CN111202259A - Smoke-free electronic cigarette liquid and preparation method thereof - Google Patents

Smoke-free electronic cigarette liquid and preparation method thereof Download PDF

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Publication number
CN111202259A
CN111202259A CN202010117453.8A CN202010117453A CN111202259A CN 111202259 A CN111202259 A CN 111202259A CN 202010117453 A CN202010117453 A CN 202010117453A CN 111202259 A CN111202259 A CN 111202259A
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China
Prior art keywords
propylene glycol
parts
essence
electronic cigarette
cigarette liquid
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Pending
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CN202010117453.8A
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Chinese (zh)
Inventor
卢帅
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Shenzhen Detension Biotechnology Co ltd
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Shenzhen Detension Biotechnology Co ltd
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Priority to CN202010117453.8A priority Critical patent/CN111202259A/en
Publication of CN111202259A publication Critical patent/CN111202259A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

Abstract

The invention is suitable for the technical field of electronic cigarettes, and provides a smog-free electronic cigarette liquid and a preparation method thereof, wherein the smog-free electronic cigarette liquid comprises the following components in parts by weight: essence and spice: 10-30 parts; propylene glycol: 70-90 parts; according to the embodiment of the invention, the essence and the perfume are mixed, and the propylene glycol has good solubility to the essence and the perfume, and only a small amount of smoke is generated when atomized steam is inhaled and exhaled by a human body, so that a smokeless effect can be achieved, the influence of the smoke on other people and the surrounding environment is greatly reduced, meanwhile, the fragrance can be kept complete, and the use comfort is pure.

Description

Smoke-free electronic cigarette liquid and preparation method thereof
Technical Field
The invention belongs to the technical field of electronic cigarettes, and particularly relates to a smog-free electronic cigarette liquid and a preparation method thereof.
Background
At present, the number of people who smoke tobacco is increasing, and long-term smoking causes physical harm to people, and meanwhile, the harm of people in the surrounding environment of smokers who smoke second-hand smoke is greater, and the people are healthy for self and the surrounding environment.
The electronic cigarette replaces partial tobacco, reduces the harm of the cigarette to smokers and the harm of second-hand cigarette to surrounding people, but along with the further improvement of the awareness of people on self health and the awareness of surrounding environment quality on the influence of self health, the electronic cigarette is required to be developed towards more health and environmental protection.
However, all the electronic cigarettes mentioned above generate a large amount of smoke when in use, the smoke scatters and simultaneously carries the smell of the tobacco tar to spread, and the smoke unintentionally also has a certain adverse effect on the surrounding crowd and the environment, especially in public places or office places, and the influence on the surrounding environment is larger.
Disclosure of Invention
The invention provides a smog-free electronic cigarette liquid and a preparation method thereof, and aims to solve the problem that the existing electronic cigarette generates large smog.
The invention is realized in such a way that the electronic cigarette liquid without smoke comprises the following components in parts by weight:
essence and spice: 10-30 parts;
propylene glycol: 70-90 parts.
Further, the composition comprises the following components by weight:
the essence and spice comprises the following components: 18 parts of a mixture;
the propylene glycol: and 82 parts.
Further, the composition comprises the following components by weight:
the essence and spice comprises the following components: 15 parts of (1);
the propylene glycol: 80 parts of the raw materials.
Further, the composition comprises the following components by weight:
the essence and spice comprises the following components: 12 parts of (1);
the propylene glycol: 85 parts of the raw materials.
Further, the composition comprises the following components by weight:
the essence and spice comprises the following components: 23 parts;
the propylene glycol: 73 parts.
The invention also provides a preparation method of the electronic cigarette liquid without smoke, which comprises the following steps:
s1, pouring 10-30 parts of essence and spice and 70-90 parts of propylene glycol into a container;
s2, stirring a mixture of 10-30 parts of essence and spice and 70-90 parts of propylene glycol in the container;
and S3, taking out and standing to obtain the product.
Further, in the step S2, the stirring process is specifically performed by stirring with a stirrer.
Further, the S1 specifically includes: pouring 10 parts of the essence and the 90 parts of the propylene glycol into a container.
Still further, the container is a conventional stainless steel container.
Compared with the prior art, the invention has the following beneficial effects: through mixing essence spices and propylene glycol, because propylene glycol is to the good solubility of essence spices to when atomizing back steam is inhaled the human body and is inhaled the exhalation, only produce minute quantity smog, thereby can reach smokeless effect, the influence of smog to other people and surrounding environment that significantly reduces can also keep fragrance complete simultaneously, uses the comfort pure.
Drawings
Fig. 1 is a flow chart of a method for preparing an electronic cigarette liquid without smoke according to an embodiment of the invention.
Fig. 2 is table 1 provided by an embodiment of the present invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
According to the embodiment of the invention, the essence and the perfume are mixed, and the propylene glycol has good solubility to the essence and the perfume, and only a small amount of smoke is generated when atomized steam is inhaled and exhaled by a human body, so that a large amount of smoke generated after glycerin atomization is avoided, the smokeless effect can be achieved, the influence of the smoke on other people and the surrounding environment is greatly reduced, meanwhile, the fragrance can be kept complete, and the popularization and the use are convenient.
The technical solution and the technical effect of the present invention will be further described by specific examples.
Example one
The invention provides a smog-free electronic cigarette liquid, which comprises the following components in parts by weight:
essence and spice: 10-30 parts;
propylene glycol: 70-90 parts.
The invention is characterized in that the health and safety level of the essence and the spice is edible level, and the essence and the spice are water-soluble and oil-soluble, and are suitable for all flavors of edible essence. For example, fruit flavors, coffee, vanilla, chocolate, jasmine, rose, and the like may be used.
The propylene glycol has a chemical formula of C3H8O2, is colorless viscous liquid at normal state, is nearly odorless, and smells slightly sweet.
In specific implementation, 10-30 parts of essence and spice and 70-90 parts of propylene glycol are taken out for later use; the essence and the propylene glycol are added into a container, and the mixture of the essence and the propylene glycol in the container is stirred, so that the propylene glycol and the propylene glycol are dissolved after being uniformly stirred due to good solubility between the propylene glycol and the essence and the propylene glycol. And taking out the stirred mixture of the essence and the spice and the propylene glycol. Standing for 5-20 minutes at normal temperature to obtain the electronic cigarette liquid.
Further, the container may be a glass container or a conventional stainless steel container, etc.
According to the embodiment of the invention, the essence and the perfume are mixed, and the propylene glycol has good solubility to the essence and the perfume, and only a small amount of smoke is generated when atomized steam is inhaled and exhaled by a human body, so that a large amount of smoke generated after glycerin atomization is avoided, the smokeless effect can be achieved, the influence of the smoke on other people and the surrounding environment is greatly reduced, meanwhile, the fragrance can be kept complete, and the popularization and the use are convenient.
Example two
In the present embodiment, the following components are included by weight:
the essence and spice comprises the following components: 18 parts of a mixture;
the propylene glycol: and 82 parts.
In specific implementation, 18 parts of essence and spice and 82 parts of propylene glycol are taken out for later use; the essence and the propylene glycol are added into a container, and the mixture of the essence and the propylene glycol in the container is stirred, so that the propylene glycol and the propylene glycol are dissolved after being uniformly stirred due to good solubility between the propylene glycol and the essence and the propylene glycol. And taking out the stirred mixture of the essence and the spice and the propylene glycol. Standing for 5-20 minutes at normal temperature to obtain the electronic cigarette liquid.
EXAMPLE III
In the present embodiment, the following components are included by weight:
the essence and spice comprises the following components: 15 parts of (1);
the propylene glycol: 80 parts of the raw materials.
In specific implementation, 15 parts of essence and spice and 80 parts of propylene glycol are taken out for later use; the essence and the propylene glycol are added into a container, and the mixture of the essence and the propylene glycol in the container is stirred, so that the propylene glycol and the propylene glycol are dissolved after being uniformly stirred due to good solubility between the propylene glycol and the essence and the propylene glycol. And taking out the stirred mixture of the essence and the spice and the propylene glycol. Standing for 5-20 minutes at normal temperature to obtain the electronic cigarette liquid.
Example four
In the present embodiment, the following components are included by weight:
the essence and spice comprises the following components: 12 parts of (1);
the propylene glycol: 85 parts of the raw materials.
In specific implementation, 12 parts of essence and spice and 85 parts of propylene glycol are taken out for later use; the essence and the propylene glycol are added into a container, and the mixture of the essence and the propylene glycol in the container is stirred, so that the propylene glycol and the propylene glycol are dissolved after being uniformly stirred due to good solubility between the propylene glycol and the essence and the propylene glycol. And taking out the stirred mixture of the essence and the spice and the propylene glycol. Standing for 5-20 minutes at normal temperature to obtain the electronic cigarette liquid.
EXAMPLE five
In the present embodiment, the following components are included by weight:
the essence and spice comprises the following components: 23 parts;
the propylene glycol: 73 parts.
In specific implementation, 23 parts of essence and spice and 73 parts of propylene glycol are taken out for later use; the essence and the propylene glycol are added into a container, and the mixture of the essence and the propylene glycol in the container is stirred, so that the propylene glycol and the propylene glycol are dissolved after being uniformly stirred due to good solubility between the propylene glycol and the essence and the propylene glycol. And taking out the stirred mixture of the essence and the spice and the propylene glycol. Standing for 5-20 minutes at normal temperature to obtain the electronic cigarette liquid.
EXAMPLE six
In any one of the first to fifth embodiments, the flavor and fragrance is one or more of ethyl acetate, ethyl butyrate, ethyl maltol, caprylic aldehyde, capric acid, jasmine extract and rose oil.
Wherein, the ethyl acetate (C4H8O2) is also named as ethyl acetate, has sweet taste, is easy to volatilize, has excellent dissolubility, and is a material applied to essences and flavors. Meanwhile, the ethyl acetate has strong ether-like smell and has the bouquet of qingling and little fruity fragrance.
Ethyl butyrate (C6H12O2) is used for flavor and fragrance extraction and as a solvent. Is widely applied to edible essence formulas such as banana, pineapple and the like, and can be used for preparing various fruit-flavor essences and other flavor essences.
Ethyl maltol (C7H8O3) is increasingly used as a flavor modifier and flavoring agent. Is a food additive which is well recognized by people and has the advantages of safety, reliability, small dosage and obvious effect. The sweet potato flavor enhancer is a good flavor enhancer for tobacco, food, beverage, essence, fruit wine, daily cosmetics and the like, has a remarkable effect of improving and enhancing the flavor of food, plays a role of sweetening sweet food and can prolong the storage period of the food.
Ethyl maltol is classified into type a1 (pure flavor type), type a2 (light burnt flavor type) and type A3 (enhanced burnt flavor type). The A1 type cigarette has prominent fruity flavor, and when the A1 type cigarette is used for preparing various tobacco flavors and fragrances and is added into cigarettes, the tobacco flavor is more mellow and fragrant, the dry, astringent and bitter taste of the mouth and throat is reduced after the A1 type cigarette is smoked, and the mouth and throat feel smooth and comfortable. The A2 type has strong caramel fragrance and has strong synergistic effect on the original sweet and fresh taste of various foods. The A3 type has the advantages of high purity, high quality, high whiteness, unique fragrance, more prominent characteristic flavor, mellow and rich burnt fragrance, long aftertaste after being heated and dissolved, and lasting fragrance.
Octanal (C8H16O) has strong fruit fragrance, and can be used as edible perfume or perfume of soap detergent.
Capric acid (C10H20O2) is a by-product produced during the hydrolysis of laurel oil, coconut oil or pungent litse fruit oil to prepare lauric acid, and is mainly used for preparing decanoic acid esters, and the esters are used as spice, humectant, plasticizer, food additive, etc.
The jasmine flower extract is a pasty natural perfume product extracted from plant jasmine flowers, and has pure fragrance and good taste.
Rose oil is a natural perfume product in paste form extracted from plant rose.
When the electronic cigarette liquid is used through an electronic cigarette, a smokeless effect can be achieved, and meanwhile, the fragrance can be kept complete. The surrounding environment is not influenced, and the health protection is also realized for the user.
EXAMPLE seven
With reference to fig. 1, the present invention further provides a method for preparing a smokeless electronic cigarette liquid, comprising the steps of:
s1, pouring 10-30 parts of essence and spice and 70-90 parts of propylene glycol into a container.
Specifically, 10-30 parts of essence and flavor are taken out, 70-90 parts of propylene glycol are stored in two containers, and the essence and flavor and the propylene glycol in the two containers are respectively poured into a third container for mixing. The third container is clean and sanitary, and avoids pollution to the added essence, spice and propylene glycol and influences the purity of the essence, spice and propylene glycol.
S2, stirring the mixture of 10-30 parts of essence and spice and 70-90 parts of propylene glycol in the container.
Specifically, the mixture of the essence and the perfume and the propylene glycol is stirred in a container, and the stirring is stopped after the mixture of the essence and the perfume and the propylene glycol is uniformly stirred and mixed.
And S3, taking out and standing to obtain the product.
In the embodiment of the invention, 10-30 parts of essence and flavor and 70-90 parts of propylene glycol are taken out and stored in two containers, and the essence and flavor and the propylene glycol in the two containers are respectively poured into a third container for mixing. The mixture of the essence and the spice and the propylene glycol is stirred in a container, and the stirring is stopped after the mixture of the essence and the spice and the propylene glycol is uniformly stirred and mixed. And taking the mixture of the flavor essence and the propylene glycol which are uniformly stirred and mixed out from the container, and standing for 5-20 minutes at normal temperature to obtain the smog-free electronic cigarette liquid. This electron cigarette liquid is through mixing essence spices and propylene glycol, because propylene glycol is to the good solubility of essence spices to when atomizing back steam is inhaled the breath through the human body, only produce a minute amount of smog, avoid glycerine to produce a large amount of smog after atomizing, thereby can reach smokeless effect, the influence of smog to other people and surrounding environment that significantly reduces can also keep fragrance complete simultaneously, convenient to popularize and use.
In this embodiment, in the step S2, the stirring process is specifically performed by stirring with a stirrer.
Wherein the stirrer comprises a flap stirrer, a frame stirrer and the like.
The flap type stirrer can enable materials to circularly flow in the reaction kettle during stirring, plays a role of mainly volume circulation, has small shearing action and has good up-and-down turning effect. When a larger flow velocity is needed, a guide cylinder is arranged in the reaction kettle. The flap turbine stirrer is generally suitable for the reaction of gas-liquid phase mixing, and the rotation number of the stirrer is generally selected to be more than 300 r/min.
The frame stirrer can be regarded as a paddle stirrer, and has a firmer structure and large material stirring amount. If the shape of the bottom of the stirrer is similar to that of the bottom head of the reaction kettle, the stirrer is generally called an anchor stirrer. The gap between the frame type stirrer and the kettle wall is small, which is beneficial to the heat transfer process, and when the frame type stirrer rotates rapidly, the static layer is taken down from the wall of the reaction kettle by the liquid driven by the blades of the stirrer; the agitator with the scraper plate can produce good heat conduction when rotating at a slow speed. Such agitators are commonly used for heat transfer, crystallization operations, and agitation of high viscosity liquids, high consistency slurries, and settling slurries.
Specifically, the mixture of the essence and the spice in the container and the propylene glycol is stirred under a stirrer, so that labor is saved. Meanwhile, the essence and the spice can be uniformly mixed with the propylene glycol, so that the matching effect of the essence and the spice and the propylene glycol is better, and the using effect is good.
In this embodiment, the S1 specifically includes: pouring 10 parts of the essence and the 90 parts of the propylene glycol into a container.
Specifically, 10 parts of the flavors and 90 parts of propylene glycol are taken out and stored in two containers, and the flavors and propylene glycol in the two containers and the propylene glycol in the three containers are respectively poured into the three containers for mixing.
In this example, the vessel is a conventional stainless steel vessel.
Specifically, the mixture of the essence and the spice and the propylene glycol can be uniformly mixed under the stirring of the stirrer by using a conventional stainless steel container, the mixture of the essence and the spice and the propylene glycol can be prevented from being polluted by the external environment, the mixing effect is high, and the mixture is pure.
In order to further illustrate the beneficial effects of the smokeless electronic cigarette liquid provided by the embodiment of the invention, the following detailed description is made in combination with specific test examples:
test one: smoke volume test
1. Test samples: embodiments one to five of the invention provide a smoke-free electronic cigarette liquid product prepared from the components.
2. Preparation of test solutions: 10 g of the smokeless electronic cigarette liquid products provided in the first to fifth embodiments are weighed into electronic smoking sets (using more than two brands) with the number of 1 to 30 for sensory quality evaluation, wherein the electronic smoking sets used in the test of the invention are common electronic smoking sets on the market, the power is 8 to 10W, and the voltage is 3.3 to 4.2V.
And (3) formal test: by providing 30 test users with 1-30 randomly numbered electronic smoking sets, the test users inhale according to the common smoking habit, inhale enough amount, then return to the pharynx in a smooth manner, and exhale the inhaled atomized vapor from the nasal cavity slowly. Of the 30 trials, 28 had essentially no smoke seen, and 2 had exhaled a fine light smoke. The smokeless effect is basically achieved, and the influence of the smoke on other people and the surrounding environment is greatly reduced.
In the whole process, 28 cases of the multiple groups of data tested by the embodiment of the invention have no smoke basically, and 2 cases of the multiple groups of data have fine light smoke when being exhaled, so that the embodiment of the invention utilizes the good solubility of the propylene glycol to the essence and the perfume, and only generates a small amount of smoke when the atomized steam is inhaled by a human body and exhaled. The smokeless effect is basically achieved, and the influence of the smoke on other people and the surrounding environment is greatly reduced.
And (2) test II: comfort test
1. Test samples: embodiments one to five of the invention provide a smoke-free electronic cigarette liquid product prepared from the components.
2. Preparation of test solutions: 10 g of the smokeless electronic cigarette liquid products provided in the first to fifth embodiments are weighed into electronic smoking sets (using more than two brands) with the number of 1 to 30 for sensory quality evaluation, wherein the electronic smoking sets used in the test of the invention are common electronic smoking sets on the market, the power is 8 to 10W, and the voltage is 3.3 to 4.2V.
And (3) formal test: by providing 30 test users with 1-30 randomly numbered electronic smoking sets, the test users inhale according to the common smoking habit, inhale enough amount, then return to the pharynx in a smooth manner, and exhale the inhaled atomized vapor from the nasal cavity slowly. In 30 experiments, 27 of the experiments have comfortable and pure aftertaste, no dryness and no moistness and moderate strength; 3 cases exhaled slightly uncomfortable. The effect of comfortable feeling of the electronic cigarette is basically achieved.
And (3) test III: taste style
1. Test samples: embodiments one to five of the invention provide a smoke-free electronic cigarette liquid product prepared from the components.
2. Preparation of test solutions: 10 g of the smokeless electronic cigarette liquid products provided in the first to fifth embodiments are weighed into electronic smoking sets (using more than two brands) with the number of 1 to 30 for sensory quality evaluation, wherein the electronic smoking sets used in the test of the invention are common electronic smoking sets on the market, the power is 8 to 10W, and the voltage is 3.3 to 4.2V.
And (3) formal test: by providing 30 test users with 1-30 randomly numbered electronic smoking sets, the test users inhale according to the common smoking habit, inhale enough amount, then return to the pharynx in a smooth manner, and exhale the inhaled atomized vapor from the nasal cavity slowly. In 30 experiments, 29 experiments show that the aftertaste is slightly sweet, the fragrance is kept complete, and the fragrance is not dry and moist; the exhaled aroma of 1 case was slightly impure. The effect of keeping the fragrance of the electronic cigarette complete is basically achieved.
As shown in fig. 2, table 1 shows the results of smoking evaluation of the electronic cigarette liquid according to the embodiment of the present invention.
TABLE 1
Figure BDA0002391927800000101
In summary, the smokeless electronic cigarette liquid prepared in the first to fifth embodiments of the present invention utilizes the good solubility of propylene glycol to the flavors and fragrances, and only generates a very small amount of smoke when the atomized vapor is inhaled by a human body. Achieving smokeless effect and keeping the fragrance intact. Therefore, the electronic cigarette liquid without smoke generates no smoke when in use, has thick and full product smoking experience and slightly sweet taste, can keep complete aroma, and has higher smoking comfort.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.

Claims (9)

1. The electronic cigarette liquid without smoke is characterized by comprising the following components in parts by weight:
essence and spice: 10-30 parts;
propylene glycol: 70-90 parts.
2. The smokeless electronic cigarette liquid of claim 1, comprising the following components by weight:
the essence and spice comprises the following components: 18 parts of a mixture;
the propylene glycol: and 82 parts.
3. The smokeless electronic cigarette liquid of claim 1, comprising the following components by weight:
the essence and spice comprises the following components: 15 parts of (1);
the propylene glycol: 80 parts of the raw materials.
4. The smokeless electronic cigarette liquid of claim 1, comprising the following components by weight:
the essence and spice comprises the following components: 12 parts of (1);
the propylene glycol: 85 parts of the raw materials.
5. The smokeless electronic cigarette liquid of claim 1, comprising the following components by weight:
the essence and spice comprises the following components: 23 parts;
the propylene glycol: 73 parts.
6. A preparation method of the electronic cigarette liquid without smoke is characterized by comprising the following steps:
s1, pouring 10-30 parts of essence and spice and 70-90 parts of propylene glycol into a container;
s2, stirring a mixture of 10-30 parts of essence and spice and 70-90 parts of propylene glycol in the container;
and S3, taking out and standing to obtain the product.
7. The method for preparing an smokeless electronic cigarette liquid according to claim 6, wherein in the step S2, the stirring process is performed by a stirrer.
8. The method for preparing the smokeless electronic cigarette liquid according to claim 6, wherein the step S1 specifically comprises: pouring 10 parts of the essence and the 90 parts of the propylene glycol into the container.
9. The method of preparing a smokeless electronic cigarette liquid of claim 8 wherein the container is a conventional stainless steel container.
CN202010117453.8A 2020-02-25 2020-02-25 Smoke-free electronic cigarette liquid and preparation method thereof Pending CN111202259A (en)

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Application publication date: 20200529