CN106109272A - A kind of Longaacting fragrance-aretaining fruital floral type perfume and preparation method thereof - Google Patents

A kind of Longaacting fragrance-aretaining fruital floral type perfume and preparation method thereof Download PDF

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CN106109272A
CN106109272A CN201610525722.8A CN201610525722A CN106109272A CN 106109272 A CN106109272 A CN 106109272A CN 201610525722 A CN201610525722 A CN 201610525722A CN 106109272 A CN106109272 A CN 106109272A
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fruital
aretaining
fragrance
perfume
essence
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CN106109272B (en
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肖作兵
朱广用
周如隽
牛云蔚
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Shanghai Institute of Technology
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Shanghai Institute of Technology
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/342—Alcohols having more than seven atoms in an unbroken chain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/345—Alcohols containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/347—Phenols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/35—Ketones, e.g. benzophenone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract

A kind of Longaacting fragrance-aretaining fruital floral type perfume, calculates according to mass ratio, and fruital bouquet type composition by 10% 30%, the modified dextrins of 5% 20%, the deionized water of 10% 30%, the antioxidant of 0.1% 1%, the first ethanol of surplus form；Additionally provide the preparation method of above-mentioned perfume, add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in aqueous phase；Fruital bouquet type composition is added drop-wise in modified dextrins dispersion liquid, continues stirring, make essence be uniformly dispersed, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining；Being added to by first ethanol in the fruital floral type slow release essence of Longaacting fragrance-aretaining, continue to stir, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.The fruital floral type perfume fragrance of the Longaacting fragrance-aretaining that the present invention obtains is fine and smooth, and lasting is lasting.

Description

A kind of Longaacting fragrance-aretaining fruital floral type perfume and preparation method thereof
Technical field
The invention belongs to chemical field, relate to a kind of perfume, specifically a kind of Longaacting fragrance-aretaining fruital floral type perfume And preparation method thereof.
Background technology
Along with improving constantly of the development in epoch, the progress of science, human material and culture life, as the perfume (or spice) of cosmetics Water is quickly developed.Perfume can be divided mainly into three kinds of different forms, i.e. alcohol liquid, emulsion and pulpous state liquid, generally speaking Perfume is formulated by spice and solvent institute, and solvent used is mainly ethanol, according to essence fragrance used by perfume not With, perfume is also classified into multiple odor type.Perfume fragrance is strong, and Main Function is to be sprayed on the hem, handkerchief and hair decorations, gives out happy people Fragrance, for make up necessary.
The aroma quality of essence is the principal element of perfume quality, and the design of perfume essence odor type and type selecting are perfume Crucial.Traditional perfume is the mixture of essence and ethanol, and essence is by having volatile multiple spice in note ratio group The mixture become, volatile during directly use, fragrance remaining time is short, therefore, the design of perfume fragrance odor type and having The development of the essence of Longaacting fragrance-aretaining has very important significance.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of Longaacting fragrance-aretaining fruital floral type perfume and Its preparation method, described this Longaacting fragrance-aretaining fruital floral type perfume and preparation method thereof to solve perfume of the prior art The technical problem that fragrance remaining time is short.
The invention provides a kind of Longaacting fragrance-aretaining fruital floral type perfume, count by weight percentage, the composition of its raw material And content is as follows:
Fruital bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Count by weight percentage, its composition and content are as follows for described fruital bouquet type composition:
Oleum Citri sinensis 1%-3%；
Fructus Citri Limoniae oil 1%-3%；
Oleum Citri grandis 1%-3%；
Pinene 0.3%-1.2%；
Myrcene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Folic alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Rhizoma Acori Calami alkene 0.005%-0.05%；
Linalyl acetate 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Caryophyllene 0.01%-0.2%；
Linalool 0.01%-0.03%
Farnesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpineol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
Dipropylene glycol 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Hydroxycitronellal 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
Graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%；
Astrotone 10%-30%
Surplus is the second ethanol.
Present invention also offers a kind of fruital bouquet type composition, count by weight percentage, its composition and content are as follows:
Oleum Citri sinensis 1%-3%；
Fructus Citri Limoniae oil 1%-3%；
Oleum Citri grandis 1%-3%；
Pinene 0.3%-1.2%；
Myrcene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Folic alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Rhizoma Acori Calami alkene 0.005%-0.05%；
Linalyl acetate 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Caryophyllene 0.01%-0.2%；
Linalool 0.01%-0.03%；
Farnesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpineol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
Dipropylene glycol 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Hydroxycitronellal 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
Graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%
Astrotone 10%-30%；
Surplus is the second ethanol.
Further, described modified dextrins is a kind of derivant of starch, is a kind of commercially available prod, can be as wall Material, is coated with essence, makes essence slowly discharge, and increases the lasting of essence.
Present invention also offers the preparation method of above-mentioned a kind of Longaacting fragrance-aretaining fruital floral type perfume, including walking as follows Rapid:
1) each reacting substance is weighed according to mass ratio；
2) step preparing fruital bouquet type composition, by oleum Citri sinensis, Fructus Citri Limoniae oil, Oleum Citri grandis, pinene, myrcene, phellandrene, Limonene, grapefruit methane, folic alcohol, ligustral, Rhizoma Acori Calami alkene, linalyl acetate, carbitol, caryophyllene, linalool, farnesol, Anethole, terpineol, valencia Orange alkene, geranyl acetate, citronellol, dipropylene glycol, geraniol, alpha, beta-lonone, hydroxyl Base citronellal, carrot seed alcohol, isopropyl myristate, graceful can rowland, ambrotone, ambrox, dihydro jasmone acid first Ester, first position hexyl cinnamic aldehyde, certain herbaceous plants with big flowers seed Moschus, helional, triethyl citrate, OctMet, astrotone, Diethanol uniformly mixes and i.e. obtains fruital bouquet type composition.
3) add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in In aqueous phase, obtain modified dextrins dispersion liquid；
4) fruital bouquet type composition is added drop-wise in the modified dextrins dispersion liquid of step 3) gained, continues stirring, make essence disperse Uniformly, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining；
5), in the fruital floral type slow release essence of the Longaacting fragrance-aretaining that the first ethanol is added to step 4) gained, continue to stir, Adding antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.
The fruital fragrance of a flower is the odor type that people like, according to odor characteristic and the note of spice, chooses suitable raw material, allotment Go out soft aroma and, fine and smooth, there is the fruital bouquet type composition of fruital and fragrance of a flower rhythm；Then using modified dextrins is wall material, will To fruital bouquet type composition be coated with, thus improve the lasting of essence；Add a certain proportion of deionized water, ethanol and Antioxidant (butylated hydroxytoluene), obtains the fruital floral type perfume of Longaacting fragrance-aretaining.
The present invention compares with prior art, and its technological progress is significant.A kind of fruital flower of the Longaacting fragrance-aretaining of the present invention Odor type perfume, it is provided that a kind of exquisiteness, soft fruital fragrance of a flower odor type, and lasting is lasting.
Detailed description of the invention
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of Longaacting fragrance-aretaining fruital floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content As follows:
Fruital bouquet type composition 10%(10g)
Modified dextrins 5% (5g)
Deionized water 10% (10g)
Antioxidant 0.1% (0.1g)
Ethanol 74.9% (74.9g)；
Above-mentioned a kind of Longaacting fragrance-aretaining fruital floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by fruital bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the fruital floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.This perfume has The odor characteristic of the fruital fragrance of a flower, animal note lays particular stress on, and aroma strength is the most weak.This perfume is general with prepared by uncoated essence Logical perfume carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 10 days, and common perfume is several after 2 days Just it is not felt by fragrance.
Above-mentioned fruital bouquet type composition, it is characterised in that described fruital bouquet type composition count by weight percentage, Its composition and content are as follows:
Oleum Citri sinensis 1% (1g)
Fructus Citri Limoniae oil 1% (1g)
Oleum Citri grandis 1% (1g)
Pinene 1.2% (1.2g)
Myrcene 0.1% (0.1g)
Phellandrene 0.3% (0.3g)
Limonene 4% (4g)
Grapefruit methane 2% (2g)
Folic alcohol 0.01% (0.01g)
Ligustral 0.1% (0.1g)
Rhizoma Acori Calami alkene 0.005% (0.005g)
Linalyl acetate 0.05% (0.05g)
Carbitol 0.1% (0.1g)
Caryophyllene 0.2% (0.2g)
Linalool 0.01% (0.01g)
Farnesol 0.03% (0.03g)
Anethole 0.01% (0.01g)
Terpineol 0.07% (0.07g)
Valencia Orange alkene 0.01% (0.01g)
Geranyl acetate 0.04% (0.04g)
Citronellol 1% (1g)
Dipropylene glycol 1.2% (1.2g)
Geraniol 0.1% (0.1g)
Alpha, beta-lonone 0.5% (0.5g)
Hydroxycitronellal 0.5% (0.5g)
Carrot seed alcohol 0.6% (0.6g)
Isopropyl myristate 0.1% (0.1g)
Graceful can rowland 5% (5g)
Ambrotone 20% (20g)
Ambrox 0.01% (0.01g)
MDJ 25% (25g)
First position hexyl cinnamic aldehyde 1% (1g)
Certain herbaceous plants with big flowers seed Moschus 2% (2g)
Helional 0.1% (0.1g)
Triethyl citrate 0.6% (0.6g)
OctMet 1% (1g)
Astrotone 30% (30g)
Ethanol 0.055% (0.055g)；
Above-mentioned fruital bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By oleum Citri sinensis, Fructus Citri Limoniae oil, Oleum Citri grandis, pinene, myrcene, phellandrene, limonene, grapefruit methane, folic alcohol, ligustral, white Chang alkene, linalyl acetate, carbitol, caryophyllene, linalool, farnesol, anethole, terpineol, valencia Orange alkene, second Acid geraniol ester, citronellol, dipropylene glycol, geraniol, alpha, beta-lonone, hydroxycitronellal, carrot seed alcohol, myristic acid isopropyl Ester, graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, certain herbaceous plants with big flowers seed Moschus, new ocean jasmine Jasmine aldehyde, triethyl citrate, OctMet, astrotone, ethanol uniformly mix and i.e. obtain fruital bouquet type composition. The essence fragrance obtained is fine and smooth, and animal note is laid particular stress on, and has the characteristic perfume of the fruital fragrance of a flower.
Embodiment 2
A kind of Longaacting fragrance-aretaining fruital floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content As follows:
Fruital bouquet type composition 30% (30g)
Modified dextrins 12% (12g)
Deionized water 15% (15g)
Antioxidant 1% (1g)
Ethanol 39% (39g)；
Above-mentioned a kind of Longaacting fragrance-aretaining fruital floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by fruital bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the fruital floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.This perfume has The odor characteristic of the fruital fragrance of a flower, citrus fruit note lays particular stress on, and aroma strength is the strongest.Prepared by this perfume and uncoated essence Common perfume carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 15 days, and common perfume is after 2 days The most just it is not felt by fragrance.
Above-mentioned fruital bouquet type composition, it is characterised in that described fruital bouquet type composition count by weight percentage, Its composition and content are as follows:
Oleum Citri sinensis 3% (3g)
Fructus Citri Limoniae oil 3% (3g)
Oleum Citri grandis 3% (3g)
Pinene 0.3% (0.3g)
Myrcene 0.3% (0.3g)
Phellandrene 0.08% (0.08g)
Limonene 10% (10g)
Grapefruit methane 0.5% (0.5g)
Folic alcohol 0.1% (0.1g)
Ligustral 0.01% (0.01g)
Rhizoma Acori Calami alkene 0.05% (0.05g)
Linalyl acetate 0.01% (0.01g)
Carbitol 0.8% (0.8g)
Caryophyllene 0.01% (0.01g)
Linalool 0.03% (0.03g)
Farnesol 0.01% (0.01g)
Anethole 0.1% (0.1g)
Terpineol 0.01% (0.01g)
Valencia Orange alkene 0.06% (0.06g)
Geranyl acetate 0.005% (0.005g)
Citronellol 2% (2g)
Dipropylene glycol 0.1% (0.1g)
Geraniol 0.7% (0.7g)
Alpha, beta-lonone 0.1% (0.1g)
Hydroxycitronellal 1.5% (1.5g)
Carrot seed alcohol 0.1% (0.1g)
Isopropyl myristate 1% (1g)
Graceful can rowland 1% (1g)
Ambrotone 5% (5g)
Ambrox 0.1% (0.1g)
MDJ 10% (10g)
First position hexyl cinnamic aldehyde 3% (3g)
Certain herbaceous plants with big flowers seed Moschus 0.5% (0.5g)
Helional 0.9% (0.9g)
Triethyl citrate 0.1% (0.1g)
OctMet 3% (3g)
Astrotone 10% (10g)
Ethanol 39.525% (39.525g)；
Above-mentioned fruital bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By oleum Citri sinensis, Fructus Citri Limoniae oil, Oleum Citri grandis, pinene, myrcene, phellandrene, limonene, grapefruit methane, folic alcohol, ligustral, white Chang alkene, linalyl acetate, carbitol, caryophyllene, linalool, farnesol, anethole, terpineol, valencia Orange alkene, second Acid geraniol ester, citronellol, dipropylene glycol, geraniol, alpha, beta-lonone, hydroxycitronellal, carrot seed alcohol, myristic acid isopropyl Ester, graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, certain herbaceous plants with big flowers seed Moschus, new ocean jasmine Jasmine aldehyde, triethyl citrate, OctMet, astrotone, ethanol uniformly mix and i.e. obtain fruital bouquet type composition. The essence fragrance obtained is fine and smooth, and citrus fruit note is laid particular stress on, and has the characteristic perfume of the fruital fragrance of a flower.
Embodiment 3
A kind of Longaacting fragrance-aretaining fruital floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content As follows:
Fruital bouquet type composition 15% (15g)
Modified dextrins 20% (20g)
Deionized water 30% (30g)
Antioxidant 0.5% (0.5g)
Ethanol 34.5% (34.5g)；
Above-mentioned a kind of Longaacting fragrance-aretaining fruital floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by fruital bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the fruital floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.This perfume fragrance Moderate strength, fragrance is coordinated, is had the feature note of the fruital fragrance of a flower.That this perfume and uncoated essence are prepared is common fragrant Water carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 15 days, and common perfume after 2 days the most just It is not felt by fragrance.
Above-mentioned fruital bouquet type composition, it is characterised in that described fruital bouquet type composition count by weight percentage, Its composition and content are as follows:
Oleum Citri sinensis 1.5% (1.5g)
Fructus Citri Limoniae oil 1.5% (1.5g)
Oleum Citri grandis 1.5% (1.5g)
Pinene 0.8% (0.8g)
Myrcene 0.2% (0.2g)
Phellandrene 0.2% (0.2g)
Limonene 6% (6g)
Grapefruit methane 1% (1g)
Folic alcohol 0.05% (0.05g)
Ligustral 0.05% (0.05g)
Rhizoma Acori Calami alkene 0.03% (0.03g)
Linalyl acetate 0.03% (0.03g)
Carbitol 0.5% (0.5g)
Caryophyllene 0.1% (0.1g)
Linalool 0.02% (0.02g)
Farnesol 0.02% (0.02g)
Anethole 0.05% (0.05g)
Terpineol 0.04% (0.04g)
Valencia Orange alkene 0.03% (0.03g)
Geranyl acetate 0.02% (0.02g)
Citronellol 1.5% (1.5g)
Dipropylene glycol 0.7% (0.7g)
Geraniol 0.4% (0.4g)
Alpha, beta-lonone 0.3% (0.3g)
Hydroxycitronellal 1% (1g)
Carrot seed alcohol 0.3% (0.3g)
Isopropyl myristate 0.5% (0.5g)
Graceful can rowland 3% (3g)
Ambrotone 12% (12g)
Ambrox 0.05% (0.05g)
MDJ 17% (17g)
First position hexyl cinnamic aldehyde 2% (2g)
Certain herbaceous plants with big flowers seed Moschus 1.2% (1.2g)
Helional 0.5% (0.5g)
Triethyl citrate 0.3% (0.3g)
OctMet 2% (2g)
Astrotone 15% (15g)
Ethanol 28.61% (28.61g)；
Above-mentioned fruital bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By oleum Citri sinensis, Fructus Citri Limoniae oil, Oleum Citri grandis, pinene, myrcene, phellandrene, limonene, grapefruit methane, folic alcohol, ligustral, white Chang alkene, linalyl acetate, carbitol, caryophyllene, linalool, farnesol, anethole, terpineol, valencia Orange alkene, second Acid geraniol ester, citronellol, dipropylene glycol, geraniol, alpha, beta-lonone, hydroxycitronellal, carrot seed alcohol, myristic acid isopropyl Ester, graceful can rowland, ambrotone, ambrox, MDJ, first position hexyl cinnamic aldehyde, certain herbaceous plants with big flowers seed Moschus, new ocean jasmine Jasmine aldehyde, triethyl citrate, OctMet, astrotone, ethanol uniformly mix and i.e. obtain fruital bouquet type composition. The essence fragrance obtained is coordinated, and has the characteristic perfume of the fruital fragrance of a flower.
Above said content is only the basic explanation under present inventive concept, and according to appointing that technical scheme is done What equivalent transformation, belongs to the scope of protection of the invention.

Claims (3)

1. a Longaacting fragrance-aretaining fruital floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and containing Measure as follows:
Fruital bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Count by weight percentage, its composition and content are as follows for described fruital bouquet type composition:
Oleum Citri sinensis 1%-3%；
Fructus Citri Limoniae oil 1%-3%；
Oleum Citri grandis 1%-3%；
Pinene 0.3%-1.2%；
Myrcene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Folic alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Rhizoma Acori Calami alkene 0.005%-0.05%；
Linalyl acetate 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Caryophyllene 0.01%-0.2%；
Linalool 0.01%-0.03%
Farnesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpineol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
Dipropylene glycol 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Hydroxycitronellal 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
Graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%；
Astrotone 10%-30%
Surplus is the second ethanol.
2. the preparation method of a kind of Longaacting fragrance-aretaining fruital floral type perfume described in claim 1, it is characterised in that include as follows Step:
1) each reacting substance is weighed according to mass ratio；
2) step preparing fruital bouquet type composition, by oleum Citri sinensis, Fructus Citri Limoniae oil, Oleum Citri grandis, pinene, myrcene, phellandrene, Limonene, grapefruit methane, folic alcohol, ligustral, Rhizoma Acori Calami alkene, linalyl acetate, carbitol, caryophyllene, linalool, farnesol, Anethole, terpineol, valencia Orange alkene, geranyl acetate, citronellol, dipropylene glycol, geraniol, alpha, beta-lonone, hydroxyl Base citronellal, carrot seed alcohol, isopropyl myristate, graceful can rowland, ambrotone, ambrox, dihydro jasmone acid first Ester, first position hexyl cinnamic aldehyde, certain herbaceous plants with big flowers seed Moschus, helional, triethyl citrate, OctMet, astrotone, Diethanol uniformly mixes and i.e. obtains fruital bouquet type composition；
3) add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in aqueous phase In, obtain modified dextrins dispersion liquid；
4) fruital bouquet type composition is added drop-wise in the modified dextrins dispersion liquid of step 3) gained, continues stirring, make essence disperse Uniformly, and make modified dextrins form the cladding to essence molecule, obtain the fruital floral type slow release essence of Longaacting fragrance-aretaining；
5), in the fruital floral type slow release essence of the Longaacting fragrance-aretaining that the first ethanol is added to step 4) gained, continue to stir, Adding antioxidant, stirring and dissolving, through being aged, be filtrated to get the fruital floral type perfume of Longaacting fragrance-aretaining.
3. a fruital bouquet type composition, it is characterised in that count by weight percentage, its composition and content are as follows:
Oleum Citri sinensis 1%-3%；
Fructus Citri Limoniae oil 1%-3%；
Oleum Citri grandis 1%-3%；
Pinene 0.3%-1.2%；
Myrcene 0.1%-0.3%；
Phellandrene 0.08%-0.3%；
Limonene 4%-10%；
Grapefruit methane 0.5%-2%；
Folic alcohol 0.01%-0.1%；
Ligustral 0.01%-0.1%；
Rhizoma Acori Calami alkene 0.005%-0.05%；
Linalyl acetate 0.01%-0.05%；
Carbitol 0.1%-0.8%；
Caryophyllene 0.01%-0.2%；
Linalool 0.01%-0.03%；
Farnesol 0.01%-0.03%；
Anethole 0.01%-0.1%；
Terpineol 0.01%-0.07%；
Valencia Orange alkene 0.01%-0.06%；
Geranyl acetate 0.005%-0.04%；
Citronellol 1%-2%；
Dipropylene glycol 0.1%-1.2%；
Geraniol 0.1%-0.7%；
Alpha, beta-lonone 0.1%-0.5%；
Hydroxycitronellal 0.5%-1.5%；
Carrot seed alcohol 0.1%-0.6%；
Isopropyl myristate 0.1%-1%；
Graceful can rowland 1%-5%；
Ambrotone 5%-20%；
Ambrox 0.01%-0.1%；
MDJ 10%-25%；
First position hexyl cinnamic aldehyde 1%-3%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-2%；
Helional 0.1%-0.9%；
Triethyl citrate 0.1%-0.6%；
OctMet 1%-3%
Astrotone 10%-30%；
Surplus is the second ethanol.
CN201610525722.8A 2016-07-06 2016-07-06 A kind of Longaacting fragrance-aretaining fruity floral type perfume and preparation method thereof Expired - Fee Related CN106109272B (en)

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