CN112957299A - Moisturizing and skin-moistening oil-based acyl amino acid salt shower gel and preparation method thereof - Google Patents
Moisturizing and skin-moistening oil-based acyl amino acid salt shower gel and preparation method thereof Download PDFInfo
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- CN112957299A CN112957299A CN202110402237.2A CN202110402237A CN112957299A CN 112957299 A CN112957299 A CN 112957299A CN 202110402237 A CN202110402237 A CN 202110402237A CN 112957299 A CN112957299 A CN 112957299A
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- amino acid
- acid salt
- acyl amino
- moisturizing
- deionized water
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- 150000003839 salts Chemical class 0.000 title claims abstract description 49
- 125000004442 acylamino group Chemical group 0.000 title claims abstract description 48
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title description 5
- 238000001879 gelation Methods 0.000 title description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 35
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000008367 deionised water Substances 0.000 claims abstract description 33
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 33
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 32
- 239000000284 extract Substances 0.000 claims abstract description 25
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000004094 surface-active agent Substances 0.000 claims abstract description 18
- 239000004519 grease Substances 0.000 claims abstract description 17
- 239000011780 sodium chloride Substances 0.000 claims abstract description 16
- HLERILKGMXJNBU-UHFFFAOYSA-N norvaline betaine Chemical compound CCCC(C([O-])=O)[N+](C)(C)C HLERILKGMXJNBU-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229960003237 betaine Drugs 0.000 claims abstract description 10
- 239000002738 chelating agent Substances 0.000 claims abstract description 8
- 239000003755 preservative agent Substances 0.000 claims abstract description 7
- 230000002335 preservative effect Effects 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229940024606 amino acid Drugs 0.000 claims description 48
- 238000003756 stirring Methods 0.000 claims description 44
- 239000003921 oil Substances 0.000 claims description 25
- 235000019198 oils Nutrition 0.000 claims description 25
- 241001116389 Aloe Species 0.000 claims description 11
- 241000207840 Jasminum Species 0.000 claims description 11
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 11
- -1 acyl sodium glycinate Chemical compound 0.000 claims description 11
- 235000011399 aloe vera Nutrition 0.000 claims description 11
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 11
- 235000012343 cottonseed oil Nutrition 0.000 claims description 10
- 239000002385 cottonseed oil Substances 0.000 claims description 9
- 229940065859 sodium cocoyl glycinate Drugs 0.000 claims description 8
- IKGKWKGYFJBGQJ-UHFFFAOYSA-M sodium;2-(dodecanoylamino)acetate Chemical compound [Na+].CCCCCCCCCCCC(=O)NCC([O-])=O IKGKWKGYFJBGQJ-UHFFFAOYSA-M 0.000 claims description 8
- 239000000419 plant extract Substances 0.000 claims description 7
- 108700004121 sarkosyl Proteins 0.000 claims description 7
- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims description 7
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 7
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims description 7
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 7
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 6
- 229960001950 benzethonium chloride Drugs 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims description 6
- 229940079781 sodium cocoyl glutamate Drugs 0.000 claims description 6
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 5
- 235000013905 glycine and its sodium salt Nutrition 0.000 claims description 5
- 239000004247 glycine and its sodium salt Substances 0.000 claims description 5
- 229940029258 sodium glycinate Drugs 0.000 claims description 5
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 4
- 235000010241 potassium sorbate Nutrition 0.000 claims description 4
- 239000004302 potassium sorbate Substances 0.000 claims description 4
- 229940069338 potassium sorbate Drugs 0.000 claims description 4
- 239000006071 cream Substances 0.000 claims description 3
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 2
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims description 2
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 2
- 235000013923 monosodium glutamate Nutrition 0.000 claims description 2
- 229940073490 sodium glutamate Drugs 0.000 claims description 2
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 2
- 239000003974 emollient agent Substances 0.000 claims 3
- 150000002632 lipids Chemical class 0.000 claims 3
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 claims 1
- OCZLHFXYCIDGNN-RJXKWAGSSA-N N[C@@H](CCC(O)=O)C(O)=O.CCCCCCCCCCCC([Na])=O Chemical compound N[C@@H](CCC(O)=O)C(O)=O.CCCCCCCCCCCC([Na])=O OCZLHFXYCIDGNN-RJXKWAGSSA-N 0.000 claims 1
- 239000006210 lotion Substances 0.000 claims 1
- 230000007794 irritation Effects 0.000 abstract description 8
- 238000004140 cleaning Methods 0.000 abstract description 7
- 239000006260 foam Substances 0.000 abstract description 3
- 238000004090 dissolution Methods 0.000 description 16
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 8
- 238000001816 cooling Methods 0.000 description 8
- 229960001484 edetic acid Drugs 0.000 description 6
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 5
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 description 5
- 229940043351 ethyl-p-hydroxybenzoate Drugs 0.000 description 5
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 239000002280 amphoteric surfactant Substances 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 2
- 229940073507 cocamidopropyl betaine Drugs 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 230000037307 sensitive skin Effects 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- FJKROLUGYXJWQN-UHFFFAOYSA-M 4-hydroxybenzoate Chemical compound OC1=CC=C(C([O-])=O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-M 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 206010048245 Yellow skin Diseases 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- GETQZCLCWQTVFV-UHFFFAOYSA-N anhydrous trimethylamine Natural products CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 1
- 238000003287 bathing Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 1
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
- 239000000693 micelle Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a moisturizing oil-based acyl amino acid salt shower gel, which comprises the following raw materials in percentage by weight: 5-15% of natural extract, 15-30% of grease-based acyl amino acid salt surfactant, 2-15% of cocoyl propyl betaine and/or 1-5% of cocamide MEA, 0-2% of betaine, 3-10% of glycerol, 0.01-0.1% of chelating agent, 0.5-2% of sodium chloride, 0-1% of citric acid, 0.1-0.3% of preservative, 0.1-0.3% of essence and the balance of deionized water. The shower gel disclosed by the invention is rich in foam, strong in cleaning capability, mild and low in irritation, has a good skin moisturizing effect, and can enhance the self-repairing capability of skin.
Description
Technical Field
The invention relates to grease-based acyl amino acid salt shower gel, in particular to moisturizing grease-based acyl amino acid salt shower gel and a preparation method thereof, and belongs to the technical field of daily chemical products.
Background
With the continuous improvement of living standard, the requirements of people on washing and caring articles are continuously improved, and more people tend to select the shower gel with lower irritation, higher moisture retention and better biocompatibility. The shower gel is a daily necessary washing and protecting article for cleaning skin dirt during bathing, and is very popular with consumers compared with the prior soap washing and protecting. The traditional shower gel is generally prepared by mixing various chemicals, has great irritation and side effects, can remove skin dirt, can also remove natural oil and fat of the skin, and natural conditioning and moisturizing components, and causes a plurality of problems of dry and tight skin, rough and yellow skin, full body itching and the like, especially sensitive skin. The harm of the traditional shower gel to human bodies is usually greater than the cleaning function of the traditional shower gel. Aiming at the existing defects, the traditional formula is improved, and a certain amount of grease-based acyl amino acid salt surfactant and amphoteric surfactant are added to prepare the novel grease-based acyl amino acid salt shower gel. Compared with the traditional formula, the oil-based acyl amino acid salt shower gel is mild in property, low in irritation and closer in pH value to the pH value of human skin, can enhance the self-repairing capacity of the skin, and can inhibit inflammation, relieve pain and improve skin moisture retention.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides the grease-based acyl amino acid salt shower gel with moisturizing and skin-moistening effects and the preparation method thereof. The mild shower gel is prepared by adding natural plant extracts, the grease-based acyl amino acid salt surfactant, the amphoteric surfactant and other components, has low affinity and irritation, has moisture retention property and can obviously change the skin state.
In order to achieve the purpose, the invention adopts the following technical scheme:
the moisturizing and skin-moistening oil-based acyl amino acid salt shower gel is prepared from the following raw materials in percentage by mass: 5-15% of natural extract, 15-30% of fatty acyl amino acid salt surfactant, 2.5-10% of cocoyl propyl betaine and/or 1-5% of cocoamide (also called as coconut monoethanolamide, MEA), 0-2% of betaine (also called as trimethylamine ethyl lactone, N-trimethylglycine or 1-carboxyl-N, N, N-trimethylglycine), 3-10% of glycerol, 0.01-0.1% of chelating agent, 0.5-2% of sodium chloride, 0.1-1% of citric acid, 0.1-0.3% of preservative, 0.1-0.3% of essence and the balance of deionized water.
Preferably, the essence is food-grade essence.
Preferably, the natural plant extract with the moisturizing and skin-moistening effects in the formula of the oil-based acyl amino acid salt shower gel is one or more of jasmine extract, linlan sugar and aloe leaf juice extract.
Preferably, the natural plant extract in the formula of the oil-based acyl amino acid salt shower gel comprises 0-15% of jasmine extract, 0-15% of linlan sugar and 0-15% of aloe leaf juice extract by mass percent.
Preferably, the grease acyl amino acid salt surfactant in the formula of the grease acyl amino acid salt shower gel is one or a plurality of components selected from cotton seed oil acyl sodium glycinate, sodium cocoyl glutamate, sodium lauroyl glutamate and sodium lauroyl sarcosinate.
Preferably, the oil-based acyl amino acid salt surfactant in the formula of the oil-based acyl amino acid salt shower gel is prepared by compounding one or more of 5-10% of cottonseed oil acyl sodium glycinate, 5-10% of sodium cocoyl glycinate, 5-15% of sodium cocoyl glutamate, 5-15% of sodium lauroyl glutamate, 5-20% of sodium lauroyl sarcosinate and the like in percentage by mass, has good cleaning, foaming and moisturizing capabilities, has a pH value close to that of human skin, and is a basic substance forming protein by adding amino acid, so that the oil-based acyl amino acid salt shower gel is mild and moisturized, and is suitable for sensitive skin.
The soap comprises 2.5-10% of cocoyl propyl betaine and/or 1-5% of cocoamide (MEA), 0-2% of betaine and other surfactants in the formula of the grease-based acyl amino acid salt shower gel, has good foamability, thickening property and emulsibility, can improve the softness and low-temperature stability of the shower gel product, and is a main component of the shower gel product.
Preferably, the chelating agent in the formula of the oil-based acyl amino acid salt shower gel is one or two of disodium ethylene diamine tetraacetate (EDTA-2Na) and tetrasodium ethylene diamine tetraacetate (EDTA-4Na), and the chelating agent can soften water and reduce the oxidation of metal ions.
Preferably, the preservative in the formula of the oil-based acyl amino acid salt shower gel is prepared by compounding one or more of p-hydroxybenzoate, potassium sorbate and benzethonium chloride, and can effectively inhibit the growth of microorganisms, bacteria and the like and prolong the shelf life.
Preferably, the thickening agent in the grease-based acyl amino acid salt bath cream formula is 0.5-2% of sodium chloride, and the sodium chloride is used as the thickening agent, and the sodium chloride is actually salt, so that the concentration required by the surfactant for forming worm-like micelles is reduced, and the surfactant can more easily form a viscoelastic fluid.
The invention also provides a preparation method of the moisturizing and skin-moistening oil-based acyl amino acid salt shower gel, which comprises the following steps:
s1: dissolving oil-based acyl amino acid salt surfactant, cocoyl propyl betaine and/or cocamide (MEA), betaine, glycerol and chelating agent in deionized water under stirring, adding natural plant extract, and stirring;
s2: under the condition of stirring, adding sodium chloride and citric acid into the solution obtained in S1, and uniformly stirring;
s3: under the condition of stirring, dissolving the preservative and the essence in deionized water, adding the deionized water into the solution obtained in the step S2, stirring uniformly, standing and defoaming;
wherein the amount of the deionized water in the step S1 is 85% -95% of the total amount of the deionized water, and the amount of the deionized water in the step S3 is the rest of the deionized water.
The invention has the beneficial effects that: the oil-based acyl amino acid salt bath cream disclosed by the invention adopts an oil-based acyl amino acid salt surfactant, an amphoteric surfactant and the like, has excellent quality, has excellent foaming and cleaning functions, is low in mild irritation, and can enhance the self-repairing capacity of skin, and enhance the moisture retention and skin smoothness. The amphoteric surfactant has good washing performance and dispersibility, can generate a large amount of foam, and improves the mild softness of the washing and protecting product. The shower gel can effectively clean body dirt, enhance skin smoothness and preserve moisture. The shower gel disclosed by the invention is rich in foam, strong in cleaning capability, mild and low in irritation, has a good skin moisturizing effect, and can enhance the self-repairing capability of skin.
Detailed Description
The present invention will be further described with reference to specific examples, which are provided for the purpose of illustration only and are not intended to be limiting.
In the following examples jasmine extract, linlan sugar and aloe leaf juice extract were purchased from clean water biotechnology limited of Beijing cloud; sodium cottonseed oil acyl glycinate was prepared in the following examples by using cottonseed oil as the oil and fat, see patent document (publication No. CN102266737B, method for preparing N-fatty acyl amino acid surfactant from oil and fat). The flavors in the following examples are food grade flavors.
Example 1
The oil-based acyl amino acid salt shower gel comprises the following raw material components in percentage by mass: phase A: 53% of deionized water, 0.05% of EDTA-2Na, 5% of sodium cottonseed oil acyl glycinate, 15% of sodium cocoyl glutamate, 2% of cocamide MEA, 5% of cocoyl propyl betaine, 5% of glycerol, 2% of jasmine extract, 4% of linlan sugar, 2% of aloe leaf juice extract and phase B: 1% of sodium chloride, 0.1% of citric acid, and phase C: 5.45 percent of deionized water, 0.2 percent of ethyl p-hydroxybenzoate and 0.2 percent of essence.
The method for preparing the grease-based acyl amino acid salt shower gel comprises the following specific steps:
s1: dissolving the cottonseed oil acyl sodium glycinate in the phase A in deionized water while stirring, setting the rotating speed to be 350-year-old 500rpm, the temperature to be 60 ℃, standing and cooling to room temperature after complete dissolution, then adding the cocoyl sodium glutamate and the cocoyl propyl betaine while stirring, setting the rotating speed to be 350-year-old 500rpm, the temperature to be 60 ℃, stirring for about 15min until dissolution, continuously stirring, adding the components of glycerol, cocamide MEA and EDTA-2Na, stirring until uniform dissolution is realized, finally adding the jasmine flower extract, the linlan sugar and the aloe leaf juice extract, and stirring for uniform dissolution;
s2: after the phase A is completely dissolved, adding sodium chloride and citric acid in the phase B while stirring, wherein the temperature is 60 ℃, and adding the phase C after the phase B is completely dissolved;
s3: dissolving ethyl p-hydroxybenzoate and essence in phase C in deionized water, adding into S2 solution, stirring for 20min until completely dissolved, standing for defoaming, and cooling.
Example 2
The oil-based acyl amino acid salt shower gel comprises the following raw material components in percentage by mass: phase A: 52% of deionized water, 0.05% of EDTA-2Na, 10% of sodium lauroyl sarcosinate, 6% of sodium lauroyl glutamate, 6% of sodium cocoyl glycinate, 2% of cocamide MEA, 3% of cocamidopropyl betaine, 1% of betaine, 4% of glycerol, 2% of jasmine extract, 4% of forest blue sugar, 2% of aloe leaf juice extract and phase B: 1% of sodium chloride, 0.2% of citric acid, and phase C: 6.25 percent of deionized water, 0.25 percent of potassium sorbate, 0.05 percent of benzethonium chloride and 0.2 percent of essence.
The method for preparing the grease-based acyl amino acid salt shower gel comprises the following specific steps:
s1: dissolving sodium lauroyl sarcosinate in the phase A in deionized water while stirring, setting the rotating speed to be 350-500rpm and the temperature to be 60 ℃, standing and cooling to room temperature after complete dissolution, then adding sodium lauroyl glutamate, sodium cocoyl glycinate, cocoyl propyl betaine and betaine while stirring, setting the rotating speed to be 350-500rpm and the temperature to be 60 ℃, stirring for about 15min until dissolution, continuously stirring, adding glycerol, cocamide MEA and EDTA components, stirring until uniform dissolution, finally adding jasmine flower extract, linlan sugar and aloe leaf juice extract, and stirring uniformly for dissolution;
s2: after the phase A is completely dissolved, adding sodium chloride and citric acid in the phase B while stirring, wherein the temperature is 60 ℃, and adding the phase C after the phase B is completely dissolved;
s3: dissolving potassium sorbate, benzethonium chloride and essence in phase C in deionized water, adding into S2 solution, stirring for 20min, standing for defoaming, and cooling.
Example 3
The oil-based acyl amino acid salt shower gel comprises the following raw material components in percentage by mass: phase A: 52% of deionized water, 0.05% of EDTA-4Na, 5% of sodium cocoyl glutamate, 10% of sodium lauroyl sarcosinate, 5% of sodium cocoyl glycinate, 1% of cocamide MEA, 6% of cocamidopropyl betaine, 2% of glycerol, 3% of jasmine extract, 6% of forest blue sugar, 3% of aloe leaf juice extract and phase B: 1% of sodium chloride, 0.1% of citric acid, and phase C: 5.45 percent of deionized water, 0.3 percent of methyl p-hydroxybenzoate and 0.1 percent of essence.
The method for preparing the grease-based acyl amino acid salt shower gel comprises the following specific steps:
s1: dissolving sodium lauroyl sarcosinate in the phase A in deionized water while stirring, setting the rotating speed to be 350-year 500rpm, the temperature to be 60 ℃, standing and cooling to room temperature after complete dissolution, then adding sodium cocoyl glutamate, sodium cocoyl glycinate and cocoyl propyl betaine while stirring, setting the rotating speed to be 350-year 500rpm, the temperature to be 60 ℃, stirring for about 15min until dissolution, continuously stirring, adding glycerol, cocamide MEA and EDTA-4Na components, stirring until uniform dissolution, finally adding jasmine extract, lincomose and aloe leaf juice extract, and stirring for uniform dissolution;
s2: after the phase A is completely dissolved, adding sodium chloride and citric acid in the phase B while stirring, wherein the temperature is 60 ℃, and adding the phase C after the phase B is completely dissolved;
s3: dissolving ethyl p-hydroxybenzoate and essence in phase C in deionized water, adding into S2 solution, stirring for 20min until completely dissolved, standing for defoaming, and cooling.
Example 4
The oil-based acyl amino acid salt shower gel comprises the following raw material components in percentage by mass: phase A: 54% of deionized water, 0.05% of EDTA-4Na, 5% of sodium cottonseed oil acyl glycinate, 10% of sodium cocoyl glycinate, 8% of sodium lauroyl glutamate, 2% of cocamide MEA, 4% of cocoyl propyl betaine, 0.05% of betaine, 2% of glycerol, 8% of lincose and phase B: sodium chloride 1%, phase C: 5.5 percent of deionized water; 0.15 percent of ethyl p-hydroxybenzoate, 0.05 percent of benzethonium chloride and 0.2 percent of essence.
The method for preparing the grease-based acyl amino acid salt shower gel comprises the following specific steps:
s1: dissolving sodium cocoyl glycinate in the phase A in deionized water while stirring, setting the rotating speed to be 350-year-old 500rpm, setting the temperature to be 60 ℃, standing and cooling to room temperature after complete dissolution, then adding sodium cottonseed oleoyl glycinate, sodium lauroyl glutamate, cocoyl propyl betaine and betaine while stirring, setting the rotating speed to be 350-year-old 500rpm, setting the temperature to be 60 ℃, stirring for about 15min until dissolution, continuously stirring, adding glycerol, cocamide MEA (membrane electrode assembly) and EDTA-4Na (ethylene diamine tetraacetic acid), stirring until uniform dissolution, finally adding forest sugar, and stirring for uniform dissolution;
s2: after the phase A is completely dissolved, adding sodium chloride in the phase B while stirring, wherein the temperature is 60 ℃, and adding the phase C after the phase B is completely dissolved;
s3: dissolving ethyl p-hydroxybenzoate, benzethonium chloride and essence in phase C in deionized water, adding into S2 solution, stirring for 20min until completely dissolved, standing for defoaming, and cooling.
The invention adopts the grease-based acyl amino acid salt surfactant as a main active ingredient to replace the traditional fatty alcohol-polyoxyethylene ether sulfate surfactant, and the prepared shower gel has good cleaning ability, low mild irritation, better skin moisturizing ability and enhanced self-repairing function of the skin.
It should be noted that the above description is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and the related technical solutions and the inventive concepts thereof are within the scope of the present invention.
Claims (8)
1. The moisturizing and skin-moistening oil-based acyl amino acid salt bath lotion is characterized by comprising the following raw materials in percentage by mass: 5-15% of natural extract, 15-30% of grease-based acyl amino acid salt surfactant, 2.5-10% of cocoyl propyl betaine and/or 1-5% of cocamide, 0-2% of betaine, 3-10% of glycerol, 0.01-0.1% of chelating agent, 0.5-2% of sodium chloride, 0-1% of citric acid, 0.1-0.3% of preservative, 0.1-0.3% of essence and the balance of deionized water.
2. The moisturizing and skin-moistening lipid-based acyl amino acid salt body wash as claimed in claim 1, wherein the natural plant extract is one or more of jasmine extract, linlan sugar and aloe leaf juice extract.
3. The moisturizing emollient oil-based acyl amino acid salt bath cream according to claim 2, wherein the natural plant extract comprises 0-15% of jasmine extract, 0-15% of linlan sugar and 0-15% of aloe leaf juice extract.
4. The moisturizing and skin-moistening fat-based acyl amino acid salt shower gel according to claim 1, wherein the fat-based acyl amino acid salt surfactant is one or more of cottonseed oil acyl sodium glycinate, cocoyl sodium glutamate and lauroyl sodium glutamate.
5. The moisturizing and skin-moistening fat-based acyl amino acid salt shower gel as claimed in claim 1 or 4, wherein the fat-based acyl amino acid salt surfactant is one or more of 5-10% of cottonseed oil acyl sodium glycinate, 5-10% of sodium cocoyl glycinate, 5-15% of sodium cocoyl glutamate, 5-15% of sodium lauroyl glutamate and 5-20% of sodium lauroyl sarcosinate.
6. The moisturizing emollient lipid-based acyl amino acid salt body wash of claim 1, wherein said chelating agent is one of disodium ethylenediaminetetraacetate and tetrasodium ethylenediaminetetraacetate.
7. The moisturizing and skin-moistening oil-based acyl amino acid salt shower gel as claimed in claim 1, wherein the preservative is one or more of paraben, potassium sorbate and benzethonium chloride.
8. The method for preparing the moisturizing emollient lipid-based acyl amino acid salt body wash according to any one of claims 1-7, comprising the steps of:
s1: dissolving oil-based acyl amino acid salt surfactant, cocoyl propyl betaine and/or cocoamide, betaine, glycerol and chelating agent in deionized water under stirring, adding natural plant extract, and stirring;
s2: under the condition of stirring, adding sodium chloride and citric acid into the solution obtained in S1, and uniformly stirring;
s3: under the condition of stirring, dissolving the preservative and the essence in deionized water, adding the deionized water into the solution obtained in the step S2, stirring uniformly, standing and defoaming;
wherein the amount of the deionized water in the step S1 is 85% -95% of the total amount of the deionized water, and the amount of the deionized water in the step S3 is the rest of the deionized water.
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| WO2014170025A1 (en) * | 2013-04-20 | 2014-10-23 | Clariant International Ltd | Composition containing oil bodies, fatty acids, amino acid surfactants, and n-methyl-n-acylglucamines |
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| WO2014170025A1 (en) * | 2013-04-20 | 2014-10-23 | Clariant International Ltd | Composition containing oil bodies, fatty acids, amino acid surfactants, and n-methyl-n-acylglucamines |
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