CN114053180B - 脱毛组合物及其制备方法和应用 - Google Patents
脱毛组合物及其制备方法和应用 Download PDFInfo
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- CN114053180B CN114053180B CN202010762276.9A CN202010762276A CN114053180B CN 114053180 B CN114053180 B CN 114053180B CN 202010762276 A CN202010762276 A CN 202010762276A CN 114053180 B CN114053180 B CN 114053180B
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Abstract
本发明提供一种脱毛组合物及其制备方法和应用，涉及日化用品技术领域。本发明的脱毛组合物包括以下重量份数的原料：增稠剂1.5～5份，乳化剂2～6份，表面活性剂3～6份，脱毛剂3～5份，pH调节剂1～2份，相溶剂0.5～1.5份，物理发泡剂1～5份，水50～70份；所述脱毛剂选自：巯基乙酸钙和巯基乙酸钾中的一种或两种。本发明的脱毛组合物应用于脱毛慕斯，喷出的泡沫细腻、无堆积，不易堵塞喷头，脱毛效果好，对人体刺激性小。
Description
技术领域
本发明涉及日化用品技术领域，特别是涉及一种脱毛组合物及其制备方法和应用。
背景技术
随着社会生活水平的提升，人们对外貌和形象越来越重视，脱毛产品的需求量也不断增加。脱毛慕斯喷雾是利用推进剂将脱毛物料喷出成泡沫状的脱毛产品，使用时，将喷出的泡沫覆盖在皮肤上，停留一定时间后将泡沫擦拭即可。由于其具有使用快捷、清理方便的优点，脱毛慕斯喷雾越来越受到消费者的青睐。
现有的脱毛慕斯一般是将脱毛制剂灌入铝罐内，并在铝罐内填充液化石油气(LPG)，利用液化石油气将囊袋内的脱毛制剂挤出，通过气雾阀门形成泡沫。但是，由于脱毛制剂组合物的配方还不够完善，存在乳化体系不稳定、物料溶解不均匀等问题，导致使用过程中容易出现料液堆积、堵塞喷孔的现象，不仅造成物料的浪费，降低了产品的使用周期，还增加了消费者的经济负担。现有技术中也有通过增大气雾阀门喷头孔径的方法缓解物料堵塞的问题，但是孔径增大又会带来其它问题，例如喷出量过大、喷出不均匀、形成的泡沫过大等，严重影响脱毛效果。
发明内容
基于此，有必要针对上述问题，提供一种脱毛组合物，该组合物的增稠流变体系好，乳化体系稳定，物料溶解性好，经喷出后形成的泡沫细腻、无堆积，不易堵塞喷头，而且脱毛效果好。
一种脱毛组合物，包括以下重量份数的原料：
所述脱毛剂选自：巯基乙酸钙和巯基乙酸钾中的一种或两种。
在现有技术中，为了使脱毛料液在使用时可以被持续喷出，液化石油气填充量要求较大；发明人在实践中发现，液化石油气含量大容易导致喷出的泡沫体积偏大、泡沫内部较虚，泡沫体积相差较大、泡沫形成不均匀，在皮肤上的覆盖均匀度较差，使得脱毛效果不均一。本发明选用的增稠剂皆为非金属复合纳米材料，无机矿物质，具有不被细菌、加热破坏分解，高pH值适用的特点，尤其是机械剪切容易变稀，静置后容易恢复到原料的稠度；本发明选用的乳化剂具有高pH适用性和高效稳泡性，这种增稠剂和乳化剂组合选择使本发明在产品静置时保持一定稠度增加稳定性，料体喷出时经过压力喷出和喷头剪切变稀使其能连续通过更小孔径(0.15mm-0.46mm)的喷头。本发明的脱毛组合物，通过增稠剂和乳化剂原料种类和配比的选择，得到具有高效乳化、稳定增稠和流变改性的体系，减少物理发泡剂的用量，使得组合物料液和物理发泡剂混合更均匀，无需摇晃也可以喷出细腻、稳定的泡沫，泡沫体积相对较小、较实，能绵密地覆盖在皮肤表面，脱毛效果均匀；而且，组合物浆料溶解更均匀，与喷头的材质相容性好，不容易发生堆积堵塞的现象，产品喷出率高。
在其中一个实施例中，所述增稠剂选自：硅酸钠铝镁、硅酸镁钠、硅酸镁锂、硅酸钠镁锂、硅酸镁、氟硅酸镁钠、三硅酸镁中的一种或两种以上。
在其中一个实施例中，所述乳化剂选自：甘油硬脂酸酯、PEG-100甘油硬脂酸酯、鲸蜡醇、PEG-7硬脂酸酯、鲸蜡醇聚醚-20、硬脂醇聚醚-2、硬脂醇聚醚-21、鲸蜡硬脂醇聚醚-6、鲸蜡硬脂醇聚醚-25、鲸蜡硬脂醇、鲸蜡硬脂基葡糖苷、鲸蜡硬脂醇聚醚-20、鲸蜡硬脂醇聚醚-12、鲸蜡硬脂醇聚醚-20中的一种或两种以上。
在其中一个实施例中，所述表面活性剂选自：月桂醇聚醚硫酸酯钠、月桂醇聚醚硫酸酯铵、椰油酰胺丙基甜菜碱、月桂酰胺丙基甜菜碱、月桂酰胺丙基羟磺基甜菜碱、C12-16烷基葡糖苷、棕榈仁油酰胺DEA、椰油酰胺MEA中的一种或两种以上。
在其中一个实施例中，所述pH调节剂选自：氢氧化钾和氢氧化钙中的一种或两种。相比于采用氢氧化钠作为pH调节剂，使用氢氧化钾或氢氧化钙作为pH调节剂，产品的碱腐蚀性更小，对皮肤的刺激性也更小。
在其中一个实施例中，所述相溶剂选自：乙醇。优选地，相溶剂选用95％乙醇溶液。一般发泡剂为丁烷，不溶于水，但可溶于醇类。
在其中一个实施例中，所述发泡剂选自：丁烷和丙烷中的一种或两种
在其中一个实施例中，所述脱毛组合物还包括以下质量百分比的原料：
保湿剂 3～15份，
皮肤调理剂 0.1～5份，
抗敏剂 0.1～5份。
在其中一个实施例中，所述脱毛组合物还包括香精0.1～0.5wt％。优选地，所述香精选自：哈密瓜香、青瓜香、栀子花香等。
在其中一个实施例中，所述保湿剂选自：甘油、丙二醇、矿油、角鲨烷、聚二甲基硅氧烷。
在其中一个实施例中，所述皮肤调理剂选自：尿囊素、海藻糖、生育酚乙酸酯、尿素、互生叶白千层叶油中的一种或两种以上。
在其中一个实施例中，所述抗敏剂选自：红没药醇和甜扁桃提取物中的一种或两种。抗敏剂可以减少皮肤敏感。
本发明一方面还提供一种上述脱毛组合物的制备方法，包括以下步骤：
S1、将增稠剂、乳化剂混合均匀，均质，过滤；
S2、向步骤S1所得体系中加入表面活性剂，混合均匀，均质，加入脱毛剂，混合均匀，均质；
S3、向步骤S2所得体系中加入pH调节剂，混合均匀，加入其它原料，混合均匀，得组合物浆料；
S4、将物理发泡剂和步骤S3所得的组合物浆料同时进行混合灌装，即得脱毛组合物。
上述制备方法得到的脱毛组合物，降低了物理发泡剂的使用量，使组合物浆料和物理发泡剂混合更均匀，体系更稳定和高效，应用于脱毛慕斯时，喷出的泡沫细腻、均匀，泡沫体积较小、较实，可以绵密地覆盖在皮肤表面，基本能脱除覆盖区域所有的毛发，脱毛效果好、均匀度高；脱毛组合物溶解更均匀，与喷头的材质相容性好，不容易发生堆积堵塞的现象，产品喷出率高。
本发明一方面还提供一种上述脱毛组合物在制备脱毛慕斯中的应用。
本发明另一方面还提供一种脱毛慕斯喷雾，该脱毛慕斯喷雾包括罐体和气雾阀门；所述罐体内设置有密封的囊袋，所述囊袋内填充有发泡剂和上述脱毛组合物；所述罐体和所述囊袋之间的夹层内填充有压缩空气；所述囊袋内设有引料管，所述引料管的一端伸入所述囊袋内，所述引料管的另一端伸出所述囊袋与所述气雾阀门连接；所述气雾阀门连接喷头，通过按压所述气雾阀门可以挤压所述囊袋使脱毛组合物沿所述引料管从所述喷头喷出。
上述脱毛慕斯喷雾，采用二元包装，即在罐体内增设囊袋，囊袋内填充脱毛组合物和少量物理发泡剂，使脱毛组合物和物理发泡剂能够均匀混合，并在囊袋和罐体的夹层内填充压缩空气，压缩空气可以挤压囊袋使脱毛组合物喷出，形成细腻、均匀的泡沫，泡沫体积较小、较实，可以绵密地覆盖在皮肤表面，基本能脱除覆盖区域所有的毛发，脱毛效果好、均匀度高；脱毛组合物溶解更均匀，与喷头的材质相容性好，不容易发生堆积堵塞的现象，产品喷出率高。
在其中一个实施例中，所述囊袋选用四层真空囊袋。四层真空囊袋安全性较高。
与现有技术相比，本发明具有以下有益效果：
本发明的脱毛组合物，通过增稠剂、流变改性剂和乳化剂原料种类和配比的选择，得到具有高效乳化、稳定增稠和流变改性的体系，减少物理发泡剂的用量，使得组合物料液和物理发泡剂混合更均匀，无需摇晃也可以喷出细腻、稳定的泡沫，泡沫体积相对较小、较实，能绵密地覆盖在皮肤表面，脱毛效果均匀；而且，组合物浆料溶解更均匀，与喷头的材质相容性好，不容易发生堆积堵塞的现象，产品喷出率高。该脱毛组合物应用于脱毛慕斯喷雾，可以具有泡沫绵密，脱毛效果好，刺激性小，喷出时不易堵塞的优点。
附图说明
图1为现有的脱毛喷雾的包装示意图；
图2为实施例的脱毛喷雾的包装示意图。
图中，100、罐体；110、夹层；200、囊袋；210、引料管；300、气雾阀门；400、喷头；500、脱毛组合物。
具体实施方式
为了便于理解本发明，以下将给出较佳实施例对本发明进行更全面的描述。但是，本发明可以以许多不同的形式来实现，并不限于本文所描述的实施例。相反地，提供这些实施例的目的是使对本发明的公开内容的理解更加透彻全面。
除非另有定义，本文所使用的所有的技术和科学术语与属于本发明的技术领域的技术人员通常理解的含义相同。本文中在本发明的说明书中所使用的术语只是为了描述具体的实施例的目的，不是旨在于限制本发明。本文所使用的术语“和/或”包括一个或多个相关的所列项目的任意的和所有的组合。
实施例1
一种脱毛组合物，由表1所示原料制备而成，具体通过以下方法制备得到：
(1)在反应容器中加入水，加热升温至83℃，加入甘油和尿囊素，搅拌均匀；
(2)将乳化剂和增稠剂加入至反应容器中，搅拌均匀，3000rpm均质5min，20Hz超声保温15min，用400目滤布抽滤，保留滤液，将滤液转移至真空乳化锅；
(3)将表面活性剂加入真空乳化锅中，2000rpm均质4min，开启降温；
(4)待降温至50℃，停止搅拌，加入事先均质好的巯基乙酸钙水溶液，2000rpm均质3min；
(5)待降温至45℃，向加入事先溶解好的pH调节剂，搅拌均匀；
(6)待冷却至40℃，加入其余原料，搅拌均匀，得组合物浆料；
(7)将组合物浆料和物理发泡剂定量灌装到囊袋中，密封，即得。
将上述脱毛组合物制成脱毛慕斯，脱毛慕斯包括罐体100和气雾阀门300，罐体100可以使用铝罐；罐体100内设置有密封的囊袋200，囊袋200内填充有步骤(7)中的脱毛组合物500；罐体100和囊袋200之间的夹层内填充有压缩空气；囊袋200内设有引料管210，引料管210的一端伸入囊袋200内，引料管210的另一端伸出囊袋200与气雾阀门300连接；气雾阀门300连接喷头400，通过按压所述气雾阀门300可以挤压囊袋200，使脱毛组合物500沿引料管210从喷头400喷出。
实施例2
一种脱毛组合物，与实施例1的区别在于原料和配比不同，具体如表1所示。将该脱毛组合物制作成脱毛慕斯，制作方法与实施例1的方法相同。
实施例3
一种脱毛组合物，与实施例1的区别在于原料和配比不同，具体如表1所示。将该脱毛组合物制作成脱毛慕斯，制作方法与实施例1的方法相同。
实施例4
一种脱毛组合物，与实施例1的区别在于原料和配比不同，具体如表1所示。将该脱毛组合物制作成脱毛慕斯，制作方法与实施例1的方法相同。
实施例5
一种脱毛组合物，与实施例1的区别在于原料和配比不同，具体如表1所示。将该脱毛组合物制作成脱毛慕斯，制作方法与实施例1的方法相同。
实施例1-5的脱毛组合物原料种类和含量如表1所示：
表1.实施例1-5的脱毛组合物原料和含量(含量单位为wt％)
对比例1-6
对比例1-6的脱毛组合物原料种类和含量如表2所示，制作方法与实施例1的方法基本相同。
表2.对比例1-6的脱毛组合物原料和含量(含量单位为wt％)
实验例1
对实施例和对比例的脱毛慕斯进行测试，测试方法如下：
(1)泡沫大小检测：将脱毛慕斯喷涂于载玻片上，立刻放置于显微镜上观察并测量泡沫尺寸，放置8min后用显微镜观察并测量泡沫尺寸；
(2)泡沫状态检测：将脱毛慕斯喷涂于载玻片上，划定1×1cm2的范围，用显微镜计量该范围表层的泡沫数量；当泡沫数量≥100个/cm2时，判定为细腻；当泡沫数量＜50个/cm2时，判定为不细腻；
(3)pH稳定性测试：在不同时间测试用pH测试仪测试浆组合物浆料的pH值，当pH变化值≤0.2时，判定为pH值稳定；
(4)脱毛效果测试：将脱毛慕斯喷涂于人手臂，记录脱毛时间；
(5)刺激性测试：随机选择20位测试者，在手臂四个位置分别喷涂脱毛慕斯，8min后记录测试者的刺激性感受，统计有刺激性感受的人数；
(6)喷孔堆积率测试：按压脱毛慕斯罐体上的阀门100次，统计阻塞次数；
(7)喷出率：按压脱毛慕斯罐体上的阀门，直至无法再按压出料体，计算喷出的料体重量和占比。
(8)稳定性：把产品分别放在(40±2)℃和(-5±2)℃，24h后恢复至室温观察稳定性。
测试结果如下表所示：
表3.脱毛慕斯测试结果
从上表可以看出，本发明实施例的脱毛慕斯泡沫小、尺寸均匀，喷出后8min泡沫尺寸变化小，泡沫细腻程度高；产品的pH约为12.15～12.23，pH值较为稳定，变化值较小；8min即可达到较好的脱毛效果；刺激性小；几乎无喷头堵塞现象，产品喷出率大于97％，利用率较高。
相比之下，对比例1由于未添加增稠剂，导致料体过稀且容易分层，制作成成品喷出来的慕斯泡沫不够稠密，流动性大，皮肤吸附性差，影响脱毛体验感，而且料体不稳定且有一定刺激性。对比例2中表面活性化剂含量过高，导致产品喷出来后慕斯泡沫过多，直径偏大，而且不稳泡，喷出来的脱毛剂相对含量偏少，脱毛效果变差。对比例3由于乳化剂添加量不足，容易导致产品稳泡性能差，稳泡时间不够，3分钟后泡沫容易消失，达不到8分钟的脱毛等待时间，影响脱毛效果。对比例4中发泡剂气体比例过大，导致泡沫不够稠密，泡沫直径大，而且稳泡性差，脱毛剂与皮肤接触面减少，影响脱毛效果。对比例2～4产品的泡沫都不够细腻，脱毛时间均大于10分钟。对比例5未添加相溶剂，导致发泡剂气体与料体溶合不好，一般添加发泡剂为灌装料体后充气，不添加相溶剂容易导致气体与料体分别喷出来，无法达到混合慕斯状喷出来的效果；同理，若不添加发泡剂气体作发泡剂，则只形成脱毛喷雾，达不到慕斯的细腻泡沫体验效果；对比例5的产品后期不发泡且刺激性较大。对比例6未选用合适的增稠剂与乳化剂组合物，得出的料体制作成成品通过0.46mm孔径的喷头并不能达到剪切变稀的效果，也不能形成喷雾状态，而是呈线型喷出，而且料体不能通过0.15mm孔径的喷头，阻塞喷头无法喷出。
综上所述，本发明实施例的脱毛慕斯在稳定性、温和性、喷出率以及泡沫细腻性都优于对比例。
以上所述实施例的各技术特征可以进行任意的组合，为使描述简洁，未对上述实施例中的各个技术特征所有可能的组合都进行描述，然而，只要这些技术特征的组合不存在矛盾，都应当认为是本说明书记载的范围。
以上所述实施例仅表达了本发明的几种实施方式，其描述较为具体和详细，但并不能因此而理解为对发明专利范围的限制。应当指出的是，对于本领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干变形和改进，这些都属于本发明的保护范围。因此，本发明专利的保护范围应以所附权利要求为准。
Claims (7)
1.一种脱毛组合物，其特征在于，包括以下重量份数的原料：
增稠剂1.5~5份，
乳化剂2~6份，
表面活性剂3~6份，
脱毛剂3~5份，
pH调节剂1~2份，
相溶剂0.5~1.5份，
物理发泡剂1~5份，
水50~70份；
所述脱毛剂选自：巯基乙酸钙和巯基乙酸钾中的一种或两种；
所述增稠剂选自：硅酸钠镁锂；
所述乳化剂选自：甘油硬脂酸酯、PEG-100甘油硬脂酸酯、硬脂醇聚醚-2、硬脂醇聚醚-21、鲸蜡硬脂醇聚醚-6、鲸蜡硬脂醇聚醚-25、鲸蜡硬脂醇、鲸蜡硬脂醇聚醚-20中的一种或两种以上；
所述表面活性剂选自：月桂醇聚醚硫酸酯钠、月桂酰胺丙基羟磺基甜菜碱、C12-16 烷基葡糖苷中的一种或两种以上；
所述相溶剂选自：乙醇。
2.根据权利要求1所述的脱毛组合物，其特征在于，所述pH调节剂选自：氢氧化钾和氢氧化钙中的一种或两种；
所述物理发泡剂选自：丁烷和丙烷中一种或两种以上。
3.根据权利要求1~2任一项所述的脱毛组合物，其特征在于，所述脱毛组合物还包括以下重量份数的原料：
保湿剂3~15份，
皮肤调理剂0.1~5份，
抗敏剂0.1~5份。
4.根据权利要求3所述的脱毛组合物，其特征在于，所述保湿剂选自：甘油、丙二醇、矿油、角鲨烷、聚二甲基硅氧烷；
所述皮肤调理剂选自：尿囊素、海藻糖、生育酚乙酸酯、尿素、互生叶白千层叶油中的一种或两种以上；
所述抗敏剂选自：红没药醇和甜扁桃提取物中的一种或两种。
5.一种如权利要求3~4任一项所述的脱毛组合物的制备方法，其特征在于，包括以下步骤：
S1、将增稠剂、乳化剂混合均匀，均质，过滤；
S2、向步骤S1所得体系中加入表面活性剂，混合均匀，均质，加入脱毛剂，混合均匀，均质；
S3、向步骤S2所得体系中加入pH调节剂，混合均匀，加入保湿剂、抗敏剂、皮肤调理剂、香精、相溶剂、水，混合均匀，得组合物浆料；
S4、将物理发泡剂和步骤S3所得的组合物浆料同时进行混合灌装，即得脱毛组合物。
6.一种如权利要求1~4任一项所述的脱毛组合物在制备脱毛慕斯中的应用。
7.一种脱毛慕斯，其特征在于，包括罐体和气雾阀门；所述罐体内设置有密封的囊袋，所述囊袋内填充有如权利要求1~4任一项所述的脱毛组合物；所述罐体和所述囊袋之间的夹层内填充有压缩空气；所述囊袋内设有引料管，所述引料管的一端伸入所述囊袋内，所述引料管的另一端伸出所述囊袋与所述气雾阀门连接；所述气雾阀门连接喷头，通过按压所述气雾阀门挤压所述囊袋使脱毛组合物沿所述引料管从所述喷头喷出。
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