CN104473249A - Pine pollen liquid preparation and preparation method thereof - Google Patents
Pine pollen liquid preparation and preparation method thereof Download PDFInfo
- Publication number
- CN104473249A CN104473249A CN201410673100.0A CN201410673100A CN104473249A CN 104473249 A CN104473249 A CN 104473249A CN 201410673100 A CN201410673100 A CN 201410673100A CN 104473249 A CN104473249 A CN 104473249A
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- Prior art keywords
- pollen pini
- juice
- water
- homogeneous
- inspissated juice
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- 239000000203 mixture Substances 0.000 claims abstract description 44
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
- A23L2/06—Extraction of juices from citrus fruits
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention provides a pine pollen liquid preparation. The content of water in the liquid preparation is greater than 85% by weight, and the liquid preparation exists in a form of a uniform liquid mixture, such as a solution, a suspension, an emulsion, an emulsion and a colloidal solution, or is a form of an evenly dispersed solid-liquid mixture, the stable mass and quality of functional ingredients and aroma in pine pollen during thermal production, transportation and storage can be guaranteed, in addition, the formula and preparation method of the pine pollen liquid preparation play a good role when pine pollen forms a homogenous and stable system in water media, and the liquid preparation is more easily absorbed and utilized; the invention further provides a preparation method of the pine pollen liquid preparation and applications of the pine pollen liquid preparation in terms of regulating immunity, delaying senescence, protecting heart and cerebral vessels, resisting fatigue, beautifying, regulating gastrointestinal function, and nourishing and preserving health of people with deficiency and weakness or subhealth.
Description
Technical field
The present invention relates to a kind of liquid preparation of pollen pini, comprise beverage, oral liquid, slurry etc., and preparation method thereof.
Background technology
Preserved egg, make again pine yellow, it is the dry pollen that pinaceae plant stamen produces, in powdery, be commonly referred to pollen pini, for foresythia or faint yellow fine powder, gas is fragrant, and taste is sweet flat nontoxic, and preserved egg is the elite of pine tree, mainly originate from China, there is the value such as fabulous medical science, nutrition, include the multiple nutritional components needed for the most long-lived life entity, comprising multiple healthy functions compositions such as multiple proteins, monose, polysaccharide, flavones, nucleic acid, choline, amino acid, mineral matter, enzyme and coenzyme, and collocation rationally, can supplement, nutrition needed for balancing human body comprehensively.Compared with the pollen of honeybee source, pollen pini is artificial collection, has that Hua Yuan is single, quality is pure, stable components, and non agricultural chemical residuum, not containing features such as zoohormones.Pollen pini is all good compared with other any one plant pollen mouthfeel, has light fragrance when taking, and is full nutrition pollen unique in the world, can be rated as " king of pollen ", be the treasure of health, health care since ancient times by honor; Ancients claim " gas of pine and cypress can make people's longevity ", and Chinese Shennong's Herbal is recorded: " preserved egg, smell is sweet flat nontoxic, and disappear extravasated blood, takes beneficial strength of making light of one's life by commiting suicide for a long time, prolong life "; Bright Compendium of Material Medica is recorded: " preserved egg, sweet, warm, nontoxic.Profit cardiopulmonary, beneficial gas ".
Modern medicine study shows, preserved egg have anti-oxidant, delay senility, improve immunity of organism, antitumor, many-sided effect such as antifatigue, protection cardiovascular and cerebrovascular, liver protecting, beautifying face and moistering lotion, adjustment gastrointestinal function, balanced nutrients.
Pollen pini with delay senility: containing a large amount of anti-oxidant composition in pollen pini, as vitamin E, carrotene and trace elements of selenium etc., they all can suppress body lipid and protein peroxidization speed, thus there is the effect delayed senility, about the function that it delays senility, a large amount of documents and experiment is had to be card both at home and abroad.Informal dress pollen pini can eliminate senile plaque expelling, and human body is renewed one's youth vigor, and this is also the reason of pollen pini " clothes are made light of one's life by commiting suicide for a long time, prolong life ".
Pollen pini and antifatigue: pollen pini includes balanced nutrition comprehensively, can strengthen muscle power, energy, fatigue is comprehensively recovered.Pollen pini should be very useful to being easy to tired the elderly or being engaged in superpower physical worker.In addition, pollen pini detects through Chinese Olympics drug-testing center, not containing any violated composition, is also thus a kind of desirable excellent tonic product for sportsman.
Pollen pini and beauty treatment: pollen pini not only has unique regulation of physiological functions, and promotes skin cell metabolism in addition, delaying skin cell ageing, increase skin elasticity, make the special-effect of the pure white ruddy fitness of skin, be described as " cosmetics eaten ".Pollen pini is both containing the abundant amino acid that directly can be absorbed by Skin Cell, and again containing all natural vitamin required for Skin Cell and multiple enzyme, this is just for complete beautification provides the foundation.Injection Vitamin B_6 particularly in pollen pini and the effect of B family vitamin matching coordinative, can activating cell, makes proper interior SOD value remain on high level, thus can scavenging free radicals better, block the approach producing chloasma, butterfly macules, eliminate the melanin of skin, make the pure white beauty of skin.Meanwhile, long-term edible pollen pini is to control senile skin itch Be very effective.In addition, pollen pini has good effect to minimizing, removal whelk.Moreover, the effect that pollen pini also has bright healthy hair is taken.
Pollen pini and gastrointestinal dysfunction disease: pollen pini contains nearly hundred kinds of enzymes, can promote gastrointestinal peristalsis, improve a poor appetite, help digest, and has obvious regulating action to gastrointestinal dysfunction disease.
Pollen pini and liver protecting: pollen pini can promote hepatocyte activity, make choleresis normal, prevent the generation of hepatopathy, and can promote liver detoxification function.Many experiments show, pollen pini has good protective effect to liver cell.In addition, the liver injury that in advance heavy dose of pollen pini may cause for excessive consumption of alcohol has good prevention effect, and takes the rehabilitation that pollen pini also contributes to damaged liver function after drinking.
Pollen pini and cardiovascular maintenance: pollen pini, with the nutrition library of its pure natural, enhances metabolism, have adjusted incretory, mobilized substituting excretion, also improved the situation of heart, blood, blood vessel, served health-care effect to cardiovascular.As the magnesium in pollen pini both can kinase system, can be used as again the carrier of various nutriment; Flavonoid substances can obviously reduce blood fat and cholesterol; Various vitamin can increase vessel wall elasticity, improves the microcirculation of heart and brain.
Pollen pini and constipation: pollen pini includes abundant and various nutrients completely, has good therapeutic action to constipation.Such as the constipation that indigestion and disease of upper digestive tract cause, because pollen pini has good curative effect to gastrointestinal dysfunction, thus, after taking pollen pini, this kind of constipation has improvement immediately.For the nervous constipation causing involuntary muscle spasm to cause, the magnesium in pollen pini and vitamin B6, have good sedation to involuntary muscle, and thus constipation can be eliminated naturally.
Pollen pini and other diseases: pollen pini is a natural nutrition storehouse, it is started with from solving human nutrition equilibrium problem comprehensively, greatly improve immunity of human body itself, thus beyond thought auxiliary therapeutic action is had to numerous disease, as flu, prostate diseases, anaemia, diabetes, hypertension, asthma, rhinitis etc.What is particularly worth mentioning is that, external application can eliminating dampness astringing to arrest bleeding without the pollen pini of broken wall treatment, and, traumatism and bleeding dripping to eczema, impetigo, skin erosion, dense water, diaper dermatitis etc. have good therapeutic action.Thus it is not only the good medicine of various sore patient, takees good care of the good merchantable brand of the tender skin of baby especially.
Natural miniature nutrition library: the Nature creates the miracle that pine tree is green for a long time, thousand are not old, its Source of life is exactly the spermatid of pine tree--pollen pini, containing the whole nutritions needed for the most long-lived life entity, comprising multiple proteins, amino acid, mineral matter, enzyme and coenzyme, nucleic acid, monose, polysaccharide etc., total content reaches more than 200 and plants, and has outstanding balanced nutrients and the effect of extra-nutrition.
Preserved egg has been processed to various health care, health product, as pine pollen tablets, electuary, milk powder, facial mask, wine, beverage etc.Research finds, in modern Product processing production process and Product transport, storage process, especially pollen pini is in moisture product, as in beverage, oral liquid, sauce based food, by higher temperature processing, filling, transport, store in engineering, the healthy functions composition of preserved egg is all easy to degraded, loss, and the intrinsic fragrance of preserved egg also can greatly reduce, and has a strong impact on its quality and flavouring essence quality.
Pollen pini is made liquid preparation, such as oral liquid, beverage etc., be more conducive to absorption of human body, but the functional component less stable of pollen pini in liquid preparation, and in preparation process, very large to the fragrance loss of pollen pini, in addition, the wet water-based of pollen pini is poor, is not easy in aqueous medium, form homogeneous, stable system.
Summary of the invention
The object of this invention is to provide a kind of liquid preparation of pollen pini, in described liquid preparation, the content of water is greater than 85% with mass ratio range, and liquid preparation exists with uniform liquid mixture form, such as solution, suspension, emulsion, emulsion, colloidal solution, etc., or homodisperse solid-liquid mixtures, common, preferred composition of the present invention is water fluid preparation, as homogenate or the mash of oral liquid or beverage, thickness, wherein said water is purified water, distilled water, mineral water or drinking water etc.
Pollen pini of the present invention, also comprise the extract of pollen pini or the deep processing product of pollen pini, the water extract of such as pollen pini is or/and ethanol extract, preserved egg tunning (as ferment etc.), and preserved egg is used for the present invention with the form of the powder morphology of pulverous dry product, wall cell disruption powder, its extract or zymotic fluid usually.
Especially, liquid preparation of the present invention, preferably stable system, even, homogeneous liquid beverage or oral liquid, common, comprise the beverage, the underflow that mix, or the milk drink containing pollen pini, or the fruit drink containing pollen pini;
The liquid preparation of pollen pini of the present invention, contain in every 100 weight portions: pollen pini 0.05 ~ 3 weight portion, stabilizing agent 0.1 ~ 1.5 weight portion, sweetener 0.001 ~ 10 weight portion, antioxidant 0 ~ 0.5 weight portion, milk or milk powder 0 ~ 10 weight portion, Juice 0 ~ 10 weight portion, acid-base modifier 0 ~ 1.2 weight portion, taste modifying agent 0 ~ 1.5 weight portion, surplus is water, and the content of preferred water is greater than 75% with mass ratio range, and more preferably the content of water is greater than 85% with mass ratio range;
Preferably, the liquid preparation of pollen pini of the present invention, contains in every 100 weight portions: pollen pini 0.1 ~ 1 weight portion, stabilizing agent 0.1 ~ 1.5 weight portion, sweetener 0.001 ~ 8 weight portion, antioxidant 0 ~ 0.5 weight portion, milk or milk powder 0 ~ 8 weight portion, Juice 0 ~ 10 weight portion, acid-base modifier 0 ~ 1.2 weight portion, taste modifying agent 0 ~ 1.5 weight portion, surplus is water, and the content of preferred water is greater than 85% with mass ratio range;
Preferably, the liquid preparation of pollen pini of the present invention, contains in every 100 weight portions: pollen pini 0.2 ~ 0.8 weight portion, stabilizing agent 0.1 ~ 1 weight portion, sweetener 0.001 ~ 5 weight portion, antioxidant 0 ~ 0.3 weight portion, milk or milk powder 0 ~ 8 weight portion, Juice 0 ~ 8 weight portion, acid-base modifier 0 ~ 1.2 weight portion, taste modifying agent 0 ~ 1.5 weight portion, surplus is water, and the content of preferred water is greater than 85% with mass ratio range;
Wherein, described stabilizing agent is selected from least one in glycerin monostearate, bi-tristearin, polyglyceryl fatty acid ester, hard ester acyl lactylate, sucrose fatty ester, sorbitan carboxylic esters, casein sodium, sodium phosphate trimer, lecithin, sodium carboxymethylcellulose, xanthans, guar gum, carragheen, Arabic gum, sodium alginate, konjac glucomannan, agar, microcrystalline cellulose, gellan gum and pectin;
Described sweetener is selected from that stevioside, fructose, xylitol, sucrose, Sucralose, D-sorbite, HFCS, protein sugar, Aspartame, acesulfame potassium, stachyose, knob are sweet, at least one in glucose, honey, polyglucose;
Described antioxidant is selected from least one in vitamin C (that is: L-AA), L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E;
Described acid-base modifier is selected from least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium acid carbonate, sodium pyrophosphate, sodium phosphate trimer, calgon;
Described Juice includes but not limited to fruit, vegetables, the kernel of dry fruit, squeezing the juice of fruit or pulp etc., slurries, defibrination juice, water immiscible material, water extract etc., such as be selected from orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, almond water, peanut juice, jujube juice, wolfberry juice, coconut palm fruit juice, at least one in rose extractive juice,
Described taste modifying agent is selected from flavoring essence, maltol, ethyl maltol, vanillic aldehyde, citric acid, lactic acid, malic acid, acetic acid, tartaric acid, WS-23 (that is: the N of various taste, 2,3-trimethyl-2-butanamide) at least one;
Further; in liquid preparation composition of the present invention; other one or more functional components can also be contained, nutrition or other compositions wholesome etc. such as such as lecithin, inositol, l-cn, vitamin B2, vitamin B12, vitamin C, vitamin E, vitamin D, DHA (DHA), arachidonic acid, taurine, oligoisomaltose, probio, Bifidobacterium, ginseng, Antrodia camphorata, barrenwort, Cordyceps militaris, agate coffee, eucommia Bark male flower.
Especially, because preserved egg is a kind of natural pollen, likely allergy can be produced when edible, therefore the invention provides and desensitization treatment technology is carried out to preserved egg, as follows: to take pollen pini by formula and put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, 1 ~ 10 hour is left standstill after stirring, go upper liquid, well can be stripped of the allergin of pollen pini surface attachment, reach the effect of desensitization.
Preferably, the liquid preparation of pollen pini of the present invention is a kind of colloid being rich in protein and fat, is complicated a, thermodynamic stable system, the colloidal solution that in system, existing protein is formed, there is again the emulsion that chyle fat is formed, also have sugar to wait the true solution formed.
Another object of the present invention is to provide the preparation method of aforesaid liquid preparation, it comprises puts into water by pollen pini, the weight ratio of described pollen pini and water is 1:(5 ~ 18), in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, 1 ~ 10 hour is left standstill after stirring, go upper liquid, again the pollen pini processed and water mixing mixing are made uniform liquid, or make homodisperse solid-liquid mixtures, and the content of water is greater than 75% with mass ratio range, preferably composition is made uniform liquid form, such as solution, suspension, emulsion, emulsion, colloidal solution, etc., or composition is made homodisperse solid-liquid mixtures.
Especially, the invention provides a kind of preparation method of liquid preparation of pollen pini, it comprises:
(1) clean: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, mix, obtain pollen pini leaching liquor;
(3) allocate: take stabilizing agent, sweetener, antioxidant, taste modifying agent, milk or milk powder, Juice by formula, after using the water-soluble solution of 2 ~ 10 times or grinding distribution evenly respectively, join in the obtained pollen pini slurries of step (2) or pollen pini leaching liquor more respectively, be uniformly mixed, add water and be settled to required output, add acid-base modifier and regulate pH, mixing and stirring;
(4) homogeneous: the mixed liquor that step (3) is obtained is carried out 80 ~ 200 orders and filters, filtrate is in temperature 50 ~ 98 DEG C, pressure is that 15 ~ 58MPa carries out homogeneous, optionally repeatedly homogeneous can be carried out, pollen pini is made to reach broken wall, and make the fat globule granularity in liquid be less than 5 μm, the fat globule granularity in liquid is preferably made to be less than 3 μm, the fat globule granularity in liquid is such as made to be 2 μm, 1 μm, 0.5 μm, 0.3 μm etc., homogeneous, refer to that the feed liquid of material is in extruding, material refinement is made under the triple role that thump and decompression expand, broken is more tiny, thus make material energy evenly mutual mixing, whole product system is more stable, preferably, the present invention proposes homogeneous treatment technology, through repeatedly homogeneous process, make pollen pini, stabilizing agent, sweetener, the Homogeneous phase mixing such as water also keep stable homogeneous,
(5) filling, sterilizing: by after homogeneous mixed liquor carry out vacuum outgas, canned, sealing, and sterilization 4 seconds ~ 35 minutes under 85 ~ 135 DEG C of conditions;
(6) pack, check, obtain product of the present invention;
Contain in every 100 weight portions of described liquid preparation: pollen pini 0.05 ~ 3 weight portion, stabilizing agent 0.1 ~ 1.5 weight portion, sweetener 0.001 ~ 10 weight portion, antioxidant 0 ~ 0.5 weight portion, milk or milk powder 0 ~ 10 weight portion, Juice 0 ~ 10 weight portion, acid-base modifier 0 ~ 1.2 weight portion, taste modifying agent 0 ~ 1.5 weight portion, surplus is water, and the content of preferred water is greater than 75% with mass ratio range;
Wherein, described stabilizing agent is selected from least one in glycerin monostearate, bi-tristearin, polyglyceryl fatty acid ester, hard ester acyl lactylate, sucrose fatty ester, sorbitan carboxylic esters, casein sodium, sodium phosphate trimer, lecithin, sodium carboxymethylcellulose, xanthans, guar gum, carragheen, Arabic gum, sodium alginate, konjac glucomannan, agar, microcrystalline cellulose, gellan gum and pectin;
Described sweetener is selected from that stevioside, fructose, xylitol, sucrose, Sucralose, D-sorbite, HFCS, protein sugar, Aspartame, acesulfame potassium, stachyose, knob are sweet, at least one in glucose, honey, polyglucose;
Described antioxidant is selected from vitamin C (that is: L-AA), L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E;
Described acid-base modifier is selected from least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium acid carbonate, sodium pyrophosphate, sodium phosphate trimer, calgon;
Described Juice includes but not limited to fruit, vegetables, the kernel of dry fruit, squeezing the juice of fruit or pulp etc., slurries, defibrination juice, water immiscible material, water extract etc., such as be selected from orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, almond water, peanut juice, jujube juice, wolfberry juice, coconut palm fruit juice, at least one in rose extractive juice,
Described taste modifying agent is selected from least one in the flavoring essence of various taste, maltol, ethyl maltol, vanillic aldehyde, citric acid, lactic acid, malic acid, acetic acid, WS-23 (that is: WS-23).
Should illustrate, the material nature of pollen pini decides the quality of key factor in process and finished product, such as homogeneity, color and luster, smell etc., and the fineness of slurries, the loss of material, the oxygen barrier condition of liquid preparation and the color, smell and taste of deoxidation effect and beverage and the emulsifying effectiveness of ester class, wherein the fineness of slurries depends on and filters order number; Material loss relevant with the situation of being heated of material in process; Oxygen barrier condition and the deoxidation effect of liquid preparation depend on the vacuum of the time that material contacts with air and vacuum outgas; The color, smell and taste of liquid preparation and the emulsifying effectiveness of ester class depend on fill a prescription, processing condition and sterilization conditions.Special, filtration order number of the present invention is 80 ~ 500 orders, preferred filtration order number is 100 ~ 200 orders, most preferably filtering order number is 250 ~ 450 orders, the heating temperature of preferred feed 35 ~ 80 DEG C, preferred homogenization pressure is 25-58Mpa, and the vacuum of preferred vacuum outgas is 0.04 ~ 0.09Mpa, preferred sterilization conditions be 115 ~ 121 DEG C 20 minutes.
Further, pollen pini has good pharmacological action, for health, especially at immunity moderation, delay senility, protection cardiovascular and cerebrovascular, antifatigue, beautifying face and moistering lotion, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the effect aspects such as the nourishing and health preserving of sub-health population, there is good synergy, present invention also offers the above-mentioned composition containing pollen pini and water for the preparation of immunity moderation, delay senility, protection cardiovascular and cerebrovascular, antifatigue, beautifying face and moistering lotion, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, application in the healthy product of the nourishing and health preserving of sub-health population, described healthy product comprise beverage/food, health food, medicine, etc..
The present invention contains the Aquo-composition of pollen pini, ensure that the functional component in pollen pini, fragrance hot-working produce, transport and the storage life between quality and stay in grade, in addition, the formula of pollen pini liquid preparation and preparation method form homogeneous, stable system for pollen pini in aqueous medium good effect, and liquid preparation is easier to absorb.
In implementation process of the present invention, those of ordinary skill in the art are not departing from the scope of the present invention various embodiment that the basis with Spirit Essence produces and are modifying apparent and be easily carry out.By the following examples application of the present invention etc. done and illustrate further, but do not represent embodiment limitation of the present invention.
Embodiment 1, pollen pini oral liquid and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini (or broken masson pine pollen) 0.1% ~ 1%, is preferably 0.3%,
Lecithin 0 ~ 0.2%, is preferably 0.08%,
Xanthans 0.02% ~ 0.3%, is preferably 0.06%,
Sodium carboxymethylcellulose 0.02% ~ 0.3%, is preferably 0.06%,
Sucralose 0 ~ 0.2%, is preferably 0.008%,
Xylitol or sucrose 0.5% ~ 5%; Be preferably 2%,
Vitamin C 0 ~ 0.2%, is preferably 0.05%,
Citric acid 0 ~ 0.8%, is preferably 0.1%,
Malic acid 0 ~ 0.8%, is preferably 0.1%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, mix, obtain pollen pini leaching liquor;
(3) allocate: take lecithin, xanthans, sodium carboxymethylcellulose, Sucralose, xylitol or sucrose, vitamin C, citric acid, malic acid by formula, after using the water-soluble solution of 10 ~ 20 times or grinding distribution evenly respectively, the pollen pini slurries obtained with step (2) or pollen pini leaching liquor mix, stir, add water and be settled to required output, mixing and stirring;
(4) homogeneous: the mixed liquor that step (3) is obtained carries out 100 order filtrations, and filtrate is that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, makes the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, obtain product of the present invention, taste is sour-sweet, preserved egg good smell.
Get above liquid preparation 10 milliliters, centrifugal in centrifuges, adopt centrifugal process to judge its emulsion stability, its emulsion stability reaches 99%, demonstrates and in aqueous medium, forms homogeneous, stable system for pollen pini.
Embodiment 2, pollen pini compounded milk product and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini 0.1% ~ 0.5%, is preferably 0.2%,
Glycerin monostearate 0% ~ 0.03%, is preferably 0.015%,
Xylitol or sucrose 0.5% ~ 8%; Be preferably 6%,
Milk or milk powder 10% ~ 60%; Preferred milk is 50%, or preferably milk powder is 10%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, obtain pollen pini leaching liquor;
(3) allocate: take after glycerin monostearate, xylitol or sucrose uses the water-soluble solution of 5 ~ 10 times or grinding distribution evenly respectively by formula, the pollen pini slurries obtained with step (2) or pollen pini leaching liquor mix, stir, add milk or milk powder, add water again and be settled to required output, mixing and stirring;
(4) homogeneous: mixed liquor 80 ~ 150 order obtained for step (3) is filtered, be that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, and make the fat globule granularity in liquid be less than 3 μm, preferably make the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, obtain product of the present invention, taste is sweet, has milk and preserved egg fragrance concurrently.
Get above liquid preparation 10 milliliters, centrifugal in centrifuges, adopt centrifugal process to judge its emulsion stability, its emulsion stability reaches 99%, demonstrates and in aqueous medium, forms homogeneous, stable system for pollen pini.
Embodiment 3, pollen pini Juice goods and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini 0.2% ~ 0.5%, is preferably 0.3%,
HFCS 2% ~ 10%; Be preferably 5%,
Juice 20% ~ 60%; Be preferably 40%,
Purified water adds to 100%;
Wherein, described Juice is selected from least one in orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, almond water, peanut juice, jujube juice, wolfberry juice, coconut palm fruit juice, rose extractive juice;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, obtain pollen pini leaching liquor;
(3) allocate: take HFCS by formula and add Juice with after the water-soluble solution of 3 ~ 5 times, pollen pini slurries obtained with step (2) again or pollen pini leaching liquor mix, add water again and be settled to required output, mixing and stirring;
(4) homogeneous: mixed liquor 80 ~ 150 order obtained for step (3) is filtered, be that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, and make the fat globule granularity in liquid be less than 3 μm, preferably make the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, obtain product of the present invention, taste is sweet, has fruity and preserved egg fragrance concurrently.
Get above liquid preparation 10 milliliters, centrifugal in centrifuges, adopt centrifugal process to judge its emulsion stability, its emulsion stability reaches 97%, demonstrates and in aqueous medium, forms homogeneous, stable system for pollen pini.
Embodiment 4, preserved egg honey jam product and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini 1% ~ 5%, is preferably 2.5%,
Honey 3% ~ 10%; Be preferably 8%,
Sucralose 0 ~ 0.01%; Be preferably 0.005%,
Sodium alginate 0.2% ~ 0.8%, is preferably 0.3%,
Carboxymethyl cellulose 0.2% ~ 0.8%, is preferably 0.4%,
Xanthans 0.05% ~ 0.3%, is preferably 0.1%,
Tartaric acid 0.2% ~ 1%, is preferably 0.4%;
Vitamin C 0 ~ 0.2%, is preferably 0.05%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying: the pollen pini that step (1) will be processed, add the water of 5 ~ 10 times and vitamin C in room temperature ~ 60 DEG C defibrination, and 5min is boiled in heating, obtains pollen pini mixed serum;
(3) allocate: take the dissolving of honey, Sucralose and the tartaric acid purified water of 2 ~ 4 times by formula, obtain honey acid solution, another formula takes sodium alginate, carboxymethyl cellulose, xanthans, after even with the purified water grinding distributions of 8 ~ 20 times, add the heating of surplus purified water to make to dissolve completely, mix with honey acid solution again, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(4) homogeneous: the pressure of sweet sauce 15MPa is carried out homogeneous in homogenizer, makes sweet sauce mouthfeel finer and smoother;
(5) filling, sterilizing: in vacuum, the sweet sauce after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and adopt steam sterilizing, the time is 10min;
(6) pack, inspection, obtain product of the present invention, taste sour and sweet palatability, fine and smooth soft, bright color and be easy to smear, coating uniform is smooth, preserved egg good smell.
Embodiment 5, preserved egg fruit spreads and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini 1% ~ 5%, is preferably 3.5%,
Juice 30% ~ 80%, is preferably 60%,
Konjac glucomannan 0.2% ~ 0.8%, is preferably 0.4%,
Pectin 0.2% ~ 0.8%, is preferably 0.4%,
Xanthans 0.05% ~ 0.3%, is preferably 0.15%,
Polyglucose 2% ~ 10%, is preferably 8%,
Citric acid 0.02% ~ 0.2%, is preferably 0.05%,
Natrium citricum 0.1% ~ 0.5%, is preferably 0.2%,
Sucralose 0.004-0.1%;
Purified water adds to 100%;
Wherein, described Juice is selected from least one in orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, jujube juice, wolfberry juice, coconut palm fruit juice, rose extractive juice;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying: the pollen pini that step (1) will be processed, the purified water adding 5 ~ 8 times is DEG C defibrination in room temperature ~ 60, and heating boils 5min, filter and remove residue, obtains pollen pini mixed serum;
(3) allocate: take polyglucose, Sucralose, citric acid, natrium citricum, konjac glucomannan, pectin, xanthans by formula, add successively in Juice, mix, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(3) allocate: take the dissolving of honey, Sucralose and the tartaric acid purified water of 2 ~ 4 times by formula, obtain honey acid solution, another formula takes sodium alginate, carboxymethyl cellulose, xanthans, after even with the purified water grinding distributions of 8 ~ 20 times, add the heating of surplus purified water to make to dissolve completely, mix with honey acid solution again, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(4) homogeneous: jam is heated and stirs, infusion 15min, after cooling, carries out homogeneous at the pressure of 15MPa, makes jam mouthfeel finer and smoother in homogenizer;
(5) filling, sterilizing: in vacuum, the honey slurry after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and adopts steam sterilizing, the time is 10min;
(6) pack, check, obtain product of the present invention, taste sour and sweet palatability, fine and smooth soft, and be easy to smear, coating uniform is smooth, preserved egg good smell.
Fragrant walnut Lu of embodiment 6, preserved egg and preparation method thereof
Recipe quantity by weight percentage, contains:
Pollen pini 0.1% ~ 0.5%, is preferably 0.25%,
Sucrose or xylitol 2% ~ 10%, be preferably 5%,
Walnut juice 20% ~ 60%, is preferably 35%,
Cys 0.005% ~ 0.05%, is preferably 0.01%,
Sodium carboxymethylcellulose 0.05% ~ 0.5%, is preferably 0.08%,
Guar gum 0.05% ~ 0.4%, is preferably 0.08%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) lixiviate: pollen pini step (1) the processed water of 6 ~ 10 times is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue, optionally carries out milled processed, mixes, obtain pollen pini leaching liquor;
(3) allocate: take Cys, sucrose or xylitol by formula and add Walnut juice with after the water-soluble solution of 3 ~ 5 times, pollen pini leaching liquor obtained with step (2) again mixes, separately add the glue that sodium carboxymethylcellulose and guar gum are formed in the purified water of 20 times amount, be uniformly mixed, add water and be settled to required output, mixing;
(4) homogeneous: the mixed liquor that step (3) is obtained filters in 60 ~ 100 orders, is that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, obtain product of the present invention, taste is sweet, has walnut fragrance and preserved egg fragrance concurrently;
Wherein, the preparation method of described Walnut juice is as follows:
By walnut kernel peeling, be placed in vacuum drying chamber, temperature 40 DEG C, pressure 0.01 ~ 0.02MPa, dry moisture to 3% ~ 5%, with disintegrating machine, the walnut kernel that decortication is dried is broken into below 0.2cm aperture, low-temperature cold pressing removal unit divides walnut oil, and pressure is 70 ~ 80MPa, pressing temperature 30 ~ 35 DEG C, the walnut grouts oil content controlled after cold press is 35 ~ 40%, obtains low fat walnut grouts, low fat walnut grouts is added the purified water defibrination of 10 ~ 20 times of weight, then vibratory sieve filters, and obtains Walnut juice.
Get above liquid preparation 10 milliliters, centrifugal in centrifuges, adopt centrifugal process to judge its emulsion stability, its emulsion stability reaches 99%, demonstrates and in aqueous medium, forms homogeneous, stable system for pollen pini.
Embodiment 7, preserved egg has good pharmacological action, for health, especially at immunity moderation, delay senility, protection cardiovascular and cerebrovascular, antifatigue, beautifying face and moistering lotion, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the effect aspects such as the nourishing and health preserving of sub-health population, there is good synergy, the composition containing preserved egg and water of any one in the embodiment of the present invention 1 to 6, for human body immunity moderation, delay senility, protection cardiovascular and cerebrovascular, antifatigue, beautifying face and moistering lotion, regulate gastrointestinal function, the nourishing and health preserving of the empty sick and weak crowd of body, the aspects such as the nourishing and health preserving of sub-health population, there is significant effect.
Claims (10)
1. the liquid preparation of a pollen pini, containing pollen pini 0.05 ~ 3 weight portion in every 100 weight portions, stabilizing agent 0.1 ~ 1.5 weight portion, sweetener 0.001 ~ 10 weight portion, antioxidant 0 ~ 0.5 weight portion, milk or milk powder 0 ~ 10 weight portion, Juice 0 ~ 10 weight portion, acid-base modifier 0 ~ 1.2 weight portion, taste modifying agent 0 ~ 1.5 weight portion, surplus is water, and the content of water is greater than 85% with mass ratio range; Wherein:
Described stabilizing agent is selected from least one in glycerin monostearate, bi-tristearin, polyglyceryl fatty acid ester, hard ester acyl lactylate, sucrose fatty ester, sorbitan carboxylic esters, casein sodium, sodium phosphate trimer, lecithin, sodium carboxymethylcellulose, xanthans, guar gum, carragheen, Arabic gum, sodium alginate, konjac glucomannan, agar, microcrystalline cellulose, gellan gum and pectin;
Described sweetener is selected from that stevioside, fructose, xylitol, sucrose, Sucralose, D-sorbite, HFCS, protein sugar, Aspartame, acesulfame potassium, stachyose, knob are sweet, at least one in glucose, honey, polyglucose;
Described antioxidant is selected from least one in vitamin C, L-AA calcium, L-AA fatty acid ester, sodium sulfite, Cys, vitamin E;
Described acid-base modifier is selected from least one in citric acid, malic acid, lactic acid, acetic acid, sodium carbonate, sodium acid carbonate, sodium pyrophosphate, sodium phosphate trimer, calgon;
Described Juice includes but not limited to fruit, vegetables, the kernel of dry fruit, squeezing the juice of fruit or pulp etc., slurries, defibrination juice, water immiscible material, water extract etc., such as be selected from orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, almond water, peanut juice, jujube juice, wolfberry juice, coconut palm fruit juice, at least one in rose extractive juice,
Described taste modifying agent is selected from flavoring essence, maltol, ethyl maltol, vanillic aldehyde, citric acid, lactic acid, malic acid, acetic acid, tartaric acid, WS-23 (that is: the N of various taste, 2,3-trimethyl-2-butanamide) at least one.
2. in the liquid preparation of pollen pini described in claim 1, further can containing one or more following functional components: lecithin, inositol, l-cn, vitamin B2, vitamin B12, vitamin C, vitamin E, vitamin D, DHA (DHA), arachidonic acid, taurine, oligoisomaltose, probio, Bifidobacterium, ginseng, Antrodia camphorata, barrenwort, Cordyceps militaris, agate coffee, eucommia Bark male flower.
3. the preparation method of the liquid preparation of pollen pini described in claim 1, it comprises puts into water by pollen pini, the weight ratio of described pollen pini and water is 1:(5 ~ 18), in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, 1 ~ 10 hour is left standstill after stirring, go upper liquid, again the pollen pini processed and water mixing mixing are made uniform liquid, or make homodisperse solid-liquid mixtures, and the content of water is greater than 75% with mass ratio range.
4. the preparation method of the liquid preparation of pollen pini described in claim 1, it comprises:
(1) clean: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, and then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, mix, obtain pollen pini leaching liquor;
(3) allocate: take stabilizing agent, sweetener, antioxidant, taste modifying agent, milk or milk powder, Juice by formula, after using the water-soluble solution of 2 ~ 10 times or grinding distribution evenly respectively, join in the obtained pollen pini slurries of step (2) or pollen pini leaching liquor more respectively, be uniformly mixed, add water and be settled to required output, add acid-base modifier and regulate pH, mixing and stirring;
(4) homogeneous: the mixed liquor that step (3) is obtained is carried out 80 ~ 200 orders and filters, filtrate is that 15 ~ 58MPa carries out homogeneous in temperature 50 ~ 98 DEG C, pressure, makes pollen pini reach broken wall, and makes the fat globule granularity in liquid be less than 5 μm;
(5) filling, sterilizing: by after homogeneous mixed liquor carry out vacuum outgas, canned, sealing, and sterilization 4 seconds ~ 35 minutes under 85 ~ 135 DEG C of conditions;
(6) pack, check, to obtain final product.
5. a pollen pini oral liquid, its recipe quantity by weight percentage, contains:
Pollen pini 0.1% ~ 1%, is preferably 0.3%,
Lecithin 0 ~ 0.2%, is preferably 0.08%,
Xanthans 0.02% ~ 0.3%, is preferably 0.06%,
Sodium carboxymethylcellulose 0.02% ~ 0.3%, is preferably 0.06%,
Sucralose 0 ~ 0.2%, is preferably 0.008%,
Xylitol or sucrose 0.5% ~ 5%; Be preferably 2%,
Vitamin C 0 ~ 0.2%, is preferably 0.05%,
Citric acid 0 ~ 0.8%, is preferably 0.1%,
Malic acid 0 ~ 0.8%, is preferably 0.1%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, mix, obtain pollen pini leaching liquor;
(3) allocate: take lecithin, xanthans, sodium carboxymethylcellulose, Sucralose, xylitol or sucrose, vitamin C, citric acid, malic acid by formula, after using the water-soluble solution of 10 ~ 20 times or grinding distribution evenly respectively, the pollen pini slurries obtained with step (2) or pollen pini leaching liquor mix, stir, add water and be settled to required output, mixing and stirring;
(4) homogeneous: the mixed liquor that step (3) is obtained carries out 100 order filtrations, and filtrate is that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, makes the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, to obtain final product.
6. a pollen pini compounded milk product, its recipe quantity by weight percentage, contains:
Pollen pini 0.1% ~ 0.5%, is preferably 0.2%,
Glycerin monostearate 0% ~ 0.03%, is preferably 0.015%,
Xylitol or sucrose 0.5% ~ 8%; Be preferably 6%,
Milk or milk powder 10% ~ 60%; Preferred milk is 50%, or preferably milk powder is 10%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, at 80 ~ 100 DEG C, process 10 ~ 30min, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, obtain pollen pini leaching liquor;
(3) allocate: take after glycerin monostearate, xylitol or sucrose uses the water-soluble solution of 5 ~ 10 times or grinding distribution evenly respectively by formula, the pollen pini slurries obtained with step (2) or pollen pini leaching liquor mix, stir, add milk or milk powder, add water again and be settled to required output, mixing and stirring;
(4) homogeneous: mixed liquor 80 ~ 150 order obtained for step (3) is filtered, be that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, and make the fat globule granularity in liquid be less than 3 μm, preferably make the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, to obtain final product.
7. pollen pini Juice goods, its recipe quantity by weight percentage, contains:
Pollen pini 0.2% ~ 0.5%, is preferably 0.3%,
HFCS 2% ~ 10%; Be preferably 5%,
Juice 20% ~ 60%; Be preferably 40%,
Purified water adds to 100%;
Wherein, described Juice is selected from least one in orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, almond water, peanut juice, jujube juice, wolfberry juice, coconut palm fruit juice, rose extractive juice;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying or lixiviate: by the pollen pini low temperature drying processed, and pollen pini is toasted 10 ~ 55min at 100 ~ 120 DEG C, the fragrance making pollen pini intrinsic is stronger, then by water in the room temperature ~ 60 DEG C defibrination process of pollen pini with 3 ~ 10 times, filter and remove residue, mix, obtain pollen pini slurries; Or pollen pini is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue with the water of 6 ~ 10 times, optionally carries out milled processed, obtain pollen pini leaching liquor;
(3) allocate: take HFCS by formula and add Juice with after the water-soluble solution of 3 ~ 5 times, pollen pini slurries obtained with step (2) again or pollen pini leaching liquor mix, add water again and be settled to required output, mixing and stirring;
(4) homogeneous: mixed liquor 80 ~ 150 order obtained for step (3) is filtered, be that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure, and make the fat globule granularity in liquid be less than 3 μm, preferably make the fat globule granularity in liquid be less than 1 μm;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, to obtain final product.
8. a preserved egg honey jam product, its recipe quantity by weight percentage, contains:
Pollen pini 1% ~ 5%, is preferably 2.5%,
Honey 3% ~ 10%; Be preferably 8%,
Sucralose 0 ~ 0.01%; Be preferably 0.005%,
Sodium alginate 0.2% ~ 0.8%, is preferably 0.3%,
Carboxymethyl cellulose 0.2% ~ 0.8%, is preferably 0.4%,
Xanthans 0.05% ~ 0.3%, is preferably 0.1%,
Tartaric acid 0.2% ~ 1%, is preferably 0.4%;
Vitamin C 0 ~ 0.2%, is preferably 0.05%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying: the pollen pini that step (1) will be processed, add the water of 5 ~ 10 times and vitamin C in room temperature ~ 60 DEG C defibrination, and 5min is boiled in heating, obtains pollen pini mixed serum;
(3) allocate: take the dissolving of honey, Sucralose and the tartaric acid purified water of 2 ~ 4 times by formula, obtain honey acid solution, another formula takes sodium alginate, carboxymethyl cellulose, xanthans, after even with the purified water grinding distributions of 8 ~ 20 times, add the heating of surplus purified water to make to dissolve completely, mix with honey acid solution again, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(4) homogeneous: the pressure of sweet sauce 15MPa is carried out homogeneous in homogenizer, makes sweet sauce mouthfeel finer and smoother;
(5) filling, sterilizing: in vacuum, the sweet sauce after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and adopt steam sterilizing, the time is 10min;
(6) pack, check, to obtain final product.
9. a preserved egg fruit spreads, its recipe quantity by weight percentage, contains:
Pollen pini 1% ~ 5%, is preferably 3.5%,
Juice 30% ~ 80%, is preferably 60%,
Konjac glucomannan 0.2% ~ 0.8%, is preferably 0.4%,
Pectin 0.2% ~ 0.8%, is preferably 0.4%,
Xanthans 0.05% ~ 0.3%, is preferably 0.15%,
Polyglucose 2% ~ 10%, is preferably 8%,
Citric acid 0.02% ~ 0.2%, is preferably 0.05%,
Natrium citricum 0.1% ~ 0.5%, is preferably 0.2%,
Sucralose 0.004-0.1%;
Purified water adds to 100%;
Wherein, described Juice is selected from least one in orange inspissated juice, orange inspissated juice, pineapple concentrated juice, blueberry inspissated juice, grape inspissated juice, aloe condensed juice, mango concentrated juice, strawberry inspissated juice, AJC, pears inspissated juice, peach inspissated juice, cucumber inspissated juice, celery inspissated juice, carrot condensed juice, tomato inspissated juice, banana inspissated juice, pawpaw inspissated juice, Walnut juice, jujube juice, wolfberry juice, coconut palm fruit juice, rose extractive juice;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) slurrying: the pollen pini that step (1) will be processed, the purified water adding 5 ~ 8 times is DEG C defibrination in room temperature ~ 60, and heating boils 5min, filter and remove residue, obtains pollen pini mixed serum;
(3) allocate: take polyglucose, Sucralose, citric acid, natrium citricum, konjac glucomannan, pectin, xanthans by formula, add successively in Juice, mix, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(3) allocate: take the dissolving of honey, Sucralose and the tartaric acid purified water of 2 ~ 4 times by formula, obtain honey acid solution, another formula takes sodium alginate, carboxymethyl cellulose, xanthans, after even with the purified water grinding distributions of 8 ~ 20 times, add the heating of surplus purified water to make to dissolve completely, mix with honey acid solution again, finally add the pollen pini mixed serum that step (2) is obtained, be uniformly mixed;
(4) homogeneous: jam is heated and stirs, infusion 15min, after cooling, carries out homogeneous at the pressure of 15MPa, makes jam mouthfeel finer and smoother in homogenizer;
(5) filling, sterilizing: in vacuum, the honey slurry after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and adopts steam sterilizing, the time is 10min;
(6) pack, check, to obtain final product.
10. a pollen pini walnut Lu, its recipe quantity by weight percentage, contains:
Pollen pini 0.1% ~ 0.5%, is preferably 0.25%,
Sucrose or xylitol 2% ~ 10%, be preferably 5%,
Walnut juice 20% ~ 60%, is preferably 35%,
Cys 0.005% ~ 0.05%, is preferably 0.01%,
Sodium carboxymethylcellulose 0.05% ~ 0.5%, is preferably 0.08%,
Guar gum 0.05% ~ 0.4%, is preferably 0.08%,
Purified water adds to 100%;
Preparation: (1) is cleaned: pollen pini is put into water, the weight ratio of described pollen pini and water is 1:(5 ~ 18), be placed in closed container, be forced into 1.2 ~ 2.5 atmospheric pressure, 10 ~ 30min is processed at 80 ~ 100 DEG C, then temperature is down to room temperature gradually, gradually vacuum is returned to normal atmosphere (An) again, leave standstill 1 ~ 10 hour after stirring, go upper liquid, the pollen pini of precipitation is drained away the water, low temperature drying is less than 10% to moisture, pulverize with low-temperature airflow and carry out ultramicro grinding, make pollen pini sporoderm-broken rate reach more than 90%, for subsequent use;
(2) lixiviate: pollen pini step (1) the processed water of 6 ~ 10 times is heated to 75 ~ 100 DEG C of lixiviate 60 ~ 90min, filter and remove residue, optionally carries out milled processed, mixes, obtain pollen pini leaching liquor;
(3) allocate: take Cys, sucrose or xylitol by formula and add Walnut juice with after the water-soluble solution of 3 ~ 5 times, pollen pini leaching liquor obtained with step (2) again mixes, separately add the glue that sodium carboxymethylcellulose and guar gum are formed in the purified water of 20 times amount, be uniformly mixed, add water and be settled to required output, mixing;
(4) homogeneous: the mixed liquor that step (3) is obtained filters in 60 ~ 100 orders, is that 35 ~ 58MPa carries out 2 homogeneous in temperature 50 ~ 98 DEG C, pressure;
(5) filling, sterilizing: in vacuum, the liquid after homogeneous is that 0.04 ~ 0.09Mpa carries out degassed, canned, sealing sealing, and 115 ~ 121 DEG C of sterilizings 20 minutes;
(6) pack, check, to obtain final product;
Wherein, the preparation method of described Walnut juice is as follows: by walnut kernel peeling, be placed in vacuum drying chamber, temperature 40 DEG C, pressure 0.01 ~ 0.02MPa, dry moisture to 3% ~ 5%, with disintegrating machine, the walnut kernel that decortication is dried is broken into below 0.2cm aperture, low-temperature cold pressing removal unit divides walnut oil, pressure is 70 ~ 80MPa, pressing temperature 30 ~ 35 DEG C, and the walnut grouts oil content controlled after cold press is 35 ~ 40%, obtain low fat walnut grouts, low fat walnut grouts are added the purified water defibrination of 10 ~ 20 times of weight, then vibratory sieve filters, and obtains Walnut juice.
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| CN201410673100.0A CN104473249B (en) | 2014-11-23 | 2014-11-23 | A kind of liquid preparation of Pollen Pini and preparation method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105266155A (en) * | 2015-11-20 | 2016-01-27 | 延边利孚生物科技有限公司 | Composition used for improving sub-health of brain and preparing method thereof |
| CN105285617A (en) * | 2015-07-31 | 2016-02-03 | 滁州学院 | Composite functional type flos chrysanthemi bee pollen suspension beverage containing galacto oligosaccharides and preparation method of composite functional type flos chrysanthemi bee pollen suspension beverage |
| CN105494851A (en) * | 2015-12-02 | 2016-04-20 | 阿衣吐拉·阿不力米提 | Maca-containing anti-fatigue candy suitable for females and production process of maca-containing anti-fatigue candy |
| CN105998536A (en) * | 2016-07-27 | 2016-10-12 | 浙江省磐安县外贸药业有限公司 | Maca tablet and preparation method thereof |
| CN106490557A (en) * | 2016-10-19 | 2017-03-15 | 辽宁海吉诺健康品有限公司 | A kind of pine pollen functional food and preparation method thereof |
| CN106721693A (en) * | 2016-11-18 | 2017-05-31 | 和国荣 | A kind of Mulberry beverage formula and preparation method thereof |
| CN107372845A (en) * | 2017-08-15 | 2017-11-24 | 云南摩尔农庄生物科技开发有限公司 | Natural plant protein drink and its stabilizer |
| CN107397097A (en) * | 2017-09-04 | 2017-11-28 | 姚光隆 | A kind of preserved egg drinks |
| CN108813492A (en) * | 2018-07-11 | 2018-11-16 | 绩溪县老胡家生态农业专业合作社 | A kind of shaddock tremella jam with the effect of filling blood |
| CN109122858A (en) * | 2018-09-19 | 2019-01-04 | 烟台新时代健康产业有限公司 | A kind of one-step shaping technique of preserved egg calcium dried milk |
| CN109349606A (en) * | 2018-10-12 | 2019-02-19 | 杭州花宝生物科技有限公司 | A kind of purification furnace drying method of pollen pini |
| CN112535225A (en) * | 2020-09-23 | 2021-03-23 | 梧州市华夏医药科技有限公司 | Eucommia ulmoides male flower substitutional tea and preparation method thereof |
| CN112741321A (en) * | 2021-01-12 | 2021-05-04 | 沈阳荣药堂医药科技有限公司 | Pine pollen oral liquid and preparation method thereof |
| CN115192655A (en) * | 2022-06-29 | 2022-10-18 | 董克玲 | Traditional Chinese medicine oral liquid and preparation method and application thereof |
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| CN102960462A (en) * | 2012-12-05 | 2013-03-13 | 陈佳黎 | Pollen pini soybean milk and preparation method thereof |
| CN103689708A (en) * | 2013-11-08 | 2014-04-02 | 吉林海吉雅生物科技有限公司 | Pine pollen-fragrant solomonseal rhizome liquid beverage |
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| CN1129083A (en) * | 1995-12-06 | 1996-08-21 | 零文祥 | Pine pollen series food and preparation method thereof |
| CN102919371A (en) * | 2012-11-14 | 2013-02-13 | 赵有康 | Pine flower milk tea and preparation method thereof |
| CN102960462A (en) * | 2012-12-05 | 2013-03-13 | 陈佳黎 | Pollen pini soybean milk and preparation method thereof |
| CN103689708A (en) * | 2013-11-08 | 2014-04-02 | 吉林海吉雅生物科技有限公司 | Pine pollen-fragrant solomonseal rhizome liquid beverage |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105285617B (en) * | 2015-07-31 | 2018-07-17 | 滁州学院 | One kind chu chrysanthemum Bee Pollen suspending beverage of complex function type containing galactooligosaccharide and preparation method thereof |
| CN105285617A (en) * | 2015-07-31 | 2016-02-03 | 滁州学院 | Composite functional type flos chrysanthemi bee pollen suspension beverage containing galacto oligosaccharides and preparation method of composite functional type flos chrysanthemi bee pollen suspension beverage |
| CN105266155A (en) * | 2015-11-20 | 2016-01-27 | 延边利孚生物科技有限公司 | Composition used for improving sub-health of brain and preparing method thereof |
| CN105494851A (en) * | 2015-12-02 | 2016-04-20 | 阿衣吐拉·阿不力米提 | Maca-containing anti-fatigue candy suitable for females and production process of maca-containing anti-fatigue candy |
| CN105998536A (en) * | 2016-07-27 | 2016-10-12 | 浙江省磐安县外贸药业有限公司 | Maca tablet and preparation method thereof |
| CN106490557A (en) * | 2016-10-19 | 2017-03-15 | 辽宁海吉诺健康品有限公司 | A kind of pine pollen functional food and preparation method thereof |
| CN106721693A (en) * | 2016-11-18 | 2017-05-31 | 和国荣 | A kind of Mulberry beverage formula and preparation method thereof |
| CN107372845A (en) * | 2017-08-15 | 2017-11-24 | 云南摩尔农庄生物科技开发有限公司 | Natural plant protein drink and its stabilizer |
| CN107397097A (en) * | 2017-09-04 | 2017-11-28 | 姚光隆 | A kind of preserved egg drinks |
| CN108813492A (en) * | 2018-07-11 | 2018-11-16 | 绩溪县老胡家生态农业专业合作社 | A kind of shaddock tremella jam with the effect of filling blood |
| CN109122858A (en) * | 2018-09-19 | 2019-01-04 | 烟台新时代健康产业有限公司 | A kind of one-step shaping technique of preserved egg calcium dried milk |
| CN109349606A (en) * | 2018-10-12 | 2019-02-19 | 杭州花宝生物科技有限公司 | A kind of purification furnace drying method of pollen pini |
| CN112535225A (en) * | 2020-09-23 | 2021-03-23 | 梧州市华夏医药科技有限公司 | Eucommia ulmoides male flower substitutional tea and preparation method thereof |
| CN112741321A (en) * | 2021-01-12 | 2021-05-04 | 沈阳荣药堂医药科技有限公司 | Pine pollen oral liquid and preparation method thereof |
| CN115192655A (en) * | 2022-06-29 | 2022-10-18 | 董克玲 | Traditional Chinese medicine oral liquid and preparation method and application thereof |
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Address after: 215000 No.8, Jinfeng Road, science and Technology City, Suzhou high tech Zone, Suzhou City, Jiangsu Province Patentee after: Suzhou Medical Device Industry Development Co.,Ltd. Address before: 215000 No.8, Jinfeng Road, science and Technology City, Suzhou high tech Zone, Suzhou City, Jiangsu Province Patentee before: Suzhou science and Technology City Biomedical Technology Development Co.,Ltd. Address after: 215000 No.8, Jinfeng Road, science and Technology City, Suzhou high tech Zone, Suzhou City, Jiangsu Province Patentee after: Suzhou Medical Device Industry Development Group Co.,Ltd. Address before: 215000 No.8, Jinfeng Road, science and Technology City, Suzhou high tech Zone, Suzhou City, Jiangsu Province Patentee before: Suzhou Medical Device Industry Development Co.,Ltd. |