CN1132569C - Jinbianruixiang flower perfume and its supercritical extraction process - Google Patents
Jinbianruixiang flower perfume and its supercritical extraction process Download PDFInfo
- Publication number
- CN1132569C CN1132569C CN 01135914 CN01135914A CN1132569C CN 1132569 C CN1132569 C CN 1132569C CN 01135914 CN01135914 CN 01135914 CN 01135914 A CN01135914 A CN 01135914A CN 1132569 C CN1132569 C CN 1132569C
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- Prior art keywords
- flower
- aureomariginatn
- jinbianruixiang
- perfume
- extractum
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- Expired - Fee Related
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention discloses perfume of fresh VC. Aureomariginatn with the action on health care, skin care and beautification, and a supercritical extraction technique thereof, which belongs to the technical field of the production of tincture type external cosmetics. The present invention uses the supercritical extraction technique to extract effective components of fresh VC. Aureomariginatn so as to obtain extract; 70% ethanol is used as base materials, and a small quantity of vitamin B6, antioxidants and stabilizing agents is added in the base materials; the product of the present invention can be obtained after the materials are stirred, discolored with a distillation method, stood and separated. The product of the present invention can prevent the sting of mosquitoes, promote the metabolism of skin and smooth skin, and has delightful perfume.
Description
The invention discloses a kind of Jinbianruixiang flower perfume and production method thereof that health care, skin protection and beautification function are one that collect, belong to tincture type cosmetics for external use production technical field.
Tincture is that the active ingredient with medicine or medicine is dissolved in the ethanol of debita spissitudo; make a kind of easy coating or be sprayed at containing of skin surface of alcoholic acid liquid preparation for external application; mainly protection, lubrication are played in the surface that skin is not had breakage, a no ulcer place, or specific aim plays protection, therapeutical effect to some symptom.The tincture that at present domestic and international pharmacopeia is recorded has hundreds of, China's version pharmacopeia in 2000 and ministry standard have kind more than 80, tincture perfume in the market is also quite a lot, but they do not have a kind of on prescription is for mainly containing effective constituent with VC.Aureomariginatn, no a kind of tincture perfume integrates health care, skin protection and beautification function on function, most of tincture perfume can only play lasting, beautification function, and health care, therapeutical effect are very little.
The objective of the invention is to provide a kind of with natural VC.Aureomariginatn flower for mainly containing effective constituent, integrate the tincture perfume-Jinbianruixiang flower perfume and the production method thereof of health care, skin protection, beauty treatment, lasting.
Be rich in daphnin (daphnin), C in the natural Jinbianruixiang flower perfume
15H
16O
9About 0.2-0.4% is daphnetin-7-glycoside (daphnetin-7-glucoside) and daphnetin-8-glycoside (daphnetin-8-glucoside).Be rich in about 0.024% volatile oil in the inflorescence, it mainly contains effective constituent β-phellandrene (β-phellandrene); Daphnetin methyl ether (Daphnetin methyl ether); Daphneolon: (DaphjeoloneC
17H
17O
3); Daphnetin: Daphnetin; Normal butane, γ-vinyl alcohol, nonyl alcohol, cis and trans epoxylinalol (linalool oxide), fragrant fragrant and mellow [(-)-citronellol]; Nerol (nerol); Geraniol (geranio); The active ingredients such as (Umbe-lliferone) of many umbellate form flower lactones.Stronger antiinflammatory, analgesia, anti-allergic effects are arranged.The inflammation that (physics, chemistry, biology, immunity) causes for a variety of causes has stronger anti-allergic effects, and itch for alleviating symptoms such as early stage redness, telangiectasis, improvement be red, swollen, alleviating, pain etc. feels to have good effect.
Carbon dioxide changes liquid critical pressure into by gaseous state and is generally 31Mpa, and what the present invention adopted is that supercritical process extracts VC.Aureomariginatn flower extractum mixture.
The present invention adopts following technical scheme to reach goal of the invention: Jinbianruixiang flower perfume, and its each component and percentage by weight are as follows: VC.Aureomariginatn flower extractum 0.015-0.02%; Vitamin B
60.15-0.2%; 97% ethanol 70-75%; Antioxidant ascorbic acid 1.0-1.2%; Stabilizing agent tween 80 0.6-0.8%; Natural pigment 0.5-0.55%; All the other are distilled water, form 100% gross weight, and wherein VC.Aureomariginatn flower extractum adopts process for super-critical extracting to obtain.
Above-mentioned Jinbianruixiang flower perfume makes according to following production stage:
1, the decompression of VC.Aureomariginatn flower is predrying, control moisture weighs less than 20%.
2, with the cyclohexane extraction be entrainer, calcium oxide is a gas dryer, and the predrying gained VC.Aureomariginatn of above-mentioned decompression flower is placed the supercritical extraction special equipment, adopts CO
2Process for super-critical extracting extracts VC.Aureomariginatn extractum mixture, and the adopting process condition is: pressure is that 40Mpa, temperature are that 35-38 ℃, time are 30-35 minute.
3, gained VC.Aureomariginatn extractum mixture in the above-mentioned steps is reduced pressure through secondary, get natural VC.Aureomariginatn flower extractum rectification thing after the separation.
4, according to each component ratio requirement of the technical program, vitamin B6, antioxidant ascorbic acid and stabilizing agent tween 80 be dissolved in the middle of 70% the ethanol, adding natural VC.Aureomariginatn flower extractum rectification thing again stirs and gets final product, operative temperature is controlled in below 20 ℃, and this step obtains the Jinbianruixiang flower perfume first product.
5, the Jinbianruixiang flower perfume first product is carried out molecular distillation decolouring, the Jinbianruixiang flower perfume after must decolouring.
6, above-mentioned Jinbianruixiang flower perfume is statically placed in 8-10 ℃ the refrigerator after 48 hours, draws supernatant in another container, after 8-10 ℃ leaves standstill 48 hours, be sub-packed in the container of regulation again, obtain final products-Jinbianruixiang flower perfume.
Product fragrance of the present invention is pure, can promote metabolism, the moistening and smoothing skin of skin, can prevent the mosquito bite insect bite, is a kind of natural perfume that integrates health care, skin protection, improves looks.
Claims (2)
1, a kind of Jinbianruixiang flower perfume is characterised in that: its each component and percentage by weight are as follows:
VC.Aureomariginatn flower extractum: 0.015-0.02%; Vitamin B6: 0.15-0.2%; 97% ethanol: 70-75%; Antioxidant ascorbic acid: 1.0-1.2%; Stabilizing agent tween 80: 0.6-0.8%; Natural pigment: 0.5-0.55%; All the other are distilled water, form 100% gross weight; VC.Aureomariginatn flower extractum in the middle of the said components adopts process for super-critical extracting to obtain.
2, a kind of production Jinbianruixiang flower perfume method as claimed in claim 1 is characterized in that: undertaken by following production stage:
(1), VC.Aureomariginatn flower decompression is predrying, control moisture weighs less than 20%;
(2), be entrainer with the cyclohexane extraction, calcium oxide is a gas dryer, and the predrying gained VC.Aureomariginatn of above-mentioned decompression flower is placed the supercritical extraction special equipment, adopts CO
2Process for super-critical extracting extracts VC.Aureomariginatn extractum mixture, and the adopting process condition is: pressure is that 40Mpa, temperature are that 35-38 ℃, time are 30-35 minute;
(3), gained VC.Aureomariginatn extractum mixture in the above-mentioned steps is reduced pressure through secondary, after the separation natural VC.Aureomariginatn flower extractum rectification thing;
(4), according to described each the component ratio requirement of claim 1, vitamin B6, antioxidant ascorbic acid and stabilizing agent tween 80 be dissolved in the middle of 70% the ethanol, adding natural VC.Aureomariginatn flower extractum rectification thing again stirs and gets final product, operative temperature is controlled in below 20 ℃, and this step obtains the Jinbianruixiang flower perfume first product;
(5), the Jinbianruixiang flower perfume first product is carried out molecular distillation decolouring, the Jinbianruixiang flower perfume after must decolouring;
(6), above-mentioned Jinbianruixiang flower perfume is statically placed in 8-10 ℃ the refrigerator after 48 hours, draw supernatant in another container, after 8-10 ℃ leaves standstill 48 hours, be sub-packed in the container of regulation again, obtain final products-Jinbianruixiang flower perfume.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01135914 CN1132569C (en) | 2001-10-17 | 2001-10-17 | Jinbianruixiang flower perfume and its supercritical extraction process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01135914 CN1132569C (en) | 2001-10-17 | 2001-10-17 | Jinbianruixiang flower perfume and its supercritical extraction process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1344788A CN1344788A (en) | 2002-04-17 |
| CN1132569C true CN1132569C (en) | 2003-12-31 |
Family
ID=4673349
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 01135914 Expired - Fee Related CN1132569C (en) | 2001-10-17 | 2001-10-17 | Jinbianruixiang flower perfume and its supercritical extraction process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1132569C (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102719315B (en) * | 2012-07-11 | 2013-12-25 | 青岛农业大学 | Ginger seedling essential oil extracted from ginger seedlings by supercritical extraction method and extracting method thereof |
| CN106109263B (en) * | 2016-07-06 | 2018-11-13 | 上海应用技术学院 | A kind of Longaacting fragrance-aretaining east floral type perfume and preparation method thereof |
| CN106109262B (en) * | 2016-07-06 | 2018-10-12 | 上海应用技术学院 | A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance type perfume and preparation method thereof |
| CN106109272B (en) * | 2016-07-06 | 2017-09-29 | 上海应用技术大学 | A kind of Longaacting fragrance-aretaining fruity floral type perfume and preparation method thereof |
-
2001
- 2001-10-17 CN CN 01135914 patent/CN1132569C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1344788A (en) | 2002-04-17 |
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