CN106109272B - A kind of Longaacting fragrance-aretaining fruity floral type perfume and preparation method thereof - Google Patents
A kind of Longaacting fragrance-aretaining fruity floral type perfume and preparation method thereof Download PDFInfo
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- CN106109272B CN106109272B CN201610525722.8A CN201610525722A CN106109272B CN 106109272 B CN106109272 B CN 106109272B CN 201610525722 A CN201610525722 A CN 201610525722A CN 106109272 B CN106109272 B CN 106109272B
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- A61K8/34—Alcohols
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Abstract
A kind of Longaacting fragrance-aretaining fruity floral type perfume, is calculated according to mass ratio, is made up of the first ethanol of 10% 30% fruity bouquet type composition, 5% 20% modified dextrins, 10% 30% deionized water, 0.1% 1% antioxidant, surplus；The preparation method of above-mentioned perfume is additionally provided, modified dextrins are added in a reservoir, deionized water is added, stirring is opened, modified dextrins is uniformly dispersed in aqueous phase；Fruity bouquet type composition is added drop-wise in modified dextrins dispersion liquid, continues to stir, essence is uniformly dispersed, and modified dextrins is formed the cladding to essence molecule, the fruity floral type sustained release essence of Longaacting fragrance-aretaining is obtained；First ethanol is added in the fruity floral type of Longaacting fragrance-aretaining sustained release essence, continues to stir, adds antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.The fruity floral type perfume fragrance for the Longaacting fragrance-aretaining that the present invention is obtained is fine and smooth, and lasting is lasting.
Description
Technical field
The invention belongs to chemical field, it is related to a kind of perfume, specifically a kind of Longaacting fragrance-aretaining fruity floral type perfume
And preparation method thereof.
Background technology
With the development in epoch, the progress of science, the continuous improvement of human material and culture life is used as the perfume (or spice) of cosmetics
Water is developed quickly.Perfume can be divided mainly into three kinds of different forms, i.e. alcohol liquid, emulsion and pulpous state liquid, generally speaking
Perfume is formulated by spices and solvent, and solvent used is mainly ethanol, and essence fragrance is not according to used in perfume
Together, perfume is also classified into a variety of odor types.Perfume fragrance is strong, and main function is to be sprayed on the hem, handkerchief and hair decorations, gives out happy people
Fragrance, for the necessity of cosmetic.
The aroma quality of essence is the principal element of perfume quality, and perfume is perfume with the design and type selecting of essence odor type
It is crucial.Traditional perfume is the mixture of essence and ethanol, essence be by with volatile a variety of spices in note ratio group
Into mixture, volatile during direct use, fragrance remaining time is short, therefore, the design of perfume fragrance odor type and has
The development of the essence of Longaacting fragrance-aretaining has very important significance.
The content of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of Longaacting fragrance-aretaining fruity floral type perfume and
Its preparation method, described this Longaacting fragrance-aretaining fruity floral type perfume and preparation method thereof will solve perfume of the prior art
The short technical problem of fragrance remaining time.
The invention provides a kind of Longaacting fragrance-aretaining fruity floral type perfume, count by weight percentage, the composition of its raw material
And content is as follows：
Fruity bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Count by weight percentage, it is constituted described fruity bouquet type composition and content is as follows：
Orange oil 1%-3%；
Lemon oil 1%-3%；
Grapefruit oil 1%-3%；
Firpene 0.3%-1.2%；
Laurene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Leaf-alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Calamus alkene 0.005%-0.05%；
Bergamio 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Carypohyllene 0.01%-0.2%；
Linalool 0.01%-0.03%
Fanesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpinol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
DPG 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Laurine 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
It is graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Sunflower seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%；
Astrotone 10%-30%
Surplus is the second ethanol.
Present invention also offers a kind of fruity bouquet type composition, count by weight percentage, it is constituted and content is as follows：
Orange oil 1%-3%；
Lemon oil 1%-3%；
Grapefruit oil 1%-3%；
Firpene 0.3%-1.2%；
Laurene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Leaf-alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Calamus alkene 0.005%-0.05%；
Bergamio 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Carypohyllene 0.01%-0.2%；
Linalool 0.01%-0.03%；
Fanesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpinol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
DPG 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Laurine 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
It is graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Sunflower seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%
Astrotone 10%-30%；
Surplus is the second ethanol.
Further, described modified dextrins are a kind of derivatives of starch, are a kind of commercially available prod, can be used as wall
Material, coats essence, essence is slowly discharged, and increases the lasting of essence.
Present invention also offers a kind of preparation method of above-mentioned Longaacting fragrance-aretaining fruity floral type perfume, including following step
Suddenly：
1) each reactive material is weighed according to mass ratio；
2) one the step of prepare fruity bouquet type composition, by orange oil, lemon oil, grapefruit oil, firpene, laurene, water
Celery alkene, limonene, grapefruit methane, leaf-alcohol, ligustral, Calamus alkene, bergamio, carbitol, carypohyllene, linalool, Jin He
Joyous alcohol, anethole, terpinol, valencia Orange alkene, geranyl acetate, citronellol, DPG, geraniol, β-violet
Ketone, laurine, carrot seed alcohol, isopropyl myristate, it is graceful can rowland, ambrotone, ambrox, dihydro jasmone
Sour methyl esters, first position hexyl cinnamic aldehyde, sunflower seed Moschus, helional, triethyl citrate, OctMet, Moschus
Uniformly mixing obtains fruity bouquet type composition for T, the second ethanol.
3) modified dextrins are added in a reservoir, deionized water is added, and are opened stirring, are uniformly dispersed in modified dextrins
In aqueous phase, modified dextrins dispersion liquid is obtained；
4) fruity bouquet type composition is added drop-wise to step 3）In the modified dextrins dispersion liquid of gained, continue to stir, make essence
It is uniformly dispersed, and modified dextrins is formed the cladding to essence molecule, obtains the fruity floral type sustained release essence of Longaacting fragrance-aretaining；
5) the first ethanol is added to step 4）In the fruity floral type sustained release essence of the Longaacting fragrance-aretaining of gained, continue to stir equal
It is even, add antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.
The fruity fragrance of a flower is the odor type that people like, according to the odor characteristic and note of spices, chooses suitable raw material, allotment
Go out soft aroma and, fine and smooth, the fruity bouquet type composition with fruity and fragrance of a flower rhythm；Then modified dextrins are used for wall material, will
To fruity bouquet type composition coated, so as to improve the lasting of essence；Add a certain proportion of deionized water, ethanol and
Antioxidant（Butylated hydroxytoluene）, obtain the fruity floral type perfume of Longaacting fragrance-aretaining.
The present invention is compared with prior art, and its technological progress is significant.A kind of fruity flower of Longaacting fragrance-aretaining of the present invention
Odor type perfume is there is provided a kind of fine and smooth, soft fruity fragrance of a flower odor type, and lasting is lasting.
Embodiment
The present invention is further described below by embodiment, but does not influence protection scope of the present invention.
Embodiment 1
A kind of Longaacting fragrance-aretaining fruity floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and
Content is as follows：
Fruity bouquet type composition 10%（10g）
Modified dextrins 5% (5g)
Deionized water 10% (10g)
Antioxidant 0.1% (0.1g)
Ethanol 74.9% (74.9g)；
A kind of above-mentioned Longaacting fragrance-aretaining fruity floral type perfume is prepared via a method which that the preparation process includes following step
Suddenly：
（1）, add modified dextrins in a reservoir, add deionized water, open stirring, modified dextrins is uniformly disperseed
In aqueous phase, modified dextrins dispersion liquid is obtained；
（2）, fruity bouquet type composition is added drop-wise to step（1）In the modified dextrins dispersion liquid of gained, continue to stir, make perfume (or spice)
Essence is uniformly dispersed, and modified dextrins is formed the cladding to essence molecule, obtains the fruity floral type sustained release essence of Longaacting fragrance-aretaining.
（3）, ethanol is added to step（2）In the fruity floral type sustained release essence of the Longaacting fragrance-aretaining of gained, continue to stir equal
It is even, add antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.The perfume has
The odor characteristic of the fruity fragrance of a flower, animal note is laid particular stress on, and aroma strength is slightly weak.By the perfume and uncoated essence prepare it is general
Logical perfume carries out sensory evaluation by hearing fragrant paper, and the perfume can still feel obvious fragrance after 10 days, and common perfume is several after 2 days
Just it is not felt by fragrance.
Above-mentioned fruity bouquet type composition, it is characterised in that described fruity bouquet type composition count by weight percentage,
It is constituted and content is as follows：
Orange oil 1% (1g)
Lemon oil 1% (1g)
Grapefruit oil 1% (1g)
Firpene 1.2% (1.2g)
Laurene 0.1% (0.1g)
Phellandrene 0.3% (0.3g)
Limonene 4% (4g)
Grapefruit methane 2% (2g)
Leaf-alcohol 0.01% (0.01g)
Ligustral 0.1% (0.1g)
Calamus alkene 0.005% (0.005g)
Bergamio 0.05% (0.05g)
Carbitol 0.1% (0.1g)
Carypohyllene 0.2% (0.2g)
Linalool 0.01% (0.01g)
Fanesol 0.03% (0.03g)
Anethole 0.01% (0.01g)
Terpinol 0.07% (0.07g)
Valencia Orange alkene 0.01% (0.01g)
Geranyl acetate 0.04% (0.04g)
Citronellol 1% (1g)
DPG 1.2% (1.2g)
Geraniol 0.1% (0.1g)
Alpha, beta-lonone 0.5% (0.5g)
Laurine 0.5% (0.5g)
Carrot seed alcohol 0.6% (0.6g)
Isopropyl myristate 0.1% (0.1g)
It is graceful can rowland 5% (5g)
Ambrotone 20% (20g)
Ambrox 0.01% (0.01g)
MDJ 25% (25g)
First position hexyl cinnamic aldehyde 1% (1g)
Sunflower seed Moschus 2% (2g)
Helional 0.1% (0.1g)
Triethyl citrate 0.6% (0.6g)
OctMet 1% (1g)
Astrotone 30% (30g)
Ethanol 0.055% (0.055g)；
Method preparation is prepared by the following procedure in above-mentioned fruity bouquet type composition, and its preparation process specifically includes following steps：
By orange oil, lemon oil, grapefruit oil, firpene, laurene, phellandrene, limonene, grapefruit methane, leaf-alcohol, glossy privet
Aldehyde, Calamus alkene, bergamio, carbitol, carypohyllene, linalool, fanesol, anethole, terpinol, valencia Orange
Alkene, geranyl acetate, citronellol, DPG, geraniol, alpha, beta-lonone, laurine, carrot seed alcohol, nutmeg
Isopropyl propionate, it is graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, sunflower seed Moschus,
Uniformly mixing obtains fruity floral type for helional, triethyl citrate, OctMet, astrotone, ethanol
Essence.Obtained essence fragrance is fine and smooth, and animal note is laid particular stress on, the characteristic perfume with the fruity fragrance of a flower.
Embodiment 2
A kind of Longaacting fragrance-aretaining fruity floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and
Content is as follows：
Fruity bouquet type composition 30% (30g)
Modified dextrins 12% (12g)
Deionized water 15% (15g)
Antioxidant 1% (1g)
Ethanol 39% (39g)；
A kind of above-mentioned Longaacting fragrance-aretaining fruity floral type perfume is prepared via a method which that the preparation process includes following step
Suddenly：
（1）, add modified dextrins in a reservoir, add deionized water, open stirring, modified dextrins is uniformly disperseed
In aqueous phase, modified dextrins dispersion liquid is obtained；
（2）, fruity bouquet type composition is added drop-wise to step（1）In the modified dextrins dispersion liquid of gained, continue to stir, make perfume (or spice)
Essence is uniformly dispersed, and modified dextrins is formed the cladding to essence molecule, obtains the fruity floral type sustained release essence of Longaacting fragrance-aretaining.
（3）, ethanol is added to step（2）In the fruity floral type sustained release essence of the Longaacting fragrance-aretaining of gained, continue to stir equal
It is even, add antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.The perfume has
The odor characteristic of the fruity fragrance of a flower, citrus fruit note is laid particular stress on, and aroma strength is slightly strong.The perfume is prepared with uncoated essence
Common perfume carries out sensory evaluation by hearing fragrant paper, and the perfume can still feel obvious fragrance after 15 days, and common perfume is after 2 days
Almost just it is not felt by fragrance.
Above-mentioned fruity bouquet type composition, it is characterised in that described fruity bouquet type composition count by weight percentage,
It is constituted and content is as follows：
Orange oil 3% (3g)
Lemon oil 3% (3g)
Grapefruit oil 3% (3g)
Firpene 0.3% (0.3g)
Laurene 0.3% (0.3g)
Phellandrene 0.08% (0.08g)
Limonene 10% (10g)
Grapefruit methane 0.5% (0.5g)
Leaf-alcohol 0.1% (0.1g)
Ligustral 0.01% (0.01g)
Calamus alkene 0.05% (0.05g)
Bergamio 0.01% (0.01g)
Carbitol 0.8% (0.8g)
Carypohyllene 0.01% (0.01g)
Linalool 0.03% (0.03g)
Fanesol 0.01% (0.01g)
Anethole 0.1% (0.1g)
Terpinol 0.01% (0.01g)
Valencia Orange alkene 0.06% (0.06g)
Geranyl acetate 0.005% (0.005g)
Citronellol 2% (2g)
DPG 0.1% (0.1g)
Geraniol 0.7% (0.7g)
Alpha, beta-lonone 0.1% (0.1g)
Laurine 1.5% (1.5g)
Carrot seed alcohol 0.1% (0.1g)
Isopropyl myristate 1% (1g)
It is graceful can rowland 1% (1g)
Ambrotone 5% (5g)
Ambrox 0.1% (0.1g)
MDJ 10% (10g)
First position hexyl cinnamic aldehyde 3% (3g)
Sunflower seed Moschus 0.5% (0.5g)
Helional 0.9% (0.9g)
Triethyl citrate 0.1% (0.1g)
OctMet 3% (3g)
Astrotone 10% (10g)
Ethanol 39.525% (39.525g)；
Method preparation is prepared by the following procedure in above-mentioned fruity bouquet type composition, and its preparation process specifically includes following steps：
By orange oil, lemon oil, grapefruit oil, firpene, laurene, phellandrene, limonene, grapefruit methane, leaf-alcohol, glossy privet
Aldehyde, Calamus alkene, bergamio, carbitol, carypohyllene, linalool, fanesol, anethole, terpinol, valencia Orange
Alkene, geranyl acetate, citronellol, DPG, geraniol, alpha, beta-lonone, laurine, carrot seed alcohol, nutmeg
Isopropyl propionate, it is graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, sunflower seed Moschus,
Uniformly mixing obtains fruity floral type for helional, triethyl citrate, OctMet, astrotone, ethanol
Essence.Obtained essence fragrance is fine and smooth, and citrus fruit note is laid particular stress on, the characteristic perfume with the fruity fragrance of a flower.
Embodiment 3
A kind of Longaacting fragrance-aretaining fruity floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and
Content is as follows：
Fruity bouquet type composition 15% (15g)
Modified dextrins 20% (20g)
Deionized water 30% (30g)
Antioxidant 0.5% (0.5g)
Ethanol 34.5% (34.5g)；
A kind of above-mentioned Longaacting fragrance-aretaining fruity floral type perfume is prepared via a method which that the preparation process includes following step
Suddenly：
（1）, add modified dextrins in a reservoir, add deionized water, open stirring, modified dextrins is uniformly disperseed
In aqueous phase, modified dextrins dispersion liquid is obtained；
（2）, fruity bouquet type composition is added drop-wise to step（1）In the modified dextrins dispersion liquid of gained, continue to stir, make perfume (or spice)
Essence is uniformly dispersed, and modified dextrins is formed the cladding to essence molecule, obtains the fruity floral type sustained release essence of Longaacting fragrance-aretaining.
（3）, ethanol is added to step（2）In the fruity floral type sustained release essence of the Longaacting fragrance-aretaining of gained, continue to stir equal
It is even, add antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.The perfume fragrance
Moderate strength, fragrance is coordinated, the feature note with the fruity fragrance of a flower.The common perfume (or spice) that the perfume is prepared with uncoated essence
Water carries out sensory evaluation by hearing fragrant paper, and the perfume can still feel obvious fragrance after 15 days, and common perfume after 2 days almost
It is not felt by fragrance.
Above-mentioned fruity bouquet type composition, it is characterised in that described fruity bouquet type composition count by weight percentage,
It is constituted and content is as follows：
Orange oil 1.5% (1.5g)
Lemon oil 1.5% (1.5g)
Grapefruit oil 1.5% (1.5g)
Firpene 0.8% (0.8g)
Laurene 0.2% (0.2g)
Phellandrene 0.2% (0.2g)
Limonene 6% (6g)
Grapefruit methane 1% (1g)
Leaf-alcohol 0.05% (0.05g)
Ligustral 0.05% (0.05g)
Calamus alkene 0.03% (0.03g)
Bergamio 0.03% (0.03g)
Carbitol 0.5% (0.5g)
Carypohyllene 0.1% (0.1g)
Linalool 0.02% (0.02g)
Fanesol 0.02% (0.02g)
Anethole 0.05% (0.05g)
Terpinol 0.04% (0.04g)
Valencia Orange alkene 0.03% (0.03g)
Geranyl acetate 0.02% (0.02g)
Citronellol 1.5% (1.5g)
DPG 0.7% (0.7g)
Geraniol 0.4% (0.4g)
Alpha, beta-lonone 0.3% (0.3g)
Laurine 1% (1g)
Carrot seed alcohol 0.3% (0.3g)
Isopropyl myristate 0.5% (0.5g)
It is graceful can rowland 3% (3g)
Ambrotone 12% (12g)
Ambrox 0.05% (0.05g)
MDJ 17% (17g)
First position hexyl cinnamic aldehyde 2% (2g)
Sunflower seed Moschus 1.2% (1.2g)
Helional 0.5% (0.5g)
Triethyl citrate 0.3% (0.3g)
OctMet 2% (2g)
Astrotone 15% (15g)
Ethanol 28.61% (28.61g)；
Method preparation is prepared by the following procedure in above-mentioned fruity bouquet type composition, and its preparation process specifically includes following steps：
By orange oil, lemon oil, grapefruit oil, firpene, laurene, phellandrene, limonene, grapefruit methane, leaf-alcohol, glossy privet
Aldehyde, Calamus alkene, bergamio, carbitol, carypohyllene, linalool, fanesol, anethole, terpinol, valencia Orange
Alkene, geranyl acetate, citronellol, DPG, geraniol, alpha, beta-lonone, laurine, carrot seed alcohol, nutmeg
Isopropyl propionate, it is graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, sunflower seed Moschus,
Uniformly mixing obtains fruity floral type for helional, triethyl citrate, OctMet, astrotone, ethanol
Essence.Obtained essence fragrance is coordinated, the characteristic perfume with the fruity fragrance of a flower.
Above said content is only the basic explanation under present inventive concept, and times that technique according to the invention scheme is done
What equivalent transformation, belongs to the scope of protection of the invention.
Claims (2)
1. a kind of Longaacting fragrance-aretaining fruity floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and contain
Amount is as follows：
Fruity bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Count by weight percentage, it is constituted described fruity bouquet type composition and content is as follows：
Orange oil 1%-3%；
Lemon oil 1%-3%；
Grapefruit oil 1%-3%；
Firpene 0.3%-1.2%；
Laurene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Leaf-alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Calamus alkene 0.005%-0.05%；
Bergamio 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Carypohyllene 0.01%-0.2%；
Linalool 0.01%-0.03%
Fanesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpinol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
DPG 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Laurine 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
It is graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Sunflower seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%；
Astrotone 10%-30%
Surplus is the second ethanol；
A kind of preparation method of above-mentioned Longaacting fragrance-aretaining fruity floral type perfume comprises the following steps：
1）One the step of prepare fruity bouquet type composition, by orange oil, lemon oil, grapefruit oil, firpene, laurene, phellandrene,
Limonene, grapefruit methane, leaf-alcohol, ligustral, Calamus alkene, bergamio, carbitol, carypohyllene, linalool, fanesol,
Anethole, terpinol, valencia Orange alkene, geranyl acetate, citronellol, DPG, geraniol, alpha, beta-lonone, hydroxyl
Base citronellal, carrot seed alcohol, isopropyl myristate, it is graceful can rowland, ambrotone, ambrox, the sour first of dihydro jasmone
Ester, first position hexyl cinnamic aldehyde, sunflower seed Moschus, helional, triethyl citrate, OctMet, astrotone, the
Uniformly mixing obtains fruity bouquet type composition to diethanol；
2）Modified dextrins are added in a reservoir, deionized water is added, and are opened stirring, modified dextrins is uniformly dispersed in aqueous phase
In, obtain modified dextrins dispersion liquid；
3）Fruity bouquet type composition is added drop-wise to step 2）In the modified dextrins dispersion liquid of gained, continue to stir, disperse essence
Uniformly, and modified dextrins is formed the cladding to essence molecule, obtain the fruity floral type sustained release essence of Longaacting fragrance-aretaining；
4）First ethanol is added to step 3）In the fruity floral type sustained release essence of the Longaacting fragrance-aretaining of gained, continue to stir,
Add antioxidant, stirring and dissolving, by the fruity floral type perfume for being aged, being filtrated to get Longaacting fragrance-aretaining.
2. a kind of fruity bouquet type composition, it is characterised in that count by weight percentage, it is constituted and content is as follows：
Orange oil 1%-3%；
Lemon oil 1%-3%；
Grapefruit oil 1%-3%；
Firpene 0.3%-1.2%；
Laurene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Leaf-alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Calamus alkene 0.005%-0.05%；
Bergamio 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Carypohyllene 0.01%-0.2%；
Linalool 0.01%-0.03%；
Fanesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpinol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
DPG 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Laurine 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
It is graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Sunflower seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%
Astrotone 10%-30%；
Surplus is the second ethanol.
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| CN1344788A (en) * | 2001-10-17 | 2002-04-17 | 熊学敏 | Jinbianruixiang flower perfume and its supercritical extraction process |
| CN101618003A (en) * | 2008-07-06 | 2010-01-06 | 朱述兴 | Preparation method of lucid ganoderma essence |
| CN102703221A (en) * | 2012-05-29 | 2012-10-03 | 商洛学院 | Preparation method of rose essence beta-cyclodextrin polymer microsphere inclusion compound |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1344788A (en) * | 2001-10-17 | 2002-04-17 | 熊学敏 | Jinbianruixiang flower perfume and its supercritical extraction process |
| CN101618003A (en) * | 2008-07-06 | 2010-01-06 | 朱述兴 | Preparation method of lucid ganoderma essence |
| CN102703221A (en) * | 2012-05-29 | 2012-10-03 | 商洛学院 | Preparation method of rose essence beta-cyclodextrin polymer microsphere inclusion compound |
Non-Patent Citations (1)
| Title |
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| 玫瑰香精—羟丙基-β-环糊精包合物的制备及其性能表征的研究;吕翠翠;《中国优秀硕士学位论文》;20151231(第5期);第"2.2.1"实验原理 * |
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