CN104473249B - A kind of liquid preparation of Pollen Pini and preparation method thereof - Google Patents
A kind of liquid preparation of Pollen Pini and preparation method thereof Download PDFInfo
- Publication number
- CN104473249B CN104473249B CN201410673100.0A CN201410673100A CN104473249B CN 104473249 B CN104473249 B CN 104473249B CN 201410673100 A CN201410673100 A CN 201410673100A CN 104473249 B CN104473249 B CN 104473249B
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- China
- Prior art keywords
- pollen pini
- juice
- purified water
- concentrated juice
- fructus
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- A—HUMAN NECESSITIES
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- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
- A23L2/06—Extraction of juices from citrus fruits
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention provides the liquid preparation of a kind of Pollen Pini, in described liquid preparation the content of water with mass ratio range more than 85%, and liquid preparation is to exist with uniform liquid mixture form, such as solution, suspension, emulsion, emulsion, colloid solution, etc., or homodisperse solid-liquid mixtures, this invention ensures that the functional component in Pollen Pini, fragrance produces in hot-working, transport and store during quality and stay in grade, additionally, the formula of Pollen Pini liquid preparation and preparation method are formed homogeneous for Pollen Pini in aqueous medium, stable system has good effect, and liquid preparation more easily absorbs utilization；The preparation method that invention further provides described Pollen Pini liquid preparation, and the application at the nourishing and health preserving regulating immunity, slow down aging, protection cardiovascular and cerebrovascular vessel, resisting fatigue, looks improving and the skin nourishing, adjustment gastrointestinal function, the body sick and weak or sub-health population of void.
Description
Technical field
The present invention relates to the liquid preparation of a kind of Pollen Pini, including beverage, oral liquid, slurry etc., and preparation method thereof.
Background technology
Flos pini, make again pine yellow, it it is dry pollen produced by pinaceae plant stamen, in powdery, it is commonly referred to Pollen Pini, for foresythia or faint yellow fine powder, gas is fragrant, and sweet in the mouth is put down nontoxic, and Flos pini is the elite of pinaster, mainly originate from China, there are fabulous medical science, nutrition etc. be worth, include the multiple nutritional components needed for the most long-lived life entity, including multiple healthy functions compositions such as multiple proteins, monosaccharide, polysaccharide, flavone, nucleic acid, choline, aminoacid, mineral, enzyme and coenzyme, and collocation is rationally, it is possible to supplement, nutrition needed for balancing human body comprehensively.Compared with the pollen of honeybee source, Pollen Pini is artificial collection, has that Hua Yuan is single, quality is pure, stable components, and non agricultural chemical residuum, without features such as zoohormones.Pollen Pini is all good compared with other any plant pollen mouthfeel, has light fragrance when taking, and is unique full nutrition pollen in the world, can be rated as " king of pollen ", since ancient times by treasure that honor is health preserving, health care；Ancients claim " gas of pine and cypress can make people's longevity ", and Chinese Shennong's Herbal is recorded: " Flos pini, abnormal smells from the patient is sweet flat nontoxic, and disappear congestion, takes physical strength profiting of making light of one's life by commiting suicide for a long time, prolongs life "；Bright Compendium of Material Medica is recorded: " Flos pini, sweet, warm, nontoxic.Profit cardiopulmonary, QI invigorating ".
Modern medicine study shows, many-sided effect such as Flos pini has antioxidation, slow down aging, improves immunity of organism, antitumor, resisting fatigue, protection cardiovascular and cerebrovascular vessel, hepatoprotective, looks improving and the skin nourishing, adjustment gastrointestinal function, balanced nutrients.
Pollen Pini and slow down aging: containing a large amount of antioxidation compositions in Pollen Pini, such as vitamin E, carotene and trace element-selenium etc., they all can suppress body lipid and protein peroxidization speed, thus having the effect of slow down aging, about the function of its slow down aging, there are substantial amounts of document and experiment both at home and abroad for card.Informal dress Pollen Pini can eliminate senile plaque, makes human body renew one's youth vigor, and this is also the reason of Pollen Pini " clothes are made light of one's life by commiting suicide for a long time, life prolonging ".
Pollen Pini and resisting fatigue: Pollen Pini includes balanced nutrition comprehensively, it is possible to physical strength reinforcing, energy, makes fatigue comprehensively be recovered.Pollen Pini is to being prone to tired middle-aged and elderly people or to be engaged in superpower muscle power worker should be highly beneficial.It addition, Pollen Pini is through the detection of Olympics drug-testing center of China, without any violated composition, also it is a kind of desirably excellent tonic product thus for athlete.
Pollen Pini and beauty treatment: Pollen Pini not only has the regulation of physiological functions of uniqueness, and also has and promote skin cell metabolism, skin-cell aging delaying increases skin elasticity, makes the special-effect of the pure white ruddy fitness of skin, be described as " cosmetics eaten ".Pollen Pini had both contained the abundant aminoacid that directly can be absorbed by Skin Cell, all natural vitamin required for containing again Skin Cell and multiple enzyme, and this just provides the foundation for complete beautification.The particularly injection Vitamin B_6 in Pollen Pini and vitamin B group matching coordinative effect, it is possible to activating cell so that internal SOD value is maintained at high level, thus can scavenging free radicals better, block the approach producing chloasma, butterfly spot, eliminate the melanin of skin so that the pure white beauty of skin.Meanwhile, long-term edible Pollen Pini is notable to preventing and treating senile skin pruritus effect.It addition, Pollen Pini has good effect to reducing, remove comedo.Moreover, take Pollen Pini and also there is the effect of bright healthy hair.
Pollen Pini and gastrointestinal dysfunction disease: Pollen Pini contains nearly hundred kinds of enzymes, it is possible to promote gastrointestinal peristalsis, appetite stimulator, help digest, gastrointestinal dysfunction disease is had obvious adjustment effect.
Pollen Pini and hepatoprotective: Pollen Pini can promote hepatocyte activity, make bile secretion normal, it is prevented that the generation of hepatopathy, and can promote liver detoxification function.Many experiments show that, hepatocyte is had good protective effect by Pollen Pini.It addition, the liver injury that Pollen Pini heavy dose of in advance is likely to result in for excessive consumption of alcohol has good preventive effect, and take Pollen Pini after drinking and also contribute to the rehabilitation of damaged liver function.
Pollen Pini and cardiovascular maintenance: Pollen Pini, with the nutrition library of its pure natural, enhances metabolism, have adjusted endocrine gland, has mobilized substituting excretion, also improves the situation of heart, blood, blood vessel, cardiovascular is served health-care effect.Magnesium in Pollen Pini both can kinase system, again can as the carrier of various nutrient substance；Flavonoid substances can obviously reduce blood fat and cholesterol；Various vitamin can increase vessel wall elasticity, improves the microcirculation of heart and brain.
Pollen Pini and constipation: Pollen Pini includes abundant and various nutrients completely, and constipation has good therapeutical effect.The constipation such as dyspepsia and upper digestive disease caused, because gastrointestinal dysfunction is had good curative effect by Pollen Pini, thus, after taking Pollen Pini, this kind of constipation has improvement immediately.For the nervous constipation causing involuntary muscle spasm to cause, magnesium in Pollen Pini and vitamin B6, involuntary muscle is had good sedation, thus constipation can eliminate naturally.
Pollen Pini and other diseases: Pollen Pini is a natural nutrition storehouse, it is started with from solution human nutrition equilibrium problem comprehensively, it is greatly improved immunity of human body itself, thus numerous disease is suffered from beyond thought auxiliary therapeutic action, such as flu, prostate diseases, anemia, diabetes, hypertension, asthma, rhinitis etc..What is particularly worth mentioning is that, external without broken wall treatment Pollen Pini can dampness astringing to arrest bleeding, eczema, impetigo, skin erosion, dense water is dripping, traumatic hemorrhage, diaper dermatitis etc. have good therapeutical effect.Thus it is not only the good medicine of various skin infection patient, take good care of the good merchantable brand of the tender skin of baby especially.
Natural miniature nutrition library: the Nature creates that pinaster is green for a long time, not old miracle in thousand, its Source of life is exactly the spermatid of pinaster---Pollen Pini, containing the whole nutritions needed for the most long-lived life entity, including multiple proteins, aminoacid, mineral, enzyme and coenzyme, nucleic acid, monosaccharide, polysaccharide etc., total content reaches more than 200 kinds, has the effect of outstanding balanced nutrients and extra-nutrition.
Flos pini has been machined on various health care, health preserving product, such as pine pollen tablets, electuary, milk powder, facial film, wine, beverage etc..Research finds, in modern Product processing production process and Product transport, storage process, especially Pollen Pini is in moisture product, in beverage, oral liquid, beans based food, by in higher temperature processing, fill, transport, storage engineering, the healthy functions composition of Flos pini is all easy to degraded, loss, and the intrinsic fragrance of Flos pini also can greatly reduce, and has a strong impact on its quality and flavouring essence quality.
Pollen Pini is made liquid preparation, such as oral liquid, beverage etc., it is more conducive to absorption of human body, but the functional component less stable of Pollen Pini in liquid preparation, and in preparation process, the fragrance loss of Pollen Pini is very big, additionally, the wet aqueous of Pollen Pini is poor, is not easy to form homogeneous, stable system in aqueous medium.
Summary of the invention
It is an object of the invention to provide the liquid preparation of a kind of Pollen Pini, in described liquid preparation the content of water with mass ratio range more than 85%, and liquid preparation is to exist with uniform liquid mixture form, such as solution, suspension, emulsion, emulsion, colloid solution, etc., or homodisperse solid-liquid mixtures, common, preferred compositions of the present invention is water fluid preparation, such as oral liquid or beverage, the homogenate of thickness or mash, wherein said water is purified water, distilled water, mineral water or drinking water etc..
Pollen Pini of the present invention, also include the extract of Pollen Pini or the deep processing product of Pollen Pini, the water extract of such as Pollen Pini is or/and ethanol extraction, Flos pini tunning (such as ferment etc.), and Flos pini is generally used for the present invention with pulverous dry product, wall cell disruption powder, the powder morphology of its extract or the form of fermentation liquid.
Especially, liquid preparation of the present invention, it will be preferred that stable system, uniform, homogeneous liquid beverage or oral liquid, common, including the beverage of mix homogeneously, underflow, or the milk drink containing Pollen Pini, or the fruit drink containing Pollen Pini；
The liquid preparation of Pollen Pini of the present invention, every 100 weight portions contain: Pollen Pini 0.05～3 weight portion, stabilizer 0.1～1.5 weight portion, sweeting agent 0.001～10 weight portion, antioxidant 0～0.5 weight portion, milk or milk powder 0～10 weight portion, fruit and vegetable juice 0～10 weight portion, acid-base modifier 0～1.2 weight portion, taste modifying agent 0～1.5 weight portion, surplus is water, it is preferable that the content of water with mass ratio range more than 75%, more preferably the content of water with mass ratio range more than 85%；
Preferably, the liquid preparation of Pollen Pini of the present invention, contains in every 100 weight portions: Pollen Pini 0.1～1 weight portion, stabilizer 0.1～1.5 weight portion, sweeting agent 0.001～8 weight portion, antioxidant 0～0.5 weight portion, milk or milk powder 0～8 weight portion, fruit and vegetable juice 0～10 weight portion, acid-base modifier 0～1.2 weight portion, taste modifying agent 0～1.5 weight portion, surplus is water, it is preferable that the content of water with mass ratio range more than 85%；
Preferably, the liquid preparation of Pollen Pini of the present invention, contains in every 100 weight portions: Pollen Pini 0.2～0.8 weight portion, stabilizer 0.1～1 weight portion, sweeting agent 0.001～5 weight portion, antioxidant 0～0.3 weight portion, milk or milk powder 0～8 weight portion, fruit and vegetable juice 0～8 weight portion, acid-base modifier 0～1.2 weight portion, taste modifying agent 0～1.5 weight portion, surplus is water, it is preferable that the content of water with mass ratio range more than 85%；
Wherein, described stabilizer at least one in glyceryl monostearate, glycerol distearate, polyglyceryl fatty acid ester, stearoylketene sodium lactate, sucrose fatty acid ester, sorbitan carboxylic esters, sodium caseinate, sodium tripolyphosphate, lecithin, sodium carboxymethyl cellulose, xanthan gum, guar gum, carrageenan, arabic gum, sodium alginate, Konjac glucomannan, agar, microcrystalline Cellulose, gellan gum and pectin；
Described sweeting agent at least one in steviol glycosides, fructose, xylitol, sucrose, sucralose, Sorbitol, high fructose syrup, protein sugar, aspartame, acesulfame potassium, stachyose, neotame, glucose, Mel, polyglucose；
Described antioxidant at least one in vitamin C (that is: L-AA), L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E；
Described acid-base modifier at least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium bicarbonate, sodium pyrophosphate, sodium tripolyphosphate, sodium hexameta phosphate；
Described fruit and vegetable juice includes but not limited to fruit, vegetable, the kernel of dry fruit, squeezing the juice of fruit or sarcocarp etc., serosity, defibrination juice, water immiscible material, water extract etc., it is selected from Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, almond water, Semen arachidis hypogaeae juice, jujube juice, wolfberry juice, Cortex cocois radicis gel juice, at least one in Flos Rosae Rugosae extractive juice；
Described taste modifying agent at least one in the edible essence of various tastes, maltol, ethylmaltol, vanillin, citric acid, lactic acid, malic acid, acetic acid, fruit acid, WS-23 (that is: N, 2,3-trimethyl-2-butanamide)；
Further; in fluid present invention preparation compositions; other one or more functional components can also be contained, for instance nutrition or other compositions wholesome etc. such as lecithin, inositol, L-carnitine, vitamin B2, vitamin B12, vitamin C, vitamin E, vitamin D, docosahexenoic acid (DHA), arachidonic acid, taurine, oligomeric isomaltose, probiotic bacteria, bacillus bifidus, Radix Ginseng, Antrodia Camphorata, Herba Epimedii, Cordyceps militaris (L.) Link., Lepidinm meyenii Walp, eucommia Bark male flower.
Especially, owing to Flos pini is a kind of natural pollen, allergy likely can be produced when edible, therefore the invention provides and Flos pini is carried out desensitization treatment technology, as follows: to weigh Pollen Pini by formula and put in water, the weight ratio of described Pollen Pini and water is 1:(5～18), in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, can well be stripped of the allergin of Pollen Pini surface attachment, reach the effect of desensitization.
Preferably, the liquid preparation of Pollen Pini of the present invention is a kind of rich in proteins and the colloid of fat, is complicated a, thermodynamic stable system, the colloid solution that in system, existing protein is formed, there is again the emulsion that chyle fat is formed, also have the true solution that sugar etc. is formed.
The preparation method that it is a further object to provide aforesaid liquid preparation, it includes putting in water by Pollen Pini, the weight ratio of described Pollen Pini and water is 1:(5～18), in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, again the Pollen Pini processed and water are mixed mixing and make uniform liquid, or make homodisperse solid-liquid mixtures, and the content of water with mass ratio range more than 75%；Preferably compositions is made uniform liquid form, for instance solution, suspension, emulsion, emulsion, colloid solution, etc., or compositions is made homodisperse solid-liquid mixtures.
Especially, the preparation method that the present invention provides the liquid preparation of a kind of Pollen Pini, it includes:
(1) clean: Pollen Pini is put in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination with the water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh stabilizer, sweeting agent, antioxidant, taste modifying agent, milk or milk powder, fruit and vegetable juice by formula, respectively with the water dissolution of 2～10 times or grinding distribution uniformly after, it is added separately in the prepared Pollen Pini serosity of step (2) or Pollen Pini lixiviating solution again, it is uniformly mixed, add water and be settled to required volume of production, add acid-base modifier and regulate pH, mixing and stirring；
(4) homogenizing: the mixed liquor that step (3) prepares is carried out 80～200 orders and filters, filtrate is in temperature 50～98 DEG C, pressure is that 15～58MPa carries out homogenizing, optionally can carry out repeatedly homogenizing, Pollen Pini is made to reach breaking cellular wall, and make the Oil globule granularity in liquid less than 5 μm, preferably make the Oil globule granularity in liquid less than 3 μm, such as making the Oil globule granularity in liquid is 2 μm, 1 μm, 0.5 μm, 0.3 μm etc., homogenizing, refer to that the feed liquid of material is in extruding, material is made to refine under the triple role that thump and decompression expand, broken is more tiny, so that material can evenly be mutually mixed, whole product system is more stable, preferably, the present invention proposes homogenizing treatment technology, process through repeatedly homogenizing, make Pollen Pini, stabilizer, sweeting agent, the Homogeneous phase mixing such as water also keep stable homogeneous；
(5) fill, sterilizing: by after homogenizing mixed liquor carry out vacuum outgas, canned, sealing, and under 85～135 DEG C of conditions sterilize 4 seconds～35 minutes；
(6) pack, check, obtain product of the present invention；
Every 100 weight portions of described liquid preparation contain: Pollen Pini 0.05～3 weight portion, stabilizer 0.1～1.5 weight portion, sweeting agent 0.001～10 weight portion, antioxidant 0～0.5 weight portion, milk or milk powder 0～10 weight portion, fruit and vegetable juice 0～10 weight portion, acid-base modifier 0～1.2 weight portion, taste modifying agent 0～1.5 weight portion, surplus is water, it is preferable that the content of water with mass ratio range more than 75%；
Wherein, described stabilizer at least one in glyceryl monostearate, glycerol distearate, polyglyceryl fatty acid ester, stearoylketene sodium lactate, sucrose fatty acid ester, sorbitan carboxylic esters, sodium caseinate, sodium tripolyphosphate, lecithin, sodium carboxymethyl cellulose, xanthan gum, guar gum, carrageenan, arabic gum, sodium alginate, Konjac glucomannan, agar, microcrystalline Cellulose, gellan gum and pectin；
Described sweeting agent at least one in steviol glycosides, fructose, xylitol, sucrose, sucralose, Sorbitol, high fructose syrup, protein sugar, aspartame, acesulfame potassium, stachyose, neotame, glucose, Mel, polyglucose；
Described antioxidant is selected from vitamin C (that is: L-AA), L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E；
Described acid-base modifier at least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium bicarbonate, sodium pyrophosphate, sodium tripolyphosphate, sodium hexameta phosphate；
Described fruit and vegetable juice includes but not limited to fruit, vegetable, the kernel of dry fruit, squeezing the juice of fruit or sarcocarp etc., serosity, defibrination juice, water immiscible material, water extract etc., it is selected from Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, almond water, Semen arachidis hypogaeae juice, jujube juice, wolfberry juice, Cortex cocois radicis gel juice, at least one in Flos Rosae Rugosae extractive juice；
Described taste modifying agent at least one in the edible essence of various tastes, maltol, ethylmaltol, vanillin, citric acid, lactic acid, malic acid, acetic acid, WS-23 (that is: N, 2,3-trimethyl-2-butanamide).
Should illustrate, the material nature of Pollen Pini decides the quality of the key factor in the course of processing and finished product, such as homogeneity, color and luster, abnormal smells from the patient etc., and the emulsifying effectiveness of the loss of the fineness of serosity, material, the oxygen barrier condition of liquid preparation and the color, smell and taste of deoxidation effect and beverage and esters, wherein the fineness of serosity depends on filtering order number；Material loss with in the course of processing material by thermal conditions relevant；The oxygen barrier condition of liquid preparation and deoxidation effect depend on the vacuum of the material time with air contact and vacuum outgas；The color, smell and taste of liquid preparation and the emulsifying effectiveness of esters depend on formula, processing condition and sterilization conditions.Special, filtration order number of the present invention is 80～500 orders, preferably filtering order number is 100～200 orders, most preferably filtering order number is 250～450 orders, the heating temperature of preferred feed 35～80 DEG C, preferred homogenization pressure is 25-58Mpa, it is preferable that the vacuum of vacuum outgas is 0.04～0.09Mpa, it is preferable that sterilization conditions be 115～121 DEG C 20 minutes.
Further, Pollen Pini has good pharmacological action, for health, especially immunity is being regulated, slow down aging, protection cardiovascular and cerebrovascular vessel, resisting fatigue, looks improving and the skin nourishing, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the effect aspects such as the nourishing and health preserving of sub-health population, there is good synergism, present invention also offers the above-mentioned compositions containing Pollen Pini and water for preparing adjustment immunity, slow down aging, protection cardiovascular and cerebrovascular vessel, resisting fatigue, looks improving and the skin nourishing, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, application in the healthy product of the nourishing and health preserving of sub-health population, described healthy product include beverage/food, health food, medicine, etc..
The present invention contains the Aquo-composition of Pollen Pini, ensure that the functional component in Pollen Pini, the fragrance quality during hot-working production, transport and storage and stay in grade, additionally, the formula of Pollen Pini liquid preparation and preparation method form homogeneous, stable system for Pollen Pini in aqueous medium good effect, and liquid preparation more easily absorbs utilization.
In the implementation process of the present invention, the various embodiments that those of ordinary skill in the art produce on the basis without departing from scope and spirit of the present invention essence and modification are apparent from and easily carry out.By the following examples, the application etc. of the present invention is further elaborated with, it is not intended that embodiment limitation of the present invention.
Embodiment 1, Pollen Pini oral liquid and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini (or breaking cellular wall Pollen Pini) 0.1%～1%, it is preferred to 0.3%,
Lecithin 0～0.2%, it is preferred to 0.08%,
Xanthan gum 0.02%～0.3%, it is preferred to 0.06%,
Sodium carboxymethyl cellulose 0.02%～0.3%, it is preferred to 0.06%,
Sucralose 0～0.2%, it is preferred to 0.008%,
Xylitol or sucrose 0.5%～5%；It is preferably 2%,
Vitamin C 0～0.2%, it is preferred to 0.05%,
Citric acid 0～0.8%, it is preferred to 0.1%,
Malic acid 0～0.8%, it is preferred to 0.1%,
Purified water adds to 100%；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination with the water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh lecithin, xanthan gum, sodium carboxymethyl cellulose, sucralose, xylitol or sucrose, vitamin C, citric acid, malic acid by formula, respectively with the water dissolution of 10～20 times or grinding distribution uniformly after, the Pollen Pini serosity or the Pollen Pini lixiviating solution that prepare with step (2) mix, stir, add water and be settled to required volume of production, mixing and stirring；
(4) homogenizing: the mixed liquor that step (3) prepares is carried out 100 order filtrations, and filtrate is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, makes the Oil globule granularity in liquid less than 1 μm；
(5) fill, sterilizing: in vacuum, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, canned, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) packing, check, obtain product of the present invention, taste is sour-sweet, Flos pini good smell.
Taking above liquid preparation 10 milliliters, be centrifuged in centrifuges, adopt centrifuging to judge its emulsion stability, its emulsion stability reaches 99%, it is shown that form homogeneous, stable system in aqueous medium for Pollen Pini.
Embodiment 2, Pollen Pini compounded milk product and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini 0.1%～0.5%, it is preferred to 0.2%,
Glyceryl monostearate 0%～0.03%, it is preferred to 0.015%,
Xylitol or sucrose 0.5%～8%；It is preferably 6%,
Milk or milk powder 10%～60%；Preferred milk is 50%, or preferably milk powder is 10%,
Purified water adds to 100%；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination with the water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, obtains Pollen Pini lixiviating solution；
(3) allotment: by formula weigh glyceryl monostearate, xylitol or sucrose respectively with the water dissolution of 5～10 times or grinding distribution uniform after, the Pollen Pini serosity or the Pollen Pini lixiviating solution that prepare with step (2) mix, stir, add milk or milk powder, add water and be settled to required volume of production, mixing and stirring；
(4) homogenizing: mixed liquor 80～150 order step (3) prepared filters, it is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, and make the Oil globule granularity in liquid less than 3 μm, it is preferable that make the Oil globule granularity in liquid less than 1 μm；
(5) fill, sterilizing: in vacuum, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, canned, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) packing, check, obtain product of the present invention, taste is sweet, has milk and Flos pini fragrance concurrently.
Taking above liquid preparation 10 milliliters, be centrifuged in centrifuges, adopt centrifuging to judge its emulsion stability, its emulsion stability reaches 99%, it is shown that form homogeneous, stable system in aqueous medium for Pollen Pini.
Embodiment 3, Pollen Pini fruit and vegetable juice goods and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini 0.2%～0.5%, it is preferred to 0.3%,
High fructose syrup 2%～10%；It is preferably 5%,
Fruit and vegetable juice 20%～60%；It is preferably 40%,
Purified water adds to 100%；
Wherein, described fruit and vegetable juice at least one in Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, almond water, Semen arachidis hypogaeae juice, jujube juice, wolfberry juice, Cortex cocois radicis gel juice, Flos Rosae Rugosae extractive juice；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, make Pollen Pini sporoderm-broken rate reach more than 90%, standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination with the water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh high fructose syrup with adding fruit and vegetable juice after the water dissolution of 3～5 times by formula, then the Pollen Pini serosity prepared with step (2) or Pollen Pini lixiviating solution are mixed homogeneously, and add water and are settled to required volume of production, mixing and stirring；
(4) homogenizing: mixed liquor 80～150 order step (3) prepared filters, it is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, and make the Oil globule granularity in liquid less than 3 μm, it is preferable that make the Oil globule granularity in liquid less than 1 μm；
(5) fill, sterilizing: in vacuum, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, canned, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) packing, check, obtain product of the present invention, taste is sweet, has fruity and Flos pini fragrance concurrently.
Taking above liquid preparation 10 milliliters, be centrifuged in centrifuges, adopt centrifuging to judge its emulsion stability, its emulsion stability reaches 97%, it is shown that form homogeneous, stable system in aqueous medium for Pollen Pini.
Embodiment 4, Flos pini honey jam product and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini 1%～5%, it is preferred to 2.5%,
Mel 3%～10%；It is preferably 8%,
Sucralose 0～0.01%；It is preferably 0.005%,
Sodium alginate 0.2%～0.8%, it is preferred to 0.3%,
Carboxymethyl cellulose 0.2%～0.8%, it is preferred to 0.4%,
Xanthan gum 0.05%～0.3%, it is preferred to 0.1%,
Fruit acid 0.2%～1%, it is preferred to 0.4%；
Vitamin C 0～0.2%, it is preferred to 0.05%,
Purified water adds to 100%；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, make Pollen Pini sporoderm-broken rate reach more than 90%, standby；
(2) slurrying: the Pollen Pini that step (1) will be processed, adds the water of 5～10 times and vitamin C in room temperature～60 DEG C defibrination, and heated and boiled 5min, obtains Pollen Pini mixed serum；
(3) allotment: weigh Mel, sucralose and fruit acid by formula and dissolve by the purified water of 2～4 times, obtain Mel acid solution, another formula weighs sodium alginate, carboxymethyl cellulose, xanthan gum, with the purified water grinding distributions of 8～20 times uniformly after, add the heating of surplus purified water to make to be completely dissolved, mix homogeneously with Mel acid solution again, be eventually adding the Pollen Pini mixed serum that step (2) prepares, be uniformly mixed；
(4) homogenizing: the pressure of honey beans 15MPa is carried out homogenizing in homogenizer, makes honey beans mouthfeel finer and smoother；
(5) fill, sterilizing: be that 0.04～0.09Mpa carries out by the sweet beans after homogenizing in vacuum degassed, canned, sealing seals, and adopts steam sterilization, and the time is 10min；
(6) packaging, inspection, obtain product of the present invention, taste sour and sweet palatability, fine and smooth soft, bright color and tending to smear out, coating uniform is smooth, Flos pini good smell.
Embodiment 5, Flos pini fruit spreads and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini 1%～5%, it is preferred to 3.5%,
Fruit and vegetable juice 30%～80%, it is preferred to 60%,
Konjac glucomannan 0.2%～0.8%, it is preferred to 0.4%,
Pectin 0.2%～0.8%, it is preferred to 0.4%,
Xanthan gum 0.05%～0.3%, it is preferred to 0.15%,
Polyglucose 2%～10%, it is preferred to 8%,
Citric acid 0.02%～0.2%, it is preferred to 0.05%,
Sodium citrate 0.1%～0.5%, it is preferred to 0.2%,
Sucralose 0.004-0.1%；
Purified water adds to 100%；
Wherein, described fruit and vegetable juice at least one in Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, jujube juice, wolfberry juice, Cortex cocois radicis gel juice, Flos Rosae Rugosae extractive juice；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, make Pollen Pini sporoderm-broken rate reach more than 90%, standby；
(2) slurrying: the Pollen Pini that step (1) will be processed, adds the purified water of 5～8 times in room temperature～60 DEG C defibrination, and heated and boiled 5min, filter and remove residue, obtains Pollen Pini mixed serum；
(3) allotment: weigh polyglucose, sucralose, citric acid, sodium citrate, Konjac glucomannan, pectin, xanthan gum by formula, it is sequentially added in fruit and vegetable juice, mix homogeneously, is eventually adding the Pollen Pini mixed serum that step (2) prepares, is uniformly mixed；
(3) allotment: weigh Mel, sucralose and fruit acid by formula and dissolve by the purified water of 2～4 times, obtain Mel acid solution, another formula weighs sodium alginate, carboxymethyl cellulose, xanthan gum, with the purified water grinding distributions of 8～20 times uniformly after, add the heating of surplus purified water to make to be completely dissolved, mix homogeneously with Mel acid solution again, be eventually adding the Pollen Pini mixed serum that step (2) prepares, be uniformly mixed；
(4) homogenizing: heated by fruit jam and stir, infusion 15min, after cooling, the pressure at 15MPa carries out homogenizing in homogenizer, makes fruit jam mouthfeel finer and smoother；
(5) fill, sterilizing: being that 0.04～0.09Mpa carries out by the honey slurry after homogenizing in vacuum degassed, canned, sealing seals, and adopts steam sterilization, and the time is 10min；
(6) packing, check, obtain product of the present invention, taste sour and sweet palatability, exquisiteness is soft, and tends to smear out, and coating uniform is smooth, Flos pini good smell.
Embodiment 6, Flos pini perfume (or spice) walnut Lu and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen Pini 0.1%～0.5%, it is preferred to 0.25%,
Sucrose or xylitol 2%～10%, it is preferred to 5%,
Walnut juice 20%～60%, it is preferred to 35%,
Cys 0.005%～0.05%, it is preferred to 0.01%,
Sodium carboxymethyl cellulose 0.05%～0.5%, it is preferred to 0.08%,
Guar gum 0.05%～0.4%, it is preferred to 0.08%,
Purified water adds to 100%；
Preparation: (1) is cleaned: put into by Pollen Pini in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually vacuum is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, make Pollen Pini sporoderm-broken rate reach more than 90%, standby；
(2) lixiviate: Pollen Pini step (1) processed heats to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh Cys, sucrose or xylitol with adding Walnut juice after the water dissolution of 3～5 times by formula, the Pollen Pini lixiviating solution prepared with step (2) again is mixed homogeneously, the glue that another addition sodium carboxymethyl cellulose and guar gum are formed in the purified water of 20 times amount, it is uniformly mixed, add water and be settled to required volume of production, mixing；
(4) homogenizing: the mixed liquor that step (3) prepares is filtered in 60～100 orders, is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure；
(5) fill, sterilizing: in vacuum, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, canned, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) packing, check, obtain product of the present invention, taste is sweet, has Semen Juglandis fragrance and Flos pini fragrance concurrently；
Wherein, the preparation method of described Walnut juice is as follows:
By walnut kernel peeling, it is placed in vacuum drying oven, temperature 40 DEG C, pressure 0.01～0.02MPa, dry moisture to 3%～5%, with disintegrating machine, the Semen Juglandis that decortication is dried being broken into below 0.2cm aperture, low-temperature cold pressing removes part walnut oil, and pressure is 70～80MPa, pressing temperature 30～35 DEG C, controlling the Semen Juglandis grouts oil content after cold pressing is 35～40%, obtains low fat Semen Juglandis grouts, adds 10 by low fat Semen Juglandis grouts～the purified water defibrination of 20 times of weight, then vibrosieve filters, and obtains Walnut juice.
Taking above liquid preparation 10 milliliters, be centrifuged in centrifuges, adopt centrifuging to judge its emulsion stability, its emulsion stability reaches 99%, it is shown that form homogeneous, stable system in aqueous medium for Pollen Pini.
Embodiment 7, Flos pini has good pharmacological action, for health, especially immunity is being regulated, slow down aging, protection cardiovascular and cerebrovascular vessel, resisting fatigue, looks improving and the skin nourishing, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the effect aspects such as the nourishing and health preserving of sub-health population, there is good synergism, the compositions containing Flos pini and water of any one in the embodiment of the present invention 1 to 6, immunity is regulated for human body, slow down aging, protection cardiovascular and cerebrovascular vessel, resisting fatigue, looks improving and the skin nourishing, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the aspects such as the nourishing and health preserving of sub-health population, there is obvious action.
Claims (2)
1. the liquid preparation of a Pollen Pini, containing Pollen Pini 0.05～3 weight portion in every 100 weight portions, stabilizer 0.1～1.5 weight portion, sweeting agent 0.001～10 weight portion, antioxidant 0～0.5 weight portion, milk or milk powder 0～10 weight portion, fruit and vegetable juice 0～10 weight portion, acid-base modifier 0～1.2 weight portion, taste modifying agent 0～1.5 weight portion, surplus is water, and the content of water with mass ratio range more than 85%；Wherein:
Described stabilizer at least one in glyceryl monostearate, glycerol distearate, polyglyceryl fatty acid ester, stearoylketene sodium lactate, sucrose fatty acid ester, sorbitan carboxylic esters, sodium caseinate, sodium tripolyphosphate, lecithin, sodium carboxymethyl cellulose, xanthan gum, guar gum, carrageenan, arabic gum, sodium alginate, Konjac glucomannan, agar, microcrystalline Cellulose, gellan gum and pectin；
Described sweeting agent at least one in steviol glycosides, fructose, xylitol, sucrose, sucralose, Sorbitol, high fructose syrup, protein sugar, aspartame, acesulfame potassium, stachyose, neotame, glucose, Mel, polyglucose；
Described antioxidant at least one in vitamin C, L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E；
Described acid-base modifier at least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium bicarbonate, sodium pyrophosphate, sodium tripolyphosphate, sodium hexameta phosphate；
Described fruit and vegetable juice includes at least one in Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, almond water, Semen arachidis hypogaeae juice, jujube juice, wolfberry juice；
Described taste modifying agent at least one in maltol, ethylmaltol, vanillin, citric acid, lactic acid, malic acid, acetic acid, fruit acid, WS-23；
The preparation method of the liquid preparation of described Pollen Pini, it includes:
(1) clean: Pollen Pini is put in water, the weight ratio of described Pollen Pini and water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min；Then Pollen Pini is processed in room temperature～60 DEG C defibrination with the water of 3～10 times, filter and remove residue, mix homogeneously, obtain Pollen Pini serosity, or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue with the water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh stabilizer, sweeting agent, antioxidant, taste modifying agent, milk or milk powder, fruit and vegetable juice by formula, respectively with the water grinding distribution of 2～10 times uniformly after, it is added separately in the prepared Pollen Pini serosity of step (2) or Pollen Pini lixiviating solution again, it is uniformly mixed, add water and be settled to required volume of production, add acid-base modifier and regulate pH, mixing and stirring；
(4) homogenizing: the mixed liquor that step (3) prepares being carried out 80～200 orders and filters, filtrate is that 15～58MPa carries out homogenizing in temperature 50～98 DEG C, pressure, makes Pollen Pini reach breaking cellular wall, and makes the Oil globule granularity in liquid less than 5 μm；
(5) fill, sterilizing: the mixed liquor after homogenizing is carried out vacuum outgas, fill, sealing, and sterilizes 4 seconds～35 minutes under 85～135 DEG C of conditions；
(6) pack, check, to obtain final product.
2. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 0.1%～1%,
Lecithin 0～0.2%,
Xanthan gum 0.02%～0.3%,
Sodium carboxymethyl cellulose 0.02%～0.3%,
Sucralose 0～0.2%,
Xylitol or sucrose 0.5%～5%,
Vitamin C 0～0.2%,
Citric acid 0～0.8%,
Malic acid 0～0.8%,
Purified water adds to 100%；
Its preparation method includes: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination by the purified water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue by the purified water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh lecithin, xanthan gum, sodium carboxymethyl cellulose, sucralose, xylitol or sucrose, vitamin C, citric acid, malic acid by formula, dissolve by the purified water of 10～20 times respectively or grinding distribution uniformly after, the Pollen Pini serosity or the Pollen Pini lixiviating solution that prepare with step (2) mix, stir, add purified water and be settled to required volume of production, mixing and stirring；
(4) homogenizing: the mixed liquor that step (3) prepares is carried out 100 order filtrations, and filtrate is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, makes the Oil globule granularity in liquid less than 1 μm；
(5) fill, sterilizing: at air pressure, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, fill, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) pack, check, to obtain final product.
3. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 0.1%～0.5%,
Glyceryl monostearate 0～0.03%,
Xylitol or sucrose 0.5%～8%,
Milk or milk powder 10%～60%,
Purified water adds to 100%；
Its preparation method includes: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, at 80～100 DEG C, processes 10～30min, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination by the purified water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue by the purified water of 6～10 times, is optionally ground processing, obtains Pollen Pini lixiviating solution；
(3) allotment: by formula weigh glyceryl monostearate, xylitol or sucrose dissolve by the purified water of 5～10 times respectively or grinding distribution uniform after, the Pollen Pini serosity or the Pollen Pini lixiviating solution that prepare with step (2) mix, stir, add milk or milk powder, add purified water again and be settled to required volume of production, mixing and stirring；
(4) homogenizing: mixed liquor 80～150 order step (3) prepared filters, and is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, and makes the Oil globule granularity in liquid less than 3 μm；
(5) fill, sterilizing: at air pressure, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, fill, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) pack, check, to obtain final product.
4. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 0.2%～0.5%,
High fructose syrup 2%～10%,
Fruit and vegetable juice 20%～60%,
Purified water adds to 100%；
Wherein, described fruit and vegetable juice at least one in Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, almond water, Semen arachidis hypogaeae juice, jujube juice, wolfberry juice；
Preparation: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, Pollen Pini sporoderm-broken rate is made to reach more than 90%, standby；
(2) slurrying or lixiviate: the Pollen Pini oven drying at low temperature that will process, and Pollen Pini is toasted at 100～120 DEG C 10～55min, the fragrance making Pollen Pini intrinsic is stronger, then Pollen Pini is processed in room temperature～60 DEG C defibrination by the purified water of 3～10 times, filter and remove residue, mix homogeneously, obtains Pollen Pini serosity；Or Pollen Pini is heated to 75～100 DEG C of lixiviate 60～90min, filter and remove residue by the purified water of 6～10 times, is optionally ground processing, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh after high fructose syrup dissolves by the purified water of 3～5 times by formula and add fruit and vegetable juice, the Pollen Pini serosity or the Pollen Pini lixiviating solution that prepare with step (2) are mixed homogeneously again, add purified water again and be settled to required volume of production, mixing and stirring；
(4) homogenizing: mixed liquor 80～150 order step (3) prepared filters, and is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure, and makes the Oil globule granularity in liquid less than 3 μm；
(5) fill, sterilizing: at air pressure, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, fill, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) pack, check, to obtain final product.
5. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 1%～5%,
Mel 3%～10%,
Sucralose 0～0.01%,
Sodium alginate 0.2%～0.8%,
Carboxymethyl cellulose 0.2%～0.8%,
Xanthan gum 0.05%～0.3%,
Fruit acid 0.2%～1%,
Vitamin C 0～0.2%,
Purified water adds to 100%；
Its preparation method includes: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, Pollen Pini sporoderm-broken rate is made to reach more than 90%, standby；
(2) slurrying: the Pollen Pini that step (1) will be processed, adds the purified water of 5～10 times and vitamin C in room temperature～60 DEG C defibrination, and heated and boiled 5min, obtains Pollen Pini mixed serum；
(3) allotment: weigh Mel, sucralose and fruit acid by formula and dissolve by the purified water of 2～4 times, obtain Mel acid solution, another formula weighs sodium alginate, carboxymethyl cellulose, xanthan gum, with the purified water grinding distributions of 8～20 times uniformly after, add the heating of surplus purified water to make to be completely dissolved, then mix homogeneously with Mel acid solution, be eventually adding the Pollen Pini mixed serum that step (2) prepares, it is uniformly mixed, obtains honey beans；
(4) homogenizing: at the pressure of 15MPa, honey beans is carried out in homogenizer homogenizing, makes honey beans mouthfeel finer and smoother；
(5) fill, sterilizing: be that 0.04～0.09Mpa carries out by the sweet beans after homogenizing at air pressure degassed, fill, sealing seals, and adopts steam sterilization, and the time is 10min；
(6) pack, check, to obtain final product.
6. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 1%～5%,
Fruit and vegetable juice 30%～80%,
Konjac glucomannan 0.2%～0.8%,
Pectin 0.2%～0.8%,
Xanthan gum 0.05%～0.3%,
Polyglucose 2%～10%,
Citric acid 0.02%～0.2%,
Sodium citrate 0.1%～0.5%,
Sucralose 0.004%-0.1%,
Purified water adds to 100%；
Wherein, described fruit and vegetable juice at least one in Fructus Citri junoris concentrated juice, Fructus Citri tangerinae concentrated juice, pineapple concentrated juice, blue berry concentrated juice, Fructus Vitis viniferae concentrated juice, aloe condensed juice, mango concentrated juice, Fructus Fragariae Ananssae concentrated juice, AJC, pears concentrated juice, Fructus Persicae concentrated juice, Fructus Cucumidis sativi concentrated juice, Herba Apii graveolentis concentrated juice, carrot condensed juice, Fructus Lycopersici esculenti concentrated juice, Fructus Musae concentrated juice, Fructus Chaenomelis concentrated juice, Walnut juice, jujube juice, wolfberry juice；
Its preparation method includes: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, Pollen Pini sporoderm-broken rate is made to reach more than 90%, standby；
(2) slurrying: the Pollen Pini that step (1) will be processed, adds the purified water of 5～8 times in room temperature～60 DEG C defibrination, and heated and boiled 5min, filter and remove residue, obtains Pollen Pini mixed serum；
(3) allotment: weigh polyglucose, sucralose, citric acid, sodium citrate, Konjac glucomannan, pectin, xanthan gum by formula, it is sequentially added in fruit and vegetable juice, mix homogeneously, it is eventually adding the Pollen Pini mixed serum that step (2) prepares, it is uniformly mixed, obtains fruit jam；
(4) homogenizing: heated by fruit jam and stir, infusion 15min, after cooling, the pressure at 15MPa carries out homogenizing in homogenizer, makes fruit jam mouthfeel finer and smoother；
(5) fill, sterilizing: be that 0.04～0.09Mpa carries out by the fruit jam after homogenizing at air pressure degassed, fill, sealing seals, and adopts steam sterilization, and the time is 10min；
(6) pack, check, to obtain final product.
7. a liquid preparation for Pollen Pini, its recipe quantity by weight percentage, contains:
Pollen Pini 0.1%～0.5%,
Sucrose or xylitol 2%～10%,
Walnut juice 20%～60%,
Cys 0.005%～0.05%,
Sodium carboxymethyl cellulose 0.05%～0.5%,
Guar gum 0.05%～0.4%,
Purified water adds to 100%；
Its preparation method includes: (1) is cleaned: put into by Pollen Pini in purified water, the weight ratio of described Pollen Pini and purified water is 1:(5～18), it is placed in hermetic container, it is forced into 1.2～2.5 atmospheric pressure, 10～30min is processed at 80～100 DEG C, then temperature is gradually decreased to room temperature, gradually air pressure is recovered to normal atmosphere (An) again, stand 1～10 hour after stirring, go upper liquid, the Pollen Pini of precipitation is drained away the water, oven drying at low temperature to moisture less than 10%, pulverize with low-temperature airflow and carry out micronizing, Pollen Pini sporoderm-broken rate is made to reach more than 90%, standby；
(2) lixiviate: Pollen Pini step (1) processed heats to 75～100 DEG C of lixiviate 60～90min, filter and remove residue by the purified water of 6～10 times, is optionally ground processing, mix homogeneously, obtains Pollen Pini lixiviating solution；
(3) allotment: weigh after Cys, sucrose or xylitol dissolve by the purified water of 3～5 times by formula and add Walnut juice, the Pollen Pini lixiviating solution prepared with step (2) again is mixed homogeneously, the glue that another addition sodium carboxymethyl cellulose and guar gum are formed in the purified water of 20 times amount, it is uniformly mixed, add purified water and be settled to required volume of production, mixing；
(4) homogenizing: the mixed liquor that step (3) prepares is filtered in 60～100 orders, is that 35～58MPa carries out 2 homogenizing in temperature 50～98 DEG C, pressure；
(5) fill, sterilizing: at air pressure, the liquid after homogenizing is that 0.04～0.09Mpa carries out degassed, fill, sealing seals, and 115～121 DEG C of sterilizings 20 minutes；
(6) pack, check, to obtain final product；
Wherein, the preparation method of described Walnut juice is as follows: by walnut kernel peeling, it is placed in vacuum drying oven, temperature 40 DEG C, pressure 0.01～0.02MPa, dry moisture to 3%～5%, with disintegrating machine, the Semen Juglandis that decortication is dried is broken into below 0.2cm aperture, low-temperature cold pressing removes part walnut oil, pressure is 70～80MPa, pressing temperature 30～35 DEG C, and controlling the Semen Juglandis grouts oil content after cold pressing is 35～40%, obtain low fat Semen Juglandis grouts, adding 10 by low fat Semen Juglandis grouts～the purified water defibrination of 20 times of weight, then vibrosieve filters, and obtains Walnut juice.
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| CN112741321A (en) * | 2021-01-12 | 2021-05-04 | 沈阳荣药堂医药科技有限公司 | Pine pollen oral liquid and preparation method thereof |
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| CN102919371A (en) * | 2012-11-14 | 2013-02-13 | 赵有康 | Pine flower milk tea and preparation method thereof |
| CN102960462A (en) * | 2012-12-05 | 2013-03-13 | 陈佳黎 | Pollen pini soybean milk and preparation method thereof |
| CN103689708B (en) * | 2013-11-08 | 2015-01-07 | 吉林海吉雅生物科技有限公司 | Pine pollen-fragrant solomonseal rhizome liquid beverage |
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