CN113756092A - 一种耐水洗抗菌面料及其制备方法 - Google Patents

一种耐水洗抗菌面料及其制备方法 Download PDF

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CN113756092A
CN113756092A CN202111082856.4A CN202111082856A CN113756092A CN 113756092 A CN113756092 A CN 113756092A CN 202111082856 A CN202111082856 A CN 202111082856A CN 113756092 A CN113756092 A CN 113756092A
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fabric
washable
antibacterial
cloth
water
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洪朝坑
刘宁
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Anhui Dongjin Clothing Co ltd
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Abstract

本发明涉及一种耐水洗抗菌面料及其制备方法，属于纺织面料技术领域，该耐水洗抗菌面料包括耐水洗抗菌布料、防静电布料和柔性布料，耐水洗抗菌物中环氧基的三元环张力很大，在碱性条件下，棉纤纤维分子上的羟基失去质子变成氧负离子，作为亲核试剂攻击环氧基中呈现正电性的碳原子，三元环打开，生成醚键和羟基，生成的羟基和环氧基继续反应，这样会产生交联反应，使得抗菌剂与布料纤维之间的结合更加牢固，最终耐水洗抗菌面料更耐水洗。

Description

一种耐水洗抗菌面料及其制备方法
技术领域
本发明属于纺织面料技术领域，涉及一种耐水洗抗菌面料及其制备方法。
背景技术
针织面料是利用织针将纱线弯曲成圈并相互串套而成的织物。针织面料与梭织面料的不同之处在于纱线在织物中的形态不同。针织面料具有质地柔软、吸湿透气、优良的弹性与延展性及其可生产性等特点，广泛应用于服装面料及里料，家纺等产品中，受到广大消费者的喜爱。
随着人们生活水平的提高，人们对针织面料的要求越来越高，纯棉类的针织面料穿着时，存在如下问题：
(1)人体在大量出汗的情况下，会使纯棉针织面料吸收大量的汗液后变湿变重，导湿和放湿速度变慢，汗液残留在服装和皮肤上，极易出现异味，甚至滋生细菌，进而影响身体健康；
(2)水洗的次数过多会对面料经常磨损。
发明内容
本发明的目的在于提供一种耐水洗抗菌面料及其制备方法。
本发明的目的可以通过以下技术方案实现：
一种耐水洗抗菌面料，包括耐水洗抗菌布料、防静电布料和柔性布料，所述耐水洗抗菌布料通过如下步骤制备：
步骤一：往反应釜内加入聚六亚甲基胍盐酸盐和二甲基亚砜，随后加入去离子水，超声辅助溶解1h，随后往反应釜加入丙三醇三缩水甘油醚，在50℃-60℃的水浴条件下，反应5h，制得混合液A；
步骤二：往混合液A内倒入丙酮，搅拌反应30-40min后放入离心机中，控制离心机转速为3000-4000r/min，离心10min，倒去上层清液，随后继续用丙酮洗涤2-4次，制得耐水洗抗菌物；
步骤三：将耐水洗抗菌物加入到去离子水中，随后加入无水碳酸钾，搅拌30min，制得碱性耐水洗抗菌物，将布料浸泡在碱性耐水洗抗菌物内，浸泡1h，控制温度为50℃，取出、干燥，制得耐水洗抗菌布料。
作为本发明的一种耐水洗抗菌面料优选技术方案，所述聚六亚甲基胍盐酸盐、二甲基亚砜、去离子水和丙三醇三缩水甘油醚的用量比为1.78g：5.71mL：50.00mL：2.53mL。
作为本发明的一种耐水洗抗菌面料优选技术方案，所述混合液A与丙酮的体积比为1：2.5。
作为本发明的一种耐水洗抗菌面料优选技术方案，所述耐水洗抗菌物、去离子水和无水碳酸钾的用量比为10.58mL：40.00mL：0.13g。
作为本发明的一种耐水洗抗菌面料优选技术方案，所述防静电布料是由涤纶纤维与不锈钢纤维混纺纱线编织形成。
作为本发明的一种耐水洗抗菌面料优选技术方案，所述柔性布料是由亲水性纤维编织形成。
作为本发明的一种耐水洗抗菌面料的制备方法优选技术方案，具体包括如下步骤：
步骤一：制备耐水洗抗菌布料；
步骤二：制备防静电布料：
步骤三：制备柔性布料；
步骤四：将耐水洗抗菌布料、防静电布料、柔性布料依次叠放，使用缝纫机进行面料缝制，最后制得耐水洗抗菌面料。
本发明的有益效果：
(1)本发明耐水洗抗菌物中环氧基的三元环张力很大，在碱性条件下，棉纤纤维分子上的羟基失去质子变成氧负离子，作为亲核试剂攻击环氧基中呈现正电性的碳原子，三元环打开，生成醚键和羟基，生成的羟基和环氧基继续反应，这样会产生交联反应，使得抗菌剂与布料纤维之间的结合更加牢固，最终耐水洗抗菌面料更耐水洗。
(2)本发明聚六亚甲基胍盐酸盐中的胍基有很高的活性，使制备的耐水洗抗菌物呈正电性，通常能吸附呈负电性的各类细菌、病毒，从而起到良好的抗菌效果。
具体实施方式
下面将结合实施例对本发明的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其它实施例，都属于本发明保护的范围。
实施例1
耐水洗抗菌布料通过如下步骤制备：
步骤一：控制聚六亚甲基胍盐酸盐、二甲基亚砜、去离子水和丙三醇三缩水甘油醚的用量比为1.78g：5.71mL：50.00mL：2.53mL，往反应釜内加入聚六亚甲基胍盐酸盐和二甲基亚砜，随后加入去离子水，超声辅助溶解1h，随后往反应釜加入丙三醇三缩水甘油醚，在50℃的水浴条件下，反应5h，制得混合液A；
步骤二：控制混合液A与丙酮的体积比为1：2.5，往混合液A内倒入丙酮，搅拌反应30min后放入离心机中，控制离心机转速为3000r/min，离心10min，倒去上层清液，随后继续用丙酮洗涤2次，制得耐水洗抗菌物；
步骤三：控制耐水洗抗菌物、去离子水和无水碳酸钾的用量比为10.58mL：40.00mL：0.13g，将耐水洗抗菌物加入到去离子水中，随后加入无水碳酸钾，搅拌30min，制得碱性耐水洗抗菌物，将布料浸泡在碱性耐水洗抗菌物内，浸泡1h，控制温度为50℃，取出、干燥，制得耐水洗抗菌布料。
实施例2
耐水洗抗菌布料通过如下步骤制备：
步骤一：控制聚六亚甲基胍盐酸盐、二甲基亚砜、去离子水和丙三醇三缩水甘油醚的用量比为1.78g：5.71mL：50.00mL：2.53mL，往反应釜内加入聚六亚甲基胍盐酸盐和二甲基亚砜，随后加入去离子水，超声辅助溶解1h，随后往反应釜加入丙三醇三缩水甘油醚，在55℃的水浴条件下，反应5h，制得混合液A；
步骤二：控制混合液A与丙酮的体积比为1：2.5，往混合液A内倒入丙酮，搅拌反应35min后放入离心机中，控制离心机转速为3500r/min，离心10min，倒去上层清液，随后继续用丙酮洗涤3次，制得耐水洗抗菌物；
步骤三：控制耐水洗抗菌物、去离子水和无水碳酸钾的用量比为10.58mL：40.00mL：0.13g，将耐水洗抗菌物加入到去离子水中，随后加入无水碳酸钾，搅拌30min，制得碱性耐水洗抗菌物，将布料浸泡在碱性耐水洗抗菌物内，浸泡1h，控制温度为50℃，取出、干燥，制得耐水洗抗菌布料。
实施例3
耐水洗抗菌布料通过如下步骤制备：
步骤一：控制聚六亚甲基胍盐酸盐、二甲基亚砜、去离子水和丙三醇三缩水甘油醚的用量比为1.78g：5.71mL：50.00mL：2.53mL，往反应釜内加入聚六亚甲基胍盐酸盐和二甲基亚砜，随后加入去离子水，超声辅助溶解1h，随后往反应釜加入丙三醇三缩水甘油醚，在60℃的水浴条件下，反应5h，制得混合液A；
步骤二：控制混合液A与丙酮的体积比为1：2.5，往混合液A内倒入丙酮，搅拌反应40min后放入离心机中，控制离心机转速为4000r/min，离心10min，倒去上层清液，随后继续用丙酮洗涤4次，制得耐水洗抗菌物；
步骤三：控制耐水洗抗菌物、去离子水和无水碳酸钾的用量比为10.58mL：40.00mL：0.13g，将耐水洗抗菌物加入到去离子水中，随后加入无水碳酸钾，搅拌30min，制得碱性耐水洗抗菌物，将布料浸泡在碱性耐水洗抗菌物内，浸泡1h，控制温度为50℃，取出、干燥，制得耐水洗抗菌布料。
实施例4
该耐水洗抗菌面料的制备方法，具体包括如下步骤：
步骤一：制备耐水洗抗菌布料；
步骤二：制备防静电布料，是由涤纶纤维与不锈钢纤维混纺纱线编织形成；
步骤三：制备柔性布料，是由柔性布料是由棉丝纤维编织形成；
步骤四：将耐水洗抗菌布料、防静电布料、柔性布料依次叠放，使用缝纫机进行面料缝制，最后制得耐水洗抗菌面料。
实施例5
该耐水洗抗菌面料的制备方法，具体包括如下步骤：
步骤一：制备耐水洗抗菌布料；
步骤二：制备防静电布料，是由涤纶纤维与不锈钢纤维混纺纱线编织形成；
步骤三：制备柔性布料，是由柔性布料是由棉丝纤维编织形成；
步骤四：将耐水洗抗菌布料、防静电布料、柔性布料依次叠放，使用缝纫机进行面料缝制，最后制得耐水洗抗菌面料。
实施例6
该耐水洗抗菌面料的制备方法，具体包括如下步骤：
步骤一：制备耐水洗抗菌布料；
步骤二：制备防静电布料，是由涤纶纤维与不锈钢纤维混纺纱线编织形成；
步骤三：制备柔性布料，是由柔性布料是由棉丝纤维编织形成；
步骤四：将耐水洗抗菌布料、防静电布料、柔性布料依次叠放，使用缝纫机进行面料缝制，最后制得耐水洗抗菌面料。
对比例1
使用普通的抗菌剂进行对耐水洗抗菌布料制备。
按照GB/T12490中的标准对对比例1和实施例4-6中的面料进行洗涤，从面料上剪取长宽都为10cm的正方形试样，水温为40℃，加入洗涤剂，洗2h；取对比例1和实施例4-6中的面料剪取长宽都为1cm的正方形试样，放入试管中，往试管内加入1mL大肠杆菌菌液，培养24h后，放入酶标仪测试；
表1为实施例4-6中面料与对比例1中面料的使用效果
Figure BDA0003264717830000061
由表1可知，实施例4-6中的面料在洗涤2h后与加入大肠杆菌24h后，仍具有耐水性和抗菌性。
以上所述，仅是本发明的较佳实施例而已，并非对本发明作任何形式上的限制，虽然本发明已以较佳实施例揭示如上，然而并非用以限定本发明，任何本领域技术人员，在不脱离本发明技术方案范围内，当可利用上述揭示的技术内容做出些许更动或修饰为等同变化的等效实施例，但凡是未脱离本发明技术方案内容，依据本发明的技术实质对以上实施例所作的任何简介修改、等同变化与修饰，均仍属于本发明技术方案的范围内。

Claims (7)

1.一种耐水洗抗菌面料，其特征在于：包括耐水洗抗菌布料、防静电布料和柔性布料，所述耐水洗抗菌布料通过如下步骤制备：
步骤一：往反应釜内加入聚六亚甲基胍盐酸盐和二甲基亚砜，随后加入去离子水，超声辅助溶解1h，随后往反应釜加入丙三醇三缩水甘油醚，在50℃-60℃的水浴条件下，反应5h，制得混合液A；
步骤二：往混合液A内倒入丙酮，搅拌反应30-40min后放入离心机中，控制离心机转速为3000-4000r/min，离心10min，倒去上层清液，随后继续用丙酮洗涤2-4次，制得耐水洗抗菌物；
步骤三：将耐水洗抗菌物加入到去离子水中，随后加入无水碳酸钾，搅拌30min，制得碱性耐水洗抗菌物，将布料浸泡在碱性耐水洗抗菌物内，浸泡1h，控制温度为50℃，取出、干燥，制得耐水洗抗菌布料。
2.根据权利要求1所述的一种耐水洗抗菌面料，其特征在于：所述聚六亚甲基胍盐酸盐、二甲基亚砜、去离子水和丙三醇三缩水甘油醚的用量比为1.78g：5.71mL：50.00mL：2.53mL。
3.根据权利要求1所述的一种耐水洗抗菌面料，其特征在于：所述混合液A与丙酮的体积比为1：2.5。
4.根据权利要求1所述的一种耐水洗抗菌面料，其特征在于：所述耐水洗抗菌物、去离子水和无水碳酸钾的用量比为10.58mL：40.00mL：0.13g。
5.根据权利要求1所述的一种耐水洗抗菌面料，其特征在于：所述防静电布料是由涤纶纤维与不锈钢纤维混纺纱线编织形成。
6.根据权利要求1所述的一种耐水洗抗菌面料，其特征在于：所述柔性布料是由亲水性纤维编织形成。
7.根据权利要求1-6任一所述的一种耐水洗抗菌面料的制备方法，其特征在于：具体包括如下步骤：
步骤一：制备耐水洗抗菌布料；
步骤二：制备防静电布料：
步骤三：制备柔性布料；
步骤四：将耐水洗抗菌布料、防静电布料、柔性布料依次叠放，使用缝纫机进行面料缝制，最后制得耐水洗抗菌面料。
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