CN113349204A - Scutellaria seed coating agent and coating method and application thereof - Google Patents

Scutellaria seed coating agent and coating method and application thereof Download PDF

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Publication number
CN113349204A
CN113349204A CN202110492155.1A CN202110492155A CN113349204A CN 113349204 A CN113349204 A CN 113349204A CN 202110492155 A CN202110492155 A CN 202110492155A CN 113349204 A CN113349204 A CN 113349204A
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China
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scutellaria
seeds
seed
coating agent
seed coating
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CN202110492155.1A
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Chinese (zh)
Inventor
王继永
曾燕
尚兴朴
包芳
邓庭伟
樊良帅
张峰
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China Traditional Chinese Medicine Seed & Seedling Co ltd
China National Traditional Chinese Medicine Co ltd
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China Traditional Chinese Medicine Seed & Seedling Co ltd
China National Traditional Chinese Medicine Co ltd
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Priority to CN202110492155.1A priority Critical patent/CN113349204A/en
Publication of CN113349204A publication Critical patent/CN113349204A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A01N37/46N-acyl derivatives
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N51/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Pest Control & Pesticides (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Soil Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Toxicology (AREA)
  • Pretreatment Of Seeds And Plants (AREA)

Abstract

The invention provides a scutellaria seed coating agent and a coating method and application thereof, the scutellaria seed coating agent consists of 0.46-0.92% metalaxyl-M, 0.31-0.62% fludioxonil, 1.38% thiamethoxam, 2.5% agricultural emulsion 700, 0.3% xanthan gum, 0.2% sodium carboxymethylcellulose, 5% glycol and purified water, the components are simple, the safety and the low toxicity are realized, the production process is simple, the cost is lower, and the scutellaria seed coating agent is suitable for large-scale industrial production; the seed coating agent is added with a film forming agent and an antifreezing agent, so that the coated scutellaria baicalensis seeds have certain low temperature resistance, and the germination rate of the scutellaria baicalensis seeds in adverse circumstances can be improved; the coating method is that the scutellaria seed coating agent and the scutellaria seeds are directly mixed and stirred evenly according to a certain medicine seed ratio and then dried, and the coating method is simple; the invention optimally designs the coating method of the scutellaria seed coating agent, and the coating method can effectively solve the problems of pathogenic bacteria, seedling diseases and insect pests and the like carried by scutellaria seeds when the coating method is used for seedling raising of scutellaria seeds, and simultaneously increases the emergence rate and root length of scutellaria, thereby improving the germination rate of the seeds and the quality of medicinal materials.

Description

Scutellaria seed coating agent and coating method and application thereof
Technical Field
The invention belongs to the technical field of traditional Chinese medicine seed treatment agents, and particularly relates to a scutellaria seed coating agent and a coating method and application thereof.
Background
The scutellaria is a perennial herb of the scutellaria of the labiatae, is one of the bulk medicinal materials in China, and has the effects of clearing heat, drying dampness, purging fire, detoxifying, stopping bleeding, preventing miscarriage and the like. Along with the increasing shortage of wild scutellaria resources, scutellaria cultivation becomes a main source and is commonly used for seed propagation. The scutellaria baicalensis seeds are used as the most basic and important production resources for the production of scutellaria baicalensis medicinal materials, the quality of the seeds is a key factor for determining the high and low yield of the medicinal materials and is also a main condition for determining the quality and quality of the medicinal materials, and pathogenic bacteria carried by the scutellaria baicalensis seeds or pathogenic bacteria in soil, underground pests and other factors can seriously influence the germination of seed seedlings to cause the reduction of the emergence rate, yield and quality of scutellaria baicalensis. The seed coating technology can prevent and control plant diseases and insect pests in the seedling stage, promote the growth of seedlings and has obvious economic effect. At present, the seed coating agent is mainly applied to crop seeds, and the research on the seed coating agent of the traditional Chinese medicine seeds is less. The seed coating agent can promote the germination and growth of the scutellaria baicalensis seeds, but the seed coating agent of the existing crop seeds can not effectively promote the germination of the scutellaria baicalensis seeds. Therefore, a seed coating agent capable of improving the germination rate of scutellaria baicalensis seeds is needed.
Disclosure of Invention
The invention aims to provide a scutellaria seed coating agent, a coating method and application thereof, which are used for solving pathogenic bacteria, seedling diseases and insect pests and the like carried by scutellaria seeds and increasing root length biomass of scutellaria so as to improve the germination rate of the seeds and the quality of medicinal materials thereof.
In order to achieve the technical purpose, the technical scheme adopted by the invention is as follows: a seed coating agent for scutellaria baicalensis consists of the following raw materials in percentage by mass: 0.46-0.92% of metalaxyl-M, 0.31-0.62% of fludioxonil, 1.38% of thiamethoxam, 2.5% of agricultural emulsion 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 5% of ethylene glycol and the balance of purified water.
The invention also provides a coating method of the scutellaria seed coating agent, which comprises the following steps:
preparing a scutellaria seed coating agent: the material is prepared by mixing the following raw materials in percentage by mass: 0.46-0.92% of metalaxyl-M, 0.31-0.62% of fludioxonil, 1.38% of thiamethoxam, 2.5% of agricultural emulsion 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 5% of ethylene glycol and the balance of purified water;
mixing the seed coating agent with Scutellariae radix seed, stirring, and air drying to obtain Scutellariae radix seed coating.
Further, the drug seed ratio of the scutellaria seed coating agent to the scutellaria seeds is 1 mL: 63-130 g.
Further, the scutellaria seed coating agent is composed of the following raw materials in percentage by mass: 0.69% metalaxyl-M, 0.46% fludioxonil, 1.38% thiamethoxam, 2.5% agricultural milk 700, 0.3% xanthan gum, 0.2% sodium carboxymethylcellulose, 5% ethylene glycol, and the balance of purified water.
Further, the drug seed ratio of the scutellaria seed coating agent to the scutellaria seeds is 1 mL: 125 g.
The invention also provides the application of the scutellaria seed coating agent in scutellaria seed seedling raising.
The invention also provides the application of the coating method of the scutellaria seed coating agent in scutellaria seed seedling culture.
Compared with the prior art, the invention has the following beneficial effects: the invention provides a scutellaria seed coating agent and a coating method and application thereof, the scutellaria seed coating agent consists of 0.46-0.92% metalaxyl-M, 0.31-0.62% fludioxonil, 1.38% thiamethoxam, 2.5% agricultural emulsion 700, 0.3% xanthan gum, 0.2% sodium carboxymethylcellulose, 5% glycol and purified water, and the scutellaria seed coating agent has the advantages of simple components, convenient preparation, safety and low toxicity, simple production process and lower cost, and is suitable for large-scale industrial production; the seed coating agent is added with a film forming agent and an antifreezing agent, and the coating treatment of the seed coating agent on the scutellaria baicalensis can improve the film forming property, the uniformity and the falling rate of the coating, and the coated scutellaria baicalensis seeds have certain low temperature resistance and can improve the germination rate of the scutellaria baicalensis seeds in adverse circumstances; the coating method is that the scutellaria seed coating agent and the scutellaria seeds are directly mixed and stirred evenly according to a certain medicine seed ratio and then dried, and the coating method is simple; the method for coating the scutellaria seed coating agent is optimally designed, and germination box experiments and sand box experiments show that when the scutellaria seed coating agent and the coating method thereof are used for treating scutellaria seeds, the germination rate of the coated scutellaria seeds is improved by 13-18 percent, and the mildew rate is reduced by 7-8 percent; the emergence rate is improved by 3-9 percentage points, the root is increased by 0.8-2.4 cm, and therefore, when the scutellaria seed coating agent and the coating method thereof are used for scutellaria seed seedling culture, pathogenic bacteria, seedling diseases and insect pests and the like carried by scutellaria seeds can be effectively solved, the root length biomass of scutellaria is increased, and the germination rate of seeds and the quality of medicinal materials are improved.
Drawings
FIG. 1 is a front and back view of a coating of Scutellaria baicalensis Georgi seeds of example 2 of the present invention, wherein a is uncoated Scutellaria baicalensis Georgi seeds and b is coated Scutellaria baicalensis Georgi seeds;
FIG. 2 is a diagram of the germination box of Scutellaria baicalensis Georgi before and after coating in example 2 of the present invention, wherein a is a diagram of the germination box of uncoated Scutellaria baicalensis Georgi seeds, and b is a diagram of the germination box of coated Scutellaria baicalensis Georgi seeds;
fig. 3 is a diagram of a sandbox of scutellaria baicalensis seeds before and after coating according to example 2 of the present invention, wherein a is a diagram of an uncoated scutellaria baicalensis seed sandbox, and b is a diagram of a coated scutellaria baicalensis seed sandbox.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and examples. The following examples are intended to illustrate the invention only and are not intended to limit the scope of the invention. The experimental procedures used in the examples below are, unless otherwise specified, conventional procedures and the reagents, methods and equipment used are, unless otherwise specified, conventional in the art.
The raw material components of the scutellaria seed coating agent in the following embodiments are all expressed by mass percent of effective components.
Example 1
A coating method of a scutellaria seed coating agent comprises the following steps:
preparing a scutellaria seed coating agent: is prepared by mixing 0.46 percent of metalaxyl-M, 0.31 percent of fludioxonil, 1.38 percent of thiamethoxam, 2.5 percent of agricultural milk 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 5 percent of glycol with purified water;
coating: pouring 1mL of the prepared scutellaria seed coating agent into a plastic bag filled with 125g of scutellaria seeds, fully shaking and mixing uniformly, and drying in the air to finish the coating of the scutellaria seeds.
Example 2
A coating method of a scutellaria seed coating agent comprises the following steps:
preparing a scutellaria seed coating agent: is prepared by mixing 0.69 percent of metalaxyl-M, 0.46 percent of fludioxonil, 1.38 percent of thiamethoxam, 2.5 percent of agricultural milk 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 5 percent of glycol with purified water;
coating: pouring 1mL of the prepared scutellaria seed coating agent into a plastic bag filled with 125g of scutellaria seeds, fully shaking and uniformly mixing, and drying in the air to finish the coating of the scutellaria seeds, wherein the front and the back of the coating of the scutellaria seeds in the embodiment are shown in figure 1.
Example 3
A coating method of a scutellaria seed coating agent comprises the following steps:
preparing a scutellaria seed coating agent: is prepared by mixing 0.92 percent of metalaxyl-M, 0.62 percent of fludioxonil, 1.38 percent of thiamethoxam, 2.5 percent of agricultural milk 700, 0.3 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose and 5 percent of glycol with purified water;
coating: pouring 1mL of the prepared scutellaria seed coating agent into a plastic bag filled with 125g of scutellaria seeds, fully shaking and mixing uniformly, and drying in the air to finish the coating of the scutellaria seeds.
Example 4
The difference between the embodiment and the embodiment 2 is that the mixed drug seed ratio of the scutellaria seed coating agent to the scutellaria seeds is 1 mL: 63 g.
Example 5
The difference between the embodiment and the embodiment 2 is that the mixed drug seed ratio of the scutellaria seed coating agent to the scutellaria seeds is 1 mL: 84 g.
Example 6
The difference between the embodiment and the embodiment 2 is that the mixed drug seed ratio of the scutellaria seed coating agent to the scutellaria seeds is 1 mL: 130 g.
Verification example
1) Germination Box experiment
Randomly placing 50 coated scutellaria seeds on a paper bed of a germination box, alternately carrying out 12-hour illumination and 12-hour dark culture every day, keeping the temperature at 20 ℃, regularly spraying a proper amount of water every day to keep the germination paper moist, counting the germination rate (the length of radicle exceeds the length of the seeds) from the fourth day of the experiment, recording the germination rate and the mildew rate when two leaves grow out, and considering that the germination is finished;
wherein the coated scutellaria seeds are obtained by adopting the coating method of any one of embodiments 1 to 6; uncoated scutellaria seeds were used as control; five replicates of each set of experiments above were performed; the results are shown in Table 1, wherein each example refers to the coated Scutellaria baicalensis Georgi seeds obtained by the coating method of the corresponding numbered example; FIG. 2 is a diagram of the germination box for Scutellaria baicalensis Georgi seeds before and after coating in example 2.
TABLE 1 germination and mold growth rates before and after coating of Scutellaria baicalensis Georgi seeds
Figure BDA0003052835140000041
The results in table 1 show that the scutellaria seed coating agent and the coating method thereof are adopted to coat scutellaria seeds, the germination percentage of the scutellaria seeds is improved by 13-18 percent after the scutellaria seeds are coated, the mildew rate is reduced by 7-8 percent, and the germination percentage of the scutellaria seeds and the mildew rate of the scutellaria seeds can be obviously improved.
2) Sandbox experiment
Randomly placing 100 coated scutellaria seeds in a sandbox, alternately carrying out 12-hour illumination and 12-hour dark culture every day, keeping the temperature at 20 ℃, regularly spraying a proper amount of water every day to keep the sandbox moist, beginning to emerge the seeds, counting the rate of emergence, judging that the germination is finished when three leaves grow out, and randomly taking out 30 plants to measure the root length;
wherein, the coated scutellaria seeds are obtained by adopting the coating method of any one of the embodiments 1 to 6; uncoated scutellaria seeds were used as control; five replicates of each set of experiments above were performed. The experimental results are shown in table 2, wherein each example refers to the coated scutellaria seeds obtained by the coating method of the corresponding numbered example; fig. 3 is a sand box diagram of scutellaria baicalensis seeds before and after coating in example 2.
TABLE 2 emergence rate and root length before and after coating of Scutellaria baicalensis Georgi seeds
Figure BDA0003052835140000051
The results in table 2 show that the scutellaria seed coating agent and the coating method thereof are adopted to coat scutellaria seeds, after the scutellaria seeds are coated, the emergence rate is improved by 3-9 percentage points, the root is increased by 0.8-2.4 cm, and the emergence rate and the root length of the scutellaria seeds can be obviously improved.
The above is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above-mentioned embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may be made by those skilled in the art without departing from the principle of the invention.

Claims (7)

1. The seed coating agent for the scutellaria baicalensis is characterized by comprising the following raw materials in percentage by mass: 0.46-0.92% of metalaxyl-M, 0.31-0.62% of fludioxonil, 1.38% of thiamethoxam, 2.5% of agricultural emulsion 700, 0.3% of xanthan gum, 0.2% of sodium carboxymethylcellulose, 5% of ethylene glycol and the balance of purified water.
2. A coating method of a scutellaria seed coating agent is characterized by comprising the following steps:
formulating a scutellaria seed coating of claim 1;
mixing the seed coating agent with Scutellariae radix seed, stirring, and air drying to obtain Scutellariae radix seed coating.
3. The coating process according to claim 2, characterized in that: the drug-seed ratio of the scutellaria seed coating to the scutellaria seeds is 1 mL: 63-130 g.
4. The coating process according to claim 2, characterized in that: the scutellaria seed coating agent is composed of the following raw materials in percentage by mass: 0.69% metalaxyl-M, 0.46% fludioxonil, 1.38% thiamethoxam, 2.5% agricultural milk 700, 0.3% xanthan gum, 0.2% sodium carboxymethylcellulose, 5% ethylene glycol, and the balance of purified water.
5. The coating method according to claim 4, wherein: the drug-seed ratio of the scutellaria seed coating to the scutellaria seeds is 1 mL: 125 g.
6. The use of the scutellaria seed coating of claim 1 in scutellaria seed seedling raising.
7. Use of the coating method according to any one of claims 2 to 5 in raising seedlings of scutellaria baicalensis seeds.
CN202110492155.1A 2021-05-06 2021-05-06 Scutellaria seed coating agent and coating method and application thereof Pending CN113349204A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115067338A (en) * 2022-07-14 2022-09-20 陇西稷丰种业有限责任公司 Longxi region Chinese herbal medicine seed pelleting composition and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111493077A (en) * 2020-06-08 2020-08-07 辽宁壮苗生化科技股份有限公司 10% thiacloprid, pyrrole and Shuangling pesticide composition and pesticide preparation thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111493077A (en) * 2020-06-08 2020-08-07 辽宁壮苗生化科技股份有限公司 10% thiacloprid, pyrrole and Shuangling pesticide composition and pesticide preparation thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115067338A (en) * 2022-07-14 2022-09-20 陇西稷丰种业有限责任公司 Longxi region Chinese herbal medicine seed pelleting composition and preparation method thereof

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Application publication date: 20210907