CN113768829A - High-foaming shower gel and preparation method thereof - Google Patents

High-foaming shower gel and preparation method thereof Download PDF

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Publication number
CN113768829A
CN113768829A CN202111275798.7A CN202111275798A CN113768829A CN 113768829 A CN113768829 A CN 113768829A CN 202111275798 A CN202111275798 A CN 202111275798A CN 113768829 A CN113768829 A CN 113768829A
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China
Prior art keywords
stirring
parts
surfactant
essential oil
body wash
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CN202111275798.7A
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Chinese (zh)
Inventor
戴钰诚
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Yangzhou Yongchun Tourism Products Factory
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Yangzhou Yongchun Tourism Products Factory
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Priority to CN202111275798.7A priority Critical patent/CN113768829A/en
Publication of CN113768829A publication Critical patent/CN113768829A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/362—Polycarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A61K8/416—Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/596—Mixtures of surface active compounds

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical & Material Sciences (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to the technical field of preparation of daily necessities, in particular to high-foam shower gel and a preparation method thereof. The shower gel consists of lemon grass essential oil, basil essential oil, sweet wormwood oil, an anionic surfactant, a zwitterionic surfactant, a nonionic surfactant, a preservative, a humectant, a metal chelating agent, an organic acid and water. According to the invention, by adding dodecyl dimethyl amine oxide and disodium cocoyl amphoteric diacetate, both of which are zwitterionic surfactants, and using the two surfactants in a compatible manner, the use of anionic surfactants can be reduced, so that the skin irritation is reduced; secondly, the compatibility of the two components can enhance the stability of the shower gel, and the skin cleaning effect is good; in addition, the compatibility of the two can increase the amount of foam generated during friction, the foaming performance is excellent, the foam is rich, and the use comfort is improved.

Description

High-foaming shower gel and preparation method thereof
Technical Field
The invention relates to the technical field of preparation of daily necessities, in particular to high-foam shower gel and a preparation method thereof.
Background
For shower gel, the irritation is mainly caused by the contained surfactant, the skin application test shows that the irritation of the active agent is generally cationic active agent > anionic active agent > zwitterionic active agent ≈ nonionic active agent, and the anion active agent is used in the largest amount in the shower gel. The irritation or sensitization of the surfactant to the skin or mucosa is mainly caused by the following three factors: (ii) dissolution: the surfactant has the function of dissolving out moisture-retaining components, intercellular lipid and free amino acids and fat in the horny layer of the skin, and the dissolving-out of the components can cause the surface layer of the skin to be damaged, the water-retaining capacity of the skin to be reduced, and finally, skin cells are formed into scurf to fall off, thereby causing the skin to be tight, irritated or dry. Penetration property: the surfactant has the ability to penetrate through the skin, and this ability has been confirmed to be one of the causes of various inflammations of the skin. The penetration of the surfactant changes the original structural state of the skin and the compatibility between adjacent molecules, thereby causing skin irritation and even causing anaphylactic reaction, and causing the skin to have erythema and edema. ③ reactivity: the surfactant has effects of adsorbing protein, denaturing protein, and changing skin pH condition.
Based on the above three factors, it is possible to reduce the irritation of the surfactant by adding some substance in combination with the anionic surfactant to increase the micelle of the surfactant and reduce the penetrability thereof. Such as johnson corporation, effectively reduce the irritation of cleansing products to the skin and eyes by adding hydrophobically modified acrylic polymers, hydrophobically modified cellulose, hydrophobically modified starch to personal cleansing type cleansing products. But this reduction in irritation is accompanied by an inevitable sacrifice in the foaming or foam stabilizing properties of the cleaning product portion. .
Based on the situation, the invention provides the high-foaming shower gel and the preparation method thereof, and the problems can be effectively solved.
Disclosure of Invention
The invention aims to provide high-foaming shower gel and a preparation method thereof.
In order to achieve the purpose, the invention provides high-foam shower gel which is composed of lemon grass essential oil, basil essential oil, sweet wormwood oil, an anionic surfactant, a zwitterionic surfactant, a nonionic surfactant, a preservative, a humectant, a metal chelating agent, an organic acid and water.
Preferably, the shower gel consists of the following raw materials in parts by weight: 10-20 parts of lemon grass essential oil, 10-20 parts of basil essential oil, 30-60 parts of sweet wormwood oil, 30-40 parts of anionic surfactant, 25-45 parts of zwitterionic surfactant, 10-20 parts of nonionic surfactant, 2-6 parts of preservative, 2-6 parts of humectant, 1-3 parts of metal chelating agent, 1-3 parts of organic acid and 120-160 parts of water.
Preferably, the anionic surfactant is an N-acyl amino acid salt; the N-acyl amino acid salt comprises at least one or more of cocoyl sarcosinate, cocoyl sarcosinate TEA, lauroyl sarcosinate and salts thereof, myristoyl sarcosinate, palmitoyl sarcosinate, oleoyl sarcosinate and lauroyl methyl aminopropionate.
Preferably, the anionic surfactant is lauroyl methyl aminopropionate, which is a sodium salt.
Preferably, the zwitterionic surfactant is at least one or a combination of more than two of lecithin, betaine derivatives, imidazoline compounds, alkyl amine oxides and carboxylate.
Preferably, the zwitterionic surfactant is a combination of an alkylamine oxide which is dodecyldimethylamine oxide and an imidazoline compound which is disodium cocoamphodiacetate.
Preferably, the nonionic surfactant is at least one or a combination of more than two of polyoxyethylene alkyl alcohol amide, polyoxyethylene alkylamine, polyoxyethylene fatty acid ester, alkylphenol polyoxyethylene ether, long-chain fatty alcohol polyoxyethylene ether, polyoxypropylene-polyoxyethylene copolymer and alkanolamide.
Preferably, the nonionic surfactant is an alkanolamide, which is cocoyl monoethanolamine.
Preferably, the preservative comprises one or a combination of more than two of methylisothiazolinone, nipagin ester, methyl hydroxybenzoate and ethyl hydroxybenzoate.
Preferably, the preservative is ethylparaben.
Preferably, the humectant comprises one or a combination of more than two of simethicone, glycerol, propylene glycol and butanediol.
Preferably, the humectant is dimethicone.
Preferably, the metal chelating agent is an aminocarboxylic acid; the aminocarboxylic acid is one of ethylenediamine tetraacetic acid, aminotriacetic acid and diethylenetriamine pentaacetic acid.
Preferably, the metal chelating agent is ethylenediaminetetraacetic acid.
Preferably, the organic acid is salicylic acid.
The invention also provides a preparation method of the high-foaming shower gel, which comprises the following steps:
(1) mixing lemon grass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate, dodecyl dimethyl amine oxide and disodium cocoyl amphoteric diacetic acid, heating and stirring uniformly, wherein the stirring temperature is 80-85 ℃, the stirring time is 10-15 min, and the stirring speed is 1000-1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 70-75 ℃, stirring at a constant temperature for 30-40 min, and the stirring speed is 2000-2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling for 30-40 ℃ while stirring, stirring at the speed of 1500-1700 r/min for 5-8 min, and standing for defoaming to obtain the product.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, by adding dodecyl dimethyl amine oxide and disodium cocoyl amphoteric diacetate, both of which are zwitterionic surfactants, and using the two surfactants in a compatible manner, the use of anionic surfactants can be reduced, so that the skin irritation is reduced; secondly, the compatibility of the two components can enhance the stability of the shower gel, and the skin cleaning effect is good; in addition, the compatibility of the two can increase the amount of foam generated during friction, the foaming performance is excellent, the foam is rich, and the use comfort is improved.
2. The raw materials of the invention are sufficient in China and proper in price, so that the large-scale production of the invention is not limited by too high cost; meanwhile, the preparation method is simple, the total production cost is low, and the industrial large-scale production is facilitated.
Detailed Description
Examples1
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing lemongrass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate, dodecyl dimethyl amine oxide and disodium cocoyl amphodiacetate, heating and stirring uniformly at 80 ℃ for 15min at 1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 70 ℃, and stirring at a constant temperature for 40min, and the stirring speed is 2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling for 30 ℃ while stirring, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the defoaming agent.
Examples2
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing lemongrass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate, dodecyl dimethyl amine oxide and disodium cocoyl amphodiacetate, heating and stirring uniformly at 85 ℃ for 10min at the stirring speed of 1000 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 75 ℃, and stirring at a constant temperature for 30min, wherein the stirring speed is 2000 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling to 40 ℃ while stirring, stirring for 5min at the stirring speed of 1500r/min, and standing for defoaming to obtain the product.
Examples3
The specific raw materials were weighed as in table 1, and the remaining steps were as follows:
(1) mixing lemongrass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate, dodecyl dimethyl amine oxide and disodium cocoyl amphodiacetate, heating and stirring uniformly at 85 ℃ for 15min at 1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 75 ℃, and stirring at a constant temperature for 40min at the stirring speed of 2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling to 40 ℃ while stirring, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Comparative example1
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) mixing lemongrass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl amino propionate and dodecyl dimethyl amine oxide, heating and stirring uniformly, wherein the stirring temperature is 85 ℃, the stirring time is 15min, and the stirring speed is 1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 75 ℃, and stirring at a constant temperature for 40min at the stirring speed of 2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling to 40 ℃ while stirring, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
Comparative example2
The specific raw materials were weighed as in table 1, and the preparation steps were as follows:
(1) mixing lemongrass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate and disodium cocoyl amphodiacetate, heating and stirring uniformly, wherein the stirring temperature is 85 ℃, the stirring time is 15min, and the stirring speed is 1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 75 ℃, and stirring at a constant temperature for 40min at the stirring speed of 2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling to 40 ℃ while stirring, stirring for 8min at the stirring speed of 1700r/min, and standing for defoaming to obtain the product.
TABLE 1
Kind of material Example 1 Example 2 Example 3 Comparative example 1 Comparative example 2
Lemon grass essential oil 10 15 20 20 20
Basil essential oil 10 15 20 20 20
Sweet wormwood oil 30 45 60 60 60
Sodium lauroyl methylaminopropionate 30 35 40 40 40
Dodecyl dimethyl amine oxide 15 20 25 45 /
Cocoiloyl amphodiacetic acid disodium salt 10 15 20 / 45
Coconut oil acyl monoethanolamine 10 15 20 20 20
Dimethyl silicone oil 2 4 6 6 6
Hydroxyphenyl Ethyl ester 2 4 6 6 6
Ethylenediaminetetraacetic acid 1 2 3 6 6
Salicylic acid 1 2 3 3 3
Deionized water 120 140 160 160 160
Example 4 Performance testing
And (3) stability testing: the shower gels prepared in examples 1 to 3 and comparative examples 1 to 2 were used, and 10 parallel samples were set for each sample. The samples are sequentially placed at 50 ℃, 40 ℃, 26 ℃ and-4 ℃ for one week respectively, and then are taken out to observe whether the shower gel has the phenomena of layering, turbidity, discoloration and peculiar smell. And recording the number of samples with layering, turbidity, color change and peculiar smell.
And (3) testing the foaming force: with reference to GB/T7462-.
The test results are shown in Table 2.
Table 2 results of performance testing
Stability of Foaming power (mm)
Example 1 0 192
Example 2 0 190
Example 3 0 194
Comparative example 1 1 125
Comparative example 2 7 139
The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and its practical application to enable one skilled in the art to make and use various exemplary embodiments of the invention and various alternatives and modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.

Claims (9)

1. The high-foaming shower gel is characterized by comprising the following raw materials in parts by weight: 10-20 parts of lemon grass essential oil, 10-20 parts of basil essential oil, 30-60 parts of sweet wormwood oil, 30-40 parts of anionic surfactant, 25-45 parts of zwitterionic surfactant, 10-20 parts of nonionic surfactant, 2-6 parts of preservative, 2-6 parts of humectant, 1-3 parts of metal chelating agent, 1-3 parts of organic acid and 120-160 parts of water.
2. The body wash of claim 1, wherein the anionic surfactant is an N-acyl amino acid salt; preferably, the N-acyl amino acid salt comprises at least one of cocoyl sarcosinate, cocoyl sarcosinate TEA, lauroyl sarcosinate and salts thereof, myristoyl sarcosinate, palmitoyl sarcosinate, oleoyl sarcosinate, lauroyl methylaminopropionate or a combination of two or more thereof.
3. The body wash of claim 2, wherein the anionic surfactant is lauroyl methyl aminopropionate, which is a sodium salt.
4. The body wash of claim 1, wherein the zwitterionic surfactant is at least one of lecithin, betaine derivatives, imidazoline compounds, alkylamine oxides, and carboxylates, or a combination of two or more thereof.
5. The body wash of claim 4, wherein the zwitterionic surfactant is a combination of an alkylamine oxide which is dodecyldimethylamine oxide and an imidazoline compound which is disodium cocoamphodiacetate.
6. The body wash of claim 1, wherein the nonionic surfactant is at least one of polyoxyethylene alkylolamides, polyoxyethylene alkylamines, fatty acid polyoxyethylene esters, alkylphenol ethoxylates, long-chain fatty alcohol polyoxyethylene ethers, polyoxypropylene-polyoxyethylene copolymers, and alkanolamides, or a combination of two or more thereof.
7. The body wash of claim 6, wherein the non-ionic surfactant is an alkanolamide, and the alkanolamide is cocoyl monoethanolamine.
8. The body wash of claim 1, wherein the preservative is ethylparaben; the humectant is dimethyl silicone oil; the metal chelating agent is ethylenediamine tetraacetic acid; the organic acid is salicylic acid.
9. A method of preparing the body wash of any one of claims 1 to 8, comprising the steps of:
(1) mixing lemon grass essential oil, basil essential oil and sweet wormwood oil with sodium lauroyl methyl aminopropionate, dodecyl dimethyl amine oxide and disodium cocoyl amphoteric diacetic acid, heating and stirring uniformly, wherein the stirring temperature is 80-85 ℃, the stirring time is 10-15 min, and the stirring speed is 1000-1500 r/min;
(2) sequentially adding the cocoyl monoethanolamine and the salicylic acid into the mixture obtained in the step (1), uniformly stirring, adding water while stirring, wherein the stirring temperature is 70-75 ℃, stirring at a constant temperature for 30-40 min, and the stirring speed is 2000-2500 r/min;
(3) and (3) cooling to below 50 ℃, sequentially adding the dimethyl silicone oil, the ethylparaben and the ethylenediamine tetraacetic acid into the mixture obtained in the step (2), uniformly stirring, cooling for 30-40 ℃ while stirring, stirring at the speed of 1500-1700 r/min for 5-8 min, and standing for defoaming to obtain the product.
CN202111275798.7A 2021-10-29 2021-10-29 High-foaming shower gel and preparation method thereof Pending CN113768829A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020177535A1 (en) * 2001-02-06 2002-11-28 Playtex Products, Inc. Cleansing compositions with milk protein and aromatherapy
CN105147538A (en) * 2015-09-21 2015-12-16 江苏素问化妆品有限公司 Transparent bathing mousse free of silicone oil and preparation method thereof
CN105726423A (en) * 2016-05-11 2016-07-06 于文 Multifunctional concentrated cleaner for pets and preparation method thereof
CN113509414A (en) * 2021-06-17 2021-10-19 广东菁萃生物科技有限公司 Antibacterial and anti-inflammatory shower gel and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020177535A1 (en) * 2001-02-06 2002-11-28 Playtex Products, Inc. Cleansing compositions with milk protein and aromatherapy
CN105147538A (en) * 2015-09-21 2015-12-16 江苏素问化妆品有限公司 Transparent bathing mousse free of silicone oil and preparation method thereof
CN105726423A (en) * 2016-05-11 2016-07-06 于文 Multifunctional concentrated cleaner for pets and preparation method thereof
CN113509414A (en) * 2021-06-17 2021-10-19 广东菁萃生物科技有限公司 Antibacterial and anti-inflammatory shower gel and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
国家食品药品监督管理总局: "《化妆品安全技术规范》" *

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