KR101849981B1 - Perfume composition having the fragrnace of flower of tagetes minuta - Google Patents

Abstract

The present invention relates to a fragrance composition having a fragrance of marigold flowers, which comprises 0.1 to 2% by weight of tagete oil, 0.1 to 1% by weight of leek oil, 0.5 to 2% by weight of veterinary oil, 3 to 9 wt% of wood oil, 2 to 6 wt% of bergamot oil, 1.5 to 4.5 wt% of sweet orange oil, 2 to 5 wt% of lemon oil, 0.5 to 2 wt% of peppermint oil, 10 to 30 wt% The present invention relates to a cosmetic composition comprising a super 7 to 20% by weight, ethylenerglyle 3 to 9% by weight, phenoxanols 3 to 9% by weight, styrallylacetate 2 to 5% by weight, linalyl acetate 2 to 5% by weight, galactosolide 1 to 5 1 to 5% by weight of alpha-isomethylionone, 1 to 5% by weight of coumarin, 0.5 to 2% by weight of lily acid and 0.1 to 2% by weight of ethyl maltol.

Description

TECHNICAL FIELD [0001] The present invention relates to a perfume composition having a fragrance of marigold flowers,

The present invention relates to a flavor composition recreating the fragrance of marigold flowers, and more particularly, to fragrance compositions that reproduce fragrance of marigold flowers, and more particularly to fragrance compositions containing fragrance compositions of Tagget oil, Buchu oil, Vetyver oil, Cedarwood oil, Bergamot oil, Oil, sweet orange oil, lemon oil, and peppermint oil and a synthetic perfume.

Tagetes minuta is native to South America and Mexico and now grows in Africa, Europe, Asia, and North America. It is a perennial herb that grows up to about 30cm in height. Its flower is bright orange and similar to daisy. Leaves are egg-shaped and dark green.

In India, marigold is harvested when it is blossomed, distilled and mixed with a solvent containing sandalwood oil to create a fragrance called attar genda, and in China, it has an exotic marigold flower, Abdominal pain, mumps, mastitis, and eye pain.

The taget is mostly produced in South Africa, France, Argentina, and Egypt, and its color is a dark orange or yellow oil with a sweet green fruit flavor. The main ingredient is Tagetone, which is ocimene, myrcene, linalool, limonene, pinene, carvone, citral, (camphene), valeric acid, and the like. TAGETONE, the main component of oil, is an aliphatic compound of ketones. Ketones are used as sedatives and mucous membrane remedies. They help to treat wounds quickly but they can cause side effects. Do.

Natural essential oils play an important role in enhancing palatability in perfumes and foods, but they have limitations that vary in flavor and price depending on the time of cultivation and environment. In order to keep the fragrance of such natural oil constant, a method of increasing the palatability of the product by keeping a natural fragrance of a certain quality by combining synthetic fragrance with a certain natural essential oil has been widely used.

Korean Patent No. 10-1608883 discloses a perfume composition having a Cymbidium goeringii Reichb flower scent.

In the present invention, a study was conducted to reproduce the fragrance of marigold oil using natural fragrance and synthetic fragrance. As a result, it was found that Tagete oil, Buchu oil, Vetyver oil, Cedarwood oil, Bergamot Oil, Sweet Orange Oil, Lemon Oil and Peppermint Oil, and Hedione, Iso E Super, Ethyl linalool, Phenoxanol, Styrallyl Acetate, Synthesis of Lilyl acetate, Galaxolide, Alpha-isomethyl ionone, Coumarine, Lilial, and Ethyl maltol were synthesized in the same manner as in Example 1, The fragrance can be reproduced at a certain ratio to reproduce the fragrance of natural marigold, thereby completing the present invention.

The present invention relates to a fragrance composition having a scent of marigold flowers, which comprises 0.1 to 2% by weight of tartrate oil, 0.1 to 1% by weight of leek oil, 0.5 to 2% by weight of veterinary oil, cedarwood oil 3 From 2 to 6% by weight of bergamot oil, from 1.5 to 4.5% by weight of sweet orange oil, from 2 to 5% by weight of lemon oil, from 0.5 to 2% by weight of peppermint oil, from 10 to 30% From 1 to 5% by weight of linalool acetate, from 3 to 9% by weight of ethylenually, from 3 to 9% by weight of phenoxanol, from 2 to 5% by weight of styrallylacetate, from 2 to 5% 1 to 5% by weight of alpha-isomethylionone, 1 to 5% by weight of coumarin, 0.5 to 2% by weight of lily and 0.1 to 2% by weight of ethyl maltol.

Furthermore, the object of the present invention is achieved by a cosmetic composition or an external preparation for skin containing the perfume composition.

The present invention relates to a method for the treatment and / or prophylaxis of rheumatoid arthritis, including, but not limited to, tartrate oil, leek oil, vetiver oil, cedar wood oil, bergamot oil, sweet orange oil, lemon oil, peppermint oil, It is possible to provide scent of marigold by using this perfume composition as a perfume composition containing acetate, galactoside, alpha-isomethylionone, coumarin, lily, ethyl maltol.

The perfume composition according to the present invention is natural, warm and sweet, has a pleasant woody flavor and is not only excellent in palatability but also rich in other fragrances and can be used for perfumes and cosmetics. Also, the perfume composition according to the present invention can be applied variously to orient products, skin care products, and the like.

In addition, the perfume composition according to the present invention is applicable to an external preparation for skin.

Unless defined otherwise, all technical terms used in the present invention have the following definitions and are consistent with the meaning as commonly understood by one of ordinary skill in the art to which this invention pertains. Also, preferred methods or samples are described in this specification, but similar or equivalent ones are also included in the scope of the present invention. The contents of all publications referred to herein are incorporated herein by reference. The term " drug " is used in reference to a reference amount, level, value, number, frequency, percentage, dimension, size, amount, weight, or length of 30, 25, 20, 25, 10, 9, 8, 7, 6, Level, value, number, frequency, percentage, dimension, size, quantity, weight or length of a sample,

Throughout this specification, the words " comprising " and " comprising ", unless the context clearly requires otherwise, include the steps or components, or groups of steps or elements, And that they are not excluded.

It is an object of the present invention to provide a fragrance composition that reproduces fragrance of marigold flowers. Specifically, the perfume composition according to the present invention can be used as a perfume composition, such as tablets oil, vermiculite oil, vetiver oil, cedarwood oil, bergamot oil, sweet orange oil, lemon oil, peppermint oil and herdone, isosuper, The composition according to the present invention may contain, as the active ingredient, stearyl acetate, linalyl acetate, galactosylide, alpha-isomethylionone, coumarin, lily and ethyl maltol as active ingredients. More specifically, 0.1 to 2 wt% tartach oil, 0.1 to 1 wt% of leek oil, 0.5 to 2 wt% of vetiver oil, 3 to 9 wt% of cedarwood oil, 2 to 6 wt% of bergamot oil, 1.5 to 4.5 wt% From 2 to 5% by weight of lemon oil, from 0.5 to 2% by weight of peppermint oil, from 10 to 30% by weight of hydrazine, from 7 to 20% by weight of iso-super, from 3 to 9% by weight of ethyl linoleate, 3 to 9 wt%, styrallylacetate 2 to 5 wt%, linalyl acetate 2 to 5 wt%, galactosolide 1 to 5 wt%, alpha-isomethylionone 1 to 5 wt%, coumarin 1 to 5 wt% %, 0.5 to 2% by weight of lily alcohol, and 0.1 to 2% by weight of ethyl maltol. When the content of the oil is out of the above range with respect to the total weight of the composition, the expected effect can not be obtained and the preference of the fragrance is remarkably decreased to lower the value of the product.

Tagetes minuta oil is mostly produced in South Africa, France, Argentina, and Egypt, and its color is a dark orange or yellow oil with a sweet green fruit flavor. The main ingredient is Tagetone, which is an ocimene, myrcene, linalool, limonene, pinene, carvone, citral, (camphene), valeric acid, and the like.

Leek (agotbosma betulina) is a plant native to South Africa. Leaves are used locally for the purpose of exterminating the antiseptic effect and insects. Western herbal medicine has been used to infect urinary tract infections such as cystitis, urethritis, and prostatitis, and has been recorded for use in the UK herbal pharmacopoeia to treat bladder inflammation. The oil is a dark yellowish brown liquid with a scent like mint and camphor. The major constituent is diosphene (25-40%).

Vetiveria zizanoides is a Poaceae plant that grows in southern India and Indonesia and forms a large discard of 1 to 2 meters high. Leaves are 1 cm wide and somewhat white in color. Vetiver extracts vetiver oil from the root and root, which is known as "the oil that brings peace" in India and Sri Lanka. Vetiver oil is a dark brown, orange, and olive viscous oil, which is rich in dark musk, wood, and sweet scent. Vetiver oil is a rich, unique and complex fragrance that is used as a base and fixative in fragrances to help make fragrances rich and long lasting. In aromatherapy, vetiver oil is used effectively for acne, oily skin, arthritis, myalgia and depression and insomnia. The main constituents are vetiverol, vetivone, vetivenes and terpenes.

Cedarwood (Juniperus asliei) is native to the southwestern and central parts of the United States, Mexico. Cedarwood oil is a colorless or pale yellow liquid containing sweet and balsam that smells like a pencil. In New Mexico, Native Americans used skin rashes, and in aromatherapy, cedarwood oil is used for arthritis, rheumatism, and stress-related diseases. The main constituents are cedrene, cedrol, thujopsene, and sabinene.

Citrus bergamia oil is an extract of bergamot that is native to the equatorial Asian region. It is a light greenish yellow liquid with a cool fruity flavor and a thin scent of spicy balsam. Recent studies in Italy have shown very good effects on skin, respiratory and urinary tract infections, and the main constituents are linalyl acetate, linalool, and other alcohols, sesquiterpenes.

Citrus sinensis oil is an oil that is mainly produced in Israel, Cyprus, Brazil and North America. It is yellowish orange, fresh, and has a soft fruit flavor. In aromatherapy, sweet orange oil is used as an anti-depressant, anti-inflammatory, cosmetic, perfume and detergent. Major constituents are more than 90% monoterpenes, most of which are limonene.

Lemon (Citrus Limon) oil is an oil extracted by cooling crushing fresh fruit husk shells. It is grown in Asia, some eastern India, and cultivated extensively in Italy, Sicily and America. The major constituent is limonene, which is about 70%. It is also composed of pinene, sabinene, myrcene and citra l. In cosmetics and food, Widely used.

Peppermint (mentba piperita) has been cultivated in China and Japan for a long time and has been used for various symptoms such as indigestion, nausea, sore throat and abdominal pain in East and West. The oils are camphor fragrance with strong yellowish or green liquid stinging like strong mint. The main constituent is menthol 29-48%, menthyl acetate, minthofuran, limonene and so on.

Hedione is a substance that gives a freshness and a transparent floral scent. It is used for various fragrance types by giving a natural softness and a brilliant image.

Iso E Super has a scent of woody and amber and expresses incense smoothly like velvet.

Ethyl linalool is a fragrance with a fresh bergamot-like character. It has some woody and green fragrance along with a flower.

Phenoxanol is a fragrance that has the character of Rose and has green fragrance along with rose fragrance and affects the persistence of fragrance.

Styrallyl acetate has a fragrant green fragrance that can be felt in gardenias, plums, and apples.

Linalyl acetate is one of the major components of bergamot and lavender essential oils and has a herb-like aroma.

Galaxolide is a representative example of a musk fragrance that lengthens the consistency of the fragrance and gives a softer image.

Alpha-isomethyl ionone is a fragrant substance like violet woody which acts to strengthen the top and body of fragrance.

Coumarine is a substance found in many plants, giving off a sweet smell and acting as an insecticide in plants that produce coumarin.

Lilial is a substance that gives a moist, fresh floral feel, and is often used as a mucha and cyclamen note.

Ethyl maltol is also used as a spice in white solids with a sweet scent such as caramelised sugar and cooked fruit.

The perfume composition according to the present invention has an excellent fragrance such as marigold flowers and is cheaper than the essential oil of marigold, so that the price competitiveness of the product can be increased.

The perfume composition according to the present invention may be formulated not only as cosmetics such as lotions, creams, emulsions and the like but also as external preparations for skin such as ointments, soluble images, suspensions, gels, spray, papermaking, . The blending amount of each of these formulations may be suitably selected and blended in order to achieve the desired effect according to a conventional technique in the art, and may be contained in an amount of 0.001 to 30% by weight based on the total weight of the cosmetic composition have.

Hereinafter, the present invention will be described more specifically with reference to Examples. It will be understood by those of ordinary skill in the art that various changes in form and details may be made therein without departing from the spirit and scope of the present invention as defined by the following claims. something to do.

Manufacturing example  - Merigold  Preparation of perfume composition recreating floral fragrance

As a composition of the perfume composition according to the present invention, a perfume composition was prepared according to the composition shown in Table 1 below.

Component name (content:% by weight) Production Example 1 Production Example 2 Comparative Preparation Example 1 Comparative Production Example 2 Tar oil One One One One Leek oil 0.5 One - Vetiver oil One 2 One - Cedarwood oil 6 3 6 Bergamot oil 4 4 4 4 Sweet orange oil 3 3 3 3 Lemon oil 3.5 3.5 3.5 3.5 Peppermint oil 1.5 1.5 1.5 1.5 Hedione 20 20 20 20 Iso Super 14 14 14 14 Ethylenal 5.5 5.5 5.5 5.5 Phenoxanol 5.5 5.5 5.5 5.5 Styrallylacetate 3.5 3.5 3.5 3.5 Linalyl acetate 3.5 3.5 3.5 3.5 Galactoside 3 3 3 3 Alpha-isomethylionone 2.5 2.5 2.5 2.5 Coumarin 2.5 2.5 2.5 2.5 Lily 1.5 1.5 1.5 1.5 Ethyl maltol 0.5 0.5 0.5 0.5 Dipropylene glycol (solvent) 17.5 19 18 25 total 100 100 100 100

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Example  - Manufacture of perfume

To compare the flavor of the preparations 1 to 2 having the composition shown in the above Table 1 and the comparative preparations 1 to 2 and the fragrance of natural marigold flower oil (tagete essential oil) (Comparative Example 4, perfume F) Perfume was prepared as shown in Table 2.

Component name (content:% by weight) Example 1
(Fragrance A) Example 2
(Perfume B) Comparative Example 1
(Perfume C) Comparative Example 2
(Perfume D) Comparative Example 4
(Perfume F) ethanol 76.98 76.98 76.98 76.98 76.98 Uvinul A + B 0.02 0.02 0.02 0.02 0.02 Butylene glycol 3 3 3 3 3 Purified water 10 10 10 10 10 Tablet Essential Oil - - - - 10 Production Example 1 10 - - - - Production Example 2 - 10 - - - Comparative Preparation Example 1 - - 10 - - Comparative Production Example 2 - - - 10 -

Experimental Example  - sensory evaluation

The sensory evaluation was carried out on fifteen ordinary male and female persons aged from 20 to 50 years. The perfume of Examples 1 and 2, Comparative Examples 1 and 2, and 100% marigold essential oil alone (Comparative Example 4) (Question 1) and palatability (question 2) of the fragrance as shown in Table 3 were examined. The results are shown in Table 4, and the results of the fragrance preference (satisfaction) are shown in Table 5.

survey 1. Compare the fragrance F with the fragrance A to D perfume similarities.
(1) It is not at all similar.
(2) Not very similar.
(3) It is normal.
(4) It is somewhat similar.
(5) It is very similar. 2. What are the overall fragrance preferences (satisfaction) of fragrances A to D?
(1) Very dissatisfied.
(2) Not satisfied.
(3) It is normal.
(4) is satisfied.
(5) Very satisfied.
Flavor similarity comparison result Perfume A Perfume B Perfume C Perfume D ① not quite similar One 2 One 4 ② Not very similar One One 2 4 ③ It is normal. 2 2 3 3 ④ Somewhat similar 4 5 5 3 ⑤ It is very similar 7 5 4 One ④ + ⑤ (%) 11 (73%) 10 (67%) 9 (60%) 4 (27%)
Overall fragrance preference (satisfaction) Perfume A Perfume B Perfume C Perfume D Very unsatisfied 0 One 2 0 I am unsatisfied One One 3 One is average 2 3 One 6 Satisfies 10 9 8 6 Very satisfied 2 One One 2 ④ + ⑤ (%) 12 (80%) 10 (67%) 9 (60%) 8 (53%)
As can be seen in Tables 4 and 5, in the sensory evaluation against the general public, Examples 1 to 2 (Fragrances A and B) comprising Preparation Examples 1 and 2 prepared according to the present invention were 100% natural marigold It is most similar to the fragrance of fragrance (fragrance F) containing flower essential oil, and the fragrance preference is also excellent.

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Claims (3)

A fragrance composition having a scent of marigold flowers,
0.1 to 2 wt% of tagete oil, 0.1 to 1 wt% of leek oil, 0.5 to 2 wt% of veterinary oil, 3 to 9 wt% of cedarwood oil, 2 to 6 wt% of bergamot oil, 1.5 to 4.5% by weight of sweet orange oil, 2 to 5% by weight of lemon oil, 0.5 to 2% by weight of peppermint oil, 10 to 30% by weight of hydrazine, 7 to 20% 3 to 9 wt% of phenoxanol, 2 to 5 wt% of styrallylacetate, 2 to 5 wt% of linalool acetate, 1 to 5 wt% of galactosolide, 1 to 5 wt% of alpha-isomethylionone, 1 to 5% by weight, lily 0.5 to 2% by weight and ethyl maltol 0.1 to 2% by weight, based on the total weight of the fragrance composition. A cosmetic composition comprising the perfume composition of claim 1. delete