CN113332203B - Agilawood skin care product and preparation method thereof - Google Patents
Agilawood skin care product and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P37/00—Drugs for immunological or allergic disorders
- A61P37/08—Antiallergic agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
- A61Q7/02—Preparations for inhibiting or slowing hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention provides an agilawood skin care product and a preparation method thereof, wherein the agilawood skin care product comprises the following substances in percentage by mass: 0.5-3% of agilawood extract, 3-9% of plant essential oil, 5-10% of glycerol, 0.5-4.5% of gamma-aminobutyric acid, 0.5-2% of nicotinamide, 0.5-2% of squalane, 0.2-1% of hyaluronic acid, 0.5-5% of emulsifier and the balance of deionized water; the plant essential oil comprises: 1-3% of coconut oil, 0.5-2% of tea essential oil, 0.5-2% of rose essential oil, 0.5-1% of bergamot essential oil and 0.5-1% of cypress essential oil. The agilawood skin care product has the effects of resisting bacteria, diminishing inflammation and inhibiting hair follicle growth.
Description
Technical Field
The invention relates to the field of skin care products, and in particular relates to an agilawood skin care product and a preparation method thereof.
Background
The skin is at the outermost layer of the human body, and needs careful care to ensure the health of the skin. Especially, the skin of the face, neck, hands and the like exposed outside directly affects the image of people, so that daily care is very important. Daily skin care mainly comprises skin cleaning, moisture preservation and water supplement, oil control, sun protection, acne prevention, aging resistance, pore refinement and the like, and the skin condition is poor or the skin care needs to be paid attention to by cosmetic methods such as laser depilation and the like.
Lignum Aquilariae Resinatum, a resiniferous wood of Aquilaria sinensis of Thymelaeaceae, is distributed in radix rehmanniae such as Guangdong, hainan, guangxi, fujian, etc., and has effects of activating qi-flowing, relieving pain, warming middle-jiao, relieving vomit, and absorbing qi to relieve asthma. The agilawood is commonly used in skin care products, and a small amount of agilawood is added, so that the effects of tightening and repairing, resisting wrinkles and diminishing inflammation, whitening and fading spots and the like can be achieved. Can activate aged skin cells, promote skin blood circulation, improve smooth texture of skin, improve facial edema, and lighten melanin.
Modern depilatory creams use the chemicals to dissolve the hair structure to achieve the goal of depilation. The main ingredient of the preparation is thioglycolic acid (calcium), which has certain irritation and is suitable for people who are afraid of pain but have uneasy skin allergy, new hair can not grow after temporary depilation by depilatory or hair wax, and the problems of large pores, accelerated hair follicle growth and the like can be caused by multiple use.
Patent CN202010945336.0 discloses a depilatory cream and a preparation method thereof, wherein the depilatory cream comprises the following raw material components: 63-70 parts of water, 3-5 parts of humectant, 6-7 parts of emollient, 0.1-0.2 part of water-soluble thickener, 1-4 parts of oil-soluble thickener, 2-4 parts of emulsion stabilizer, 7-9 parts of emulsifier, 2-3.5 parts of pH regulator, 0.2-1 part of bisabolol, 0.1-0.3 part of allantoin, 0.2-0.5 part of skin conditioner and 4-6 parts of chemical depilatory, wherein the skin conditioner is a mixture of butanediol, water, centella asiatica extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract. This patent discloses only depilatory creams and skin conditioners, but the skin conditioners do not have a hair follicle growth inhibiting effect and do not produce a sustained effect.
Patent CN201610606065.X discloses an agilawood skin care product and a preparation method thereof, wherein the agilawood skin care product comprises agilawood extract, aloe extract, glycerol, hyaluronic acid, modified soybean phospholipid and deionized water. The skin care product has high oxidation resistance and melanin removal effect, has no side effect on human body temperature, and cannot achieve the effects of antibiosis and antiphlogosis.
Disclosure of Invention
Therefore, the invention aims to provide the agilawood skin care product which has the effects of resisting bacteria and inflammation, preserving moisture, whitening skin and resisting allergy and can inhibit the growth of hair follicles and the preparation method thereof.
The agilawood skin care product comprises the following substances in percentage by mass: 0.5-3% of agilawood extract, 3-9% of plant essential oil, 5-10% of glycerol, 0.5-4.5% of gamma-aminobutyric acid, 0.5-2% of nicotinamide, 0.5-2% of squalane, 0.2-1% of hyaluronic acid, 0.5-5% of emulsifier and the balance of deionized water.
Preferably, the agilawood skin care product consists of the following substances in percentage by mass: 2% of agilawood extract, 8% of plant essential oil, 7% of glycerol, 3% of gamma-aminobutyric acid, 1% of nicotinamide, 1% of squalane, 0.5% of hyaluronic acid, 2.5% of emulsifier and the balance of deionized water.
Preferably, the dosage ratio of the agilawood extract to the gamma-aminobutyric acid is 1.
Preferably, the plant essential oil consists of the following substances in percentage by mass: 1-3% of coconut oil, 0.5-2% of tea essential oil, 0.5-2% of rose essential oil, 0.5-1% of bergamot essential oil and 0.5-1% of cypress essential oil.
Preferably, the agilawood extract is obtained by extracting agilawood flowers and wood containing agilawood resin, wherein the agilawood flowers and the wood containing the agilawood resin are used in a weight ratio of 1.
Preferably, the agarwood resin-containing wood contains not less than 5% of resin.
The agilawood extract is prepared by the following steps:
step 1: selecting dried chiretta flowers blooming for 3 months and wood containing chiretta resin, mixing in proportion, and pulverizing;
and 2, step: extracting lignum Aquilariae Resinatum extract by supercritical carbon dioxide extraction at 10-16MPa and 30-45 deg.C for 1-2.5 hr.
Preferably, in the step 2, the supercritical carbon dioxide further includes methanol.
Preferably, in the step 2, the addition amount of methanol is 1-2%.
Compared with the prior art, the invention has the beneficial effects that:
1) The agilawood skin care product has the effects of resisting bacteria, diminishing inflammation, moisturizing, whitening and resisting allergy;
2) The agilawood skin care product can inhibit hair follicle growth.
Detailed Description
For clear and complete description of the technical solutions in the present invention, it is obvious that the inventor combines the embodiments to describe, but the following embodiments describe only some embodiments of the present invention, not all embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Preparing an agilawood extract:
the agilawood extract is prepared by the following steps:
step 1: selecting dried chiretta flowers blooming for 3 months and wood containing chiretta resin, mixing in proportion, and pulverizing;
step 2: extracting lignum Aquilariae Resinatum extract by supercritical carbon dioxide extraction at 10-16MPa and 30-45 deg.C for 1-2.5 hr.
Preferably, the agilawood extract is obtained by extracting agilawood flowers and wood containing agilawood resin, wherein the agilawood flowers and the wood containing the agilawood resin are used in a weight ratio of 1.
Preferably, the agarwood resin-containing wood contains not less than 5% of resin.
Preferably, in the step 2, the supercritical carbon dioxide further includes methanol.
Preferably, in the step 2, the addition amount of methanol is 1-2%.
The specific process parameters, the ratio of linaloe flower to linaloe resin-containing wood are shown in table 1.
Table 1:
example 1: preparing agilawood skin care product
1.5 percent of agilawood extract A, 7 percent of plant essential oil, 8 percent of glycerol, 3 percent of gamma-aminobutyric acid, 0.5 percent of nicotinamide, 1 percent of squalane, 1 percent of hyaluronic acid, 2.5 percent of emulsifier and the balance of deionized water;
wherein, the plant essential oil: 1% of coconut oil, 2% of tea essential oil, 2% of rose essential oil, 1% of bergamot essential oil and 1% of cypress essential oil;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Example 2: preparing agilawood skin care product
The preparation method comprises the following steps of preparing 2% of agilawood extract A, 6% of plant essential oil, 5% of glycerol, 0.5% of gamma-aminobutyric acid, 2% of nicotinamide, 0.5% of squalane, 0.2% of hyaluronic acid, 5% of an emulsifier and the balance of deionized water;
wherein, the plant essential oil: 3% of coconut oil, 0.5% of tea essential oil, 0.5% of rose essential oil, 1% of bergamot essential oil and 1% of cypress essential oil;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Example 3: preparing agilawood skin care product
3% of agilawood extract A, 5% of plant essential oil, 10% of glycerol, 4.5% of gamma-aminobutyric acid, 1.5% of nicotinamide, 2% of squalane, 1% of hyaluronic acid, 3% of emulsifier and the balance of deionized water are adopted;
wherein, the plant essential oil: coconut oil 2%, tea essential oil 1%, rose essential oil 1%, bergamot essential oil 0.5%, and cypress essential oil 0.5%;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Example 4: preparing agilawood skin care product
2 percent of agilawood extract A, 8 percent of plant essential oil, 7 percent of glycerol, 3 percent of gamma-aminobutyric acid, 1 percent of nicotinamide, 1 percent of squalane, 0.5 percent of hyaluronic acid, 2.5 percent of emulsifier and the balance of deionized water;
wherein, the plant essential oil: 3% of coconut oil, 1.5% of tea essential oil, 2% of rose essential oil, 0.5% of bergamot essential oil and 1% of cypress essential oil;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Example 5: preparing agilawood skin care product
1 3 percent of agilawood extract A, 4.5 percent of plant essential oil, 8 percent of glycerol, 2 percent of gamma-aminobutyric acid, 1 percent of nicotinamide, 1.5 percent of squalane, 1 percent of hyaluronic acid, 0.5 percent of emulsifier and the balance of deionized water;
wherein, the plant essential oil: coconut oil 2%, tea leaf essential oil 1%, rose essential oil 0.5%, bergamot essential oil 0.5%, and cypress essential oil 0.5%;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Comparative example 1: preparing agilawood skin care product
1.3 percent of agilawood extract A, 5 percent of plant essential oil, 7 percent of glycerol, 0.5 percent of gamma-aminobutyric acid, 3 percent of nicotinamide, 0.2 percent of squalane, 2 percent of hyaluronic acid, 2.5 percent of emulsifier and the balance of deionized water;
wherein, the plant essential oil: 1% of coconut oil, 1% of tea essential oil, 1% of rose essential oil, 1% of bergamot essential oil and 1% of cypress essential oil;
and (3) mixing the raw materials in parts by weight, and homogenizing by using a homogenizer to obtain the agilawood skin care product.
Comparative example 2:
the formula and preparation steps are the same as in example 4 except that rose, bergamot and cypress essential oil are not added.
Comparative example 3:
the formulation and preparation procedure were the same as in example 4, except that no plant essential oil was added.
Comparative example 4:
the formulation and preparation procedure were the same as in example 4, except that nicotinamide, squalane and hyaluronic acid were not added.
Comparative example 5:
the formula and preparation steps are the same as in example 4 except that no agilawood essential oil is added.
Comparative example 6:
the agilawood essential oil is prepared without linaloe flowers, and the rest formula and preparation steps are the same as those in example 4.
Comparative example 7:
the formulation and preparation procedure were the same as in example 4, except that no gamma-aminobutyric acid was added.
Comparative example 8:
agilawood skin care lotion is commercially available.
And (3) antibacterial property experiment:
product effectiveness testing
Respectively immersing staphylococcus aureus, heat-resistant coliform group bacteria, pseudomonas aeruginosa, black mold and yeast in agar culture medium, and culturing at 37 deg.C for 24-36h to form macroscopic colony (corresponding to initial colony area).
Then, the emulsions prepared in examples 1 to 5 and comparative examples 1 to 8 (diluted to 1/5) and distilled water were sprayed on the colonies of staphylococcus aureus, heat-resistant coliform group bacteria, pseudomonas aeruginosa, aspergillus niger and yeast in equal amounts, the area of each colony was counted after 1 day, and the antibacterial ratio was calculated, with the results shown in table 2.
Antibacterial rate = [ initial colony area-area of colony counted after 1 day ]/initial colony area 100%
Table 2:
| staphylococcus aureus | Thermostable E.coli | Pseudomonas aeruginosa | Black mould | Yeast | ||
| Example 1 | ％ | 98.4 | 97.3 | 96.7 | 96.9 | 96.8 |
| Example 2 | ％ | 98.6 | 96.8 | 97.2 | 98.4 | 97.9 |
| Example 3 | ％ | 97.8 | 95.2 | 96.5 | 97.1 | 95.1 |
| Example 4 | ％ | 99.2 | 97.6 | 98.3 | 98.6 | 97.9 |
| Example 5 | ％ | 99 | 98.3 | 97.7 | 98.3 | 98.2 |
| Comparative example 1 | ％ | 95.7 | 92 | 93.8 | 94.6 | 91.8 |
| Comparative example 2 | ％ | 83.7 | 86.4 | 81.6 | 84.8 | 79.2 |
| Comparative example 3 | ％ | 64.5 | 71.1 | 65.3 | 67.2 | 66.9 |
| Comparative example 4 | ％ | 79.1 | 75.3 | 74.8 | 73.9 | 77.6 |
| Comparative example 5 | ％ | 41.2 | 43.6 | 38.7 | 36.5 | 44.9 |
| Comparative example 6 | ％ | 85.9 | 88.4 | 84.3 | 82.9 | 86.2 |
| Comparative example 7 | ％ | 66.8 | 64.3 | 62.7 | 63.1 | 65.5 |
| Comparative example 8 | ％ | 32.7 | 28.5 | 29 | 29.4 | 31.3 |
It can be seen that the agilawood skin care product has good antibacterial property.
Experiment for inhibiting hair follicle growth
70 volunteers were recruited and randomly divided into 14 groups, and after axillary hairs were mechanically removed, the skin care emulsions according to examples 1-5, comparative examples 1-8 and blank control were applied 2 times in the morning and evening, and after 2 weeks of use, mechanical depilation was again performed, and the skin care emulsions were continuously used; after two consecutive months, the rate of hair follicle growth was recorded and the time taken to grow to 0.5cm is shown in Table 3.
Table 3:
| experimental group | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Comparative example 1 | Comparative example 2 |
| Time | 18 | 19 | 16 | 20 | 18 | 15 | 13 |
| Experimental group | Comparative example 3 | Comparative example 4 | Comparative example 5 | Comparative example 6 | Comparative example 7 | Comparative example 8 | CK |
| Time | 12 | 15 | 10 | 16 | 15 | 6 | 4 |
It can be seen that the agilawood skin care product has the effect of inhibiting hair follicle growth.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (6)
1. The agilawood skin care product is characterized by comprising the following substances in percentage by mass: 0.5-3% of agilawood extract, 1-3% of coconut oil, 0.5-2% of tea essential oil, 0.5-2% of rose essential oil, 0.5-1% of bergamot essential oil, 0.5-1% of cypress essential oil, 5-10% of glycerol, 0.5-4.5% of gamma-aminobutyric acid, 0.5-2% of nicotinamide, 0.5-2% of squalane, 0.2-1% of hyaluronic acid, 0.5-5% of emulsifier and the balance of deionized water;
the agilawood extract is extracted from agilawood flowers and wood containing agilawood resin, and the using weight ratio of the agilawood flowers to the wood containing the agilawood resin is 1; the content of the resin in the wood containing the agilawood resin is not less than 5 percent;
the agilawood extract is prepared by the following steps:
step 1: selecting dried chiretta flowers blooming for 3 months and wood containing chiretta resin, mixing in proportion, and pulverizing;
step 2: extracting lignum Aquilariae Resinatum extract by supercritical carbon dioxide extraction at 10-16MPa and 30-45 deg.C for 1-2.5 hr.
2. The agilawood skin care product according to claim 1, wherein the agilawood skin care product consists of the following substances in percentage by mass: 2% of agilawood extract, 3% of coconut oil, 1.5% of tea essential oil, 2% of rose essential oil, 0.5% of bergamot essential oil, 1% of cypress essential oil, 7% of glycerol, 3% of gamma-aminobutyric acid, 1% of nicotinamide, 1% of squalane, 0.5% of hyaluronic acid, 2.5% of emulsifier and the balance of deionized water.
3. The agilawood skin care product according to claim 1, wherein the ratio of the agilawood extract to the gamma-aminobutyric acid is 1.
4. The agilawood skin care product according to claim 1, wherein in step 2, the supercritical carbon dioxide further comprises methanol.
5. The agilawood skin care product according to claim 4, wherein in the step 2, the addition amount of the methanol is 1-2%.
6. Use of the agilawood skin care product of claim 1 in the preparation of a preparation for anti-bacterial, anti-inflammatory and hair follicle growth inhibition.
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