience similar to nicotine.
Example two
In this embodiment, the composition comprises the following components in parts by weight:
glycerol: 50 parts of a mixture; essence and spice: 20 parts of (1); propylene glycol: 29 parts; and throat-stimulating agents: 1 part.
Specifically, 50 parts of glycerin, 20 parts of essence and flavor, 29 parts of propylene glycol and 1 part of throat stimulating agent are respectively taken out of the corresponding container for standby application, and the mixture of the essence and flavor, the propylene glycol, the throat stimulating agent and the glycerin is uniformly mixed by adding 50 parts of glycerin, 20 parts of essence and flavor, 29 parts of propylene glycol and 1 part of throat stimulating agent into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained. The parts of the taken out glycerin, the essence and the spice, the propylene glycol and the throat stimulating agent can be matched by grams or kilograms, for example, 50 grams of glycerin, 20 grams of essence and the spice, 29 grams of propylene glycol and 1 gram of the throat stimulating agent are added into a mixing container, and a magnetic stirrer is used for stirring to uniformly mix the mixture, so that the electronic cigarette oil has good experience effect when being used by an electronic cigarette.
EXAMPLE III
In this embodiment, the composition comprises the following components in parts by weight:
glycerol: 50 parts of a mixture; essence and spice: 25 parts of (1); propylene glycol: 23 parts; and throat-stimulating agents: and 2 parts.
Specifically, 50 parts of glycerin, 25 parts of essence and flavor, 23 parts of propylene glycol and 2 parts of throat stimulating agent are respectively taken out of the corresponding container for standby application, and the mixture of the essence and flavor, the propylene glycol, the throat stimulating agent and the glycerin is uniformly mixed by adding 50 parts of glycerin, 25 parts of essence and flavor, 23 parts of propylene glycol and 2 parts of throat stimulating agent into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained.
Example four
In this embodiment, the composition comprises the following components in parts by weight:
glycerol: 40 parts of a mixture; essence and spice: 30 parts of (1); propylene glycol: 27 parts of (1); and throat-stimulating agents: and 3 parts.
Specifically, 40 parts of glycerin, 30 parts of essence and flavor, 27 parts of propylene glycol and 3 parts of throat stimulating agent are respectively taken out of the corresponding container for standby application, and the mixture of the essence and flavor, the propylene glycol, the throat stimulating agent and the glycerin is uniformly mixed by adding 40 parts of glycerin, 30 parts of essence and flavor, 27 parts of propylene glycol and 3 parts of throat stimulating agent into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained.
EXAMPLE five
In this embodiment, the composition comprises the following components in parts by weight:
glycerol: 60 parts; essence and spice: 20 parts of (1); propylene glycol: 16 parts of a mixture; and throat-stimulating agents: 4 parts.
Specifically, 60 parts of glycerin, 20 parts of essence and flavor, 16 parts of propylene glycol and 4 parts of throat stimulating agent are respectively taken out of the corresponding container for standby application, and the mixture of the essence and flavor, the propylene glycol, the throat stimulating agent and the glycerin is uniformly mixed by adding the 60 parts of glycerin, the 20 parts of essence and flavor, the 16 parts of propylene glycol and the 4 parts of throat stimulating agent into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained.
EXAMPLE six
In this embodiment, the composition comprises the following components in parts by weight:
glycerol: 60 parts; essence and spice: 25 parts of (1); propylene glycol: 10 parts of (A); and throat-stimulating agents: 5 parts of the raw materials.
Specifically, 60 parts of glycerin, 25 parts of essence and flavor, 10 parts of propylene glycol and 5 parts of throat stimulating agent are respectively taken out of the corresponding container for standby application, and the mixture of the essence and flavor, the propylene glycol, the throat stimulating agent and the glycerin is uniformly mixed by adding the 60 parts of glycerin, the 25 parts of essence and flavor, the 10 parts of propylene glycol and the 5 parts of throat stimulating agent into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained.
EXAMPLE seven
In any one of the first to sixth embodiments, the flavor and fragrance is one or more of ethyl acetate, ethyl butyrate, ethyl maltol, caprylic aldehyde, capric acid, jasmine extract, and rose oil.
Wherein, the ethyl acetate (C4H8O2) is also named as ethyl acetate, has sweet taste, is easy to volatilize, has excellent dissolubility, and is a material applied to essences and flavors. Meanwhile, the ethyl acetate has strong ether-like smell and has the bouquet of qingling and little fruity fragrance.
Ethyl butyrate (C6H12O2) is used for flavor and fragrance extraction and as a solvent. Is widely applied to edible essence formulas such as banana, pineapple and the like, and can be used for preparing various fruit-flavor essences and other flavor essences.
Ethyl maltol (C7H8O3) is increasingly used as a flavor modifier and flavoring agent. Is a food additive which is well recognized by people and has the advantages of safety, reliability, small dosage and obvious effect. The sweet potato flavor enhancer is a good flavor enhancer for tobacco, food, beverage, essence, fruit wine, daily cosmetics and the like, has a remarkable effect of improving and enhancing the flavor of food, plays a role of sweetening sweet food and can prolong the storage period of the food.
Ethyl maltol is classified into type a1 (pure flavor type), type a2 (light burnt flavor type) and type A3 (enhanced burnt flavor type). The A1 type cigarette has prominent fruity flavor, and when the A1 type cigarette is used for preparing various tobacco flavors and fragrances and is added into cigarettes, the tobacco flavor is more mellow and fragrant, the dry, astringent and bitter taste of the mouth and throat is reduced after the A1 type cigarette is smoked, and the mouth and throat feel smooth and comfortable. The A2 type has strong caramel fragrance and has strong synergistic effect on the original sweet and fresh taste of various foods. The A3 type has the advantages of high purity, high quality, high whiteness, unique fragrance, more prominent characteristic flavor, mellow and rich burnt fragrance, long aftertaste after being heated and dissolved, and lasting fragrance.
Octanal (C8H16O) has strong fruit fragrance, and can be used as edible perfume or perfume of soap detergent.
Capric acid (C10H20O2) is a by-product produced during the hydrolysis of laurel oil, coconut oil or pungent litse fruit oil to prepare lauric acid, and is mainly used for preparing decanoic acid esters, and the esters are used as spice, humectant, plasticizer, food additive, etc.
The jasmine flower extract is a pasty natural perfume product extracted from plant jasmine flowers, and has pure fragrance and good taste.
Rose oil is a natural perfume product in paste form extracted from plant rose.
When the electronic cigarette oil is specifically implemented, one or more of ethyl acetate, ethyl butyrate, ethyl maltol, caprylic aldehyde, capric acid, jasmine extract and rose oil are used as the essence and flavor, glycerol, propylene glycol and the throat stimulating agent are poured into a mixing container to be mixed, a magnetic stirrer is used for stirring for a period of time, after the essence and flavor, the glycerol, the propylene glycol and the throat stimulating agent are uniformly mixed, the electronic cigarette oil is taken out and stands at normal temperature to obtain the electronic cigarette oil with the same sensory effect as nicotine, and the electronic cigarette oil can keep complete fragrance when used through an electronic cigarette. The surrounding environment is not influenced, and the health protection is also realized for the user. The tobacco tar replaces nicotine by the throat stimulating agent, so that the same sensory effect as nicotine can be obtained, and the harm of the tobacco tar to human bodies can be reduced.
In addition, the application also provides a preparation method of the nicotine-free electronic cigarette oil, which comprises the following steps:
step S101, respectively taking out 40-60 parts of glycerin, 20-30 parts of essence and spice, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent in corresponding containers for later use.
Specifically, 40-60 parts of glycerin, 20-30 parts of flavors and fragrances, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent are taken out and respectively placed in corresponding containers for standby, for example, the corresponding containers are labeled with numbers so as to distinguish the glycerin, the flavors and fragrances, the propylene glycol and the arecoline. The number may be 1, 2, 3, 4, etc., or A, B, C, D, and the number is mainly used to distinguish the corresponding components to avoid mixing errors during the addition.
And step S102, pouring the essence, the propylene glycol, the throat stimulating agent and the glycerin into a mixing container in sequence for stirring treatment.
Specifically, the glycerol is poured into the cigarette in the largest amount, so that the essence, the perfume, the propylene glycol and the throat stimulating agent can be fully mixed, and the sensory effect of nicotine can be achieved after each smoking. The mixture is uniformly mixed by stirring the mixture in a container, and the stirring process may be a conventional manual stirring by a stirring rod or a stirrer or the like as long as the mixing can be uniformly stirred.
And step S103, taking out and standing to obtain the product.
In specific implementation, 40 parts of glycerin, 30 parts of essence and spice, 27 parts of propylene glycol and 3 parts of throat stimulating agent are respectively taken out and placed in containers with corresponding numbers 1, 2, 3 and 4 for preparation. The mixture of the essence, the propylene glycol, the throat stimulating agent and the glycerol is uniformly mixed by adding the 30 parts of the essence, the 27 parts of the propylene glycol, the 3 parts of the throat stimulating agent and the 40 parts of the glycerol into a specified mixing container and stirring. Because the propylene glycol, the essence and the spice and the glycerol have good solubility, after standing for 5-20 minutes at normal temperature, the stirred mixture is taken out, and the electronic cigarette oil can be obtained. Because the propylene glycol has good solubility, all the components can be well dissolved, the propylene glycol is uniform and stable, and after the atomized steam is absorbed by a human body, the atomized steam has sensory experience similar to nicotine.
In this embodiment, pour essence spices, propylene glycol, throat stimulating agent and glycerine into a mixing vessel in proper order and stir processing, still include: the stirring speed is 300-500 rpm.
Specifically, the essence, the propylene glycol, the throat stimulating agent and the glycerol are sequentially poured into a mixing container, and stirring treatment is carried out at the speed of 400 revolutions per minute so as to ensure that the essence, the propylene glycol, the throat stimulating agent and the glycerol can be fully mixed.
Further, the essence, the spice, the propylene glycol, the throat stimulating agent and the glycerin are poured into a mixing container in sequence for stirring treatment, and the method also comprises the following steps: the essence, the spice, the propylene glycol, the throat stimulating agent and the glycerin are stirred at normal temperature and normal pressure, and the mixing mode is simple.
In order to further illustrate the beneficial effects of the nicotine-free electronic cigarette liquid provided by the embodiment of the present invention, the following detailed description is made in conjunction with specific test examples.
Test objectives: the similarity of the throat stimulant and nicotine in tobacco tar was examined.
The test personnel: a company research and development department personnel.
The number of the evaluated persons: in order to maximize the reliability of the experiment, the minimum number of participants should be 64 according to the rule of the triangle inspection method.
And (3) experimental design: due to the limited number of companies, 12 persons were tested 5 times each (60 times), and 6 of the 12 persons were tested the last 6 times (6 times), i.e. 66 tests.
66 answer sheets were prepared and examined by twelve panelists, and a total of sixty-six samples, 33 nicotine-containing tobacco tar samples and 33 throat stimulant-containing tobacco tar samples were prepared. Description of the drawings: samples of 33 tobacco products were prepared by injecting the same amount of tobacco tar with the same content (30mg/mL) of nicotine and the same amount of tobacco tar as the throat stimulant into an electronic cigarette device with the same parameters.
TABLE 1 throat stimulant and nicotine differential test preparation worksheet
The test steps are as follows:
1. two kinds of tobacco tar were prepared, 33 each, and placed in two groups (A and B) without confusion.
2. According to the numbering of the table, 11 numbers are prepared for each number, and the two kinds of tobacco tar are respectively marked. That is, the number of samples marked with numbers 869, 466 and 695 in the tobacco tar (A) containing the throat stimulating agent is respectively 11; the number of samples labeled 771595 and 861 in nicotine-containing tobacco smoke (B) was also 11, respectively.
3. The marked samples are combined according to the table above, each combination is provided with a question and answer paper, and the corresponding group number and sample number are written on the question and answer paper and are presented to a appraiser.
4. Test instructions: the panelists had three samples with a number, two of which were identical and one was not identical. The panelist tasted 3 samples in order from left to right and then selected a different number from the other two samples. Multiple tastings are possible, but no answer is available. (evaluation mode: sucking electronic cigarette, one sample is finished each time, gargling with clean water, and the next sample is finished.)
And (3) test results: and (4) recovering the 66 answered question and answer sheets, checking the answers according to the table, and counting the number of the answered questions and answer pairs. By check, in this test, 20 persons in total have made correct responses. According to the rule of triangulation, 66 panelists were rated at least 26 times to correctly distinguish one from the other two samples to show that the sensory experience of the two materials was different. In contrast, only 20 trials made the correct choice in the experiment, indicating that the difference in sensory experience between the two substances was negligible.
From the test data, the electronic cigarette liquid without nicotine disclosed by the invention can obtain the same sensory effect as nicotine by replacing nicotine with the throat stimulating agent, and can reduce the harm of the cigarette liquid to human bodies.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or that certain features may be replaced by equivalents thereof; any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The electronic cigarette liquid without nicotine is characterized by comprising the following components in parts by weight:
glycerol: 40-60 parts;
essence and spice: 20-30 parts of a solvent;
propylene glycol: 5-39 parts; and
throat-stimulating agent: 1-5 parts.
2. The nicotine-free e-liquid of claim 1, wherein the throat stimulant is of the formula: 2-methyl-5- (1-methyl-2-pyrrolidinyl) pyridine.
3. The nicotine-free electronic cigarette liquid of claim 1, comprising the following components in parts by weight:
glycerol: 50 parts of a mixture;
essence and spice: 20 parts of (1);
propylene glycol: 29 parts; and
throat-stimulating agent: 1 part.
4. The nicotine-free electronic cigarette liquid of claim 1, comprising the following components in parts by weight:
glycerol: 50 parts of a mixture;
essence and spice: 25 parts of (1);
propylene glycol: 23 parts; and
throat-stimulating agent: and 2 parts.
5. The nicotine-free electronic cigarette liquid of claim 1, comprising the following components in parts by weight:
glycerol: 40 parts of a mixture;
essence and spice: 30 parts of (1);
propylene glycol: 27 parts of (1); and
throat-stimulating agent: and 3 parts.
6. The nicotine-free electronic cigarette liquid of claim 1, comprising the following components in parts by weight:
glycerol: 60 parts;
essence and spice: 20 parts of (1);
propylene glycol: 16 parts of a mixture; and
throat-stimulating agent: 4 parts.
7. The nicotine-free electronic cigarette liquid of claim 1, comprising the following components in parts by weight:
glycerol: 60 parts;
essence and spice: 25 parts of (1);
propylene glycol: 10 parts of (A); and
throat-stimulating agent: 5 parts of the raw materials.
8. A preparation method of electronic cigarette oil without nicotine is characterized by comprising the following steps:
respectively taking out 40-60 parts of glycerol, 20-30 parts of essence and spice, 5-39 parts of propylene glycol and 1-5 parts of throat stimulating agent in corresponding containers for later use;
pouring the essence, the perfume, the propylene glycol, the throat stimulating agent and the glycerol into a mixing container in sequence for stirring treatment; and
taking out and standing to obtain the product.
9. The nicotine-free electronic cigarette liquid of claim 8, wherein the flavor and fragrance, the propylene glycol, the throat stimulant, and the glycerin are sequentially poured into a mixing container for stirring treatment, and further comprising:
the stirring speed is 300-500 rpm.
10. The nicotine-free electronic cigarette liquid of claim 8, wherein the flavor and fragrance, the propylene glycol, the throat stimulant, and the glycerin are sequentially poured into a mixing container for stirring treatment, and further comprising:
and stirring the essence, the spice, the propylene glycol, the throat stimulating agent and the glycerin at normal temperature and normal pressure.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210159331.4A CN114403494A (en) | 2022-02-21 | 2022-02-21 | Electronic cigarette oil without nicotine and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210159331.4A CN114403494A (en) | 2022-02-21 | 2022-02-21 | Electronic cigarette oil without nicotine and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11964958B1 (en) | 2023-01-18 | 2024-04-23 | Ready Mix Naturals, LLC | Vaporizable alkaloid compositions and methods of use thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11964958B1 (en) | 2023-01-18 | 2024-04-23 | Ready Mix Naturals, LLC | Vaporizable alkaloid compositions and methods of use thereof |
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Application publication date: 20220429 |