CN113563747A - Waterproof real stone paint and preparation method thereof - Google Patents

Waterproof real stone paint and preparation method thereof Download PDF

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Publication number
CN113563747A
CN113563747A CN202110821190.3A CN202110821190A CN113563747A CN 113563747 A CN113563747 A CN 113563747A CN 202110821190 A CN202110821190 A CN 202110821190A CN 113563747 A CN113563747 A CN 113563747A
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Prior art keywords
parts
waterproof
real stone
paint
stone paint
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乔启信
朱华林
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Anhui Lencaqi Waterproof Technology Co ltd
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Anhui Lencaqi Waterproof Technology Co ltd
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Inorganic Chemistry (AREA)
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Abstract

The invention relates to the technical field of building decoration materials, in particular to a waterproof real stone paint which comprises, by weight, 15-35 parts of water-based epoxy resin, 3-15 parts of water-based curing agent, 5-18 parts of graphene, 80-120 parts of aggregate, 15-20 parts of organic modified bentonite, 10-25 parts of hydroxyethyl cellulose, 0.5-2 parts of modified siloxane, 0.5-1.5 parts of wetting dispersant, 1-4 parts of film-forming auxiliary agent, 0.5-0.8 part of defoaming agent, 0.5-1.2 parts of thickening agent, 0.5-1.5 parts of mildew preventive, 0.5-3 parts of pH regulator and a proper amount of water; wherein the aggregate is prepared from natural colored sand and quartz sand according to the weight ratio of (1-3): (1-2), wherein the granularity of the natural colored sand is 40-80 meshes, and the granularity of the quartz sand is 80-120 meshes; the invention also provides a preparation method of the composition. The waterproof real stone paint greatly enhances the water resistance, weather resistance and stain resistance of the real stone paint, and promotes the development and application of the real stone paint.

Description

Waterproof real stone paint and preparation method thereof
Technical Field
The invention relates to the technical field of building decoration materials, in particular to a waterproof real stone paint and a preparation method thereof.
Background
The stone-like paint has rich colors, strong colorability, strong adhesive force, fire resistance and corrosion resistance, can create a harmonious and elegant building atmosphere, has wider environmental adaptability compared with the traditional building paint, and is widely used for external walls. The stone paint is more and more popular in the market as one of the exterior wall paints with the fastest growing market demand.
However, in the actual construction of the exterior wall stone-like paint in the building engineering at present, due to the influence of various uncertain factors and external environment changes, the application of the exterior wall stone-like paint has many problems, such as: the main quality problems of the stone-like paint, such as the occurrence of a blooming phenomenon after being soaked in rainwater, large color difference, yellowing when meeting water, falling of a bulge and the like, are solved, and the problems not only affect the actual decorative effect of the stone-like paint, but also affect the quality of the whole project and the using effect of a building.
Disclosure of Invention
Aiming at the problems in the prior art, the invention aims to provide the waterproof stone-like paint which is good in waterproofness, simple in components, safe and environment-friendly. In order to realize the purpose of the invention, the following technical scheme is adopted:
the waterproof real stone paint comprises, by weight, 15-35 parts of waterborne epoxy resin, 3-15 parts of waterborne curing agent, 5-18 parts of graphene, 80-120 parts of aggregate, 15-20 parts of organic modified bentonite, 10-25 parts of hydroxyethyl cellulose, 0.5-2 parts of modified siloxane, 0.5-1.5 parts of wetting dispersant, 1-4 parts of film-forming assistant, 0.5-0.8 part of defoamer, 0.5-1.2 parts of thickener, 0.5-1.5 parts of mildew inhibitor, 0.5-3 parts of pH regulator and a proper amount of water;
the aggregate is a mixture of natural colored sand and quartz sand, and the weight ratio of the natural colored sand to the quartz sand is (1-3): (1-2), the granularity of the natural colored sand is 40-80 meshes, and the granularity of the quartz sand is 80-120 meshes.
Preferably, the wetting dispersant is one of polycarboxylic acid-alkyl ammonium salt or unsaturated fatty acid polyamine amide.
Preferably, the film forming aid is one of ethylene glycol or lauryl ester film forming aid.
Preferably, the defoaming agent is selected from any one of silicone, mineral oil or polyether modified defoaming agents.
Preferably, the thickener is one of polyurethane rheology modifier, cellulose thickener or their combination.
Preferably, the mildew preventive is tetrachloroisophthalonitrile emulsion.
Preferably, the pH regulator is ammonia water.
In order to achieve the purpose, the invention also provides a processing method of the waterproof real stone paint, which comprises the following steps:
(1) weighing: weighing the medicines according to the parts by weight for later use;
(2) dispersing: uniformly dispersing a graphene aqueous solution, and uniformly dispersing graphene in a water-based epoxy curing agent by using high-speed stirring and ultrasonic treatment to obtain a uniform dispersion liquid for later use;
(3) color matching: preparing proper aggregate with the weight ratio of the natural colored sand to the quartz sand for later use;
(4) high-speed mixing: putting the weighed water-based epoxy resin, wetting dispersant, film-forming assistant, defoamer, mildew preventive and a proper amount of water in the step (1) into a stirring container, adjusting the rotating speed to 400-;
(5) low-speed paint mixing: and (4) adjusting the rotation speed to be 100-200r/min, slowly adding a thickening agent and a pH regulator into the mixed solution obtained in the step (4), adjusting the viscosity and the pH value of the waterproof stone-like paint, and uniformly stirring to obtain the waterproof stone-like paint.
Preferably, the viscosity of the waterproof real stone paint is 95-115 ku.
Preferably, the pH value of the waterproof real stone paint is 7-8.
Compared with the prior art, the invention has the beneficial effects that:
according to the waterproof real stone paint, the graphene is uniformly dispersed in the water-based epoxy paint, so that the graphene is tightly connected in a paint film of the paint to form a compact physical isolation layer, the excellent shielding effect of the graphene can obviously improve the water resistance and the acid resistance of the paint film of the paint, and the added organic modified bentonite is matched with the hydroxyethyl cellulose to further improve the water resistance of the paint film.
The aggregate of the invention is composed of a mixture of natural colored sand and quartz sand, which not only gives full play to the advantages of weather resistance, acid and alkali resistance, strong color retention and bright color of the natural colored sand, but also ensures that the color tone of the paint surface is richer in layering and the stone-like effect is better; and the natural color sand and the quartz sand have different grain diameters, and aggregates with particles can be fully fused, so that the compatibility of the natural color sand and the quartz sand is improved, the compactness of the waterproof real stone paint is improved, and the waterproofness, the stain resistance and the weather resistance of the waterproof real stone paint are enhanced. In addition, the subsequent addition of the modified siloxane auxiliary agent can gradually migrate to the surface of the coating in the drying process of the coating, and a hydrophobic film is formed after complete drying, so that the water resistance and the anti-contamination capability of the paint film are greatly enhanced.
Drawings
FIG. 1 is a flow chart of a method for processing a waterproof real stone paint of the present invention;
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Detailed description of the preferred embodiment 1
In the embodiment, the specific formula comprises the following components in parts by weight:
aqueous epoxy resin 15 portions of
Aqueous curing agent 3 portions of
Graphene 5 portions of
Aggregate material 80 portions
Organically modified bentonite 15 portions of
Hydroxyethyl cellulose 10 portions of
Modified siloxanes 0.5 portion
Wetting and dispersing agent 0.5 portion
Film forming aid 1 part of
Defoaming agent 0.5 portion
Thickening agent 0.5 portion
Mildew preventive 0.5 portion
pH regulator 0.5 portion
Water (W) Proper amount of
Wherein the aggregate is a mixture of natural colored sand and quartz sand, and the weight ratio of the natural colored sand to the quartz sand is 1: 1, the granularity of the natural colored sand is 40 meshes, and the granularity of the quartz sand is 80 meshes; the wetting dispersant is polycarboxylic acid-alkyl ammonium salt; the film-forming assistant is glycol; the defoaming agent is selected from organosilicon modified defoaming agents; the thickening agent is a polyurethane rheology modifier; the mildew preventive is tetrachloroisophthalonitrile emulsion; the pH regulator is ammonia water.
Fig. 1 is a flow chart of a processing method of the waterproof real stone paint, and it can be seen that the specific preparation method of the embodiment is as follows:
step S101: weighing: weighing the medicines according to the parts by weight for later use;
step S102: dispersing: uniformly dispersing a graphene aqueous solution, and uniformly dispersing graphene in a water-based epoxy curing agent by using high-speed stirring and ultrasonic treatment to obtain a uniform dispersion liquid for later use;
step S103: color matching: preparing proper aggregate of natural color sand and quartz sand in weight ratio for standby
Step S104: high-speed mixing: putting the water-based epoxy resin, the wetting dispersant, the film-forming assistant, the defoamer, the mildew preventive and a proper amount of water weighed in the step S101 into a stirring container, adjusting the rotating speed to 400r/min, adding the dispersion liquid obtained in the step S102 and the aggregate obtained in the step S103, adding the organic modified bentonite, the hydroxyethyl cellulose and the modified siloxane, and continuously stirring to obtain a uniform mixed solution;
step S105: low-speed paint mixing: adjusting the rotation speed to 100r/min, slowly adding a thickener and a pH adjusting agent into the mixed solution obtained in step S104, adjusting the viscosity and the pH value of the waterproof real stone paint, in this embodiment, the pH value is 7, stirring uniformly, obtaining the waterproof real stone paint with the viscosity of 95ku, and performing correlation performance detection.
Specific example 2
In the embodiment, the specific formula comprises the following components in parts by weight:
aqueous epoxy resin 35 portions of
Aqueous curing agent 15 portions of
Graphene 18 portions of
Aggregate material 120 portions of
Organically modified bentonite 20 portions of
Hydroxyethyl cellulose 25 portions of
Modified siloxanes 2 portions of
Wetting and dispersing agent 1.5 parts of
Film forming aid 4 portions of
Defoaming agent 0.8 portion of
Thickening agent 1.2 parts of
Mildew preventive 1.5 parts of
pH regulator 3 portions of
Water (W) Proper amount of
Wherein the aggregate is a mixture of natural colored sand and quartz sand, and the weight ratio of the natural colored sand to the quartz sand is 3: 2, the granularity of the natural colored sand is 80 meshes, and the granularity of the quartz sand is 120 meshes; the wetting dispersant is unsaturated fatty acid polyamine amide; the film-forming assistant is dodecyl ester film-forming assistant; the defoaming agent is selected from mineral oil modified defoaming agents; the thickening agent is cellulose thickening agent; the mildew preventive is tetrachloroisophthalonitrile emulsion; the pH regulator is ammonia water.
Fig. 1 is a flow chart of a processing method of the waterproof real stone paint, and it can be seen that the specific preparation method of the embodiment is as follows:
step S101: weighing: weighing the medicines according to the parts by weight for later use;
step S102: dispersing: uniformly dispersing a graphene aqueous solution, and uniformly dispersing graphene in a water-based epoxy curing agent by using high-speed stirring and ultrasonic treatment to obtain a uniform dispersion liquid for later use;
step S103: color matching: preparing proper aggregate of natural color sand and quartz sand in weight ratio for standby
Step S104: high-speed mixing: taking the water-based epoxy resin, the wetting dispersant, the film-forming assistant, the defoamer, the mildew preventive and a proper amount of water weighed in the step S101 into a stirring container, adjusting the rotating speed to 600r/min, adding the dispersion liquid obtained in the step S102 and the aggregate obtained in the step S103, adding the organic modified bentonite, the hydroxyethyl cellulose and the modified siloxane, continuously stirring to obtain a uniform mixed solution
Step S105: low-speed paint mixing: adjusting the rotation speed to 200r/min, slowly adding a thickener and a pH adjusting agent into the mixed solution obtained in step S104, adjusting the viscosity and the pH value of the waterproof real stone paint, in this embodiment, the pH value is 8, stirring uniformly, obtaining the waterproof real stone paint with the viscosity of 115ku, and performing detection on correlation performance.
Specific example 3
In the embodiment, the specific formula comprises the following components in parts by weight:
aqueous epoxy resin 25 portions of
Aqueous curing agent 10 portions of
Graphene 12 portions of
Aggregate material 100 portions of
Organically modified bentonite 18 portions of
Hydroxyethyl cellulose 23 portions of
Modified siloxanes 1.5 parts of
Wetting and dispersing agent 0.8Portions are
Film forming aid 2 portions of
Defoaming agent 0.6 part
Thickening agent 0.8 portion of
Mildew preventive 1.0 part
pH regulator 1.5 parts of
Water (W) Proper amount of
Wherein the aggregate is a mixture of natural colored sand and quartz sand, and the weight ratio of the natural colored sand to the quartz sand is 2: 1, the granularity of the natural colored sand is 60 meshes, and the granularity of the quartz sand is 100 meshes; the wetting dispersant is unsaturated fatty acid polyamine amide; the film-forming assistant is glycol; the defoaming agent is selected from polyether modified defoaming agents; the thickening agent is a composition of cellulose thickening agents; the mildew preventive is tetrachloroisophthalonitrile emulsion; the pH regulator is ammonia water.
Fig. 1 is a flow chart of a processing method of the waterproof real stone paint, and it can be seen that the specific preparation method of the embodiment is as follows:
step S101: weighing: weighing the medicines according to the parts by weight for later use;
step S102: dispersing: uniformly dispersing a graphene aqueous solution, and uniformly dispersing graphene in a water-based epoxy curing agent by using high-speed stirring and ultrasonic treatment to obtain a uniform dispersion liquid for later use;
step S103: color matching: preparing proper aggregate of natural color sand and quartz sand in weight ratio for standby
Step S104: high-speed mixing: taking the water-based epoxy resin, the wetting dispersant, the film-forming assistant, the defoamer, the mildew preventive and a proper amount of water weighed in the step S101 into a stirring container, adjusting the rotating speed to be 500r/min, adding the dispersion liquid obtained in the step S102 and the aggregate obtained in the step S103, then adding the organic modified bentonite, the hydroxyethyl cellulose and the modified siloxane, continuously stirring to obtain a uniform mixed solution
Step S105: low-speed paint mixing: adjusting the rotation speed to 100r/min, slowly adding a thickener and a pH adjusting agent into the mixed solution obtained in step S104, adjusting the viscosity and the pH value of the waterproof real stone paint, in this embodiment, the pH value is 7, stirring uniformly, obtaining the waterproof real stone paint with the viscosity of 100ku, and performing correlation performance detection.
The detection results are as follows:
TABLE 1 results of testing the properties of the examples
Figure BDA0003172043130000061
The waterproof really stone paint has the advantages that the graphene is uniformly dispersed in the water-based epoxy paint, so that the graphene is tightly connected in a paint film of the paint to form a compact physical isolation layer, the excellent shielding effect of the graphene can obviously improve the acid resistance and the water resistance of the paint film, and the added organic modified bentonite is matched with hydroxyethyl cellulose to further improve the water resistance of the paint film; according to the invention, the mixture of the natural colored sand and the quartz sand is used as the aggregate, so that the color tone of the paint surface is richer in layering, the stone imitation effect is better, the natural colored sand and the quartz sand with different particle sizes are fully fused, the compatibility of the natural colored sand and the quartz sand can be improved, the compactness of the waterproof stone-like paint is improved, and the waterproofness, the stain resistance and the weather resistance of the waterproof stone-like paint are enhanced; in addition, the added modified siloxane auxiliary agent can gradually migrate to the surface of the coating in the drying process of the coating, and a hydrophobic film is formed after the coating is completely dried, so that the water resistance and the anti-contamination capability of the paint film are greatly enhanced.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can understand that the changes or modifications within the technical scope of the present invention are included in the scope of the present invention, and therefore, the scope of the present invention should be subject to the protection scope of the claims.

Claims (10)

1. The waterproof real stone paint is characterized in that: the coating comprises, by weight, 15-35 parts of waterborne epoxy resin, 3-15 parts of waterborne curing agent, 5-18 parts of graphene, 80-120 parts of aggregate, 15-20 parts of organic modified bentonite, 10-25 parts of hydroxyethyl cellulose, 0.5-2 parts of modified siloxane, 0.5-1.5 parts of wetting dispersant, 1-4 parts of film-forming additive, 0.5-0.8 part of defoaming agent, 0.5-1.2 parts of thickening agent, 0.5-1.5 parts of mildew inhibitor, 0.5-3 parts of pH regulator and a proper amount of water;
the aggregate is a mixture of natural colored sand and quartz sand, and the weight ratio of the natural colored sand to the quartz sand is (1-3): (1-2), the granularity of the natural colored sand is 40-80 meshes, and the granularity of the quartz sand is 80-120 meshes.
2. The waterproof real stone paint as claimed in claim 1, wherein: the wetting dispersant is one of polycarboxylic acid-alkyl ammonium salt or unsaturated fatty acid polyamine amide.
3. The waterproof real stone paint as claimed in claim 1, wherein: the film-forming assistant is one of ethylene glycol or lauryl ester film-forming assistant.
4. The waterproof real stone paint as claimed in claim 1, wherein: the defoaming agent is any one of organic silicon, mineral oil or polyether modified defoaming agent.
5. The waterproof real stone paint as claimed in claim 1, wherein: the thickening agent is one of polyurethane rheology regulator, cellulose thickening agent or the composition thereof.
6. The waterproof real stone paint as claimed in claim 1, wherein: the mildew preventive is tetrachloroisophthalonitrile emulsion.
7. The waterproof real stone paint as claimed in claim 1, wherein: the pH regulator is ammonia water.
8. A processing method of waterproof real stone paint is characterized in that: the method comprises the following steps:
(1) weighing: weighing the medicines according to the parts by weight for later use;
(2) dispersing: uniformly dispersing a graphene aqueous solution, and uniformly dispersing graphene in a water-based epoxy curing agent by using high-speed stirring and ultrasonic treatment to obtain a uniform dispersion liquid for later use;
(3) color matching: preparing proper aggregate with the weight ratio of the natural colored sand to the quartz sand for later use;
(4) high-speed mixing: putting the weighed water-based epoxy resin, wetting dispersant, film-forming assistant, defoamer, mildew preventive and a proper amount of water in the step (1) into a stirring container, adjusting the rotating speed to 400-;
(5) low-speed paint mixing: and (4) adjusting the rotation speed to be 100-200r/min, slowly adding a thickening agent and a pH regulator into the mixed solution obtained in the step (4), adjusting the viscosity and the pH value of the waterproof stone-like paint, and uniformly stirring to obtain the waterproof stone-like paint.
9. The method for processing the waterproof real stone paint as claimed in claim 8, wherein: the viscosity of the waterproof real stone paint is 95-115 ku.
10. The method for processing the waterproof real stone paint as claimed in claim 8, wherein: the pH value of the waterproof real stone paint is 7-8.
CN202110821190.3A 2021-07-20 2021-07-20 Waterproof real stone paint and preparation method thereof Pending CN113563747A (en)

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Publication number Priority date Publication date Assignee Title
CN116376397A (en) * 2023-03-28 2023-07-04 湖南神力铃胶粘剂制造有限公司 Double-component exterior wall decorative paint and preparation method thereof

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Application publication date: 20211029