CN113197826A - 一种高保湿高清洁力低刺激性按摩型洗面奶及其制备方法 - Google Patents
一种高保湿高清洁力低刺激性按摩型洗面奶及其制备方法 Download PDFInfo
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- CN113197826A CN113197826A CN202110539743.6A CN202110539743A CN113197826A CN 113197826 A CN113197826 A CN 113197826A CN 202110539743 A CN202110539743 A CN 202110539743A CN 113197826 A CN113197826 A CN 113197826A
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Abstract
本发明涉及日化领域,公开了一种高保湿高清洁力低刺激性按摩型洗面奶及其制备方法。该洗面奶包括以下成分:椰油酰氨基丙酸钠,椰油酰胺丙基甜菜碱,保湿因子囊泡,去垢颗粒,卡波姆,甲基纤维素,甘油,山梨酸钾,水;所述保湿因子囊泡的芯材为天然保湿成分,壁材为大豆卵磷脂;所述去垢颗粒包括活性炭芯层,以及包覆在活性炭芯层外的多孔疏水聚合物壁层。本发明通过添加去垢颗粒,能赋予洗面奶较好的去油、去角质效果,且对皮肤刺激性小,并具有按摩效果;将保湿因子囊泡与去垢颗粒配合使用,能防止天然保湿成分在洗面奶制备和使用过程中失效,并使其在使用过程中快速释放并被皮肤吸收,从而赋予洗面奶较好的保湿作用。
Description
技术领域
本发明涉及日化领域,尤其涉及一种高保湿高清洁力低刺激性按摩型洗面奶及其制备方法。
背景技术
洗面奶,就是面部皮肤的清洁产品,其目的是清除皮肤上的污垢,使皮肤清爽,有助于保持皮肤正常生理状态。洗面奶可以去除皮肤表面附着的皮脂、角质层屑片、汗液等皮肤生理代谢产物以及灰尘、微生物、使用的化妆品残留物等,是目前销量最大的护肤品之一。
目前,市场上的洗面奶主要包括两种类型:皂基型和氨基酸型。传统的皂基型洗面奶采用脂肪酸皂作为活性成分,具有泡沫丰富、清洁力强的优点,但对皮肤的刺激性较大,使用后易出现皮肤紧绷或发干的感觉。氨基酸型洗面奶采用弱酸性的氨基酸类表面活性剂,性质温和,对皮肤刺激性小,但清洁力较弱。
发明内容
为了解决上述技术问题,本发明提供了一种高保湿高清洁力低刺激性按摩型洗面奶及其制备方法。本发明通过添加去垢颗粒,能赋予洗面奶较好的去油、去角质效果,且对皮肤刺激性小,并具有按摩效果;将保湿因子囊泡与去垢颗粒配合使用,能防止天然保湿成分在洗面奶制备和使用过程中失效,并使其在使用过程中快速释放并被皮肤吸收,从而赋予洗面奶较好的保湿作用。
本发明的具体技术方案为:
一种高保湿高清洁力低刺激性按摩型洗面奶,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠2-3%,椰油酰胺丙基甜菜碱1-3%,保湿因子囊泡10-15%,去垢颗粒1-5%,卡波姆1-2%,甲基纤维素1-2%,甘油2-4%,山梨酸钾0.1-1.0%,余量为水;所述保湿因子囊泡的芯材为天然保湿成分,壁材为大豆卵磷脂;所述去垢颗粒包括活性炭芯层,以及包覆在活性炭芯层外的多孔疏水聚合物壁层。
本发明通过在洗面奶中添加有保湿因子囊泡。由于天然保湿成分常存在易氧化、热稳定性差的问题,在洗面奶制备及储存过程中易失效,因此本发明将天然保湿成分负载在囊泡中,能防止其氧化和热分解。
另一方面,本发明通过在洗面奶中添加具有特殊结构的去垢颗粒,能够提高洗面奶的去油、去角质效果,且对皮肤的刺激较小。具体而言,在去垢颗粒中,活性炭芯能利用其较高的孔隙率发挥去油作用,且该去垢颗粒在洗面奶揉搓的过程中还能发挥按摩、去除角质的作用。不过,质地较硬且表面粗糙的活性炭与皮肤直接接触易造成皮肤损伤,为此,本发明采用多孔疏水聚合物对活性炭进行包覆,该聚合物壁层能赋予去垢颗粒光滑且较为柔软的表面,可避免活性炭与皮肤直接接触;并且,壁层采用疏水聚合物,因此对油污也具有吸附作用,同时,壁层具有的多孔结构又可确保其不会对活性炭的吸附功能造成过度影响。
此外,去垢颗粒的作用还在于:由于囊泡在洗面奶使用过程中与皮肤接触的时间较短,会导致囊泡中的活性物质无法充分释放并被皮肤吸收,而去垢颗粒的存在,使得洗面奶在面部揉搓时,去垢颗粒与囊泡摩擦,能够破坏囊泡结构,使活性物质释放出来,并且去垢颗粒的按摩作用也能促进皮肤对天然保湿成分的吸收。由此可知本发明中保湿因子囊泡与去垢颗粒复配使用除了发挥各自功效外还具有相互配合作用。
作为优选,所述天然保湿成分按重量份计,包括以下成分:芦荟提取物8-12份,海藻提取物4-6份,透明质酸1-3份,维生素B61-3份。
作为优选,所述保湿因子囊泡的制备方法如下:
(1.1)将质量比为1:15-20的天然保湿成分和水混合,充分溶解后,获得水相;
(1.2)将质量比为8-12:1:10-15:20-25的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为2-3:1,剪切乳化,过滤,获得保湿因子囊泡。
作为优选,步骤(1.3)中,所述剪切乳化的转速为7000-8000rpm,时间为5-10min。
作为优选,所述去垢颗粒的粒径为80-100μm,其中,所述活性炭芯层的直径为40-50μm。
作为优选,所述去垢颗粒的制备方法如下:将聚二甲基硅氧烷与含氢硅油的混合液喷涂到活性炭表面,在50-60℃下预固化10-20min后,进行真空超声处理,而后继续在90-100℃下固化40-60min,获得去垢颗粒。
在真空超声处理过程中,在颗粒内外的气压差以及超声作用下,活性炭中的空气振动逃逸出来,在聚二甲基硅氧烷壁层中形成孔隙,从而防止壁层对活性炭的吸附作用造成过度影响。
本发明在初步固化后,进行真空超声处理制孔,再完全固化,原因在于:在初步固化前,聚二甲基硅氧烷壁层为液态,若在此时进行真空超声处理,则壁层易被逸出的气体过度破坏,导致其难以有效发挥阻隔活性炭与皮肤接触的作用;在完全固化后,聚二甲基硅氧烷壁层机械强度过高,若在此时进行真空超声处理,则逸出的气体难以在壁层中形成较高的孔隙率,导致去垢颗粒的去油效果不佳。
作为优选,所述聚二甲基硅氧烷与含氢硅油的质量比为10-15:1。
作为优选,所述真空超声处理的真空度为0.03-0.05Mpa,超声功率为300-500W,时间为20-30min。
作为优选,所述洗面奶还包括以下重量百分数的成分:木质颗粒0.5-1.5%;所述木质颗粒的制备方法如下:将木材粉碎成粒径为40-60μm的颗粒后,在170-180℃、0.5-0.8MPa下疏松化处理40-80min,获得木质颗粒。
在木质颗粒中,由于木纤维独特的扇形结构,能赋予木质颗粒较高的孔隙率,使其能够吸附体表的油污,同时,木质颗粒能通过摩擦机械效应而发挥去除角质的作用,且由于其柔软的质地,能够避免对皮肤造成损伤,并发挥按摩作用。
柔软的质地能够赋予木质颗粒较好的按摩作用,但同时也导致其使用过程中,孔隙易变形缩小,不利于油污的吸附;而去垢颗粒中芯层的活性炭不易变形,能保持较好的去油效果,但同时也会造成去垢颗粒硬度较高,按摩效果相对较差。因此,本发明将木质颗粒与去垢颗粒复配,能够使沐浴露兼具较好的清洁和按摩功能。
一种制备所述洗面奶的方法,包括以下步骤:
(1)将卡波姆、甲基纤维素、甘油加入水中,在80-85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70-75℃下搅拌溶解,获得初混液;
(2)将初混液降温至40-45℃,加入保湿因子囊泡和去垢颗粒,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
一种制备所述洗面奶的方法,包括以下步骤:
(1)将木质颗粒加入一部分水中,所述木质颗粒与水的质量比为1:8-10,在80-90℃下加热1-2h,获得木质颗粒分散液;
(2)将卡波姆、甲基纤维素、甘油加入剩余的中,在80-85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70-75℃下搅拌溶解,获得初混液;
(3)将初混液降温至40-45℃,加入保湿因子囊泡、去垢颗粒和木质颗粒分散液,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
与现有技术相比,本发明具有以下优点:
(1)在保湿因子囊泡中,采用囊泡包裹天然保湿成分,能防止其在洗面奶制备和储存过程中失效;
(2)在去垢颗粒中,采用多孔疏水聚合物包覆活性炭,能防止活性炭损伤皮肤,并使去垢颗粒具有较好的按摩、去角质作用,且不会对活性炭的去油效果产生不利影响;
(3)将保湿因子囊泡与去垢颗粒配合使用,能使天然保湿成分在洗面奶使用过程中快速释放出来并被皮肤吸收;
(4)将木质颗粒和去垢颗粒复配,能赋予沐浴露较好的去油、去角质和按摩效果。
具体实施方式
下面结合实施例对本发明作进一步的描述。以下实施例只是用于详细说明本发明,并不以任何方式限制本发明的保护范围。
实施例1
一种高保湿高清洁力低刺激性按摩型洗面奶,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠3%,椰油酰胺丙基甜菜碱1%,保湿因子囊泡10%,去垢颗粒1%,卡波姆1%,甲基纤维素2%,甘油2%,山梨酸钾0.1%,余量为水。
一种制备所述洗面奶的方法,包括以下步骤:
(1)制备保湿因子囊泡:
(1.1)将质量比为1:15的天然保湿成分和水混合,充分溶解后,获得水相;所述天然保湿成分按重量份计,包括以下成分:芦荟提取物12份,海藻提取物4份,透明质酸3份,维生素B61份;
(1.2)将质量比为8:1:10:20的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为3:1,以7000rpm的转速剪切乳化10min,过滤,获得保湿因子囊泡。
(2)制备去垢颗粒:将质量比为10:1的聚二甲基硅氧烷与含氢硅油的混合液喷涂到粒径为40-50μm的活性炭表面,在50℃下预固化20min后,以0.03Mpa的真空度和300W的超声功率进行真空超声处理30min,而后继续在100℃下固化40min,获得粒径为80-100μm的去垢颗粒。
(3)将卡波姆、甲基纤维素、甘油加入水中,在80℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70℃下搅拌溶解,获得初混液。
(4)将初混液降温至40℃,加入保湿因子囊泡和去垢颗粒,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
实施例2
一种高保湿高清洁力低刺激性按摩型洗面奶,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠2.5%,椰油酰胺丙基甜菜碱2%,保湿因子囊泡12%,去垢颗粒3%,卡波姆1.5%,甲基纤维素1.5%,甘油3%,山梨酸钾0.5%,余量为水。
一种制备所述洗面奶的方法,包括以下步骤:
(1)制备保湿因子囊泡:
(1.1)将质量比为1:18的天然保湿成分和水混合,充分溶解后,获得水相;所述天然保湿成分按重量份计,包括以下成分:芦荟提取物10份,海藻提取物5份,透明质酸2份,维生素B62份;
(1.2)将质量比为10:1:12:23的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为2.5:1,以7500rpm的转速剪切乳化8min,过滤,获得保湿因子囊泡。
(2)制备去垢颗粒:将质量比为12:1的聚二甲基硅氧烷与含氢硅油的混合液喷涂到粒径为40-50μm的活性炭表面,在55℃下预固化15min后,以0.04Mpa的真空度和400W的超声功率进行真空超声处理25min,而后继续在95℃下固化50min,获得粒径为80-100μm的去垢颗粒。
(3)将卡波姆、甲基纤维素、甘油加入水中,在80℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70℃下搅拌溶解,获得初混液。
(4)将初混液降温至40℃,加入保湿因子囊泡和去垢颗粒,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
实施例3
一种高保湿高清洁力低刺激性按摩型洗面奶,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠2%,椰油酰胺丙基甜菜碱4%,保湿因子囊泡15%,去垢颗粒5%,卡波姆2%,甲基纤维素1%,甘油4%,山梨酸钾1.0%,余量为水。
一种制备所述洗面奶的方法,包括以下步骤:
(1)制备保湿因子囊泡:
(1.1)将质量比为1:20的天然保湿成分和水混合,充分溶解后,获得水相;所述天然保湿成分按重量份计,包括以下成分:芦荟提取物8份,海藻提取物6份,透明质酸1份,维生素B63份;
(1.2)将质量比为12:1:15:25的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为2:1,以8000rpm的转速剪切乳化5min,过滤,获得保湿因子囊泡。
(2)制备去垢颗粒:将质量比为15:1的聚二甲基硅氧烷与含氢硅油的混合液喷涂到粒径为40-50μm的活性炭表面,在60℃下预固化10min后,以0.05Mpa的真空度和500W的超声功率进行真空超声处理20min,而后继续在90℃下固化60min,获得粒径为80-100μm的去垢颗粒。
(3)将卡波姆、甲基纤维素、甘油加入水中,在85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在75℃下搅拌溶解,获得初混液。
(4)将初混液降温至45℃,加入保湿因子囊泡和去垢颗粒,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
实施例4
一种高保湿高清洁力低刺激性按摩型洗面奶,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠2%,椰油酰胺丙基甜菜碱4%,保湿因子囊泡15%,去垢颗粒4%,卡波姆2%,甲基纤维素1%,甘油4%,山梨酸钾1.0%,木质颗粒1%,余量为水。
一种制备所述洗面奶的方法,包括以下步骤:
(1)制备保湿因子囊泡:
(1.1)将质量比为1:20的天然保湿成分和水混合,充分溶解后,获得水相;所述天然保湿成分按重量份计,包括以下成分:芦荟提取物8份,海藻提取物6份,透明质酸1份,维生素B63份;
(1.2)将质量比为12:1:15:25的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为2:1,以8000rpm的转速剪切乳化5min,过滤,获得保湿因子囊泡。
(2)制备去垢颗粒:将质量比为15:1的聚二甲基硅氧烷与含氢硅油的混合液喷涂到粒径为40-50μm的活性炭表面,在60℃下预固化10min后,以0.05Mpa的真空度和500W的超声功率进行真空超声处理20min,而后继续在90℃下固化60min,获得粒径为80-100μm的去垢颗粒。
(3)制备木质颗粒:将木材粉碎成粒径为40-60μm的颗粒后,在175℃、0.6MPa下疏松化处理1h,获得木质颗粒。
(4)将木质颗粒加入一部分水中,所述木质颗粒与水的质量比为1:8,在85℃下加热1.5h,获得木质颗粒分散液。
(5)将卡波姆、甲基纤维素、甘油加入剩余的中,在85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在75℃下搅拌溶解,获得初混液。
(6)将初混液降温至45℃,加入保湿因子囊泡、去垢颗粒和木质颗粒分散液,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
对比例1
本对比例与实施例2的区别在于,不添加去垢颗粒。
对比例2
本对比例与实施例2的区别在于,将去垢颗粒换成等质量的粒径为80-120μm的活性炭。
对比例3
本对比例与实施例2的区别在于,步骤(2)中,不进行真空超声处理。
对比例4
本对比例与实施例2的区别在于,步骤(2)中,不进行预固化,并将真空超声处理后的固化时间调整为65min。
对比例5
本对比例与实施例2的区别在于,步骤(2)中,将真空超声处理调整至“在90℃下固化60min”之后。
将90名20-40岁的受试者随机分成9组,分别对实施例1-4和对比例1-5的洗面奶进行测试,测试项目和方法如下:
(1)保湿效果:使用洗面奶清洗面部(每次5g,并使用25±2℃的清水清洗),分别在清洗前以及清洗后0h、1h、2h、3h,测试受试者面部的皮肤水分含量(在前额、下巴、两侧脸颊各取一点,取平均值),每组取平均值,结果见表1;
(2)去油效果:在使用洗面奶清洗面部(每次5g,并使用25±2℃的清水清洗)后,测试受试者面部的皮肤油脂含量(在前额、下巴、两侧脸颊各取一点,取平均值),计算各受试者在清洗前后的皮肤油脂含量降低率,每组取平均值,结果见表2;
(3)去角质效果:在使用前,测试各受试者前臂内侧的皮肤粗糙度;在使用洗面奶清洗前臂内侧30天(使用频率为每5天一次,每次1-2g)后,再次检测各受试者前臂内侧的皮肤粗糙度,计算皮肤粗糙度降低率,每组取平均值,结果见表2;
(4)感官评价:取0.5-1.0g洗面奶,在受试者脸颊上按摩2min,对皮肤疼痛情况进行打分,0分表示无疼痛感,10分表示疼痛感非常明显,每组取平均值,结果见表2。
表1
表2
实施例4将实施例3中的部分去垢颗粒换成了等质量的木质颗粒,对比实施例3与实施例4的测试结果可知:相较于采用单一的去垢颗粒而言,将其与木质颗粒复配,虽然会对去油效果产生一定影响,但能降低疼痛感。原因在于:去垢颗粒中芯层的活性炭不易变形,能保持较好的去油效果,但同时也会造成去垢颗粒硬度较高;而木质颗粒质地柔软,涂抹在皮肤上时更加舒适,不过柔软的质地也会导致其使用过程中,孔隙易变形缩小,不利于油污的吸附。
对比实施例2与对比例1的测试结果可知:相较于单独使用保湿因子囊泡而言,将其与去垢颗粒配合,能够提高保湿效果。原因在于:由于囊泡在洗面奶使用过程中与皮肤接触的时间较短,会导致囊泡中的活性物质无法充分释放并被皮肤吸收,而去垢颗粒的存在,使得洗面奶在面部揉搓时,去垢颗粒与囊泡摩擦,能够破坏囊泡结构,使活性物质释放出来,并且去垢颗粒的按摩作用也能促进皮肤对天然保湿成分的吸收。
对比实施例2与对比例2的测试结果可知:在活性炭表面包覆多孔疏水聚合物壁层后,疼痛感明显减弱,且去油效果没有显著下降。原因在于:质地较硬且表面粗糙的活性炭与皮肤直接接触易产生疼痛感,而采用多孔疏水聚合物对活性炭进行包覆后,该聚合物壁层能赋予去垢颗粒光滑且较为柔软的表面,可避免活性炭与皮肤直接接触;并且,壁层采用疏水聚合物,因此对油污也具有吸附作用,同时,壁层具有的多孔结构又可确保其不会对活性炭的吸附功能造成过度影响。
对比实施例2与对比例3的测试结果可知:采用经真空超声处理的去垢颗粒,能提高洗面奶的去油效果。原因在于:真空超声处理过程中,在颗粒内外的气压差以及微波作用下,活性炭中的空气振动逃逸出来,在聚二甲基硅氧烷壁层中形成孔隙,从而防止壁层对活性炭的吸油作用造成过度影响。
对比实施例2与对比例4的测试结果可知:在真空超声处理前进行预固化,疼痛感明显减弱。原因在于:在初步固化前,聚二甲基硅氧烷壁层为液态,若在此时进行真空超声处理,则壁层易被逸出的气体过度破坏,导致其难以有效发挥阻隔活性炭与皮肤接触的作用。
对比实施例2与对比例5的测试结果可知:在完全固化后再进行真空超声处理,会导致洗面奶的去油效果明显下降。原因在于:在完全固化后,聚二甲基硅氧烷壁层机械强度过高,若在此时进行真空超声处理,则逸出的气体难以在壁层中形成较高的孔隙率,导致去垢颗粒的去油效果不佳。
上面虽然结合实施例对本发明作了详细的说明,但是所述技术领域的技术人员能够理解,在不脱离本发明宗旨的前提下,在权利要求保护的范围内,还可以对上述实施例进行变更或改变等。
Claims (10)
1.一种高保湿高清洁力低刺激性按摩型洗面奶,其特征在于,按质量百分数计,包括以下成分:椰油酰氨基丙酸钠2-3%,椰油酰胺丙基甜菜碱1-3%,保湿因子囊泡10-15%,去垢颗粒1-5%,卡波姆1-2%,甲基纤维素1-2%,甘油2-4%,山梨酸钾0.1-1.0%,余量为水;所述保湿因子囊泡的芯材为天然保湿成分,壁材为大豆卵磷脂;所述去垢颗粒包括活性炭芯层,以及包覆在活性炭芯层外的多孔疏水聚合物壁层。
2.如权利要求1所述的洗面奶,其特征在于,所述天然保湿成分按重量份计,包括以下成分:芦荟提取物8-12份,海藻提取物4-6份,透明质酸1-3份,维生素B61-3份。
3.如权利要求1或2所述的洗面奶,其特征在于,所述保湿因子囊泡的制备方法如下:
(1.1)将质量比为1:15-20的天然保湿成分和水混合,充分溶解后,获得水相;
(1.2)将质量比为8-12:1:10-15:20-25的大豆卵磷脂、蔗糖月桂酸酯、丁二醇、甘油混合均匀后,获得油相;
(1.3)在搅拌下,将水相逐滴加入油相中,所述水相与油相的体积比为2-3:1,剪切乳化,过滤,获得保湿因子囊泡。
4.如权利要求3所述的洗面奶,其特征在于,步骤(1.3)中,所述剪切乳化的转速为7000-8000rpm,时间为5-10min。
5.如权利要求1所述的洗面奶,其特征在于,所述去垢颗粒的粒径为80-100μm,其中,所述活性炭芯层的直径为40-50μm。
6.如权利要求1或5所述的洗面奶,其特征在于,所述去垢颗粒的制备方法如下:将聚二甲基硅氧烷与含氢硅油的混合液喷涂到活性炭表面,在50-60℃下预固化10-20min后,进行真空超声处理,而后继续在90-100℃下固化40-60min,获得去垢颗粒。
7.如权利要求6所述的洗面奶,其特征在于,所述聚二甲基硅氧烷与含氢硅油的质量比为10-15:1。
8.如权利要求6所述的洗面奶,其特征在于,所述真空超声处理的真空度为0.03-0.05Mpa,超声功率为300-500W,时间为20-30min。
9.如权利要求1所述的洗面奶,其特征在于,还包括以下重量百分数的成分:木质颗粒0.5-1.5%;所述木质颗粒的制备方法如下:将木材粉碎成粒径为40-60μm的颗粒后,在170-180℃、0.5-0.8MPa下疏松化处理40-80min,获得木质颗粒。
10.一种制备如权利要求1-9之一所述洗面奶的方法,其特征在于,包括以下步骤:
方案A:
(1)将卡波姆、甲基纤维素、甘油加入水中,在80-85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70-75℃下搅拌溶解,获得初混液;
(2)将初混液降温至40-45℃,加入保湿因子囊泡和去垢颗粒,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶;
方案B:
(1)将木质颗粒加入一部分水中,所述木质颗粒与水的质量比为1:8-10,在80-90℃下加热1-2h,获得木质颗粒分散液;
(2)将卡波姆、甲基纤维素、甘油加入剩余的中,在80-85℃下搅拌溶解;再加入椰油酰氨基丙酸钠和椰油酰胺丙基甜菜碱,在70-75℃下搅拌溶解,获得初混液;
(3)将初混液降温至40-45℃,加入保湿因子囊泡、去垢颗粒和木质颗粒分散液,均质后,再加入山梨酸钾,混合均匀,获得高保湿高清洁力低刺激性按摩型洗面奶。
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