CN104745030B - A kind of supporting aqueous texture coating for internal and external wall and preparation method thereof - Google Patents

A kind of supporting aqueous texture coating for internal and external wall and preparation method thereof Download PDF

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Publication number
CN104745030B
CN104745030B CN201510182274.1A CN201510182274A CN104745030B CN 104745030 B CN104745030 B CN 104745030B CN 201510182274 A CN201510182274 A CN 201510182274A CN 104745030 B CN104745030 B CN 104745030B
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texture coating
coating
water
external wall
internal
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CN104745030A (en
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王燕彬
刘红英
陈建刚
朱海英
朱小英
张彩萍
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JIANGSU LANLING POLYMER MATERIAL CO Ltd
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JIANGSU LANLING POLYMER MATERIAL CO Ltd
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/08—Metals
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
    • C09D125/02—Homopolymers or copolymers of hydrocarbons
    • C09D125/04—Homopolymers or copolymers of styrene
    • C09D125/08—Copolymers of styrene
    • C09D125/14—Copolymers of styrene with unsaturated esters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/08—Metals
    • C08K2003/0806—Silver
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention belongs to coating research field, more particularly to a kind of supporting aqueous texture coating for internal and external wall.Its supporting component is respectively that there is provided the good ground of an intensity high adhesion force for 1, high intensity permeability texture coating base paint special；2nd, aqueous texture coating intermediate coat is there is provided the skeleton of whole coating, and its elastic characteristic prevents the cracking of coating；3rd, the hydrophobic varnish finish paint of high rigidity, fills up the gap in the middle of building stones in intermediate coat, film is not recessed significantly substantially, and its film is that hydrophobic property can be very good anti-stain.Three components are supported the use, and have the advantages that intensity height, cracking resistance, waterproof, anti-aging, dirt-resistant, meet National Environmental famous special product requirement.

Description

A kind of supporting aqueous texture coating for internal and external wall and preparation method thereof
Technical field
The invention belongs to coating research field, more particularly to a kind of supporting aqueous texture coating for internal and external wall.
Background technology
The inspiration of texture coating comes from the cabin of the different style on the Greece peninsula earliest, is main mainly by emulsion Bonding agent, a variety of auxiliary agent compositions are added by aggregate of natural colour sand.Coating layer thickness is big, uneven, has in third dimension, coating Natural colour sand assigns the gorgeous color in coating with very abundant, excellent weatherability, excellent water resistance, alkali resistance.But It is due to that natural colour sand belongs to mineral resources, with the reduction of resource, country has limited exploitation.
Common sand texture coating is because the reason such as stain resistant, water proofing property can not be used in interior wall.And aqueous texture is applied now Material is commercially using the history of existing 7 or eight years, with the extension of use time, also exposes the defects of many, 1, The stain resistance of coating, the rough texture that texture coating has in itself, while giving the aesthetic feeling of wall uniqueness, this It is the basic reason of the overproof stain resistance of coating：Texture coating specious air when firm brush, but when using Between extend after, exterior wall texture coating can adsorb dust dirt in coating gap, and film understands that darkness deepens, the meeting near gutter There is the black stain of an obvious rule, influence very much attractive in appearance；2nd, film cracking and come off, in the market texture coating is because select Be ordinary emulsion, so cracking phenomena can occur in the big place of the temperature difference, seam can be penetrated into by occurring spot after cracking phenomena In gap, obvious vestige influence is formed attractive in appearance；3rd, VOC problems, require more and more higher to the VOC of coating currently on the market, wherein It is just tightened up to interior wall requirement, it is necessary to the time very short after interior decoration can just move in, this environmental requirement to coating is just It is very high, mould inhibitor is used in wet environments such as kitchen, toilet, basements, one is that usage amount is big, and two be not environmentally.
The content of the invention
In order to solve the above technical problems, providing a kind of supporting environment-friendly type, Diamond Search, high durable, the aqueous nature of high dirt resistance Feel coating for internal and external wall, the technical solution adopted by the present invention is：
A kind of supporting aqueous texture coating for internal and external wall is provided, it is respectively that 1, high intensity permeability texture coating is special that its is supporting There is provided the good ground of an intensity high adhesion force for priming paint；2nd, aqueous texture coating intermediate coat is there is provided the skeleton of whole coating, its The characteristic of elasticity prevents the cracking of coating；3rd, the hydrophobic varnish finish paint of high rigidity, fills up the gap in the middle of building stones in intermediate coat, substantially Film is set not to be recessed significantly, its film is that hydrophobic property can be very good anti-stain,
The consumption of high intensity permeability texture coating base paint special is 10 ㎡/kg,
The consumption of aqueous texture coating intermediate coat is 0.3 ㎡/kg,
The consumption of the hydrophobic varnish finish paint of high rigidity is 3-5 ㎡/kg,
Wherein, the composition mass percent of high intensity permeability texture coating base paint special includes, high intensity permeability third Olefin(e) acid emulsion 35-50%, coalescents 3-5%, defoamer 0.1-1.0%, wetting agent 0.2%, mould inhibitor 0.09%, remaining be Water and pH adjusting agent,
The above-mentioned high intensity permanent acrylic emulsion used in high intensity permeability texture coating base paint special is Tao Shi 2133 emulsions (phenylpropyl alcohol back cover emulsion), the priming paint being made into by the emulsion has a good permeability, and Tg values are high, brushes When, the bonding that enhancing strength of wall body is played in loose wall, the wall accumulation of salt in the surface soil is prevented, improves wall and intermediate coat can be penetrated into The effect of intensity；
The composition mass percent of aqueous texture coating intermediate coat includes, high-elastic acrylic emulsion 15-25%, coalescents 3-5%, dispersant 0.5-1.0%, wetting agent 0.4%, mould inhibitor 0.09%, quartz sand 50-55%, color sand 1-5%, cellulose 3-5%, remaining be water and pH adjusting agent,
High-elastic acrylic emulsion employed in aqueous texture coating intermediate coat is Tao Shi 2468 emulsions, is matched somebody with somebody by the emulsion Into priming paint there is strong elasticity, can effectively prevent because coating cracking caused by the expanding with heat and contract with cold of wall；
The composition mass percent of the hydrophobic varnish finish paint of high rigidity includes, modified acrylic acid emulsion 70-75%, coalescents 1-3%, defoamer 0.1-1.0%, mould inhibitor 0.09%, nanoscale water-repelling agent 1%, remaining be water and pH adjusting agent,
Modified acrylic acid emulsion employed in the hydrophobic varnish finish paint of high rigidity is the SE-350 emulsions of Daikin company, The C-F chemical bonds contained in the emulsion provide superpower water resistance, stain resistant, alkali resistance and ageing resistance, film to film Densification can prevent the infiltration of water, and the fluorine carbon emulsion has certain hydrophobicity, but without reaching with lotus leaf effect situation, Therefore it is matched from the pioneering water-repelling agent in Beijing in the application, coating is reached hydrophobic and antifouling effect after film forming,
Finish paint has the gap that excellent levelability can be filled up in the middle of intermediate coat building stones well, does not have film substantially Obvious depression, is filled up after depression, the transparency based on the emulsion, make film do not lose in appearance texture coating that Stereovision,
Above-mentioned coalescents are the combination of binary coalescents, such as lauryl alcohol ester, 1,2-PD or both,
Above-mentioned dispersant is the 731A, 963 and 1124 of Rhom and Hass one or more kinds of combinations,
Above-mentioned nanoscale water-repelling agent is the water nano water-repelling agent SS-2 of Beijing Shouchuang Nano Techn Co., Ltd.,
Above-mentioned mould inhibitor is nano level metal silver, i.e., by the argent of nanosizing processing, using Nano Silver as mould inhibitor, It is i.e. safe and environmentally friendly.
The compound method of the present invention：
1st, the compound method of high intensity permeability texture coating base paint special be in material-compound tank stir under add emulsion, Water, defoamer, wetting agent, mould inhibitor, after stirring, add pH adjusting agent in right amount, regulation system pH value reaches pH value After 8.0-9.0 scopes, coalescents are added with stirring, after product is uniformly dispersed, is packed, obtained with 80-100 mesh silk screen filters Product are painted on earth；
2nd, the compound method of the hydrophobic varnish finish paint of high rigidity is to add water, modified propylene yogurt under being stirred in material-compound tank Liquid, defoamer, mould inhibitor, nanoscale water-repelling agent, after stirring, add pH adjusting agent in right amount, regulation system pH value makes pH value Reach after 8.0-9.0 scopes, coalescents are added with stirring, 80-100 mesh silk screen filter bags are used after product reaches standard Dress, obtains finish paint finished product；
3rd, the compound method of aqueous texture coating intermediate coat is that water and cellulose first are added into reactor in batching kettle In it is fully dispersed, add PH conditioning agents regulation pH value.Add high-elastic acrylic emulsion, it is coalescents, dispersant, wetting agent, anti- It is uniformly dispersed, is matched colors after quartz sand, high-speed stirred are added in the case of stirring after mould dose, is wrapped after being sufficiently stirred for Dress,
Above-mentioned pH adjusting agent is the combination of ammoniacal liquor, 2-amino-2-methyl-1-propanol or both.
The present invention is applied to the decorations of building inner-outer wall, because its excellent water resistance and water proofing property can be used for Toilet and kitchen finishing, and skyscraper exterior wall finishing.
The present invention is hydrophobic clear by high intensity permeability texture coating base paint special, aqueous texture coating intermediate coat, high rigidity The supporting composition of lacquer painting paint, has the advantages that intensity height, cracking resistance, waterproof, anti-aging, dirt-resistant, meets National Environmental mark Product requirement.Inventor obtains the supporting aqueous of the present invention by long-term experiment from above-mentioned specific components and composition Texture coating for internal and external wall, considers various components in water paint, auxiliary agent between coating surface energy and three coatings Internuncial influence, on the one hand prevent paint coatings from occurring to peel off, avoiding the defect of poor adhesive force；On the other hand prevent from applying Shielding of the various raw materials to nano level water-repelling agent and mould inhibitor Nano Silver in material, plays the advantage of nano material in coating.
Embodiment
The specific composition of component involved in each embodiment, comparative example is as shown in table 1 below：
Table 1
(note：As long as the raw material for not filling out product producer be it is same type of can be with general)
Table 2 is the component formula (calculating according to the mass fraction) of aqueous nature sense coating intermediate coat in each embodiment：
Table 2
Table 3 be each embodiment in high intensity permeability texture coating base paint special component formula (according to the mass fraction Calculate)：
Table 3
Table 4 is the component formula (calculating according to the mass fraction) of the hydrophobic varnish finish paint of high rigidity in each embodiment：
Table 4
The preparation technology of each paint vehicle is as noted in the discussion in above-mentioned table 2, table 3, table 4.When supporting the use, according to one of bottom Paint, one intermediate coat, the order of one of finish paint prepare model on ground, high intensity permeability texture coating are sprayed first special Priming paint, consumption is 10 ㎡/kg；After drying, aqueous texture coating intermediate coat is sprayed on priming paint, consumption is 0.3 ㎡/kg, sprayed Hardening 24 hours is dried after painting, the hydrophobic varnish finish paint of high rigidity is sprayed on intermediate coat, consumption is 4 ㎡/kg, hardening 24 is dried Hour.
Full performance detection is carried out to coating, testing result is as shown in table 5：
Table 5
(note：
1st, ground is uralite.
2nd, the coating antimildew and antibacterial method for testing performance on the 14th column is specially in table 5：
Laboratory sample presentation to bright chemistry Microbiological Lab of containing is detected
Experiment content is：
(1) detected according to challenge experimental method LXS-WI-MPP-TP-004 in bright Sheng tank, weekly to each sample Microbial infection of (100 grams) progress, is carried out six weeks；
(2) what is each circulated infect, and used inoculum is is made up of certain density bacterium, mould and yeast Plastc ring (table 6)；
(3) bacterium in second day after infecting every time and the 7th day detection sample, mould and yeast quantity (due to Need to infect six weeks, therefore carry out 12 detections altogether, experimental result is as shown in the column of table 5 the 14th)；
(4) judgment criteria：If the result of 7 days shows that number of viable is less than 1000Cfu/g in sample, illustrate that sample passes through inspection Survey.
Table 6
3rd, the dry film antimildew and antibacterial method for testing performance on the 15th column is specially in table 5：
(1) detected that test sample is on cardboard according to the bright Sheng mould proof experimental method LXS-WI-MPP-TP-005 of dry film It is made after film and is dried at room temperature at least 24 hours；
(2) every piece of test sample will immerse mould suspension (specific composition, proportioning are as shown in table 6)；
(3) all detection samples are cultivated 3 weeks at 24 DEG C,
Judgment criteria and result
The growing state of microorganism in test sample is estimated according to following standard after the 3rd week：
Table 7
Testing result is as shown in the 15th column in table 5.)
Comparative example 1
By in the matched coating of above-described embodiment 1, " the emulsion in high intensity permeability texture coating base paint special component 2133 " replace with " S-01 ", " TL-1 ", " Rs-998A " successively, and other each components and preparation technology are same as Example 1.Specifically Testing result is as shown in table 8.
Table 8
Comparative example 2
By in the matched coating of above-described embodiment 2, in aqueous texture coating intermediate coat component " emulsion 2468 " is replaced successively " AC-261P ", " Rs-320 ", " Rs-9389 " are changed to, other each components and preparation technology, detection method are same as Example 2. Specific testing result is as shown in table 9.
Table 9
Comparative example 3
By in the matched coating of above-described embodiment 3, in aqueous texture coating intermediate coat component " dispersant 731A " is successively " PK-100 ", " D-190 " are replaced with, other each components and preparation technology, detection method are same as Example 3.Specific detection knot Fruit is as shown in table 10.
Table 10
Dispersant kind Coating antimildew and antibacterial performance Dry film antimildew and antibacterial performance
Reference standard LXS-WI-MPP-TP-004 LXS-WI-MPP-TP-005
PK-100 Pass through for only preceding 5 times 1
D-190 Pass through for only preceding 6 times 1

Claims (8)

1. a kind of supporting aqueous texture coating for internal and external wall, it is characterised in that：Described matched coating includes 3 kinds of paint vehicles, is respectively High intensity permeability texture coating base paint special, aqueous texture coating intermediate coat, the hydrophobic varnish finish paint of high rigidity；
Wherein,
The composition mass percent of described high intensity permeability texture coating base paint special includes, high intensity permanent acrylic Emulsion 35-50%, coalescents 3-5%, defoamer 0.1-1.0%, wetting agent 0.2%, mould inhibitor 0.09%, remaining be water with And pH adjusting agent；
The composition mass percent of described aqueous texture coating intermediate coat includes, and high-elastic acrylic emulsion 15-25%, film forming are helped Agent 3-5%, dispersant 0.5-1.0%, wetting agent 0.4%, mould inhibitor 0.09%, quartz sand 50-55%, color sand 1-5%, fiber Plain 3-5%, remaining be water and pH adjusting agent；
The composition mass percent of the hydrophobic varnish finish paint of described high rigidity includes, and modified acrylic acid emulsion 70-75%, film forming are helped Agent 1-3%, defoamer 0.1-1.0%, mould inhibitor 0.09%, nanoscale water-repelling agent 1%, remaining be water and pH adjusting agent,
Described mould inhibitor is nano level metal silver, i.e., the argent handled by nanosizing.
2. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：Described high intensity penetration property Feel 2133 emulsions that the high intensity permanent acrylic emulsion in coating base paint special is Tao Shi.
3. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：In described aqueous texture coating Between paint in high-elastic acrylic emulsion be Tao Shi 2468 emulsions.
4. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：The hydrophobic varnish of described high rigidity Modified acrylic acid emulsion in finish paint is the SE-350 emulsions of Daikin company.
5. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：Described coalescents are 12 The combination of alcohol ester, 1,2-PD or both.
6. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：Described dispersant is Luo Menha One or more kinds of combinations of the 731A of this company, 963 and 1124.
7. supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：Described nanoscale water-repelling agent is Initiate the water nano water-repelling agent SS-2 of nanometer Co., Ltd in Beijing.
8. a kind of preparation method of supporting aqueous texture coating for internal and external wall as claimed in claim 1, it is characterised in that：The system Preparation Method is
(1) compound method of high intensity permeability texture coating base paint special is that emulsion, water are added under being stirred in material-compound tank, is disappeared Infusion, wetting agent, mould inhibitor, after stirring, add pH adjusting agent in right amount, regulation system pH value makes pH value reach 8.0-9.0 After scope, coalescents are added with stirring, are packed after product reaches standard with 80-100 mesh silk screen filters, obtain described Priming paint finished product；
(2) compound method of the hydrophobic varnish finish paint of high rigidity is that water, modified acrylic acid emulsion are added under being stirred in material-compound tank, is disappeared Infusion, mould inhibitor, nanoscale water-repelling agent, after stirring, add pH adjusting agent in right amount, regulation system pH value reaches pH value After 8.0-9.0 scopes, coalescents are added with stirring, are packed, obtained with 80-100 mesh silk screen filters after product reaches standard To described finish paint finished product；
(3) compound method of aqueous texture coating intermediate coat is first to be added to water in reactor with cellulose in batching kettle to fill It is scattered, it is uniformly dispersed after adding high-elastic acrylic emulsion, coalescents, dispersant, wetting agent, mould inhibitor, in the feelings of stirring Matched colors after quartz sand, high-speed stirred are added under condition, described intermediate coat finished product is obtained after being sufficiently stirred for.
CN201510182274.1A 2015-04-16 2015-04-16 A kind of supporting aqueous texture coating for internal and external wall and preparation method thereof Active CN104745030B (en)

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CN107903048A (en) * 2017-06-01 2018-04-13 广东中涂联涂料科技有限公司 A kind of antimildew and antibacterial Tao Jing color sands and preparation method thereof
CN108191415A (en) * 2017-12-29 2018-06-22 深圳市嘉达高科产业发展有限公司 A kind of color sand and preparation method thereof
CN114058239B (en) * 2021-11-25 2023-01-10 深圳安盾海洋新材料有限公司 Cement-based anti-permeability anticorrosive multilayer coating and application method thereof

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