CN113201403A - Production device and method for preparing spice by distillation method - Google Patents

Production device and method for preparing spice by distillation method Download PDF

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Publication number
CN113201403A
CN113201403A CN202110434801.9A CN202110434801A CN113201403A CN 113201403 A CN113201403 A CN 113201403A CN 202110434801 A CN202110434801 A CN 202110434801A CN 113201403 A CN113201403 A CN 113201403A
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CN
China
Prior art keywords
condenser
flange
support
clamping
steam pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110434801.9A
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Chinese (zh)
Inventor
李祥林
傅厚明
许小勇
王建军
李群伟
祝汉平
傅娟娟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Spice Chemical Industrial Co ltd
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Jiangxi Spice Chemical Industrial Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Jiangxi Spice Chemical Industrial Co ltd filed Critical Jiangxi Spice Chemical Industrial Co ltd
Priority to CN202110434801.9A priority Critical patent/CN113201403A/en
Publication of CN113201403A publication Critical patent/CN113201403A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Seasonings (AREA)

Abstract

The invention discloses a production device and a method for preparing spice by using a distillation method, and the production device comprises a heating chamber, a concentration tank, a condenser and a liquid receiving tank, wherein the condenser is fixedly arranged at the top of the liquid receiving tank; be provided with supplementary mounting structure on the flange between adjacent equipment, when the flange installation, accessible auxiliary structure carries on spacingly, but make the device connect the installation when accurate installation, be convenient for establish soon fixedly, improved the device's practicality and convenience, the device is when using, when concentrated jar is placed, if ground is unsmooth, the bottom stable support of concentrated jar is adjusted to the accessible supporting shoe, avoid the device to incline when using and incline and fall, improved the device's stability and practicality.

Description

Production device and method for preparing spice by distillation method
Technical Field
The invention belongs to the technical field of concentrators, and particularly relates to a production device and a method for preparing spices by using a distillation method.
Background
Distillation is a common method for separating and purifying liquid mixtures, and can also measure the boiling point of liquid compounds, so that the method has certain significance for identifying pure liquid compounds, and the spice is a substance which can smell fragrance by smell or taste and is a raw material for preparing essence. The concentrator is a device for concentrating production process in the industries of traditional Chinese medicine, health care products, natural seasonings, food additives, food, chemical engineering and the like, and is widely applied to various fields of chemical industry, medicine production and processing industry, ore processing industry, sewage treatment and the like since the invention of the concentrator.
The existing production device and method for preparing spice by using a distillation method generally use the distillation device when the distillation method is used for preparing spice, so that the raw materials in liquid state are ensured to be separated out, related products are prepared, generally use a concentrator when the spice is prepared, generally connect a heating chamber, a concentrating tank and a condenser when the concentrator is used, ensure that the device can stably work, generally, when the device is installed and connected, alignment cannot be carried out during flange installation, the efficiency of connection between flanges is influenced, and the practicability of the device is reduced.
Disclosure of Invention
The invention aims to provide a production device and a method for preparing spices by using a distillation method, which aim to solve the problems that the conventional production device and the conventional production method for preparing spices by using the distillation method are provided in the background art, the distillation device is usually used when the spices are prepared by using the distillation method, raw materials in liquid state are ensured to be separated out so as to prepare related products, a concentrator is usually used when the spices are prepared, a heating chamber, a concentrating tank and a condenser are required to be connected when the concentrator is used, the stable operation of the device is ensured, and when the concentrator is usually installed and connected, the alignment cannot be carried out when flanges are installed, the connection efficiency between the flanges is influenced, and the practicability of the device is reduced.
In order to achieve the purpose, the invention provides the following technical scheme: a production device and a method for preparing spice by using a distillation method comprise a heating chamber, a concentration tank, a condenser and a liquid receiving tank, wherein the condenser is fixedly arranged at the top of the liquid receiving tank, the heating chamber is connected with the bottom of the concentration tank and is provided with a circulating pipe, the bottom of the concentration tank is fixedly welded with a support, a steam pipe is connected between the concentration tank and the condenser and is provided with a connecting flange, the steam pipe is connected with the connecting flange, the connecting flange comprises a first flange and a second flange, a clamping plate for four households in a ladder is welded on the first flange, an integrated clamping seat is welded on the second flange, the first flange and the second flange are clamped with the clamping plate in a sliding manner through the clamping seat, a limiting seat is welded at one end of the clamping seat, a limiting rod is in limiting connection at the inner side of the limiting seat, and a spring is sleeved at one end of the limiting rod, which is positioned at the inner side of the limiting seat, the clamping plate is provided with a positioning limiting hole, and the clamping seat and the clamping plate are connected with the positioning limiting hole in a limiting mode through a limiting rod.
Preferably, the bottom of the bracket is connected with a support block, the bottom of the inner side of the bracket is provided with a screw in a threaded manner, and the support block is fixedly arranged at one end of the screw.
Preferably, the bottom welding of concentrated jar has three support, and three support is triangular distribution, and the supporting shoe has all been installed to the bottom of three support simultaneously.
Preferably, the circulating pipe and the steam pipe are provided with connecting flanges with the same structure.
Preferably, two clamping plates and two clamping seats are symmetrically arranged at two ends of the first flange plate and the second flange plate.
Preferably, the bottom of one end of the condenser is provided with a cooling water inlet, and the top of the other end of the condenser is provided with a cooling water outlet.
Step 1; the heating chamber is communicated with a concentration tank, the concentration tank is communicated with a condenser, the concentration tank is connected with the condenser through a steam pipe, a connecting flange is arranged on the steam pipe, an auxiliary alignment structure is arranged on the connecting flange, the auxiliary alignment structure is convenient for connecting and installing the steam pipe, heat generated by combustion in the heating chamber is transferred into the concentration tank, the pressure in the concentration tank is increased, the liquid raw material is gradually boiled and evaporated, and liquid containing the raw material is distilled and separated out;
step 2; the generated gas enters the inner side of the condenser through the steam pipe, and the steam is liquefied to flow into the liquid receiving tank through the condensation effect of the snake-shaped condensation pipe on the inner side of the condenser, and the cooling water is introduced through the cooling water inlet when the condenser is cooled.
Compared with the prior art, the invention has the beneficial effects that:
(1) when the device is used, the auxiliary mounting structure is arranged on the flange between the adjacent devices, and when the flange is mounted, the auxiliary structure can be used for limiting, so that the device can be accurately mounted when being connected and mounted, the screw holes on the flange are aligned, the screwing and fixing are convenient, the practicability and convenience of the device are improved, and the mounting efficiency is improved;
(2) the device is when using, and concentrated jar can directly be placed subaerial usually, if ground unevenness, the unable stability in bottom of concentrated jar is placed, is equipped with the supporting shoe at the support facial make-up of this concentrated jar bottom, but the supporting shoe manually regulated, when concentrated jar is placed, if ground unevenness, the bottom stable support of concentrated jar is adjusted to the accessible supporting shoe, avoids the device to incline the side when using to fall, has improved the device's stability and practicality.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged schematic view of the attachment flange of the present invention;
FIG. 3 is a schematic top view of the flange of the present invention;
FIG. 4 is a schematic structural diagram of the card socket of the present invention;
FIG. 5 is an enlarged view of the structure of FIG. 1 at A according to the present invention;
in the figure: 1. a heating chamber; 2. a circulation pipe; 3. a support; 4. a support block; 5. a concentration tank; 6. a steam pipe; 7. a connecting flange; 8. a condenser; 9. a spring; 10. a screw; 11. a liquid receiving tank; 12. a limiting rod; 13. a limiting seat; 14. a card holder; 15. a first flange plate; 16. a second flange plate; 17. and (4) clamping the board.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, fig. 2, fig. 3, fig. 4 and fig. 5, the present invention provides a technical solution: a production device and a method for preparing spice by a distillation method comprise a heating chamber 1, a concentration tank 5, a condenser 8 and a liquid receiving tank 11, wherein the condenser 8 is fixedly arranged at the top of the liquid receiving tank 11, the heating chamber 1 is connected with the bottom of the concentration tank 5 and is provided with a circulating pipe 2, the bottom of the concentration tank 5 is fixedly welded with a support 3, a steam pipe 6 is connected between the concentration tank 5 and the condenser 8 and is provided with a connecting flange 7, the connecting flange 7 comprises a first flange 15 and a second flange 16, a ladder four-door clamping plate 17 is welded on the first flange 15, an integrated clamping seat 14 is welded on the second flange 16, the first flange 15 and the second flange 16 are clamped with the clamping plate 17 in a sliding manner through the clamping seat 14, one end of the clamping seat 14 is welded with a limiting seat 13, and the inner side of the limiting seat 13 is limited and connected with a limiting rod 12, the inboard cover that the one end of gag lever post 12 is located spacing seat 13 is equipped with spring 9, sets up the spacing hole of counterpointing on the cardboard 17, and cassette 14 passes through gag lever post 12 with spacing hole spacing connection with cardboard 17, and flange 7 when the installation, accessible auxiliary structure carries on spacingly, but makes the device connect the installation time accurate installation, guarantees that the screw counterpoints on the flange 7, is convenient for establish soon fixedly, has improved the device's practicality and convenience.
For better connection and usage, in this embodiment, preferably, the circulating pipe 2 and the steam pipe 6 are provided with the connecting flange 7 having the same structure, and for better limit, in this embodiment, preferably, two clamping plates 17 and clamping seats 14 are symmetrically provided at two ends of the first flange 15 and the second flange 16, so that the first flange 15 and the second flange 16 are stably aligned to avoid inclination and deviation, for cooling convenience, in this embodiment, preferably, a cooling water inlet is provided at a bottom of one end of the condenser 8, and a cooling water outlet is provided at a top of the other end of the condenser 8, for better stable placement, in this embodiment, preferably, the bottom of the bracket 3 is connected and provided with the supporting block 4, the screw 10 is screwed at a bottom of the inner side of the bracket 3, the supporting block 4 is fixedly provided at one end of the screw 10, and the supporting block 4 can be manually adjusted to ascend and descend when placed, the device of being convenient for is stably placed, for more stable support, in this embodiment, preferred, the bottom welding of concentrated jar 5 has three support 3, and three support 3 is triangular distribution, and supporting shoe 4 has all been installed to the bottom of three support 3 simultaneously, improves the stability that the device supported.
Step 1; the heating chamber 1 is communicated with a concentration tank 5, the concentration tank 5 is communicated with a condenser 8, the concentration tank 5 is connected with the condenser 8 through a steam pipe 6, the steam pipe 6 is provided with a connecting flange 7, the connecting flange 7 is provided with an auxiliary alignment structure, the auxiliary alignment structure is convenient for connecting and installing the steam pipe 6, heat generated by combustion in the heating chamber 1 is transmitted into the concentration tank 5, the pressure in the concentration tank 5 is increased, liquid raw materials are gradually boiled and evaporated, and liquid containing the raw materials is distilled and separated out;
step 2; the generated gas enters the inner side of the condenser 8 through the steam pipe 6, the steam is liquefied through the condensation effect of the snake-shaped condensation pipe inside the condenser 8 so as to flow into the liquid receiving tank 11, and cooling water is introduced through the cooling water inlet during cooling.
The working principle and the using process of the invention are as follows: when the device is used, an auxiliary mounting structure is arranged on a connecting flange 7 between adjacent mounted equipment, the connecting flange 7 comprises a first flange 15 and a second flange 16, when the connecting flange 7 is mounted, the position can be limited through the auxiliary structure, when the device is mounted, the first flange 15 and the second flange 16 are in sliding connection with a clamping plate 17 through a clamping seat 14, when the clamping seat 14 and the clamping plate 17 are aligned and drawn, the clamping seat 14 and the clamping plate 17 are limited through a limiting rod 12, the first flange 15 and the second flange 16 can be stably aligned, the device can be accurately mounted when being connected and mounted, screw holes on the first flange 15 and the second flange 16 are aligned, the device is convenient to be fixed in a rotating manner, the practicability and convenience of the device are improved, the mounting efficiency is improved, generally, when the device is used, a concentration tank 5 can be directly placed on the ground, if the ground is uneven, the unable stability in bottom of concentrated jar 5 is placed, is equipped with supporting shoe 4 at the support 3 facial make-up of this concentrated jar 5 bottom, and supporting shoe 4 establishes in the bottom of support 3 soon through screw rod 10 screw thread, can manually establish the regulation soon through screw rod 10, when concentrated jar 5 was placed, if the unevenness of ground, the bottom stable support of concentrated jar 5 is adjusted to accessible supporting shoe 4, avoids the device to incline the side when using to fall, has improved the device's stability and practicality.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. The utility model provides an utilize production device and method of distillation method preparation spices, includes heating chamber (1), concentrated jar (5), condenser (8) and receives cistern (11), condenser (8) are fixed to be installed at the top that receives cistern (11), heating chamber (1) is connected with the bottom of concentrated jar (5) and has been installed circulating pipe (2), the bottom welded fastening of concentrated jar (5) has support (3), be connected between concentrated jar (5) and condenser (8) and have been installed steam pipe (6), flange (7) have been installed in connection on steam pipe (6), its characterized in that: the connecting flange (7) comprises a first flange plate (15) and a second flange plate (16), a clamping plate (17) of one ladder with four households is welded on the first flange plate (15), an integrated clamping seat (14) is welded on the second flange plate (16), the first flange plate (15) and the second flange plate (16) are slidably clamped with the clamping plate (17) through the clamping seat (14), a limiting seat (13) is welded at one end of the clamping seat (14), a limiting rod (12) is connected to the inner side of the limiting seat (13) in a limiting mode, a spring (9) is sleeved at one end of the limiting rod (12) located on the inner side of the limiting seat (13), a limiting hole in alignment is formed in the clamping plate (17), and the clamping seat (14) and the clamping plate (17) are connected with the limiting hole in a limiting mode through the limiting rod (12).
2. The apparatus and method for producing perfume according to claim 1, wherein: the bottom of the support (3) is connected with a support block (4), a screw (10) is screwed at the bottom of the inner side of the support (3), and the support block (4) is fixedly arranged at one end of the screw (10).
3. The apparatus and method for producing perfume according to claim 2, wherein: the bottom welding of concentrated jar (5) has three support (3), and three support (3) are triangular distribution, and supporting shoe (4) have all been installed to the bottom of three support (3) simultaneously.
4. The apparatus and method for producing perfume according to claim 1, wherein: the circulating pipe (2) and the steam pipe (6) are provided with connecting flanges (7) with the same structure.
5. The apparatus and method for producing perfume according to claim 1, wherein: two clamping plates (17) and two clamping seats (14) are symmetrically arranged at two ends of the first flange plate (15) and the second flange plate (16).
6. The apparatus and method for producing perfume according to claim 1, wherein: and a cooling water inlet is formed in the bottom of one end of the condenser (8), and a cooling water outlet is formed in the top of the other end of the condenser (8).
7. A process for the preparation of fragrances by distillation as claimed in claims 1 to 6, wherein:
step 1; the heating chamber (1) is communicated with the concentration tank (5), the concentration tank (5) is communicated with the condenser (8), the concentration tank (5) is connected with the condenser (8) through a steam pipe (6), a connecting flange (7) is arranged on the steam pipe (6), an auxiliary alignment structure is arranged on the connecting flange (7), the auxiliary alignment structure is convenient for connecting and installing the steam pipe (6), heat generated by combustion in the heating chamber (1) is transferred into the concentration tank (5), the pressure in the concentration tank (5) is increased, liquid raw materials are gradually boiled and evaporated, and liquid containing the raw materials is distilled and separated out;
step 2; the generated gas enters the inner side of the condenser (8) through the steam pipe (6), the steam is liquefied through the condensation effect of the snake-shaped condensation pipe on the inner side of the condenser (8) so as to flow into the liquid receiving tank (11), and cooling water is introduced through the cooling water inlet during cooling.
CN202110434801.9A 2021-04-22 2021-04-22 Production device and method for preparing spice by distillation method Pending CN113201403A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110434801.9A CN113201403A (en) 2021-04-22 2021-04-22 Production device and method for preparing spice by distillation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110434801.9A CN113201403A (en) 2021-04-22 2021-04-22 Production device and method for preparing spice by distillation method

Publications (1)

Publication Number Publication Date
CN113201403A true CN113201403A (en) 2021-08-03

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Application Number Title Priority Date Filing Date
CN202110434801.9A Pending CN113201403A (en) 2021-04-22 2021-04-22 Production device and method for preparing spice by distillation method

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CN (1) CN113201403A (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE20010900U1 (en) * 2000-06-20 2000-08-24 Voith Sulzer Papiertech Patent Hydrocyclone plant
CN203494188U (en) * 2013-10-19 2014-03-26 昆明赛诺制药有限公司 Double-effect concentrator
CN105013199A (en) * 2015-07-14 2015-11-04 河北智同生物制药有限公司 Single-effect external-cycle concentrator and application thereof
CN204767486U (en) * 2015-07-14 2015-11-18 河北智同生物制药有限公司 Single -action extrinsic cycle concentrator
CN206762300U (en) * 2016-12-30 2017-12-19 重庆喜旋生物科技有限公司 A kind of single-effect external circulation inspissator
CN111672424A (en) * 2020-08-04 2020-09-18 山东嘉岳新材料有限公司 Environment-friendly binder processing equipment
CN211875351U (en) * 2020-03-19 2020-11-06 江苏新澎复合材料有限公司 Flange type composite pipe convenient to connect
CN212308884U (en) * 2020-04-07 2021-01-08 江西广恩和药业股份有限公司 A extrinsic cycle concentrator for traditional chinese medicine production
CN212775623U (en) * 2020-06-30 2021-03-23 温州伟凯阀门科技有限公司 Hydraulic butterfly valve structure for water discharge control
CN212775800U (en) * 2020-07-28 2021-03-23 徐川江 Small-size water conservancy valve

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE20010900U1 (en) * 2000-06-20 2000-08-24 Voith Sulzer Papiertech Patent Hydrocyclone plant
CN203494188U (en) * 2013-10-19 2014-03-26 昆明赛诺制药有限公司 Double-effect concentrator
CN105013199A (en) * 2015-07-14 2015-11-04 河北智同生物制药有限公司 Single-effect external-cycle concentrator and application thereof
CN204767486U (en) * 2015-07-14 2015-11-18 河北智同生物制药有限公司 Single -action extrinsic cycle concentrator
CN206762300U (en) * 2016-12-30 2017-12-19 重庆喜旋生物科技有限公司 A kind of single-effect external circulation inspissator
CN211875351U (en) * 2020-03-19 2020-11-06 江苏新澎复合材料有限公司 Flange type composite pipe convenient to connect
CN212308884U (en) * 2020-04-07 2021-01-08 江西广恩和药业股份有限公司 A extrinsic cycle concentrator for traditional chinese medicine production
CN212775623U (en) * 2020-06-30 2021-03-23 温州伟凯阀门科技有限公司 Hydraulic butterfly valve structure for water discharge control
CN212775800U (en) * 2020-07-28 2021-03-23 徐川江 Small-size water conservancy valve
CN111672424A (en) * 2020-08-04 2020-09-18 山东嘉岳新材料有限公司 Environment-friendly binder processing equipment

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Application publication date: 20210803