CN114344197B - Medical cold compress repair mask containing argan oil and preparation method of medical cold compress repair mask - Google Patents

Medical cold compress repair mask containing argan oil and preparation method of medical cold compress repair mask Download PDF

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CN114344197B
CN114344197B CN202210039538.8A CN202210039538A CN114344197B CN 114344197 B CN114344197 B CN 114344197B CN 202210039538 A CN202210039538 A CN 202210039538A CN 114344197 B CN114344197 B CN 114344197B
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李�泳
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Huizhou Baishi New Material Co ltd
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Abstract

The invention belongs to the technical field of medical skin care products, and discloses an argin medical cold compress repair mask and a preparation method thereof. Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component; adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion; coating the hydrogel component on a mask base carrier to obtain a gel layer; then coating the gel layer with the argin emulsion, and finally pasting an isolating layer to obtain the medical cold compress repairing facial mask of the argin. The medical cold compress repair facial mask for the argan oil can play roles in cold compress, repair and nourishing. The utilization rate of the active ingredients of the argin oil is high, the product stability is good, and the market prospect is wide.

Description

Medical cold compress repair mask containing argan oil and preparation method of medical cold compress repair mask
Technical Field
The invention belongs to the technical field of medical skin care products, and particularly relates to an argin medical cold compress repair mask and a preparation method thereof.
Background
The Argan oil is also called Morocco oil and is extracted from the fruit pit of Argan tree. The Argan tree is a special tree species in the western Mediterranean region, is only produced in the south of Morocco, and is one of the three treasures of Morocco. The argin tree can bloom and fruit only after 40-60 years, the argin tree belongs to a local old tree species protection area, and only 300ml of argin can be extracted from more than 100 years old argin tree, and about 10 bottles of argin can be extracted. The extraction of the alglycerol is not easy, and the alglycerol still allows the world to accept the cantharis because the alglycerol is always accepted to have the effects of nourishing, relieving and protecting skin and hair, is a nursing product with excellent natural effect, and can be even used as a food material, and is called as liquid gold of Morocco.
Medical cold compress applications are generally composed of cooling substances and various forms of jackets and fixtures. The cooling substance should not contain components that exert pharmacological, immunological or metabolic effects. Is used for physical defervescence and cooling of specific parts of the surface of the human body. Only for closed soft tissue. The medical cold compress repairing facial mask is mainly used for facial skin, and has the effects of reducing fever and cooling, and also has the effects of repairing and nourishing.
Patent CN 110025524A discloses a prosthetic medical cold application mask, which is prepared from the following components: glycerol, 1, 3-butanediol, hydroxyethyl cellulose, sodium hyaluronate, cactus stem extract, nicotinamide, centella asiatica extract, chamomile extract, p-hydroxyacetophenone, 1, 2-hexanediol, qianye rose hydrosol. The facial mask has good effects of improving dryness, redness and itching of skin. Patent CN 111012691A discloses a medical cold-applied mask, which comprises a supporting layer, an essence layer and an isolating layer; the essence layer comprises the following components in percentage by mass: 6.0 to 8.0 percent of chitosan, 1.0 to 5.0 percent of vitamin C, 0.1 to 5.0 percent of nicotinamide, 0.5 to 2.0 percent of kojic acid, 0.5 to 2.0 percent of glutathione, 0.5 to 2.0 percent of compound polypeptide, 1.0 to 5.0 percent of sodium hyaluronate, 0.5 to 3.0 percent of menthol, 2.0 to 5.0 percent of collagen and the balance of water to 100 percent. The medical cold-applied mask has good repairing effect and has obvious improving effect on dryness, redness and itching of skin. Patent CN 113559043A discloses a medical cold compress gel repairing mask, which comprises aloe, chinese yam, okra, red peony root, radix sophorae flavescentis, lithospermum, prepared rehmannia root, fructus kochiae, folium artemisiae argyi, rose essential oil, hydrogel and purified water.
With the improvement of the living standard of people, the additional function requirements of people on the functional skin care products are higher and higher, and the effects of nourishing and repairing facial skin can be provided by adding the argin into the medical cold compress repairing facial mask, so that the facial mask has a wide market prospect.
Patent CN 106491385A discloses a composition for skin barrier repair, comprising the following raw materials: squalane, alglycerol, antioxidants, hexyldecanoyl myristoylalanine, ceramides, phytosphingosine, and other suitable adjuvants. The invention uses the same natural ceramide, the same arginin, the same squalane, the same tetraacetyl phytosphingosine and the same tocopheryl linoleate as human skin to simulate the lipid composition in the stratum corneum of the real skin, can penetrate into the deep layer of the skin, and greatly improves the moisture degree and the barrier function of the skin. Patent CN 108042469A discloses an anti-wrinkle mask liquid containing alglycerol, which consists of the following raw materials in parts by weight: 6-10 parts of dittany bark extract, 12-15 parts of water lily flower extract, 1-2 parts of triethanolamine, 0.2-0.5 part of sodium citrate, 3-6 parts of collagen, 1-2 parts of lecithin, 0.1-0.3 part of uronic acid, 2-3 parts of hydrolyzed pearl liquid, 0.5-0.8 part of allophanate lactam, 5-8 parts of arginin, 3-4 parts of xanthan gum and 110-120 parts of deionized water. The facial mask liquid prepared by the invention can moisten facial skin, strengthen the elasticity of the facial skin, achieve the effects of resisting and removing wrinkles on the facial skin, and has remarkable effect.
The composition or the mask liquid is prepared by simply mixing the components, the effective utilization rate of the functional components is low, and particularly for a cold compress repair mask, the gel component of the composition or the mask liquid leads to slow transfer and absorption of other functional components, and for expensive functional components such as the alaglycerol, the low utilization rate leads to reduction of the cost performance of the product.
Disclosure of Invention
Aiming at the defects and shortcomings of the prior art, the primary aim of the invention is to provide a preparation method of an argin medical cold compress repair mask.
The invention further aims to provide the medical cold compress repair facial mask of the argin oil, which is prepared by the method.
The invention aims at realizing the following technical scheme:
a preparation method of an argan oil medical cold compress repair mask comprises the following preparation steps:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion;
(3) Coating the hydrogel component in the step (1) on a mask-based carrier to obtain a gel layer; and (3) coating the argin emulsion obtained in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin.
Further, the hydrogel component in the step (1) comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000031
further preferably, the hydrogel component in the step (1) comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000032
further, in the step (2), the mass percentage of each raw material of the argin emulsion is as follows:
Figure BDA0003469651410000033
Figure BDA0003469651410000041
further preferably, the mass percentage of each raw material of the argin emulsion in the step (2) is as follows:
Figure BDA0003469651410000042
further, plant extract with the mass percentage of 1% -5% is also added into the argin emulsion in the step (2).
Further preferably, the plant extract comprises at least one of aloe extract, chamomile extract, rose extract, lotus extract, lavender extract, tea extract, peppermint extract, licorice extract, centella extract.
Further, the coating amount of the argin emulsion in the step (3) is 6-12% of the mass of the hydrogel component.
Further, in the step (3), the mask-based carrier material is at least one of silk, fruit fiber, tencel, cotton fiber, soybean fiber and viscose fiber.
The medical cold compress repair facial mask containing the argan oil is prepared by the method.
Compared with the prior art, the invention has the beneficial effects that:
(1) The medical cold compress repair facial mask of the argin oil consists of a hydrogel component and an argin oil emulsion, wherein the hydrogel component plays a role in cold compress, and the argin oil emulsion plays a role in repair and nourishing. The repairing and nourishing arginin emulsion is directly contacted with the face, and the utilization rate of the repairing and nourishing arginin and other functional substances is higher.
(2) The hydrogel component and the components of the argin emulsion of the medical cold compress repair mask are designed specifically, the argin emulsion can be adhered uniformly on the surface of the hydrogel component through the design of component proportion, no flowing or aggregation occurs, and the product stability is high.
(3) The argin emulsion of the medical cold compress repair mask provided by the invention adopts an emulsifying system of specific lecithin, polypeptide, oil-soluble silicone wax and glycerin, and the obtained argin emulsion has high stability and does not generate phenomena such as demulsification; and the prepared alaglycerol emulsion is in a viscous mucus state and can be uniformly adhered to the surface of the hydrogel component by further matching with sodium hyaluronate.
(4) The hydrogel component and the argin emulsion of the medical cold compress repair facial mask do not contain skin irritant substances such as surfactant, and the whole formula is milder.
Detailed Description
The present invention will be described in further detail with reference to examples, but embodiments of the present invention are not limited thereto.
Example 1
The medical cold compress repair mask for the argan oil is prepared by the following method:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion;
(3) Coating the hydrogel component in the step (1) on a silk fiber cloth carrier to obtain a gel layer; and (3) coating the argin emulsion obtained in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin.
The hydrogel component comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000051
Figure BDA0003469651410000061
the argan oil emulsion comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000062
the coating amount of the argin emulsion is 10% of the mass of the hydrogel component.
The argan emulsion obtained in the step (2) of the embodiment is centrifuged at 5000rpm for 15min without demulsification or delamination.
The argin emulsion in the repairing facial mask of the embodiment is uniformly adhered on the surface of the hydrogel component, and does not flow or gather after being vertically hung for 30 days through sealing; the pressure level of 50kPa is extrusion without leakage, and the product stability is high.
Example 2
The medical cold compress repair mask for the argan oil is prepared by the following method:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion;
(3) Coating the hydrogel component in the step (1) on a silk fiber cloth carrier to obtain a gel layer; and (3) coating the argin emulsion obtained in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin.
The hydrogel component comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000071
the argan oil emulsion comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000072
the coating amount of the argin emulsion is 12% of the mass of the hydrogel component.
The argan emulsion obtained in the step (2) of the embodiment is centrifuged at 5000rpm for 15min without demulsification or delamination.
The argin emulsion in the repairing facial mask of the embodiment is uniformly adhered on the surface of the hydrogel component, and does not flow or gather after being vertically hung for 30 days through sealing; the pressure level of 50kPa is extrusion without leakage, and the product stability is high.
Example 3
The medical cold compress repair mask for the argan oil is prepared by the following method:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion;
(3) Coating the hydrogel component in the step (1) on a silk fiber cloth carrier to obtain a gel layer; and (3) coating the argin emulsion obtained in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin.
The hydrogel component comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000081
the argan oil emulsion comprises the following raw materials in percentage by mass:
Figure BDA0003469651410000082
the coating amount of the argin emulsion is 6% of the mass of the hydrogel component.
The argan emulsion obtained in the step (2) of the embodiment is centrifuged at 5000rpm for 15min without demulsification or delamination.
The argin emulsion in the repairing facial mask of the embodiment is uniformly adhered on the surface of the hydrogel component, and does not flow or gather after being vertically hung for 30 days through sealing; the pressure level of 50kPa is extrusion without leakage, and the product stability is high.
Comparative example 1
In this comparative example, sodium hyaluronate was not added to the preparation of the argan emulsion as in example 1, and the remainder was identical.
The polyglycerol emulsion obtained in this comparative example was tested without breaking or delamination after centrifugation at 5000rpm for 15 min.
The argin emulsion in the repairing facial mask of the comparative example is uniformly adhered on the surface of the hydrogel component, and flows after being vertically hung for 1 day through sealing; the emulsion was squeezed to leak at a pressure level of 50 kPa.
From the above results, it can be seen that the adhesion of the present invention on the surface of the crosslinked hyaluronic acid gel can be significantly enhanced by adding sodium hyaluronate to the argin emulsion.
Comparative example 2
In this comparative example, the preparation of the argan emulsion was carried out without adding lecithin, polypeptide and oil-soluble silicone wax, and the rest was the same.
The polyglycerol emulsion obtained in this comparative example was tested and centrifuged at 5000rpm for 15min to break and separate.
The argin emulsion in the repairing mask of the comparative example is uniformly adhered on the surface of the hydrogel component, and emulsion aggregation occurs after the repairing mask is vertically hung for 5 days through sealing; the emulsion was squeezed to leak at a pressure level of 50 kPa.
From the results, the invention can obviously enhance the stability of the argin emulsion by adding the lecithin, the polypeptide and the oil-soluble silicone wax into the argin emulsion. And has an enhanced stabilizing effect on the adhesion of the crosslinked hyaluronic acid gel surface.
Comparative example 3
In this comparative example, no glycerin was added in the preparation of the argin emulsion, and the rest was the same.
The glycerol-A emulsion obtained by testing the comparative example was demulsified by centrifugation at 5000rpm for 15 min.
The argin emulsion in the repairing mask of the comparative example is uniformly adhered on the surface of the hydrogel component, and emulsion aggregation occurs after the repairing mask is vertically hung for 7 days through sealing; the emulsion was squeezed to leak at a pressure level of 50 kPa.
From the above results, it can be seen that the stability of the argin emulsion can be remarkably enhanced by adding glycerol into the argin emulsion. And has an enhanced stabilizing effect on the adhesion of the crosslinked hyaluronic acid gel surface.
Comparative example 4
In this comparative example, the hydrogel component was prepared without adding crosslinked hyaluronic acid, and the rest was the same.
The argin emulsion in the repairing mask of the comparative example is uniformly adhered on the surface of the hydrogel component, and emulsion aggregation occurs after the repairing mask is vertically hung for 7 days through sealing; the pressure level of 50kPa was squeezed to give gel and emulsion leakage.
From the above results, it can be seen that the present invention can significantly enhance gel strength by adding crosslinked hyaluronic acid to the hydrogel component. And has the function of enhancing and stabilizing the adhesiveness of the argin emulsion on the gel surface.
The above examples are preferred embodiments of the present invention, but the embodiments of the present invention are not limited to the above examples, and any other changes, modifications, substitutions, combinations, and simplifications that do not depart from the spirit and principle of the present invention should be made in the equivalent manner, and the embodiments are included in the protection scope of the present invention.

Claims (8)

1. The preparation method of the medical cold compress repair facial mask of the argan oil is characterized by comprising the following preparation steps:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the alglycerol, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate and glycerol into water, homogenizing and emulsifying to obtain an alglycerol emulsion;
(3) Coating the hydrogel component in the step (1) on a mask-based carrier to obtain a gel layer; then coating the argin emulsion in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin;
the hydrogel component in the step (1) comprises the following raw materials in percentage by mass:
1% -5% of vitamin E;
1% -5% of sodium hyaluronate;
0.5% -3% of ceramide;
3% -10% of 1, 3-butanediol;
1% -6% of water-soluble silicone wax;
0.2% -1% of crosslinked hyaluronic acid;
the balance of water;
the mass percentage of each raw material of the argin emulsion in the step (2) is as follows:
4% -10% of alglycerol
2% -4% of lecithin;
3% -6% of polypeptide;
1% -4% of oil-soluble silicone wax;
1% -5% of sodium hyaluronate;
3% -10% of glycerol;
the balance of water.
2. The preparation method of the medical cold compress repair mask containing the argin is characterized in that the hydrogel component in the step (1) comprises the following raw materials in percentage by mass:
1% -3% of vitamin E;
2% -4% of sodium hyaluronate;
1% -2% of ceramide;
6% -8% of 1, 3-butanediol;
2% -4% of water-soluble silicone wax;
0.2% -0.5% of crosslinked hyaluronic acid;
the balance of water.
3. The preparation method of the medical cold compress repair mask containing the argin oil according to claim 1, wherein the mass percentage of raw materials of the argin oil emulsion in the step (2) is as follows:
6% -8% of alglycerol;
2% -3% of lecithin;
4% -5% of polypeptide;
1% -2% of oil-soluble silicone wax;
2% -4% of sodium hyaluronate;
6% -10% of glycerol;
the balance of water.
4. The method for preparing the medical cold compress repair mask of the argin oil according to claim 1, wherein the coating amount of the argin oil emulsion in the step (3) is 6% -12% of the mass of the hydrogel component.
5. The method for preparing an argin medical cold compress repair mask according to claim 1, wherein the mask-based carrier material in the step (3) is at least one of silk, fruit fiber, tencel, cotton fiber, soybean fiber and viscose fiber.
6. The preparation method of the medical cold compress repair facial mask of the argan oil is characterized by comprising the following preparation steps:
(1) Adding vitamin E, sodium hyaluronate, ceramide, 1, 3-butanediol and water-soluble silica wax into water, stirring and mixing uniformly, adding crosslinked hyaluronic acid, stirring and swelling until the system is semitransparent gel, and obtaining a hydrogel component;
(2) Adding the arginin, lecithin, polypeptide, oil-soluble silica wax, sodium hyaluronate, plant extract and glycerol into water, homogenizing and emulsifying to obtain arginin emulsion;
(3) Coating the hydrogel component in the step (1) on a mask-based carrier to obtain a gel layer; then coating the argin emulsion in the step (2) on a gel layer, and finally, attaching an isolation layer to obtain the medical cold compress repair facial mask of the argin;
the hydrogel component in the step (1) comprises the following raw materials in percentage by mass:
1% -5% of vitamin E;
1% -5% of sodium hyaluronate;
0.5% -3% of ceramide;
3% -10% of 1, 3-butanediol;
1% -6% of water-soluble silicone wax;
0.2% -1% of crosslinked hyaluronic acid;
the balance of water;
the mass percentage of each raw material of the argin emulsion in the step (2) is as follows:
4% -10% of alglycerol
2% -4% of lecithin;
3% -6% of polypeptide;
1% -4% of oil-soluble silicone wax;
1% -5% of sodium hyaluronate;
1% -5% of plant extract;
3% -10% of glycerol;
the balance of water.
7. The method for preparing an argin medical cold compress repair mask according to claim 6, wherein the plant extract comprises at least one of aloe extract, chamomile extract, rose extract, lotus extract, lavender extract, tea extract, peppermint extract, licorice extract, centella extract.
8. An argin medical cold compress repair mask, which is characterized by being prepared by the method of any one of claims 1-7.
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