CN109645393A - Composite extract and application - Google Patents
Composite extract and application Download PDFInfo
- Publication number
- CN109645393A CN109645393A CN201811567735.7A CN201811567735A CN109645393A CN 109645393 A CN109645393 A CN 109645393A CN 201811567735 A CN201811567735 A CN 201811567735A CN 109645393 A CN109645393 A CN 109645393A
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- China
- Prior art keywords
- powder
- ginger
- extraction
- parts
- health product
- Prior art date
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/01—Instant products; Powders; Flakes; Granules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Molecular Biology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of composite extract and applications.The present invention by by raw material pulverize and sieve processing, supercritical carbon dioxide extracting obtain ginger, chrysanthemum, ampelopsis grossdentata leaf and fructus lycii, red date extract mixed liquor after add brown sugar, xylo-oligosaccharide powder mixing, spray-dried again health product be prepared.The present invention passes through optimization ginger extraction process and preparation step, the technological parameter that emphasis passes through each interrelated integration during setting supercritical carbon dioxide extracting, a variety of extracts are extracted simultaneously, the pure natural feature of ginger, chrysanthemum, ampelopsis grossdentata leaf, fructus lycii, jujube has been fully retained, high concentration health product are prepared, and this method recovery rate is high, improves utilization rate of raw materials, reduces production cost.
Description
Technical field
The present invention relates to extraction process technology fields, more particularly, to a kind of composite extract and application.
Background technique
Supercritical fluid extraction (supercritical fluidextraction, abbreviation SFE), which refers to, utilizes shooting flow
Body have very high solvability to solute in the supercritical state and under non-supercritical state very to the solvability of solute
Low characteristic, extracts special component from liquid or solid, to reach extraction and isolated process.
Supercritical CO2The process flow of extraction is set according to different extracted objects and to complete different tasks
It sets.It will receive the influence of several factors in the actual mechanical process of supercritical carbon dioxide extracting, these influences mainly have
Extracting pressure, extraction temperature, raw material granularity, CO2Flow etc..
Certainly, supercritical CO2Abstraction technique is also not a kind of omnipotent abstraction technique, the same with other any technologies,
There is its applicable range.We need to be confirmed whether the size of the solvability of different material according to it to be suitble to use.
The rhythm of the modern life is getting faster, the continuous quickening of rhythm of life, keeps requirement of the modern to health also more next
It is higher, follow the fashion, it is health, convenient, and on the basis of rich in taste, start the simplicity for pursuing life and total system
Health care.
Correspondingly, in response to the market demand, need to produce that holistic health effect is obvious and to take into account rich in taste, no impurity taste etc. comprehensive
It closes quality and stablizes secure product to meet consumer's needs, the production is inevitably thus produced using plurality of raw materials
Product, and just produce and actually analyze, plurality of raw materials extract its extraction efficiency, expend the time, technique it is simple, active material
The high standards such as content, diversification requirement acid test also is proposed to production.It is rarely seen at present to be directed to jujube, fructus lycii, ginger
The correlative study and technical report of equal compound collectings.
Summary of the invention
The technical problem to be solved by the present invention is to for ginger jujube tea nutrient composition content is few, preparation process is multiple in the prior art
The miscellaneous, technical deficiencies such as extraction efficiency is low, provide a kind of composite extract.
Another technical problem to be solved by the present invention is that providing the application of the composite extract.
The purpose of the present invention is achieved by the following technical programs:
A kind of composite extract is provided, is made using red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder
For raw material, gained extract liquor, the extraction use and are repeated 3 times extraction after supercritical carbon dioxide extracting after raw material is mixed,
First time extracting pressure is 25~30MPa, and extraction temperature is 45~55 DEG C；Second of extracting pressure is 15~20MPa, extraction temperature
Degree is 30~40 DEG C；Third time extracting pressure is 8~15MPa, and extraction temperature is 25~30 DEG C；
The red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder weight ratio are as follows: red date powder 3~10
Part, 3~8 parts of wolfberry fruit powder, 0.4~8 part of ampelopsis grossdentata leaf powder, 2~10 parts of chrysanthemum powder, 2~14 parts of ginger powder.
Gingerol in ginger powder has the function of that invigorating the spleen warm stomach, sweating cold dispelling, resolving sputum removing toxic substances, sunstroke prevention are antipyretic, preventing cold,
Also have anti-oxidant, anti-senescence function is three times of vitamin e, can improve health, promote longevity and other effects.In addition, gingerol
In the ingredients such as salad oil, zingiberone, play the role of antiemetic, mitigate nausea, antiphlogistic antibacterial.Ampelopsis grossdentata leaf powder has heat-clearing benefit
The effect of wet, calming the liver is depressured, promoting blood circulation and removing obstruction in channels, there is nutrition abundant body immunity can be improved, contained flavones can exclude people
Body nocuousness acid eliminate with ketoboidies, remove blood in blood dirt, adjust blood lipid, reduce blood pressure, softening vessel effect it is significant, secondly can also
Improve sleep, anti-aging, remove free radical, protection liver, protection eye eyesight etc..Fructus lycii contains polysaccharides, glycine betaine, atropic
Product, hyoscyamine；Separately containing zeaxanthine, wintercherry red pigment, kryptoxanthin, Scopoletin, carrotene, riboflavin, niacin, dimension life
Element.Adjustable body's immunity can effectively inhibit tumour growth and cell mutation, have anti-aging, anti-fatty liver, adjusting
Blood lipid and blood glucose, the effect for promoting hematopoiesis function etc..Jujube contains protein, carbohydrate, organic acid, vitamin A, vitamin
C, the nutrition abundant such as lot of trace calcium and amino acid.Tonifying middle-Jiao and Qi, nourishing blood and tranquilization.For spleen eating less, it is out of strength just
It is half congealed, hysteria of womam.It can prevent transfusion reaction, reduce serum glutamic pyruvic transminase, antitumor, anti-oxidant, blood pressure lowering, norcholesterol,
Liver protecting improves immunity, prevents and treats cerebral insufficiency, antiallergy, and anti-angiocardiopathy prevents and treats osteoporosis and anaemia.Cause
The cooperation of both this jujube and fructus lycii, can play the effect of QI invigorating mends replenishing the vital essence and the blood, especially because the women of menorrhagia, often
Drinking date-wolfberry fruit water and helping improves pale complexion and the ice-cold situation of trick.The present invention is with the jujube, fructus lycii, Xian Chi snake Portugal
Grape leaf, chrysanthemum and Jiang Peiwu,
For red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder multiple material mixture, by setting
Multitple extraction is set, the pressure limit of every level-one is designed, matches optimal extraction temperature, while will be each effective in all raw materials
Ingredient extracts, and balances the active principle extracted in raw material, such as ginger oil, gingerol, dihydromyricetin, vitamin battalion
Support substance.Final test effect and testing result summarize it can be appreciated that the present invention targetedly extraction process obtains preferable technology
Effect.
Preferably, the weight ratio of the red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder are as follows: jujube
4 parts of powder, 3.2 parts of wolfberry fruit powder, 2 parts of ampelopsis grossdentata leaf powder, 4 parts of chrysanthemum powder, 5.6 parts of ginger powder.
Preferably, 3 extractions, each 35~60min of extraction time, carbon dioxide flow are 30~40L/h.
The red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder are sieved respectively, and sieve is 80~90 mesh.
Material particular diameter is small can be increased and CO2Contact area, improve extraction yield, but partial size is too small, is easy to block pipeline and filter opening,
Make the CO by extraction column2It reduces to reducing extraction yield, and partial size is meticulous is easily brought into knockout drum, to mask work band
Come difficult.Therefore the partial size of 80 mesh or so is the most suitable
Preferably, the ampelopsis grossdentata leaf originates from the western Hunan, and the chrysanthemum powder is FLOS CHRYSANTHEMI ALBA from Haizhou of China powder, and the ginger powder is north latitude 27
The small yellow ginger that degree is nearby produced.
The present invention provides the application of the composite extract, is applied to, preparation health product compatible with sugar.
Health product provided by the invention include following component: 7.4~43 parts of composite extract, sugared 50~63 parts, oligomeric wood
1~5 part of Icing Sugar.
Preferably, 15~35 parts of composite extract, 55~60 parts, 1.5~4 parts of xylo-oligosaccharide powder of sugar.
Preferably, the sugar is brown sugar or brown sugar.
Present invention simultaneously provides the preparation methods of the health product, specifically includes the following steps:
S1. brown sugar or brown sugar, ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, xylo-oligosaccharide powder, aobvious tooth feedstock processing: are weighed
Porcelain ampelopsis leaf powder, crushes respectively, sieving；
S2. it extracts: leading to after ginger powder obtained by step S1, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are mixed
Enter in supercritical carbon dioxide extractor, entrainer is added, extracting pressure and extraction temperature are set, extracts to get extract liquor；
S3. it mixing: by brown sugar powder obtained by step S1 or brown sugar heating and melting, is added in extract liquor obtained by step S2, adds
Enter xylo-oligosaccharide powder high-speed stirred, obtains mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 is spray-dried, sterilizing, until moisture content is qualified, sieving, i.e.,
?.
Further, sieving sieve described in step S1 is 80~90 mesh.
Further, entrainer described in step S2 is one of water, ethyl alcohol, ethyl alcohol and mixture of water, the folder
Dosage with agent is according to the poidometer of ginger powder, about 7:1 or so.Brown sugar and extract liquor weight ratio are 1.15~7:1 in step S3.
Brown sugar adds in extract liquor the agglomeration and precipitating that can reduce brown sugar through high temperature melting, promotes mixing uniform, improves health product
Stability.
Preferably, brown sugar and extract liquor weight ratio are 3.5:1 in step S3.
The extraction is 25~30MPa using extraction, first time extracting pressure is repeated 3 times, and extraction temperature is 45~55 DEG C；
Second of extracting pressure is 15~20MPa, and extraction temperature is 30~40 DEG C；Third time extracting pressure is 8~15MPa, extraction temperature
Degree is 25~30 DEG C；
Further, 90~120 DEG C of heating temperature described in step S3, high-speed stirred speed are 1500~1800r/min,
Mixing time is 15~30min.
Preferably, 110 DEG C of heating temperature described in step S3, high-speed stirred speed are 1600r/min, and mixing time is
20min。
Further, described in step S4 spray drying rotating speed of shower nozzle be 350~380r/min, inlet air temperature be 100~
120 DEG C, leaving air temp is 60~75 DEG C, 30~40r/min of feed flow rate, and blower frequency is 20~50Hz.
Preferably, spray drying rotating speed of shower nozzle described in step S4 is 360r/min, and inlet air temperature is 110 DEG C, out wind-warm syndrome
Degree is 68 DEG C, feed flow rate 34r/min, and blower frequency is 40Hz.
Further, sterilising temp described in step S4 is 90~100 DEG C, 10~30min of sterilization time, moisture content≤
8% is qualification,
Preferably, sterilising temp described in step S4 is 96 DEG C, sterilization time 20min, and moisture content≤8% is qualification, water
It is point excessively high easily to form moisture film in surface of material, while easily material being made to agglomerate, solubility is influenced, leads to precipitating generation, influences mouthfeel,
Under the conditions of present invention process, moisture content≤8% is determined.
Preferably, sieving sieve described in step S4 is 30~50 mesh.Further preferably, sieving sieve described in step S4 is 40
Mesh.
The invention has the following advantages:
The present invention is managed with jujube, fructus lycii, ampelopsis grossdentata leaf, chrysanthemum and Jiang Peiwu, inventive formulation by Traditional Chinese Medicine
By auxiliary modern biotechnology preparation, mutual organic assembling, head takes ginger powder to be equipped with date-wolfberry fruit blood-enrich, while Xian Chi snake Portugal is added
Grape leaf plays the role of antibacterial anti-inflammatory, improves immunity, for female menstrual period special circumstances, adds ginger clearing and activating the channels and collaterals, promoting blood circulationization
The stasis of blood, the function in warm palace of warding off the cold, it is ensured that female menstrual period qi and blood is unobstructed, alleviates dysmenorrhea.Again plus brown sugar is with replenishing and activating blood, tonifying middle-Jiao and Qi,
Ensure that hemapodium gas is prosperous, strong body.Because of the warm attribute of ginger, excessive eat can cause to get angry, and addition chrysanthemum softening neutralizes this stock
It is hot, while ampelopsis grossdentata leaf assists cooperation, reaches yin-yang coordination, guarantees body health.Another addition modern biotechnology preparation is low
Xylan adjusts intestinal flora balance, so that the digestion and absorption function of enteron aisle is in normal condition, to guarantee the suction of nutriment
It receives, provides nutrition abundant for body.
On this basis, the present invention is directed to red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and a variety of materials of ginger powder
The mixture of material designs the pressure limit of every level-one, matches optimal extraction temperature, simultaneously will by the way that multitple extraction is arranged
Each effective component in all raw materials extracts, and balances the active principle extracted in raw material, such as ginger oil, gingerol, two
The nutriments such as hydrogen myricetin, vitamin.
The present invention greatly improves ginger powder, date-wolfberry fruit and ampelopsis grossdentata leaf powder by supercritical carbon dioxide extracting
The recovery rate of middle effective component, simultaneously by the effective component in a variety of raw material such as ginger powder, ampelopsis grossdentata leaf powder, date-wolfberry fruit
It extracting, concentrates the effective component in health product, active constituent content is high in obtained health product, and it is in good taste, it remains
The original mouthfeel and smell of ginger.Final test effect and testing result are summarized it can be appreciated that the present invention targetedly extraction process
Obtain preferable technical effect.
The present invention uses collocation of the supercritical carbon dioxide extracting process by best extracting pressure and extraction temperature, realizes
A variety of active principles extract simultaneously.Carbon dioxide is gas at normal temperature, and any chemical change does not occur in production process, is produced
Product are easily isolated product noresidue without miscellaneous peculiar smell, and the effective guarantee stability of heat-sensitive ingredients extraction process is protected completely
The pure natural feature of plant material is stayed；And carbon dioxide has very strong permeability and solvability, and rate of extraction is fast, extraction
Take degree high, therefore, active component content is high in extracted products.Carbon dioxide under condition of high voltage has bactericidal effect and antioxygen
Change effect.Supercritical carbon dioxide extracting carries out in totally enclosed dark field, prevents the photic decomposition of photosensitive composition.It is spray-dried skill
Art effectively prevent the wall sticking phenomenon in spray-drying process, reduces supplementary product consumption, effectively reduce ginger in spray drying fragrance and
Active constituent scatters and disappears, and it is high to obtain powder rate, and powder flowbility, laxity and rehydration are good.
Composite extract of the present invention and brown sugar or brown sugar are compatible, are aided with xylo-oligosaccharide powder, obtained health product
Chance water speed is molten, and deposit-free, stability is good, and active constituent content is high, remains the original mouthfeel and smell of ginger, fine and smooth, and
And delicate mouthfeel, thick taste, without tea grounds, nutritional ingredient is high, has the pungent perfume (or spice) of natural ginger.
The present invention is suitable for large-scale industrial production, and preparation section is simply controllable, and links up, and disposably extracting a variety of has
Ingredient is imitated, has saved extraction time, entire production process process is simple and environmentally-friendly, green safe.
Specific embodiment
It is explained further and illustrates below with reference to embodiment, but specific embodiment does not have any type of limit to the present invention
It is fixed.Unless otherwise specified, method and apparatus used in embodiment is conventional method in that art and equipment, raw materials used is normal
Advise marketable material.Water used in the present embodiment and comparative example is purified water.Ginger P.E as described below is ginger oil and gingerol.
First time extracting pressure is 25~30MPa, and extraction temperature is 45~55 DEG C；Second extracting pressure be 15~
20MPa, extraction temperature are 30~40 DEG C；Third time extracting pressure is 8~15MPa, and extraction temperature is 25~30 DEG C；
Embodiment 1
The preparation method of composite extract provided in this embodiment specifically includes following preparation step:
Ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are weighed, is crushed respectively, 80 meshes are crossed, by gained
Overcritical two are passed through after 2.1 parts of ginger powder, 2 parts of chrysanthemum powder, 3 parts of wolfberry fruit powder, 3 parts of red date powder, 0.4 part of ampelopsis grossdentata leaf powder mixing
In carbonoxide extractor, it is added 0.3 part of ethyl alcohol, extracting pressure and extraction temperature are set, extraction 3 times is repeated, extracts every time
35min, carbon dioxide flow are 30L/h to get extract liquor；Wherein, first time extracting pressure is 25MPa, extraction temperature 45
DEG C, second of extracting pressure is 15MPa, and extraction temperature is 30 DEG C, and third time extracting pressure is 8MPa, and extraction temperature is 25 DEG C；
The preparation of health product containing composite extract:
S1. feedstock processing: weighing brown sugar powder, xylo-oligosaccharide powder, crush respectively, crosses 80 meshes；
S2. extraction prepares the composite extract according to the method described above；
S3. by 50 parts of brown sugar powder obtained by step S1 in 90 DEG C of heating and meltings, 25 parts of extractions obtained by step S2 mixing: are added
In liquid, 1 part of xylo-oligosaccharide powder 1500r/min high-speed stirred 15min is added, obtains mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 being spray-dried, 90 DEG C of sterilizing 30min, until moisture content is closed
Lattice cross 30 meshes to get health product.Wherein, spray drying rotating speed of shower nozzle is 350r/min, and inlet air temperature is 100 DEG C, out wind-warm syndrome
Degree is 60 DEG C, feed flow rate 30r/min, and blower frequency is 20Hz.
Embodiment 2
The preparation method of composite extract provided in this embodiment specifically includes following preparation step:
Ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are weighed, is crushed respectively, 80 meshes are crossed, by gained
Overcritical two are passed through after 5.6 parts of ginger powder, 4 parts of chrysanthemum powder, 3.2 parts of wolfberry fruit powder, 4 parts of red date powder, 2 parts of ampelopsis grossdentata leaf powder mixing
In carbonoxide extractor, it is added 0.8 part of ethyl alcohol, extracting pressure and extraction temperature are set, extraction 3 times is repeated, extracts every time
40min, carbon dioxide flow are 32L/h to get extract liquor；Wherein, first time extracting pressure is 28MPa, extraction temperature 45
DEG C, second of extracting pressure is 18MPa, and extraction temperature is 36 DEG C, and third time extracting pressure is 9MPa, and extraction temperature is 25 DEG C；
The preparation of health product containing composite extract:
S1. feedstock processing: weighing brown sugar powder, xylo-oligosaccharide powder, crush respectively, crosses 80 meshes；
S2. extraction prepares the composite extract according to the method described above；
S3. by 55 parts of brown sugar powder obtained by step S1 in 110 DEG C of heating and meltings, 20 parts of extractions obtained by step S2 mixing: are added
It takes in liquid, 2 parts of xylo-oligosaccharide powder 1580r/min high-speed stirred 18min is added, obtain mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 being spray-dried, 94 DEG C of sterilizing 25min, until moisture content is closed
Lattice cross 35 meshes to get health product.Wherein, spray drying rotating speed of shower nozzle is 350r/min, and inlet air temperature is 100 DEG C, out wind-warm syndrome
Degree is 64 DEG C, feed flow rate 32r/min, and blower frequency is 25Hz.
Embodiment 3
The preparation method of composite extract provided in this embodiment specifically includes following preparation step:
Ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are weighed, is crushed respectively, 80 meshes are crossed, by gained
Overcritical two are passed through after 5.6 parts of ginger powder, 4 parts of chrysanthemum powder, 3.2 parts of wolfberry fruit powder, 4 parts of red date powder, 2 parts of ampelopsis grossdentata leaf powder mixing
In carbonoxide extractor, 0.8 part of water is added, extracting pressure and extraction temperature are set, repeats extraction 3 times, extracts 40min every time,
Carbon dioxide flow is 36L/h to get extract liquor, that is, composite extract；Wherein, first time extracting pressure is 28MPa, extraction
Taking temperature is 48 DEG C, and second of extracting pressure is 16MPa, and extraction temperature is 40 DEG C, and third time extracting pressure is 8MPa, extraction temperature
Degree is 30 DEG C；
The preparation of health product containing composite extract:
S1. feedstock processing: weighing brown sugar powder, xylo-oligosaccharide powder, crush respectively, crosses 80 meshes；
S2. extraction prepares the composite extract according to the method described above；
S3. mixing: by 59.6 parts of brown sugar powder obtained by step S1 in 110 DEG C of heating and meltings, 17 parts are added obtained by step S2
In extract liquor, 2.8 parts of xylo-oligosaccharide powder 1600r/min high-speed stirred 20min are added, obtain mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 being spray-dried, 96 DEG C of sterilizing 20min, until moisture content is closed
Lattice cross 40 meshes to get health product.Wherein, spray drying rotating speed of shower nozzle is 360r/min, and inlet air temperature is 110 DEG C, out wind-warm syndrome
Degree is 68 DEG C, feed flow rate 34r/min, and blower frequency is 40Hz.
Embodiment 4
The preparation method of composite extract provided in this embodiment specifically includes following preparation step:
Ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are weighed, is crushed respectively, 80 meshes are crossed, by gained
Overcritical two are passed through after 14 parts of ginger powder, 10 parts of chrysanthemum powder, 8 parts of wolfberry fruit powder, 10 parts of red date powder, 8 parts of ampelopsis grossdentata leaf powder mixing
In carbonoxide extractor, it is added 2 parts of water, extracting pressure and extraction temperature are set, repeat extraction 3 times, extracts 50min every time, two
Aoxidizing carbon flow is 40L/h to get extract liquor, that is, composite extract；Wherein, first time extracting pressure is 28MPa, extraction
Temperature is 50 DEG C, and second of extracting pressure is 15MPa, and extraction temperature is 38 DEG C, and third time extracting pressure is 10MPa, extraction temperature
Degree is 28 DEG C；
The preparation of health product containing composite extract:
S1. feedstock processing: weighing brown sugar powder, xylo-oligosaccharide powder, crush respectively, crosses 80 meshes；
S2. extraction prepares the composite extract according to the method described above；
S3. by 60 parts of brown sugar powder obtained by step S1 in 115 DEG C of heating and meltings, 13 parts of extractions obtained by step S2 mixing: are added
It takes in liquid, 3.5 parts of xylo-oligosaccharide powder 1700r/min high-speed stirred 24min is added, obtain mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 being spray-dried, 100 DEG C of sterilizing 15min, until moisture content is closed
Lattice cross 45 meshes to get health product.Wherein, spray drying rotating speed of shower nozzle is 370r/min, and inlet air temperature is 115 DEG C, out wind-warm syndrome
Degree is 70 DEG C, feed flow rate 36r/min, and blower frequency is 45Hz.
Embodiment 5
The preparation method of composite extract provided in this embodiment specifically includes following preparation step:
Ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are weighed, is crushed respectively, 90 meshes are crossed, by gained
Overcritical two are passed through after 14 parts of ginger powder, 10 parts of chrysanthemum powder, 8 parts of wolfberry fruit powder, 10 parts of red date powder, 2 parts of ampelopsis grossdentata leaf powder mixing
In carbonoxide extractor, the ethyl alcohol that 2 parts of volume by volume concentrations are 90% is added, extracting pressure and extraction temperature are set, extraction 3 is repeated
It is secondary, 60min is extracted every time, and carbon dioxide flow is 40L/h to get extract liquor, that is, composite extract；Wherein, extract for the first time
Pressure power is 30MPa, and extraction temperature is 55 DEG C, and second of extracting pressure is 20MPa, and extraction temperature is 40 DEG C, and third time extracts
Pressure is 15MPa, and extraction temperature is 30 DEG C；
The preparation of health product containing composite extract:
S1. feedstock processing: weighing brown sugar powder, xylo-oligosaccharide powder, crush respectively, crosses 90 meshes；
S2. extraction prepares the composite extract according to the method described above；
S3. mixing: by 63 parts of brown sugar powder obtained by step S1 in 120 DEG C of heating and meltings, 10.5 parts are added obtained by step S2
In extract liquor, 5 parts of xylo-oligosaccharide powder 1800r/min high-speed stirred 30min are added, obtain mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 being spray-dried, 100 DEG C of sterilizing 10min, until moisture content is closed
Lattice cross 50 meshes to get health product.Wherein, spray drying rotating speed of shower nozzle is 380r/min, and inlet air temperature is 120 DEG C, out wind-warm syndrome
Degree is 75 DEG C, feed flow rate 40r/min, and blower frequency is 50Hz.
Comparative example 1
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In feedstock processing is not sieved after crushing in step S1.
Comparative example 2
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In step S2 extraction is repeated 3 times extraction, and extracting pressure is 30MPa, and extraction temperature is 48 DEG C.
Comparative example 3
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In only extraction is primary in step S2, extracting pressure 35MPa, and extraction temperature is 60 DEG C.
Comparative example 4
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In brown sugar is directly added into extract liquor without heating and melting in step S3.
Comparative example 5
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In being spray-dried rotating speed of shower nozzle in step S4 is 390r/min, and inlet air temperature is 130 DEG C, and leaving air temp is 80 DEG C, feed flow rate
50r/min。
Comparative example 6
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In being spray-dried rotating speed of shower nozzle in step S4 is 340r/min, and inlet air temperature is 95 DEG C, and leaving air temp is 58 DEG C, feed flow rate
25r/min。
Comparative example 7
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In 20 parts of ginger powder in step S2.
Comparative example 8
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In 40 parts of extract liquor in step S3.
Comparative example 9
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In 15 parts of chrysanthemum powder in step S2.
Comparative example 10
The preparation method of health product described in this comparative example, specific preparation step is same as Example 3, and difference exists
In, direct mixing after feedstock processing, step S2 mixing is that step S1 resulting material is added in the pure water of equal quality,
1600r/min high-speed stirred 20min, obtains mixed liquor；
Experimental example 1: Detection of Stability
The stability of embodiment health product and comparative example health product is detected by observation and accelerated aging tests.Specific side
Method are as follows: the results are shown in Table 1 by the health product organoleptic requirements that operating instruction observes each embodiment, comparative example provides, then seals packet
Dress, is put into cell incubator, and setting temperature is 55 DEG C, and relative humidity 55% is stored 60 days；Respectively at 0 day, 30 days, 60
Its sampling detects the appearance of instant ginger jujube tea respectively and is reconstituted using hot water and (hot water is added with 0.1g/mL, stir 10s)；Detection
The results are shown in Table 2.
Table 1
| Project | Color | Tissue morphology | Flavour, smell | Impurity (after brewing) |
| Embodiment 1 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Embodiment 2 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Embodiment 3 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Embodiment 4 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Embodiment 5 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Comparative example 1 | Brown | Loose particles | Sweet faint scent free from extraneous odour | Slightly suspend precipitating, no visible foreign |
| Comparative example 2 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Comparative example 3 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Comparative example 4 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Slightly suspend precipitating, no visible foreign |
| Comparative example 5 | Brown | Loose particles | Slightly bitter has the smell of burning | A little precipitating |
| Comparative example 6 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | A little precipitating |
| Comparative example 7 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Comparative example 8 | Brown | Loose particles | Slightly bitter has the smell of burning | There is suspension to precipitate, no visible foreign |
| Comparative example 9 | Brown | Loose particles | Sweet faint scent free from extraneous odour | Without precipitating |
| Comparative example 10 | Yellowish-brown | Loose particles | Sweet faint scent free from extraneous odour | A little precipitating |
Health product colour stable prepared by the present invention, smell faint scent free from extraneous odour, no precipitating, mouthfeel are good.
Table 2
By 2 experimental result of table it is found that the health moral character that the present invention is prepared can be more preferable compared to comparative example stability, especially
It is the health product prepared using the composite extract of supercritical carbon dioxide extracting, optimal stability, and obtained product is equal
Even no particle, without agglomeration, dissolution is fast, and free from admixture and precipitating, hence it is evident that is better than comparative example.
Experimental example 2: taste assessment
100 volunteers of instant tea are often drunk in random selection, respectively from color, form, flavour and smell, brew
4 aspects score to health product obtained by each embodiment, and 100 volunteers make even respectively, and sum up to every total score
(total score full marks 100 divide), standards of grading are as shown in table 3.
The sense organ evaluation result for the health product that Examples 1 to 5 health product and comparative example 1~10 provide is as shown in table 4.
Table 4
| Color | Form | Flavour, smell | Brew | Total score | |
| Embodiment 1 | 19 | 18 | 36 | 18 | 91 |
| Embodiment 2 | 19 | 19 | 37 | 18 | 93 |
| Embodiment 3 | 19 | 19 | 39 | 19 | 96 |
| Embodiment 4 | 19 | 19 | 38 | 17 | 93 |
| Embodiment 5 | 19 | 18 | 38 | 18 | 93 |
| Comparative example 1 | 16 | 14 | 30 | 12 | 72 |
| Comparative example 2 | 18 | 17 | 30 | 16 | 81 |
| Comparative example 3 | 17 | 16 | 28 | 16 | 77 |
| Comparative example 4 | 16 | 14 | 30 | 13 | 73 |
| Comparative example 5 | 17 | 17 | 26 | 17 | 77 |
| Comparative example 6 | 16 | 15 | 27 | 14 | 72 |
| Comparative example 7 | 17 | 17 | 25 | 18 | 77 |
| Comparative example 8 | 16 | 17 | 24 | 17 | 74 |
| Comparative example 9 | 17 | 17 | 24 | 18 | 76 |
| Comparative example 10 | 14 | 14 | 25 | 14 | 67 |
By table 4 the experimental results showed that the health product pure in mouth feel that the present invention is prepared, fine and smooth, free from foreign meter, smell is fragrant
Dense mellow, free from extraneous odour, fragrant sense, aftertaste sense, smooth feeling are substantially better than comparative example.
Embodiment 3: composition detection
Health product sample is prepared according to the method for Examples 1 to 5 health product and comparative example 1~10 respectively, and to its sample
Composition detection is carried out, Plays provide moisture content≤8.0g/100g, and the results are shown in Table 5:
Table 5
By table 5, the experimental results showed that, active constituent content is high in the health product of the method for the present invention preparation, has in preparation process
It imitates ingredient to retain completely, impure amount is few, the health product effective component purity is high prepared, full of nutrition.
Experimental example 4: sample bacterium Indexs measure
The health product sample for randomly selecting preparation of the embodiment of the present invention carries out bacterial regrowth detection to sample, as a result accords with
It closes and requires.Wherein by taking 3 result of embodiment as an example, as shown in table 6:
Table 6
| Project | Standard regulation | Content |
| Total plate count, cfu/g | N=5, c=2, m=1000, M=50000 | < 10 |
| Coliform, cfu/g | N=5, c=2, m=10, M=100 | It is not detected |
| Mould, cfu/g | ≤50 | < 5 |
| Staphylococcus aureus, cfu/g | N=5, c=1, m=100, M=1000 | It is not detected |
| Salmonella, cfu/g | N=5, c=0, m=0 | It is not detected |
As table 6 the experimental results showed that health product prepared by the present invention meet microorganism detection index.
The above description is only a preferred embodiment of the present invention, above used general explanation, specific embodiment and
Test, the present invention is described in detail, but on the basis of the present invention, can make some modifications or improvements to it, this is to this
It is obvious for the technical staff of field.Therefore, these done without departing from theon the basis of the spirit of the present invention equally replace
It changes, modify or improve, fall within the scope of the claimed invention.
Claims (10)
1. a kind of composite extract, which is characterized in that use red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder
As raw material, gained extract liquor, the extraction use and are repeated 3 times extraction after supercritical carbon dioxide extracting after raw material is mixed
It takes, first time extracting pressure is 25~30MPa, and extraction temperature is 45~55 DEG C；Second of extracting pressure is 15~20MPa, extraction
Taking temperature is 30~40 DEG C；Third time extracting pressure is 8~15MPa, and extraction temperature is 25~30 DEG C；
The red date powder, wolfberry fruit powder, ampelopsis grossdentata leaf powder, chrysanthemum powder and ginger powder weight ratio are as follows: 3 ~ 10 parts of red date powder, Chinese holly
3 ~ 8 parts of Qi powder, 0.4 ~ 8 part of ampelopsis grossdentata leaf powder, 2 ~ 10 parts of chrysanthemum powder, 2 ~ 14 parts of ginger powder.
2. composite extract according to claim 1, which is characterized in that 3 extractions, each extraction time 35 ~
60min, carbon dioxide flow are 30 ~ 40L/h.
3. the application of any one of claims 1 or 2 composite extract, which is characterized in that be applied to preparation health product.
4. application according to claim 3, which is characterized in that the health product include following component: composite extract 7.4
~ 43 parts, 50 ~ 63 parts, 1 ~ 5 part of xylo-oligosaccharide powder of sugar.
5. application according to claim 4, which is characterized in that including following preparation step:
S1. brown sugar or brown sugar, ginger powder, chrysanthemum powder, wolfberry fruit powder, red date powder, xylo-oligosaccharide powder, Xian Chi snake Portugal feedstock processing: are weighed
Grape leaf powder, crushes respectively, sieving；
S2. it extracts: being passed through after ginger powder obtained by step S1, chrysanthemum powder, wolfberry fruit powder, red date powder, ampelopsis grossdentata leaf powder are mixed super
In critical carbon dioxide extractor, entrainer is added, extracting pressure and extraction temperature are set, extracts to get extract liquor；
S3. mixing: brown sugar powder obtained by step S1 or brown sugar heating and melting are added in extract liquor obtained by step S2, are added low
Xylan powder high-speed stirred, obtains mixed liquor；
S4. health product are prepared: mixed liquor obtained by step S3 is spray-dried, sterilizing, until moisture content is qualified, be sieved to get.
6. application according to claim 5, which is characterized in that sieving sieve described in step S1 is 70 ~ 90 mesh.
7. application according to claim 5, which is characterized in that ginger powder and entrainer weight ratio are 7:1 in step S2；Step
Brown sugar and extract liquor weight ratio are 1.15 ~ 7:1 in S3；The entrainer is one in the mixture of water, ethyl alcohol, ethyl alcohol and water
Kind.
8. application according to claim 5, which is characterized in that 90 ~ 120 DEG C of heating temperature, high-speed stirring described in step S3
Mixing speed is 1500 ~ 1800r/min, and mixing time is 15 ~ 30min.
9. application according to claim 5, which is characterized in that described in step S4 spray drying rotating speed of shower nozzle be 350 ~
380r/min, inlet air temperature are 100 ~ 120 DEG C, and leaving air temp is 60 ~ 75 DEG C, 30 ~ 40r/min of feed flow rate, and blower frequency is
20~50Hz。
10. application according to claim 5, which is characterized in that sterilising temp described in step S4 is 90 ~ 100 DEG C, when sterilizing
Between 10 ~ 30min, moisture content≤8% be qualification, sieving sieve be 30 ~ 50 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811567735.7A CN109645393A (en) | 2018-12-20 | 2018-12-20 | Composite extract and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811567735.7A CN109645393A (en) | 2018-12-20 | 2018-12-20 | Composite extract and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109645393A true CN109645393A (en) | 2019-04-19 |
Family
ID=66115491
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811567735.7A Withdrawn CN109645393A (en) | 2018-12-20 | 2018-12-20 | Composite extract and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111758869A (en) * | 2020-07-23 | 2020-10-13 | 上海旭梅食品科技股份有限公司 | Instant chrysanthemum powder, preparation method thereof and beverage |
-
2018
- 2018-12-20 CN CN201811567735.7A patent/CN109645393A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111758869A (en) * | 2020-07-23 | 2020-10-13 | 上海旭梅食品科技股份有限公司 | Instant chrysanthemum powder, preparation method thereof and beverage |
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