CN115281363B - Incense base module with soft and thorn-reducing effects, preparation method thereof and application thereof in cigarettes - Google Patents

Incense base module with soft and thorn-reducing effects, preparation method thereof and application thereof in cigarettes Download PDF

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Publication number
CN115281363B
CN115281363B CN202211022863.XA CN202211022863A CN115281363B CN 115281363 B CN115281363 B CN 115281363B CN 202211022863 A CN202211022863 A CN 202211022863A CN 115281363 B CN115281363 B CN 115281363B
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per mill
extract
base module
fragrance
tobacco
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CN115281363A (en
Inventor
张伟
王猛
廖头根
冒德寿
李先毅
李智宇
曾熠程
胡瑞林
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303Plant extracts other than tobacco

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a fragrance base module with soft and thorn-reducing effects, which has the following :Y comfort level =0.03*X1+0.01*X2+0.02*X3+0.01*X4+0.02*X5+0.02*X6+0.02*X7+0.01*X8+0.92, relations with the existing eight fragrance raw materials, wherein the value range of Y comfort level is 5.57-11.42. The invention also discloses a preparation method of the incense base module with soft and thorn-reducing effects and an application of the incense base module in tobacco leaf rolling groups.

Description

Incense base module with soft and thorn-reducing effects, preparation method thereof and application thereof in cigarettes
Technical Field
The invention belongs to the technical field of essence and spice, and particularly relates to a fragrance base module with a soft and thorn-reducing effect, a preparation method thereof and application thereof in cigarettes.
Background
The aroma of the cigarettes is core content of tobacco leaf quality, and aroma characteristics of the cigarettes directly influence smoking habits of smokers. The flavoring technology is a key link in the cigarette process, and is one of the decisive factors for improving the style of the product and the effective way for improving the fragrance quality and the smoking comfort of the cigarette. Generally, the flavor of cigarettes is derived from tobacco, but tobacco contains substances that generate unpleasant, bitter, and spicy flavors in addition to a pleasant aroma and a pleasant and pleasant taste. On the other hand, as the tobacco growth is influenced by environmental conditions, the content of aroma substances is in an unstable state, and the comprehensive application of the aroma mixing technology for maintaining brand cigarettes and developing new products can better set off and supplement the aroma of cigarettes, increase the smoke concentration, improve the taste, remove and cover unpleasant smell, reduce irritation and eliminate the influence of the quality fluctuation of tobacco on the aroma style of cigarettes so as to keep the quality of cigarettes relatively stable. In order to improve the pertinence and the popularization of the development of the functional fragrance base module, the sensory problems to be solved of the key brand cigarette products of the medium type cigarettes are researched, and the importance demonstration and the ranking are carried out according to 30 evaluation indexes of the style characteristics, the quality and the smoke characteristics of the cigarette products. Sensory indexes of more attention in the research and development process of products such as faint scent, baking scent, fruit scent, stimulus and the like are determined, so that the important commonality functional flavor base module of the tobacco is guided to be blended.
The variety of the prior art perfume is complex and various. When a certain characteristic essence and spice is configured, the selection of the perfume raw materials is difficult to determine; the proportioning and blending after the determination of the fragrance raw materials and the testing requires a great deal of work.
The invention is proposed for this purpose.
Disclosure of Invention
The invention aims to prepare the incense base module with soft and thorn-reducing effects according to the existing eight common incense raw materials, and has the advantages of high preparation speed and incense raw material consumption saving. The invention also provides a preparation method of the incense base module and application of the incense base module in cigarettes. The invention provides a soft and stab-reducing incense base module which aims at the characteristics of the existing cigarette that the style sense of the existing cigarette has urgent need of improving quality evaluation index, the fragrance of a part of Chinese cigarette leaves is enough, but the oral cavity is slightly more stimulated and the smoke is coarser, and the soft and stab-reducing incense base module is added with light sweet, herbal and spicy fragrance, so that the throat and oral cavity stimulation can be effectively reduced when the soft and stab-reducing incense base module is added in a small amount, the fineness and softness of the smoke are improved, the sweet return feeling is increased, and the interference on the smoke is small.
The technical scheme of the invention is as follows:
The first aspect of the invention discloses a fragrance base module with soft and thorn-reducing effect, which has the following :Y comfort level =0.03*X1+0.01*X2+0.02*X3+0.01*X4+0.02*X5+0.02*X6+0.02*X7+0.01*X8+0.92, relations with the existing eight fragrance raw materials, wherein the value range of Y comfort level is 5.57-11.42.
Preferably, the existing eight perfume raw materials and the weight ranges thereof are respectively: x 1: blackcurrant juice concentrate 90-125 per mill; x 2: 10 to 25 per mill of plum extract; x 3: 25-75 per mill of cranberry concentrated juice; x 4: 10 to 25 per mill of tobacco extract; x 5: 10 to 50 per mill of vanilla extract; x 6: 25-100 per mill of Roman chamomile extract; x 7: 25-50 per mill of peppermint extract; x 8: 5 to 75 per mill of dihydroactinolide.
Preferably, the existing eight perfume raw materials and the weight compositions thereof are respectively: x 1: blackcurrant juice concentrate 105%o; x 2: 15.5 per mill of plum extract; x 3: 71.6 per mill of cranberry concentrated juice; x 4: 20 per mill of tobacco extract; x 5: 40 per mill of vanilla extract; x 6: 71.7 per mill of Roman chamomile extract; x 7: 46.5% peppermint extract; x 8: the dihydro-actinide is 36 per mill.
Preferably, the other components of the perfume base module are solvents, and the solvents are propylene glycol and/or 50v/v% ethanol solution; the solvent is 100-300%o propylene glycol and 100-500%o 50v/v ethanol solution.
Preferably, the mass ratio of the total amount of perfume to the solvent is 1:3-5.
The invention discloses a preparation method of the incense base module, which comprises the following steps: mixing propylene glycol and 50v/v% ethanol, adding the eight kinds of perfume materials into the mixed solvent, mixing, and storing for 24-72 hr.
The third aspect of the invention discloses a flavoring application of the flavoring base module in a tobacco leaf rolling group.
Preferably, the fragrance base module is added according to the proportion of 0.04-0.20% of the mass of the tobacco shreds.
The invention optimizes the extraction and preparation process of the natural perfume raw materials based on the original cigarette perfume, so that the developed natural perfume has better product compatibility and quality stability to the perfume base module.
Blackcurrant juice concentrate: the sweet feeling of the smoke is increased, the coarse feeling of the smoke is improved to a certain extent, the faint green aroma and the faint costustoot of the tobacco are endowed, and the sweet feeling and the smoke fineness are improved.
Cranberry juice concentrate: the cigarette has fruit fragrance and sour fragrance, and is added with burnt fragrance and sweet fragrance, so that the light fruit fragrance and sour fragrance of the cigarette are endowed, the herbal fragrance of the cigarette is weakened, and the sour taste and the sweet taste are increased.
Roman chamomile extract: the Chinese herbal medicine is characterized by herbal medicine fragrance and flower fragrance, and fruit fragrance and sweet fragrance are added. Endowing tobacco with sweet and floral fragrance; the roughness of the smoke is reduced.
Peppermint extract: has fresh spearmint smell, slightly green grass flavor and bitter and pungent flavor, and mainly plays a role in reducing the hot and dry feel of smoke.
The application of the raw materials mainly plays roles of reducing stimulation and reducing rough feeling on the tobacco rolling group, and simultaneously effectively increases the tobacco fragrance and reduces the smoke heat dryness feeling. The fragrance base module shows light fruit fragrance, tobacco fragrance and herb fragrance, and has moderate sour fragrance and sweet fragrance. Can effectively reduce the stimulation of throat and oral cavity, promote the fine and soft degree of flue gas, increase the sweet taste simultaneously, and have less interference to the flue gas. The natural perfume raw materials in the formula of the invention are mainly developed by adopting a high static pressure extraction technology, so that the penetration of solvents can be accelerated, the dissolution of perfume components can be promoted, the perfume components of the extract are greatly improved, and the perfume intensity and the richness are obviously improved.
Compared with the prior art, the invention has the following beneficial effects:
1. The invention provides guidance for the use of the existing eight kinds of perfume raw materials and the weight range of the perfume raw materials in the perfume base module with soft and thorn-reducing effects by establishing the relation between the perfume base module and the existing eight kinds of perfume raw materials. The flavor base module has the advantages of high blending speed, consumption cost saving and accurate and reliable judging result by establishing the relation between the sensory scores and the flavor raw materials. The soft thorn-reducing fragrant base module formula is applied to tobacco shreds of a leaf group as flavoring essence, so that throat and oral cavity irritation can be effectively reduced, smoke fineness and softness are improved, hair permeability is enhanced, slightly dried fruit fragrance is increased, and the influence on the rhyme of the leaf group is small.
2. The eight kinds of perfume raw materials of the perfume base module with soft and thorn-reducing effects are common perfume raw materials, are easy to obtain, accord with international and national laws and regulations and relevant regulations, and have simple production process.
3. The incense base module with soft and thorn-reducing effects is added in the blank cigarette leaf group, has better universality and popularization in the tobacco industry, and compared with the existing commercial functional incense base module, the functional incense base module researched and produced by the invention is prepared based on monomer incense raw materials, and has obvious advantages in cost aspect.
Detailed Description
The invention will be further illustrated with reference to specific examples. For convenience of explanation, the sources of the raw materials used in the following examples of the present invention are as follows, respectively, but are not intended to limit the scope of the present invention. Other reagents, materials, methods and apparatus employed in the present invention are those conventionally used in the art unless otherwise specified.
Example 1
The embodiment provides a fragrance base module formula with soft and stab-reducing effects, which comprises the following components in percentage by mass: 95 per mill of blackcurrant juice concentrate, 15 per mill of plum extract, 25 per mill of cranberry juice concentrate, 10 per mill of tobacco extract, 20 per mill of vanilla extract, 25 per mill of chamomile extract, 25 per mill of peppermint extract, 10 per mill of dihydroactinolide, 275 per mill of propylene glycol and 500 per mill of 50v/v% ethanol, and the sensory score Y comfort level of the soft rosewood base module is 6.02.
The preparation method comprises the following steps: the method comprises the steps of adding propylene glycol and 50v/v% ethanol into a solvent, respectively dissolving the perfume raw materials with different solubilities, mixing the two systems, and preserving for 24 hours after mixing.
The application in cigarettes is as follows: the prepared soft rosewood heart wood incense base is used as feed liquid to be applied to the leaf group, and the feeding amount is added according to the proportion of 0.1% of the mass of the leaf group.
Example 2
The embodiment provides a fragrance base module formula with soft and stab-reducing effects, which comprises the following components in percentage by mass: 105 per mill of blackcurrant juice concentrate, 15.5 per mill of plum extract, 71.6 per mill of cranberry concentrated juice, 20 per mill of tobacco extract, 40 per mill of vanilla extract, 71.7 per mill of roman chamomile extract, 46.5 per mill of peppermint extract, 36 per mill of dihydroactinolide, 168.75 per mill of propylene glycol and 424.95 per mill of 50v/v% ethanol, and the sensory score Y comfort level of the soft rosewood fragrance module is 9.381.
The preparation method comprises the following steps: the method comprises the steps of adding propylene glycol and 50v/v% ethanol into a solvent, respectively dissolving the perfume raw materials with different solubilities, mixing the two systems, and preserving for 48 hours for use after mixing.
The application in cigarettes is as follows: the prepared soft rosewood heart wood incense base is used as feed liquid to be applied to the leaf group, and the feeding amount is added according to the proportion of 0.08% of the mass of the leaf group.
Example 3
The embodiment provides a fragrance base module formula with soft and stab-reducing effects, which comprises the following components in percentage by mass: 125 per mill of blackcurrant juice concentrate, 15 per mill of plum extract, 35 per mill of cranberry juice concentrate, 12.5 per mill of tobacco extract, 25 per mill of vanilla extract, 37.5 per mill of Luo Machun yellow chrysanthemum extract, 25 per mill of peppermint extract, 12.5 per mill of dihydroactinolide, 262.5 per mill of propylene glycol and 450 per mill of 50v/v% ethanol, and the sensory score Y comfort level of the soft rosewood base module is 7.347.
The preparation method comprises the following steps: the method comprises the steps of adding propylene glycol and 50v/v% ethanol into a solvent, respectively dissolving the perfume raw materials with different solubilities, mixing the two systems, and preserving for 48 hours for use after mixing.
The application in cigarettes is as follows: the prepared soft rosewood base is used as surface aroma to be applied to tobacco shreds of a leaf group, and the flavoring amount is added according to the proportion of 0.1% of the mass of the tobacco shreds.
Example 4 application evaluation
The application test was performed using the same leaf pack formulation as the cigarette flavor formulation in any of examples 1-3. For convenience of description, in this example, a blank cigarette with a certain brand without flavoring is used as an evaluation carrier, and sensory comparison is performed, and the comparison situation is shown in table 1. Evaluation of the vector: a certain brand of blank cigarettes provided by Yunnan medium cigarettes are used as an evaluation carrier.
The evaluation method comprises the following steps: aiming at the flavoring effect and style evaluation of the flavor-developing raw material cigarettes of the flavor base module, the evaluation control sample is the same blank cigarette. Fragrance module perfuming effect and style evaluation with soft thorn reducing effect: the method mainly comprises the fragrance characteristic, the taste characteristic and the fragrance style of the flavored cigarettes, wherein the fragrance and the taste are quantified in a manner of-5 to 5 minutes, the score unit is 1 minute, the fragrance style is quantified in a manner of 0 to 3 minutes, the score unit is 1 minute, and the evaluation result is the arithmetic average value (accurate to 0.1) of each panelist. The personnel involved in the evaluation needs to have the special fragrance smelling capability and the sensory cigarette smoking qualification evaluation, and the number of the participants is 5.
Table 1 table of evaluation of flavor and style of cigarettes before and after application of the flavor-based module with soft and stab-reducing effects according to the present invention
As can be seen from table 1, the flavoring formulation of the fragrant base module of example 2 has the best effect of improving the sensory of the cigarettes, and the proper addition amount in the leaf group is 0.08%, which indicates that when the soft thorn-reducing fragrant base module is designed, the score Y comfort level of sensory comfort is designed to be about 9.4, and the compatibility with the blank leaf group of the cigarettes is better. Effect on cigarette sense organ: can effectively reduce the stimulation of throat and oral cavity, promote the fine and soft degree of flue gas, increase the sweet taste simultaneously, and have less interference to the flue gas.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should make equivalent substitutions or modifications according to the technical scheme of the present invention and the inventive concept thereof, and should be covered by the scope of the present invention.

Claims (6)

1. The utility model provides a fragrant base module with soft effect of reducing thorns is used for the perfuming application in the tobacco winding group, characterized by that, the fragrant base module is following :Y comfort level =0.03*X1+0.01*X2+0.02*X3+0.01*X4+0.02*X5+0.02*X6+0.02*X7+0.01*X8+0.92, with the current eight kinds of fragrant raw materials wherein the value range of Y comfort level is 5.57 ~ 11.42; the existing eight perfume raw materials and the weight ranges thereof are respectively: x 1: blackcurrant juice concentrate 90-125 per mill; x 2: 10 to 25 per mill of plum extract; x 3: 25-75 per mill of cranberry concentrated juice; x 4: 10 to 25 per mill of tobacco extract; x 5: 10 to 50 per mill of vanilla extract; x 6: 25-100 per mill of Roman chamomile extract; x 7: 25-50 per mill of peppermint extract; x 8: 5 to 75 per mill of dihydroactinolide.
2. A perfuming application according to claim 1, characterized in that there are eight perfume raw materials and their weight compositions, respectively: x 1: blackcurrant juice concentrate 105%o; x 2: 15.5 per mill of plum extract; x 3: 71.6 per mill of cranberry concentrated juice; x 4: 20 per mill of tobacco extract; x 5: 40 per mill of vanilla extract; x 6: 71.7 per mill of Roman chamomile extract; x 7: 46.5% peppermint extract; x 8: the dihydro-actinide is 36 per mill.
3. A perfuming application according to claim 1, characterized in that the other ingredient of the fragrance module is a solvent, which is propylene glycol and/or a 50v/v% ethanol solution; the solvent is 100-300%o propylene glycol and 100-500%o 50v/v ethanol solution.
4. A perfuming use according to claim 3, characterized in that the mass ratio of the total amount of perfume to the solvent is 1:3 to 5.
5. A perfuming application according to claim 1, characterized in that the preparation method of the fragrance module comprises the steps of: mixing propylene glycol and 50v/v% ethanol, adding the eight kinds of perfume materials into the mixed solvent, mixing, and storing for 24-72 hr.
6. The use according to claim 1, wherein the fragrance module is added in a proportion of 0.04-0.20% of the mass of tobacco shreds.
CN202211022863.XA 2022-08-25 2022-08-25 Incense base module with soft and thorn-reducing effects, preparation method thereof and application thereof in cigarettes Active CN115281363B (en)

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CN116369581A (en) * 2023-03-30 2023-07-04 江苏中烟工业有限责任公司 Incense base module for showing sweet and spicy fragrance of fruits and application of incense base module in cigarettes with different circumferences

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