CN110384633B - 一种含有液晶结构的洁面乳及其制备方法 - Google Patents

一种含有液晶结构的洁面乳及其制备方法 Download PDF

Info

Publication number
CN110384633B
CN110384633B CN201910608103.9A CN201910608103A CN110384633B CN 110384633 B CN110384633 B CN 110384633B CN 201910608103 A CN201910608103 A CN 201910608103A CN 110384633 B CN110384633 B CN 110384633B
Authority
CN
China
Prior art keywords
phase
liquid crystal
crystal structure
facial cleanser
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201910608103.9A
Other languages
English (en)
Other versions
CN110384633A (zh
Inventor
周树立
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hainan Jingrun Pearl Biotechnology Co ltd
Original Assignee
Hainan Jingrun Pearl Biotechnology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hainan Jingrun Pearl Biotechnology Co ltd filed Critical Hainan Jingrun Pearl Biotechnology Co ltd
Priority to CN201910608103.9A priority Critical patent/CN110384633B/zh
Publication of CN110384633A publication Critical patent/CN110384633A/zh
Application granted granted Critical
Publication of CN110384633B publication Critical patent/CN110384633B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0295Liquid crystals
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

本发明属日用化妆品技术领域,涉及一种含有液晶结构的洁面乳及其制备方法,将月桂酰胺丙基甜菜碱、月桂醇聚醚磷酸钾等加水加热溶解后加入溶解的二聚氨基酸盐复合物液晶乳化剂,搅拌均匀,然后加入植物精油,降温后加入丙烯酸(酯)类交联聚合物,当体系温度降温到35~45℃加入聚季铵盐‑43、柠檬酸等,控制pH在6.5~7.5,理化指标检验合格后,出料得到含有液晶结构的洁面乳。本发明制备工艺简单,将液晶乳化剂与磷酸酯表活体系进行作用快速形成大量晶格,经过简单搅拌即可将加入的油脂包裹到晶格中,不影响泡沫状态,不仅带来良好清爽以及泡沫效果,并且洗后具有舒适、不刺激、不紧绷等效果,为洁面产品带来全方位的价值理念。

Description

一种含有液晶结构的洁面乳及其制备方法
技术领域
本发明属日用化妆品技术领域,涉及一种洁面乳及其制备方法,具体是一种将液晶乳化剂与磷酸酯表面活性剂进行配伍制得一种含有液晶结构的表面活性剂型洁面乳其制备方法。
背景技术
随着物质生活水平的不断提高,人们对美的追求也不断提高,希望改变自己的容貌拥有光泽透亮的健康肤色。化妆几乎是现代女性每日的必备工作,由于化妆品含有化学物质,对皮肤有一定的伤害作用,所以每天晚上必须卸掉脸上的妆容,避免化妆品残留脸上而阻塞毛孔引起痘痘。洁面能达到清洁面部皮肤的效果,是美容的根本,是护肤最重要部分之一。洁面产品是否合适,清洁是否彻底,对养颜护肤工作事半功倍的作用,但现有洁面乳是以表面活性剂作为主要清洁剂,脱脂力较强,不太适合皮肤干燥的人群。
水解珍珠是根据专利“CN1795874A”来制备,该专利公开了一种制备珍珠水解液脂质体的方法,它是将珍珠水解液溶解于磷酸盐缓冲液中,调PH值至中性,然后缓慢加入到由大豆卵磷脂干膜制成的瓶中,经振荡、超声波处理得到珍珠水解液脂质体。由这种方法制备得到的珍珠水解液脂质体能够降低水解液的导电率,减少对化妆品体系的破坏,有效地保护珍珠的有效成分不被其他组分所破坏,大大提高了珍珠营养成分的吸收效果。
发明内容
本发明的目的是提供一种含有液晶结构的洁面乳及其制备方法,将液晶乳化剂与磷酸酯表活体系快速作用形成大量晶格,把后续加入的油脂包裹到晶格中,不影响泡沫状态,不影响洁面效果,解决了现有表面活性剂洁面配方体系中随着油脂的加入而在一定程度上影响泡沫的产生,进而影响洁面效果的问题,能够使加入的功能性油脂在使用过程中具有缓释发挥作用,达到调理肌肤效果,不仅带来良好清爽以及泡沫效果,并且洗后具有舒适、不刺激不紧绷等效果。
本发明所采用的技术方案:
一种含有液晶结构的洁面乳,含有以下重量百分比组分:
A相:月桂酰胺丙基甜菜碱(LHSB-35) 5%
月桂酰肌氨酸钠(L-30) 5%
月桂酰两性基乙酸钠(AMC65L) 5%
月桂醇聚醚磷酸钾(MAEP-K) 2~15%
水解珍珠 5%
B相:二聚氨基酸盐复合物液晶乳化剂(PE-950X) 1~4%
C相:植物精油 20%以下
D相:丙烯酸(酯)类交联聚合物(SF-1) 2.5%
E相:柠檬酸 1%以下
聚季铵盐-43(Supcare 608) 1%
香精 1%以下
水至100%
本发明所提供的一种含有液晶结构的洁面乳的制备方法,其步骤如下:
1)在B相中加入适量水,加热搅拌至完全溶解,待用。在A相中加入适量水,混合加热到80~85℃,至完全溶解后加入溶解的B相,搅拌均匀。
2)保持温度将C相加入体系中,加快搅拌速度,缓慢降温。
3)当体系温度降到55~65℃加入D相,搅拌均匀。
4)当体系温度降到35~45℃加入E相,搅拌均匀,控制pH在6.5~7.5。理化指标检验合格后,出料得到含有液晶结构的洁面乳。
本发明制备工艺简单,将液晶乳化剂与磷酸酯表活体系通过离子键以及范德华力的快速作用,在不加入油脂、遮光剂、乳化剂等条件下,低温条件即可快速形成大量晶格,形成乳液状,经过简单搅拌即可将加入的油脂包裹到晶格中,不影响泡沫状态,因此该体系具有较高的油脂容忍度,并且,加入的功能性油脂在使用过程中具有缓释发挥作用,达到调理肌肤效果。在洁面产品中应用,不仅带来良好清爽以及泡沫效果,并且洗后具有舒适、不刺激、不紧绷等效果,在配方中亦可根据不同使用护理需求添加不同的功能性成分以及各类护肤精油等调整设计出滋润的洁面产品,再不影响泡沫及产品稳定性的情况下,带给局域消费者极佳的使用感受,为洁面产品带来全方位的价值理念,对于滋润型配方体系提供了一个新的思路。
具体实施方式
下面通过实例对本发明作进一步说明,但不作为对本发明的限定。
各实施例的组成配方见表1,以重量百分比表示。
表1各实施例的组成配方
Figure GDA0003684984090000031
上述实施例的制备工艺如下:
1、先将A相物料混合加热到80℃左右,至完全溶解。
2、将B相物料为液晶乳化剂,将其加入适量水中加热搅拌至完全溶解后加入A相中,搅拌均匀。
3、C相为油相物料,保持温度将C相物料加入体系中,加快搅拌速度,缓慢降温。
4、当体系温度降到60℃左右加入D相,搅拌均匀。
5、当体系温度降到40℃左右加入E相,搅拌均匀,将PH控制在7左右,理化指标检验合格后,出料。
功效验证:
随机挑选128名试用者随机使用实施例1、2、3、4、5所得的含有液晶结构的洁面产品,使用方法同现有其它洁面乳的使用方法,每个试用者使用后进行自我评价。对各项指标进行统计,计算平均数,结果见表2:
表2使用效果
Figure GDA0003684984090000041
Figure GDA0003684984090000051
从试用者的自我评估的结果可以看出,试用者对本发明所提供的含有液晶结构的洁面产品的清洁效果、滋润效果、洗后肤感、安全性有很好的评价,同时对其他各项指标都给予较高的评价,在试用过程中未发现有过敏现象。
根据调查结果显示:该含有液晶结构的洁面产品具有很好清洁肌肤的效果,是安全性和使用性很高的洁肤产品。
以上所述仅是本发明的优选实施方式,应当指出,对于本技术领域的普通技术人员来说,在不脱离本发明技术原理的前提下,还可以做出若干改进、润饰和颜色变化,这些改进、润饰及颜色变化也应视为本发明的保护范围。

Claims (2)

1.一种含有液晶结构的洁面乳,其特征在于,含有以下重量百分比组分:
A相:月桂酰胺丙基甜菜碱 5%
月桂酰肌氨酸钠 5%
月桂酰两性基乙酸钠 5%
月桂醇聚醚磷酸钾 2~15%
水解珍珠 5%
B相:二聚氨基酸盐复合物液晶乳化剂 1~4%
C相:植物精油 20%以下
D相:丙烯酸(酯)类交联聚合物 2.5%
E相:柠檬酸 1%以下
聚季铵盐-43 1%
香精 1%以下
水至100%。
2.一种权利要求1所述的含有液晶结构的洁面乳的制备方法,其特征在于,其步骤如下:
1)在B相中加入适量水,加热搅拌至完全溶解,待用;在A相中加入适量水,混合加热到80~85℃,至完全溶解后加入溶解的B相,搅拌均匀;
2)保持温度将C相加入体系中,加快搅拌速度,缓慢降温;
3)当体系温度降到55~65℃加入D相,搅拌均匀;
4)当体系温度降到35~45℃加入E相,搅拌均匀,控制pH在6.5~7.5;理化指标检验合格后,出料得到含有液晶结构的洁面乳。
CN201910608103.9A 2019-07-08 2019-07-08 一种含有液晶结构的洁面乳及其制备方法 Active CN110384633B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910608103.9A CN110384633B (zh) 2019-07-08 2019-07-08 一种含有液晶结构的洁面乳及其制备方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201910608103.9A CN110384633B (zh) 2019-07-08 2019-07-08 一种含有液晶结构的洁面乳及其制备方法

Publications (2)

Publication Number Publication Date
CN110384633A CN110384633A (zh) 2019-10-29
CN110384633B true CN110384633B (zh) 2022-11-11

Family

ID=68286422

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201910608103.9A Active CN110384633B (zh) 2019-07-08 2019-07-08 一种含有液晶结构的洁面乳及其制备方法

Country Status (1)

Country Link
CN (1) CN110384633B (zh)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100506236C (zh) * 2004-12-28 2009-07-01 海南京润珍珠生物技术股份有限公司 珍珠水解液脂质体的制作方法
CN105326733A (zh) * 2015-10-29 2016-02-17 青岛海之源智能技术有限公司 一种细致毛孔洁面乳及其制备方法

Also Published As

Publication number Publication date
CN110384633A (zh) 2019-10-29

Similar Documents

Publication Publication Date Title
CN106038330B (zh) 一种洁面乳及其制备方法
KR101117564B1 (ko) 소금 및/또는 설탕을 포함하는 스크럽 화장료 조성물
CN108096173A (zh) 一种绿色温和的氨基酸洗发水及其制备方法
CN102716044A (zh) 一种低刺激洗发组合物
CN107397686A (zh) 一种连续自发泡组合物及其应用
CN104906015A (zh) 燕窝净白美容面膜
CN108685734A (zh) 一种无硫酸盐无硅低刺激温和植物养发香波
CN111631965A (zh) 一种植物来源的具有清洁和卸妆功能的面膜
CN108403609B (zh) 一种紧致润肤洁面啫喱
CN107929106A (zh) 一种天然椰子油洁面乳及其制备方法
CN107998021A (zh) 一种人参首乌无硅油营养滋润洗发露
CN114306134A (zh) 一种温和双层卸妆液及其制备方法
CN110384633B (zh) 一种含有液晶结构的洁面乳及其制备方法
CN104146931A (zh) 一种天然滋养修护型护发素及其制备方法
CN110269815A (zh) 含有油莎草根油的沐浴露及其制备方法
CN116549307A (zh) 一种安神舒缓型眼唇卸妆液及其制备方法
CN114209637B (zh) 一种舒缓组合物及其应用
CN106333874A (zh) 燕麦补水保湿睡眠面膜
CN112336662B (zh) 一种舒缓沐浴露及其制备方法和应用
CN110063902A (zh) 一种以聚甘油类为卸妆成分的舒润净颜卸妆水及制备方法
CN104055687A (zh) 珠光浴液
CN107875079B (zh) 一种去脂肪粒精华及其制备方法
CN104887543A (zh) 活细胞沐浴液
CN104922012A (zh) 蚕丝美容防晒霜
CN105055211A (zh) 芦荟沐浴液

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant