CN114391623A - Selenium-rich water functional beverage and preparation method thereof - Google Patents
Selenium-rich water functional beverage and preparation method thereof Download PDFInfo
- Publication number
- CN114391623A CN114391623A CN202111651996.9A CN202111651996A CN114391623A CN 114391623 A CN114391623 A CN 114391623A CN 202111651996 A CN202111651996 A CN 202111651996A CN 114391623 A CN114391623 A CN 114391623A
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- CN
- China
- Prior art keywords
- selenium
- water
- enriched
- temperature
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 136
- 229910052711 selenium Inorganic materials 0.000 title claims abstract description 99
- 239000011669 selenium Substances 0.000 title claims abstract description 99
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 title claims abstract description 98
- 238000002360 preparation method Methods 0.000 title claims abstract description 42
- 235000020510 functional beverage Nutrition 0.000 title claims abstract description 27
- 239000000419 plant extract Substances 0.000 claims abstract description 46
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 27
- 230000001954 sterilising effect Effects 0.000 claims abstract description 24
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 238000001914 filtration Methods 0.000 claims abstract description 20
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000001223 reverse osmosis Methods 0.000 claims abstract description 17
- 238000005374 membrane filtration Methods 0.000 claims abstract description 16
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 12
- 235000010378 sodium ascorbate Nutrition 0.000 claims abstract description 12
- 229960005055 sodium ascorbate Drugs 0.000 claims abstract description 12
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 claims abstract description 12
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 claims abstract description 12
- 241000282414 Homo sapiens Species 0.000 claims abstract description 11
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- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 9
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- 229920001525 carrageenan Polymers 0.000 claims description 40
- 241000208340 Araliaceae Species 0.000 claims description 38
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 38
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 38
- 235000008434 ginseng Nutrition 0.000 claims description 38
- 229940113118 carrageenan Drugs 0.000 claims description 37
- 239000000679 carrageenan Substances 0.000 claims description 37
- 239000000843 powder Substances 0.000 claims description 24
- 229920001542 oligosaccharide Polymers 0.000 claims description 23
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 18
- 238000001694 spray drying Methods 0.000 claims description 17
- 235000010418 carrageenan Nutrition 0.000 claims description 16
- 150000001875 compounds Chemical class 0.000 claims description 16
- 239000008187 granular material Substances 0.000 claims description 16
- 238000010298 pulverizing process Methods 0.000 claims description 15
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000001569 carbon dioxide Substances 0.000 claims description 11
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 11
- -1 carrageenan oligosaccharide Chemical class 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 11
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 11
- 239000002245 particle Substances 0.000 claims description 10
- 241000220317 Rosa Species 0.000 claims description 9
- 238000001471 micro-filtration Methods 0.000 claims description 8
- 238000000108 ultra-filtration Methods 0.000 claims description 8
- 241000222336 Ganoderma Species 0.000 claims description 7
- 241000408747 Lepomis gibbosus Species 0.000 claims description 7
- 235000007215 black sesame Nutrition 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 235000020236 pumpkin seed Nutrition 0.000 claims description 7
- 210000002421 cell wall Anatomy 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 238000004108 freeze drying Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 230000007935 neutral effect Effects 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 210000002784 stomach Anatomy 0.000 claims description 5
- 210000000936 intestine Anatomy 0.000 claims description 4
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- 241000196324 Embryophyta Species 0.000 abstract description 5
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- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 229940091258 selenium supplement Drugs 0.000 description 81
- 238000000605 extraction Methods 0.000 description 15
- 150000002482 oligosaccharides Chemical class 0.000 description 5
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 4
- 230000001276 controlling effect Effects 0.000 description 4
- 230000006837 decompression Effects 0.000 description 4
- 238000000502 dialysis Methods 0.000 description 4
- 238000007873 sieving Methods 0.000 description 4
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 4
- 230000036039 immunity Effects 0.000 description 3
- 235000002722 Dioscorea batatas Nutrition 0.000 description 2
- 235000006536 Dioscorea esculenta Nutrition 0.000 description 2
- 240000001811 Dioscorea oppositifolia Species 0.000 description 2
- 235000003416 Dioscorea oppositifolia Nutrition 0.000 description 2
- 244000197580 Poria cocos Species 0.000 description 2
- 235000008599 Poria cocos Nutrition 0.000 description 2
- 206010039921 Selenium deficiency Diseases 0.000 description 2
- 241000700605 Viruses Species 0.000 description 2
- 229930003779 Vitamin B12 Natural products 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 description 2
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical group [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 208000019423 liver disease Diseases 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229960003512 nicotinic acid Drugs 0.000 description 2
- 235000001968 nicotinic acid Nutrition 0.000 description 2
- 239000011664 nicotinic acid Substances 0.000 description 2
- 210000000056 organ Anatomy 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000008213 purified water Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229960001471 sodium selenite Drugs 0.000 description 2
- 235000015921 sodium selenite Nutrition 0.000 description 2
- 239000011781 sodium selenite Substances 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 235000019163 vitamin B12 Nutrition 0.000 description 2
- 239000011715 vitamin B12 Substances 0.000 description 2
- PMYDPQQPEAYXKD-UHFFFAOYSA-N 3-hydroxy-n-naphthalen-2-ylnaphthalene-2-carboxamide Chemical compound C1=CC=CC2=CC(NC(=O)C3=CC4=CC=CC=C4C=C3O)=CC=C21 PMYDPQQPEAYXKD-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 240000008397 Ganoderma lucidum Species 0.000 description 1
- 235000001637 Ganoderma lucidum Nutrition 0.000 description 1
- 206010019668 Hepatic fibrosis Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 108010009736 Protein Hydrolysates Proteins 0.000 description 1
- RJFAYQIBOAGBLC-BYPYZUCNSA-N Selenium-L-methionine Chemical compound C[Se]CC[C@H](N)C(O)=O RJFAYQIBOAGBLC-BYPYZUCNSA-N 0.000 description 1
- RJFAYQIBOAGBLC-UHFFFAOYSA-N Selenomethionine Natural products C[Se]CCC(N)C(O)=O RJFAYQIBOAGBLC-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 230000036983 biotransformation Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000004064 dysfunction Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 210000002216 heart Anatomy 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
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- 230000035772 mutation Effects 0.000 description 1
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- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
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- 229940082569 selenite Drugs 0.000 description 1
- MCAHWIHFGHIESP-UHFFFAOYSA-L selenite(2-) Chemical compound [O-][Se]([O-])=O MCAHWIHFGHIESP-UHFFFAOYSA-L 0.000 description 1
- 229960002718 selenomethionine Drugs 0.000 description 1
- 229960001881 sodium selenate Drugs 0.000 description 1
- 235000018716 sodium selenate Nutrition 0.000 description 1
- 239000011655 sodium selenate Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/50—Preservation of non-alcoholic beverages by irradiation or electric treatment without heating
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/256—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seaweeds, e.g. alginates, agar or carrageenan
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/14—Yeasts or derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C—CHEMISTRY; METALLURGY
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- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C02F1/32—Treatment of water, waste water, or sewage by irradiation with ultraviolet light
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/444—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by ultrafiltration or microfiltration
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/04—Disinfection
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Inorganic Chemistry (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Microbiology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a selenium-rich water functional drink and a preparation method thereof, wherein the selenium-rich water functional drink comprises the following steps: sequentially filtering the spring water by natural coconut shell activated carbon, micro-filtering and ultra-filtering to obtain primary filtered water; carrying out ultra-high temperature full sterilization on the primary filtered water to obtain high-temperature sterilized water; heating the high-temperature sterilized water again, adding the selenocarrageenan, the selenium-enriched yeast, the sodium ascorbate and the plant extract I, homogenizing by using a homogenizer, and then carrying out pneumatic stirring to obtain selenium-enriched water; and (3) carrying out reverse osmosis membrane filtration on the selenium-enriched water, further removing generated precipitates, and then carrying out ultraviolet disinfection to obtain the selenium-enriched water functional beverage. The selenium-enriched water functional beverage prepared by the invention contains plant source selenium, is more beneficial to absorption by human bodies, has the health care and health preserving functions, is suitable for long-term drinking, has wide consumption range and high economic benefit, and is suitable for large-scale production.
Description
Technical Field
The invention relates to the technical field of beverage processing, in particular to a selenium-rich water functional beverage and a preparation method thereof.
Background
Selenium is a trace element necessary for human bodies, and is also listed as one of 15 nutrients necessary for human bodies by the Chinese academy of nutrition. Selenium deficiency in the human body can cause dysfunction of some important organs and even cause the occurrence of a plurality of serious diseases. Research shows that the people with low selenium or selenium deficiency can prevent tumor, liver disease, etc. by supplementing selenium in proper amount, improve immunity, and maintain normal functions of heart, liver, lung, stomach and other important organs. Selenium exists in nature in the form of inorganic selenium and plant active selenium, wherein the inorganic selenium is sodium selenite and sodium selenate, the plant active selenium is formed by combining amino acid through biotransformation and generally exists in the form of selenomethionine, and the plant active selenium is a selenium source which is allowed to be used by human beings and animals.
The carrageenin is a sulfate polysaccharide, can be subjected to selenylation reaction with monomer selenium or sodium selenite under an acidic condition, and sulfate radicals in the carrageenin can be easily replaced by selenite to form the seleno-carrageenin. The selenocarrageenan has the following functions: enhancing immunity and reducing recurrence of liver diseases; improving oxidation resistance, and preventing hepatic fibrosis; blocking virus mutation and accelerating the recovery of a patient; detoxicate and remove harm, protect liver; detergents for human heavy metals; anticancer activity, etc.
Chinese patent CN111955627A discloses a nano-selenium micromolecule water functional beverage, which comprises main materials and additives, wherein the main materials comprise fish peptide enzymatic hydrolysate, rhizoma polygonati, Chinese yam and poria cocos, the additives comprise nicotinic acid and vitamin B12, and the preparation method comprises the following steps: preparing purified water into selenium-rich water by a selenium-rich mineralization device, adding an extracting solution, placing into a wall breaking machine for homogenate, mixing rhizoma polygonati, Chinese yam and poria cocos according to the proportion, adding micromolecule selenium-rich water with the weight 6 times of that of the raw materials, decocting, adding nicotinic acid and vitamin B12, adding purified water, filling and sealing at 100-120 ℃, sterilizing, inspecting by a lamp and packaging. However, the functional beverage prepared by the patent has poor health-care performance.
Disclosure of Invention
Aiming at the problems, the invention provides a selenium-enriched water functional drink and a preparation method thereof.
The technical scheme adopted by the invention for solving the problems is as follows: a preparation method of a selenium-rich water functional beverage comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out ultrahigh temperature sufficient sterilization on the initial filtered water at 110-125 ℃ to obtain high-temperature sterilized water; the ultra-high temperature sterilization can be used for more effective sterilization, and the stimulation of the raw water to the intestines and stomach of a human body can be reduced as the boiled water, so that the sterilization is safer and healthier;
step S30, heating the high-temperature sterilizing water to 92-95 ℃, adding seleno-carrageenan, selenium-enriched yeast, sodium ascorbate and plant extract I, homogenizing for 5-15 minutes by adopting a homogenizer, then pneumatically stirring for 20-35 minutes to obtain selenium-enriched water;
and step S40, carrying out reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S30, further removing generated precipitates, and then carrying out ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Further, in step S30, the selenium-enriched water includes the following raw materials: 100 parts of high-temperature sterilizing water, 0.08-0.15 part of selenocarrageenan, 0.05-0.12 part of selenium-enriched yeast, 0.01-0.02 part of sodium ascorbate and 0.02-0.12 part of plant extract I.
Further, in step S30, the preparation method of the plant extract I comprises: drying Cyrtymenia Sparsa and thallus Gracilariae, mixing at a weight ratio of 10: 4-8, pulverizing to 50-100 meshes, adding water, heating to 95 deg.C, maintaining for 10-20 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I.
Further, the preparation method of the ginseng granules comprises the following steps: the ginseng is crushed and sieved by a sieve of 40 meshes to 100 meshes to obtain ginseng fine powder, 20wt% to 30wt% of water is added into the ginseng fine powder, granulation is carried out, and low-temperature drying is carried out at 50 ℃ to 55 ℃ to obtain ginseng particles. The bitter rose is from the bitter rose in Yongdeng county of Gansu province, is a rare plateau selenium-rich rose variety in the world, has high selenium content and also has strong antioxidant function; ganoderma lucidum and Ginseng radix are traditional Chinese rare medicinal materials with effects of strengthening body resistance, consolidating constitution, nourishing, and strengthening body, and can improve immunity and resist virus invasion; the pumpkin seeds and the black sesame seeds are food with high selenium content and low in price, and are matched with the lucid ganoderma and the ginseng for use, so that the selenium-rich, antioxidant and antitumor effects are ensured, the production cost is regulated and controlled, and the applicability of the product is improved.
Further, in step S30, the selenocarrageenan is a commercially available selenocarrageenan having an organic selenium content of 20 μ g/mg to 50 μ g/mg.
Further, in step S30, the selenocarrageenan is a composite selenocarrageenan.
Further, the preparation method of the compound selenocarrageenan comprises the following steps: preparing 10 parts of seleno-carrageenan solution with the concentration of 1.2-1.8 wt%, adding 1.2-10 parts of sulfuric acid with the concentration of 5wt%, performing ultrasonic oscillation at 40-55 ℃ for 30 minutes, putting the mixture into constant-temperature water at 65 ℃, stirring and mixing for 3-3.5 hours, cooling to room temperature, adjusting the pH value to be neutral, performing reduced pressure concentration, dialyzing for 60 hours, and performing freeze drying to obtain seleno-carrageenan oligosaccharide; preparing seleno-carrageenan oligosaccharide into a solution with the concentration of 0.4-0.8 wt%, adding the plant extract II, stirring and mixing uniformly, homogenizing in a homogenizer, and then spray drying to obtain the compound seleno-carrageenan; the organic selenium content of the selenocarrageenan oligosaccharide is 25 mug/mg-100 mug/mg, and the average molecular weight is 1.4 kDa-1.6 kDa; the conditions of the spray drying include: the air inlet temperature is 210-280 ℃, and the air outlet temperature is 60-80 ℃.
Further, the preparation method of the plant extract II comprises the following steps: drying and crushing 10-20 parts of pumpkin seeds, 10-15 parts of ginseng granules, 3.5-8.5 parts of lucid ganoderma, 5-12 parts of black sesame and 1.5-5 parts of bitter rose, and then crushing the materials into 100-200 meshes in an ultramicro crusher to obtain mixed micro powder; performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract liquid, namely a plant extract II; the technological parameters of the carbon dioxide supercritical extraction comprise: the extraction temperature is controlled to be 40-43 ℃, the pressure of the extraction kettle is 35-37 MPa, and the extraction time is 2-3.5 hours.
Further, the weight ratio of the plant extract II to the carrageenan oligosaccharide is 0.2-3.5: 10.
further, in step S40, the reverse osmosis membrane has a filtration particle size of 0.5 to 1.5 nm.
The invention also aims to provide the selenium-enriched water functional drink prepared by the preparation method.
The invention has the advantages that:
(1) according to the selenium-rich water functional beverage prepared by the invention, mountain spring water is filtered and then sterilized at ultrahigh temperature, so that the selenium-rich water functional beverage can be used as boiled water, can reduce the stimulation of raw water to the intestines and stomach of a human body, and is safer and healthier;
(2) according to the selenium-enriched water functional beverage prepared by the invention, specific parts by weight of seleno-carrageenan, selenium-enriched yeast, sodium ascorbate and plant extract are added into boiled water, so that the content of selenium in a water source can be improved, and the plant extract with a health-care function is also added, so that the added value of a product can be further improved;
(3) the selenium-enriched water functional beverage prepared by the invention contains plant source selenium, is more beneficial to absorption by human bodies, has the health care and health preserving functions, is suitable for long-term drinking, has wide consumption range and high economic benefit, and is suitable for large-scale production.
In addition to the objects, features and advantages described above, other objects, features and advantages of the present invention are also provided. The present invention will be described in further detail below.
Detailed Description
The following detailed description of embodiments of the invention, but the invention can be practiced in many different ways, as defined and covered by the claims.
Example 1
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, performing 110 ℃ ultra-high temperature sufficient sterilization on the initial filtered water to obtain high-temperature sterilized water;
step S30, preparation of plant extract I: drying Cyrtymenia Sparsa and thallus Gracilariae, mixing at a weight ratio of 10:4, pulverizing to 50-100 mesh, adding water, heating to 95 deg.C, maintaining for 10 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I;
step S40, preparation of plant extract II: drying and pulverizing 10 parts of pumpkin seeds, 10 parts of ginseng granules, 3.5 parts of lucid ganoderma, 5 parts of black sesame and 1.5 parts of bitter rose, and then pulverizing the mixture in an ultramicro pulverizer to 100-200 meshes to obtain mixed micro powder; performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract liquid, namely a plant extract II; the technological parameters of the carbon dioxide supercritical extraction comprise: controlling the extraction temperature to be 40 ℃, the pressure of an extraction kettle to be 35MPa, and the extraction time to be 2 hours; the preparation method of the ginseng granules comprises the following steps: pulverizing Ginseng radix, sieving with 40-100 mesh sieve to obtain Ginseng radix fine powder, adding 20wt% water into Ginseng radix fine powder, granulating, and drying at 50 deg.C to obtain Ginseng radix granule;
step S50, preparing compound selenocarrageenan: preparing 10 parts of seleno-carrageenan solution with the concentration of 1.2wt%, adding 1.2 parts of sulfuric acid with the concentration of 5wt%, ultrasonically oscillating for 30 minutes at 40 ℃, then putting the solution into constant-temperature water with the temperature of 65 ℃, stirring and mixing for 3 hours, cooling to room temperature, adjusting the pH value to be neutral, carrying out dialysis for 60 hours after decompression concentration, and carrying out freeze drying to obtain seleno-carrageenan oligosaccharide; preparing 0.4wt% solution of selenized carrageenan oligosaccharide, adding the plant extract II obtained in the step S40, stirring and mixing uniformly, homogenizing in a homogenizer, and spray drying to obtain compound selenized carrageenan; the organic selenium content of the selenocarrageenan oligosaccharide is 25 mug/mg, and the average molecular weight is 1.4 kDa; the conditions of the spray drying include: the air inlet temperature is 210 ℃, and the air outlet temperature is 60 ℃; the adding weight ratio of the plant extract II to the carrageenan oligosaccharide is 0.2: 10;
step S60, heating 100 parts of high-temperature sterilized water to 92 ℃ again, adding 0.08 part of compound seleno-carrageenan, 0.05 part of selenium-enriched yeast, 0.01 part of sodium ascorbate and 0.02 part of the plant extract I obtained in the step S30, homogenizing for 5 minutes by using a homogenizer, and then carrying out pneumatic stirring for 20 minutes to obtain selenium-enriched water;
and step S70, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S60, wherein the particle size of the reverse osmosis membrane filtration is 0.5nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Example 2
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out ultrahigh-temperature sufficient sterilization on the initial filtered water at 125 ℃ to obtain high-temperature sterilized water; the ultra-high temperature sterilization can be used for more effective sterilization, and the stimulation of the raw water to the intestines and stomach of a human body can be reduced as the boiled water, so that the sterilization is safer and healthier;
step S30, preparation of plant extract I: drying Cyrtymenia Sparsa and thallus Gracilariae, mixing at a weight ratio of 10:8, pulverizing to 50-100 mesh, adding water, heating to 95 deg.C, maintaining for 20 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I;
step S40, preparation of plant extract II: drying and pulverizing 20 parts of pumpkin seeds, 15 parts of ginseng granules, 8.5 parts of lucid ganoderma, 12 parts of black sesame and 5 parts of bitter rose, and then pulverizing the mixture in an ultramicro pulverizer to 100-200 meshes to obtain mixed micro powder; performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract liquid, namely a plant extract II; the technological parameters of the carbon dioxide supercritical extraction comprise: controlling the extraction temperature to be 43 ℃, the pressure of an extraction kettle to be 37MPa, and the extraction time to be 3.5 hours; the preparation method of the ginseng granules comprises the following steps: pulverizing Ginseng radix, sieving with 40-100 mesh sieve to obtain Ginseng radix fine powder, adding 30wt% water into Ginseng radix fine powder, granulating, and drying at 55 deg.C to obtain Ginseng radix granule;
step S50, preparing compound selenocarrageenan: preparing 10 parts of seleno-carrageenan into 10 parts of seleno-carrageenan solution with the concentration of 1.8wt%, adding 10 parts of sulfuric acid with the concentration of 5wt%, ultrasonically oscillating for 30 minutes at 55 ℃, putting the seleno-carrageenan solution into constant-temperature water with the temperature of 65 ℃, stirring and mixing for 3.5 hours, cooling to room temperature, adjusting the pH value to be neutral, carrying out dialysis for 60 hours after decompression concentration, and carrying out freeze drying to obtain seleno-carrageenan oligosaccharide; preparing 0.8wt% solution of selenized carrageenan oligosaccharide, adding the plant extract II obtained in the step S40, stirring and mixing uniformly, homogenizing in a homogenizer, and spray drying to obtain compound selenized carrageenan; the organic selenium content of the selenocarrageenan oligosaccharide is 100 mug/mg, and the average molecular weight is 1.6 kDa; the conditions of the spray drying include: the air inlet temperature is 280 ℃, and the air outlet temperature is 80 ℃; the adding weight ratio of the plant extract to the carrageenan oligosaccharide is 3.5: 10;
step S60, heating 100 parts of high-temperature sterilizing water to 95 ℃ again, adding 0.15 part of compound seleno-carrageenan, 0.12 part of selenium-enriched yeast, 0.02 part of sodium ascorbate and 0.12 part of plant extract I, homogenizing for 5 minutes by a homogenizer, and then pneumatically stirring for 20 minutes to obtain selenium-enriched water;
and step S70, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S60, wherein the particle size of the reverse osmosis membrane filtration is 1.5nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Example 3
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out 120 ℃ ultra-high temperature full sterilization on the initial filtered water to obtain high-temperature sterilized water;
step S30, preparation of the plant extract I: drying Cyrtymenia Sparsa and thallus Gracilariae for 50-20 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I;
step S40, preparation of the plant extract II: drying and pulverizing 15 parts of pumpkin seeds, 12 parts of ginseng granules, 6.0 parts of lucid ganoderma, 8.5 parts of black sesame and 3.2 parts of bitter rose, and then putting the mixture into an ultramicro pulverizer to pulverize to 100-200 meshes to obtain mixed micro powder; performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract liquid, namely a plant extract II; the technological parameters of the carbon dioxide supercritical extraction comprise: controlling the extraction temperature to be 42 ℃, the pressure of an extraction kettle to be 36MPa, and the extraction time to be 2.5 hours; the preparation method of the ginseng granules comprises the following steps: pulverizing Ginseng radix, sieving with 40-100 mesh sieve to obtain Ginseng radix fine powder, adding 25wt% water into Ginseng radix fine powder, granulating, and drying at 52 deg.C to obtain Ginseng radix granule;
step S50, preparing compound selenocarrageenan: preparing 10 parts of seleno-carrageenan solution with the concentration of 1.5wt%, adding 6 parts of sulfuric acid with the concentration of 5wt%, ultrasonically oscillating for 30 minutes at 48 ℃, putting into constant-temperature water with the temperature of 65 ℃, stirring and mixing for 3 hours, cooling to room temperature, adjusting the pH value to be neutral, carrying out dialysis for 60 hours after decompression concentration, and carrying out freeze drying to obtain seleno-carrageenan oligosaccharide; preparing 0.6wt% solution of selenized carrageenan oligosaccharide, adding the plant extract II obtained in the step S40, stirring and mixing uniformly, homogenizing in a homogenizer, and spray drying to obtain compound selenized carrageenan; the organic selenium content of the selenocarrageenan oligosaccharide is 60 mug/mg, and the average molecular weight is 1.5 kDa; the conditions of the spray drying include: the air inlet temperature is 250 ℃, and the air outlet temperature is 70 ℃; the adding weight ratio of the plant extract II to the carrageenan oligosaccharide is 2.0: 10;
step S60, heating the high-temperature sterilized water to 93 ℃ again, adding 0.12 part of compound selenocarrageenan, 0.08 part of selenium-enriched yeast, 0.015 part of sodium ascorbate and 0.7 part of the plant extract I obtained in the step S30, homogenizing for 5 minutes by using a homogenizer, and then carrying out pneumatic stirring for 20 minutes to obtain selenium-enriched water;
and step S70, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S60, wherein the particle size of the reverse osmosis membrane filtration is 1.0nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Example 4
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out 115 ℃ ultra-high temperature full sterilization on the initial filtered water to obtain high-temperature sterilized water;
step S30, heating the high-temperature sterilized water to 94 ℃ again, adding 0.12 part of selenocarrageenan, 0.1 part of selenium-enriched yeast, 0.012 part of sodium ascorbate and 0.04 part of plant extract I, homogenizing for 5 minutes by adopting a homogenizer, then carrying out pneumatic stirring, and stirring for 20 minutes to obtain selenium-enriched water; the preparation method of the plant extract I comprises the following steps: drying Cyrtymenia Sparsa and thallus Gracilariae, mixing at a weight ratio of 10:5, pulverizing to 50-100 mesh, adding water, heating to 95 deg.C, maintaining for 12 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I; the selenocarrageenan is commercial selenocarrageenan with the organic selenium content of 30 mug/mg;
and step S40, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S30, wherein the particle size of the reverse osmosis membrane filtration is 1.0nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Example 5
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out 120 ℃ ultra-high temperature full sterilization on the initial filtered water to obtain high-temperature sterilized water;
step S30, heating the high-temperature sterilized water to 93 ℃ again, adding 0.12 part of selenocarrageenan, 0.10 part of selenium-enriched yeast and 0.02 part of sodium ascorbate, homogenizing for 5 minutes by adopting a homogenizer, then carrying out pneumatic stirring, and stirring for 20 minutes to obtain selenium-enriched water; the selenocarrageenan is commercial selenocarrageenan with the organic selenium content of 30 mug/mg;
and step S40, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S30, wherein the particle size of the reverse osmosis membrane filtration is 1.0nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
Example 6
Selenium-rich water functional beverage and preparation method thereof
The preparation method of the selenium-enriched water functional drink comprises the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out ultrahigh-temperature sufficient sterilization on the initial filtered water at 125 ℃ to obtain high-temperature sterilized water;
step S30, preparation of plant extract II: drying and pulverizing 15 parts of pumpkin seeds, 12 parts of ginseng granules, 6.0 parts of lucid ganoderma, 7.5 parts of black sesame and 3.2 parts of bitter rose, and then putting the mixture into an ultramicro pulverizer to pulverize to 100-200 meshes to obtain mixed micro powder; performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract liquid, namely a plant extract II; the technological parameters of the carbon dioxide supercritical extraction comprise: controlling the extraction temperature to be 42 ℃, the pressure of an extraction kettle to be 36MPa, and the extraction time to be 2.5 hours; the preparation method of the ginseng granules comprises the following steps: pulverizing Ginseng radix, sieving with 40-100 mesh sieve to obtain Ginseng radix fine powder, adding 25wt% water into Ginseng radix fine powder, granulating, and drying at 52 deg.C to obtain Ginseng radix granule;
step S40, preparing compound selenocarrageenan: preparing 10 parts of seleno-carrageenan solution with the concentration of 1.5wt%, adding 6 parts of sulfuric acid with the concentration of 5wt%, ultrasonically oscillating for 30 minutes at 48 ℃, putting into constant-temperature water with the temperature of 65 ℃, stirring and mixing for 3 hours, cooling to room temperature, adjusting the pH value to be neutral, carrying out dialysis for 60 hours after decompression concentration, and carrying out freeze drying to obtain seleno-carrageenan oligosaccharide; preparing 0.6wt% solution of selenized carrageenan oligosaccharide, adding the plant extract II obtained in the step S30, stirring and mixing uniformly, homogenizing in a homogenizer, and spray drying to obtain compound selenized carrageenan; the organic selenium content of the selenocarrageenan oligosaccharide is 60 mug/mg, and the average molecular weight is 1.5 kDa; the conditions of the spray drying include: the air inlet temperature is 250 ℃, and the air outlet temperature is 70 ℃; the adding weight ratio of the plant extract II to the carrageenan oligosaccharide is 2.0: 10;
step S50, heating the high-temperature sterilized water to 93 ℃ again, adding 0.10 part of the compound selenocarrageenan obtained in the step S40, 0.10 part of the selenium-enriched yeast and 0.01 part of sodium ascorbate, homogenizing for 5 minutes by using a homogenizer, then carrying out pneumatic stirring, and stirring for 20 minutes to obtain selenium-enriched water;
and step S60, performing reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S50, wherein the particle size of the reverse osmosis membrane filtration is 1.0nm, further removing generated precipitates, and performing ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
The above is only a preferred embodiment of the present invention, and is not intended to limit the present invention, and various modifications and changes will occur to those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. A preparation method of a selenium-enriched water functional drink is characterized by comprising the following steps:
step S10, natural coconut shell activated carbon filtration, microfiltration and ultrafiltration are sequentially carried out on the spring water to obtain primary filtration water;
step S20, carrying out ultrahigh temperature sufficient sterilization on the initial filtered water at 110-125 ℃ to obtain high-temperature sterilized water; the ultra-high temperature sterilization can be used for more effective sterilization, and the stimulation of the raw water to the intestines and stomach of a human body can be reduced as the boiled water, so that the sterilization is safer and healthier;
step S30, heating the high-temperature sterilizing water to 92-95 ℃, adding seleno-carrageenan, selenium-enriched yeast, sodium ascorbate and plant extract I, homogenizing for 5-15 minutes by adopting a homogenizer, then pneumatically stirring for 20-35 minutes to obtain selenium-enriched water;
and step S40, carrying out reverse osmosis membrane filtration on the selenium-enriched water obtained in the step S30, further removing generated precipitates, and then carrying out ultraviolet disinfection to obtain the selenium-enriched water functional beverage.
2. The method as claimed in claim 1, wherein in step S30, the selenium-enriched water comprises: 100 parts of high-temperature sterilizing water, 0.08-0.15 part of selenocarrageenan, 0.05-0.12 part of selenium-enriched yeast, 0.01-0.02 part of sodium ascorbate and 0.02-0.12 part of plant extract I.
3. The method according to claim 1, wherein the method for preparing the plant extract I in step S30 comprises: drying Cyrtymenia Sparsa and thallus Gracilariae, mixing at a weight ratio of 10: 4-8, pulverizing to 50-100 meshes, adding water, heating to 95 deg.C, maintaining for 10-20 min, breaking cell wall, and separating solid and liquid to obtain filtrate; removing impurities and color from the filtrate, distilling under reduced pressure, concentrating, and spray drying to obtain plant extract I.
4. The preparation method according to claim 1, wherein in step S30, the selenocarrageenan is a commercially available selenocarrageenan having an organic selenium content of 20 μ g/mg to 50 μ g/mg.
5. The preparation method according to claim 1, wherein in step S30, the selenocarrageenan is a composite selenocarrageenan; the preparation method of the compound selenocarrageenan comprises the following steps: preparing 10 parts of seleno-carrageenan solution with the concentration of 1.2-1.8 wt%, adding 1.2-10 parts of sulfuric acid with the concentration of 5wt%, performing ultrasonic oscillation at 40-55 ℃ for 30 minutes, putting the mixture into constant-temperature water at 65 ℃, stirring and mixing for 3-3.5 hours, cooling to room temperature, adjusting the pH value to be neutral, performing reduced pressure concentration, dialyzing for 60 hours, and performing freeze drying to obtain seleno-carrageenan oligosaccharide; preparing the seleno-carrageenan oligosaccharide into a solution with the concentration of 0.4-0.8 wt%, adding the plant extract II, stirring and mixing uniformly, homogenizing in a homogenizer, and then spray drying to obtain the compound seleno-carrageenan.
6. The method according to claim 5, wherein the extract II is prepared by a method comprising: drying and crushing 10-20 parts of pumpkin seeds, 10-15 parts of ginseng granules, 3.5-8.5 parts of lucid ganoderma, 5-12 parts of black sesame and 1.5-5 parts of bitter rose, and then crushing the materials into 100-200 meshes in an ultramicro crusher to obtain mixed micro powder; and performing carbon dioxide supercritical extraction on the mixed micro powder to obtain an extract, namely the plant extract II.
7. The method of claim 6, wherein the ginseng granules are prepared by a method comprising: the ginseng is crushed and sieved by a sieve of 40 meshes to 100 meshes to obtain ginseng fine powder, 20wt% to 30wt% of water is added into the ginseng fine powder, granulation is carried out, and low-temperature drying is carried out at 50 ℃ to 55 ℃ to obtain ginseng particles.
8. The preparation method according to claim 5, wherein the weight ratio of the plant extract II to the carrageenan oligosaccharide is 0.2-3.5: 10.
9. the method according to claim 1, wherein in step S40, the reverse osmosis membrane filtration has a particle size of 0.5nm to 1.5 nm.
10. A selenium-enriched water functional beverage prepared by the preparation method according to any one of claims 1 to 9.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116210832A (en) * | 2023-03-15 | 2023-06-06 | 汉德康药业(临沂)股份有限公司 | Preparation method of beverage plant selenium compound cell sap |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108033615A (en) * | 2017-11-24 | 2018-05-15 | 傅远顺 | A kind of formula and manufacture method of artificial selenium-rich drinking water |
| CN108276603A (en) * | 2018-01-26 | 2018-07-13 | 青岛鑫康达生物科技有限公司 | A kind of preparation method of high Se content small molecule selenide of carragheen |
| CN110357978A (en) * | 2018-04-10 | 2019-10-22 | 青岛鹏洋生物工程有限公司 | A kind of preparation method of selenide of carragheen |
| CN111955627A (en) * | 2020-08-27 | 2020-11-20 | 山东尧旺健康科技有限公司 | Nano-selenium micromolecular water functional beverage and preparation method thereof |
| CN112220046A (en) * | 2020-10-28 | 2021-01-15 | 青岛鹏洋生物工程有限公司 | Compound nutrition enhancer containing seleno-carrageenan and preparation method thereof |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108033615A (en) * | 2017-11-24 | 2018-05-15 | 傅远顺 | A kind of formula and manufacture method of artificial selenium-rich drinking water |
| CN108276603A (en) * | 2018-01-26 | 2018-07-13 | 青岛鑫康达生物科技有限公司 | A kind of preparation method of high Se content small molecule selenide of carragheen |
| CN110357978A (en) * | 2018-04-10 | 2019-10-22 | 青岛鹏洋生物工程有限公司 | A kind of preparation method of selenide of carragheen |
| CN111955627A (en) * | 2020-08-27 | 2020-11-20 | 山东尧旺健康科技有限公司 | Nano-selenium micromolecular water functional beverage and preparation method thereof |
| CN112220046A (en) * | 2020-10-28 | 2021-01-15 | 青岛鹏洋生物工程有限公司 | Compound nutrition enhancer containing seleno-carrageenan and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116210832A (en) * | 2023-03-15 | 2023-06-06 | 汉德康药业(临沂)股份有限公司 | Preparation method of beverage plant selenium compound cell sap |
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Application publication date: 20220426 |