CN112891287A - Makeup removing composition for moisturizing, controlling oil and nourishing skin - Google Patents
Makeup removing composition for moisturizing, controlling oil and nourishing skin Download PDFInfo
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- CN112891287A CN112891287A CN202110334105.0A CN202110334105A CN112891287A CN 112891287 A CN112891287 A CN 112891287A CN 202110334105 A CN202110334105 A CN 202110334105A CN 112891287 A CN112891287 A CN 112891287A
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- 239000000203 mixture Substances 0.000 title claims abstract description 24
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 14
- 239000003814 drug Substances 0.000 claims abstract description 26
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- 229940079593 drug Drugs 0.000 claims abstract description 19
- 240000003377 Shepherdia canadensis Species 0.000 claims abstract description 16
- 235000018324 Shepherdia canadensis Nutrition 0.000 claims abstract description 16
- 235000018597 common camellia Nutrition 0.000 claims abstract description 15
- 239000000284 extract Substances 0.000 claims abstract description 13
- 240000001548 Camellia japonica Species 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 241000045403 Astragalus propinquus Species 0.000 claims abstract description 11
- 244000303040 Glycyrrhiza glabra Species 0.000 claims abstract description 11
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- 241000219287 Saponaria Species 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 8
- 239000004480 active ingredient Substances 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims description 10
- 239000000706 filtrate Substances 0.000 claims description 9
- 238000010992 reflux Methods 0.000 claims description 7
- 238000002791 soaking Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000010025 steaming Methods 0.000 claims description 3
- 241000196324 Embryophyta Species 0.000 claims description 2
- 239000006286 aqueous extract Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 17
- 238000004140 cleaning Methods 0.000 abstract description 9
- 230000037394 skin elasticity Effects 0.000 abstract description 8
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- 238000009499 grossing Methods 0.000 abstract 1
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- 238000001514 detection method Methods 0.000 description 7
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- 238000012360 testing method Methods 0.000 description 5
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- 240000007817 Olea europaea Species 0.000 description 4
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- 239000007788 liquid Substances 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- OQILCOQZDHPEAZ-UHFFFAOYSA-N octyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OCCCCCCCC OQILCOQZDHPEAZ-UHFFFAOYSA-N 0.000 description 4
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- 241000220317 Rosa Species 0.000 description 3
- 206010040925 Skin striae Diseases 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000000419 plant extract Substances 0.000 description 3
- 229940079988 potassium cocoyl glycinate Drugs 0.000 description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 3
- 239000004299 sodium benzoate Substances 0.000 description 3
- 235000010234 sodium benzoate Nutrition 0.000 description 3
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical group CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 2
- JNAYPSWVMNJOPQ-UHFFFAOYSA-N 2,3-bis(16-methylheptadecanoyloxy)propyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCC(C)C)COC(=O)CCCCCCCCCCCCCCC(C)C JNAYPSWVMNJOPQ-UHFFFAOYSA-N 0.000 description 2
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 description 2
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 2
- 241000721047 Danaus plexippus Species 0.000 description 2
- 241000220485 Fabaceae Species 0.000 description 2
- 240000002853 Nelumbo nucifera Species 0.000 description 2
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 2
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 2
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 229940041616 menthol Drugs 0.000 description 2
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 150000007949 saponins Chemical class 0.000 description 2
- 229940042585 tocopherol acetate Drugs 0.000 description 2
- 229940093609 tricaprylin Drugs 0.000 description 2
- 229940098385 triisostearin Drugs 0.000 description 2
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 2
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- GHVNFZFCNZKVNT-UHFFFAOYSA-N Decanoic acid Natural products CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000931143 Gleditsia sinensis Species 0.000 description 1
- 239000009636 Huang Qi Substances 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241000378467 Melaleuca Species 0.000 description 1
- 241000219926 Myrtaceae Species 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 241000209504 Poaceae Species 0.000 description 1
- 241000580938 Sapindus Species 0.000 description 1
- 241000580955 Sapindus mukorossi Species 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
- 206010040844 Skin exfoliation Diseases 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- -1 acyl glycinate Chemical compound 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 230000004087 circulation Effects 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000035618 desquamation Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 235000011477 liquorice Nutrition 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 208000019423 liver disease Diseases 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000004089 microcirculation Effects 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000002417 nutraceutical Substances 0.000 description 1
- 235000021436 nutraceutical agent Nutrition 0.000 description 1
- 230000037312 oily skin Effects 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 238000007427 paired t-test Methods 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- GZWNUORNEQHOAW-UHFFFAOYSA-M potassium;2-aminoacetate Chemical compound [K+].NCC([O-])=O GZWNUORNEQHOAW-UHFFFAOYSA-M 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000036548 skin texture Effects 0.000 description 1
- 230000036555 skin type Effects 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 1
- 229940093633 tricaprin Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a makeup removing composition for moisturizing, controlling oil and nourishing skin, which is characterized by consisting of a medically acceptable external-use medicine auxiliary material and effective components, wherein the effective components are water extracts of the following raw material medicines in percentage by weight: 23-30% of saponaria gleditsiae, 16-22% of camellia seeds, 16-22% of soapberry skin, 9-12% of melaleuca alternifolia, 9-12% of lophatherum gracile, 9-12% of astragalus membranaceus and 5-8% of glycyrrhiza glabra; the makeup removing composition comprises 1-20 wt% of active ingredients. The makeup removing composition has multiple effects of cleaning and protecting skin, moisturizing, balancing grease, tightening skin, smoothing skin and the like, and has remarkable effects of moisturizing, controlling oil and improving skin elasticity.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a plant extract which is originated from plants and has an undetermined structure, is suitable for makeup removing products and has the effects of moisturizing, controlling oil and nourishing skin.
Background
Currently, makeup removing products on the market are divided into three types, namely makeup removing cream, makeup removing liquid and makeup removing oil according to the texture. The three products differ in that: the oil-based cleansing product has stronger oil solubility; the cleansing milk and the cleansing liquid have moderate water-oil balance, the oily components can wash away dirt, and the aqueous components can moisten skin. In fact, products with different efficacies should be selected according to different skin types. For example, cleansing oily skin is particularly important, and makeup removing products which can clean thoroughly and have an oil control effect are preferably selected; for the skin with partial dryness, makeup removing products with moistening effect should be selected. The skin of eyes and lips of a human body is very delicate, and a professional eye and lip makeup removing product is needed, so that the eye and lip makeup remover can thoroughly clean the eyes and lips and can protect sensitive skin.
Patent application publication No. CN105796408A discloses a cleansing oil composition comprising a plant extract composition as an active ingredient, wherein the active ingredient is contained in an amount of 1 to 60% by weight based on the total weight of the cleansing oil composition; based on the total weight of the plant extract composition, the content of the camellia seed oil is 20-40 wt%, the content of the soapberry seed oil is 15-30 wt%, the content of the kelp extract is 10-20 wt%, the content of the olive extract is 15-30 wt%, and the content of the aloe extract is 20-40 wt%; and the weight ratio of the camellia seed oil, the soapberry seed oil, the kelp extract, the olive extract and the aloe extract is 1: (0.5-1): (0.5-0.8): (0.5-1): (0.8-1.5). The cleansing oil composition has the effects of moisturizing, controlling oil and improving skin elasticity, but the overall effect is still not ideal.
Disclosure of Invention
The invention aims to provide a makeup removing composition for moisturizing, controlling oil and nourishing skin, which has remarkable effects of moisturizing, controlling oil and improving skin elasticity.
The technical scheme for solving the problems is as follows:
the makeup removing composition consists of a medically acceptable external-use medicine auxiliary material and effective components, wherein the effective components are water extracts of the following raw material medicines in percentage by weight: 23-30% of saponaria gleditsiae, 16-22% of camellia seeds, 16-22% of soapberry skin, 9-12% of melaleuca alternifolia, 9-12% of lophatherum gracile, 9-12% of astragalus membranaceus and 5-8% of glycyrrhiza glabra; the makeup removing composition comprises 1-20 wt% of active ingredients.
In the scheme, the optimal mixture ratio of the raw material medicines is 26% of the saponaria gleditsiae, 19% of the camellia seed, 19% of the soapberry skin, 10% of the melaleuca alternifolia, 10% of the lophatherum gracile, 10% of the astragalus membranaceus and 6% of the glycyrrhiza glabra.
In the scheme, the preparation method of the aqueous extract comprises the following steps:
adding 8-12 times of water into the raw material medicines, soaking for 30-45 minutes, extracting for 2 times by refluxing, extracting for 1.5-3 hours each time, filtering, combining filtrates, and concentrating to obtain a concentrated solution containing 1g of the raw material medicines per milliliter; or,
adding 6-10 times of water into the raw material medicines, soaking for 30-45 minutes, extracting for 2 times by refluxing, extracting for 1.5-2 hours each time, filtering, combining filtrates, concentrating to a proper amount, adding ethanol, standing overnight, filtering, and steaming into thick paste by water bath at 100 ℃.
In the effective components of the makeup removing composition, the soapberry is fruit of Gleditsia sinensis Lamarck of Leguminosae Gleditisiamicrophhylla Gordon ex Y.T.Lee; the Camellia seed is seed of Camellia (Camellia L.) belonging to Theaceae (Theaceae); the soapberry peel is pericarp of Sapindus mukorossi Gaertn of Sapindus; branches and leaves of Melaleuca alternifolia (Maiden & Betche) Cheel of Melaleuca of Myrtaceae; the herba Lophatheri is dried stem and leaf of Lophatherum gracile Brongn of Gramineae; the radix astragali is root of Astragalus membranaceus (Fisch.) bge of Leguminosae; glycyrrhiza glabra is dried root and rhizome of Glycyrrhiza glabra L.
The external use medicine auxiliary material of the makeup removing composition consists of cocoyl potassium glycinate, decyl glucoside, sodium benzoate, essence and water, wherein the essence is menthol, rose essence or lotus leaf essence.
In the formula of the makeup removing composition, the small fruit saponin is warm in nature and pungent in taste, has the effects of opening orifices, dredging, dispersing masses, reducing swelling, eliminating phlegm as a monarch drug, opening orifices, dispersing masses, regulating skin striae, increasing skin oil, moisturizing, replenishing water, tightening skin textures and increasing skin elasticity; the tea seeds, the soapberry and the cajeput are ministerial drugs, wherein the tea seeds are sweet and smooth and moisten qi and promote the circulation of qi, benefit marrow and moisten skin, the soapberry has bitter cold and clear heat, and the cajeput aromatic and exterior-relieving co-help monarch drugs open orifices and dissipate stagnation to dredge and regulate skin striae; the lophatherum gracile and the astragalus membranaceus are adjuvant drugs, wherein the lophatherum gracile is sweet and light in taste and cold in nature, the drastic and violent movement of the pungent-warm property of the saponin and the cajeput is relieved, and the astragalus membranaceus is sweet and warm in taste, and has the effects of tonifying qi, consolidating the exterior, promoting skin microcirculation and enabling the skin to be ruddy and glossy; the liquorice is used as a guiding drug to harmonize the drug property and make the various medicines in the prescription exert the drug effect. The traditional Chinese medicine composition has the obvious effects of inducing resuscitation and resolving masses, regulating skin striae, supplementing water and moisturizing, increasing skin oil, and increasing skin compactness and elasticity by combining the medicines.
Detailed Description
Example 1
Taking 26g of saponaria gleditsiae, 19g of camellia seeds, 19g of soapberry skin, 10g of melaleuca alternifolia, 10g of lophatherum gracile, 10g of astragalus membranaceus and 6g of glycyrrhiza glabra, adding 8 times of water, soaking for 30 minutes, performing reflux extraction for 2 times, performing 1.5 hours each time, filtering, combining filtrates, concentrating to a proper amount, adding ethanol, standing overnight, filtering, and performing water bath steaming at 100 ℃ to obtain a thick paste.
Taking 2g of the thick paste, adding 1g of potassium cocoyl glycinate, 5g of decyl glucoside, 0.2g of sodium benzoate and 0.3g of menthol, adding distilled water to 100g, and uniformly mixing to obtain the ointment.
Example 2
Taking 23g of saponaria gleditsiae, 18g of camellia seed extract, 18g of soapberry skin, 11g of melaleuca alternifolia, 12g of lophatherum gracile, 11g of astragalus membranaceus and 7g of glycyrrhiza glabra, adding 12 times of water, soaking for 45 minutes, performing reflux extraction for 2 times, performing 2 hours each time, filtering, combining filtrates, concentrating to the concentration equivalent to 1g of raw material medicine contained in each milliliter, and performing concentration
Taking 12g of the filtrate, adding 5g of potassium cocoyl glycinate, 8g of decyl glucoside, 0.2g of sodium benzoate and 0.2g of rose essence, adding distilled water to 100g, and mixing uniformly to obtain the rose essence.
Example 3
Taking 29g of saponaria gleditsiae, 20g of camellia seeds, 18g of soapberry skin, 9g of melaleuca alternifolia, 9g of lophatherum gracile, 9g of astragalus membranaceus and 6g of glycyrrhiza glabra, adding 10 times of water, soaking for 40 minutes, performing reflux extraction for 2 times, 3 hours each time, filtering, combining filtrates, and concentrating to be equivalent to 1g of raw material medicine contained in each milliliter.
And (3) taking 8g of the filtrate, adding 3g of potassium cocoyl glycinate, 6g of decyl glucoside and 0.2g of lotus leaf essence, adding distilled water to 100g, and uniformly mixing to obtain the coconut oil acyl glycinate.
Example 4 (evaluation test of cleansing effect)
1. Purpose of the experiment: test of cleansing and Makeup removing effects of examples 1, 2, and 3
2. The experimental method comprises the following steps: 24 female volunteers 25-45 years old were selected and randomized into three groups of 8 individuals each, example 1, 2, 3. Standing for 30min before experiment, and collecting image data with skin magnifier (I-scope); uniformly coating an ashiranatural dw foundation liquid on a face detection area of each subject, and observing the cosmetic filling area in the skin surface texture by I-scope after coating; the subjects then performed makeup removal cleaning with the products prepared in examples 1, 2, 3, respectively, and observed again with I-scope after cleaning. All measurements were carried out in a laboratory at room temperature 18-22 ℃ and relative humidity 40-60%. The experiment is statistically analyzed by using paired t test, and p is less than 0.05, so that the difference has statistical significance.
3. The experimental results are as follows: i-scope detection result: the filling area of the cosmetics in the surface texture of the skin after sample application is obviously increased (P is less than 0.05), the filling area after cleaning is obviously reduced (P is less than 0.05) compared with the filling area after sample application, but the filling area is not obviously different (P is more than 0.05) compared with the filling area before sample application, and the experimental result shows that the cleaning and makeup removing effects of the examples 1, 2 and 3 are good.
TABLE 1
| Before coating | After sample application | After cleaning | |
| EXAMPLE 1 group | 136.15±25.21 | 386.87±128.71* | 135.59±32.14# |
| EXAMPLE 2 group | 135.54±43.35 | 389.64±155.62* | 136.65±48.22# |
| EXAMPLE 3 group | 136.85±39.43 | 387.85±144.32* | 136.95±29.81# |
In the table, the cosmetic filling area in the skin surface texture was significantly increased after application of the sample (P < 0.05); after cleaning, the filling area is obviously reduced compared with that after coating (P < 0.05)
Example 5 (evaluation experiment of moisturizing, oil-controlling and skin-caring effects)
1.1 general data 40 cases observed in 6/2020 to 9/2020, all were volunteers in industrial park, women of 25-45 years old who used cosmetics. Randomly divided into 4 groups, namely, an example 1 group, an example 2 group, an example 3 group and a comparison group (the best proportion in the patent application with the publication number of CN105796408A is selected as the comparison group, namely, the weight ratio of the camellia seed oil, the soapberry seed oil, the kelp extract, the olive extract and the aloe extract is 1 (0.5-1): 0.5-0.8: 0.5-1: 0.8-1.5), the content of active ingredients is 10-40 wt%, and based on the total weight of the auxiliary materials, the content of PEG-20 triisostearin is 4-6 wt%, the content of tricaprylin/decanoic acid glyceride is 10-20 wt%, the content of white oil is 35-45 wt%, the content of octyl palmitate is 35-45 wt%, the content of vitamin E acetate is 0.8-1.2 wt%, and the content of essence is 0.2-0.3 wt%, namely, the related proportion of CN105796408A patent application is the mixed material according to the CN example 2 Homogeneous).
1.2 Inclusion criteria cosmetic-containing women aged 25-45 were selected for skin that was slightly dry, had desquamation, and had poor skin elasticity.
1.3 eliminating standard complicated dermatitis, acne and other facial skin diseases; pregnant or lactating women; patients with liver and cardiovascular diseases; patients with malignant tumors; the effect cannot be judged or the data is not completely influenced.
2 product application method
2.1 example groups products were prepared as described above in examples 1, 2, 3, and each group of subjects used the products prepared by the examples for removing make-up and no other skin care products after removing make-up. The dosage is 5-8g each time, and the face is cleaned with clear water 15 minutes after use, and the face cleaning liquid is used once a day.
2.2 the control group is obtained by uniformly mixing the materials according to the relevant proportion of example 2 in the patent application CN 105796408A; the effective components are as follows: the weight ratio of the camellia seed oil, the soapberry seed oil, the kelp extract, the olive extract and the aloe extract is 1: 0.8: 0.5: 0.8: 1.2, wherein the effective components account for 10 percent, and the auxiliary materials are as follows: 4% of PEG-20 triisostearin, 20% of tricaprylin/tricaprin, 35% of white oil, 40% of octyl palmitate, 0.8% of vitamin E acetate and 0.2% of essence. The product was tested as described above for use.
2.3 statistical methods T test was used.
3 evaluation of Effect
3.1 tester KF-833 skin moisture oil content elasticity monitor (Kangfutong electronic Co., Ltd.)
3.2 test methods all tests were carried out in a constant temperature, constant humidity room, temperature (25 + -1) deg.C, humidity (50 + -5)%. The subjects tested the moisture and elasticity values of facial skin oil before, after 4 weeks of use, and after 8 weeks of use of the product; before using the product, the subjects used the last day of week 4 and week 8 every day, after cleaning the facial skin, sit still for 30 minutes, use the instrument to detect the skin in the middle of the cheek, and do the skin oil content detection, the moisture detection and the skin elasticity value detection respectively, and each subject does three detections in the same part of the cheek, and the average value of the detection data is taken. During the evaluation experiments, all subjects had to take orally other drugs, nutraceuticals that increase skin moisture, oil and elasticity, or skin care products of similar efficacy.
3.3 results of the experiment
The results of the changes in facial skin properties of 40 subjects after 8 weeks of use of the composition are shown in tables 2, 3 and 4. The mean values of skin oil content before experiment in the example group and the mean values of skin oil content before treatment in the control group have no statistical difference (p > 0.05) compared among the groups.
(1) Average skin oil content: after the 4 th week of the experiment, the groups of example 1, example 2 and example 3 have significant difference (p < 0.05) compared with the control group; after 8 weeks of the experiment, the groups of example 1, example 2 and example 3 were significantly different from the control group (p < 0.05). And the skin oil content data of the example groups increased with increasing experimental time.
TABLE 2
P < 0.05 compared to control group
(2) Mean skin moisture content: after the 4 th week of the experiment, the groups of example 1, example 2 and example 3 have no significant difference from the control group (p > 0.05); after 8 weeks of the experiment, the groups of example 1, example 2, example 3 and the control group all showed significant differences (p < 0.05).
TABLE 3
P < 0.05 compared to control group
(3) Facial skin elasticity: after the 4 th week of the experiment, the groups of example 1, example 2 and example 3 have no significant difference from the control group (p > 0.05); after 8 weeks of the experiment, the groups of example 1, example 2, example 3 and the control group all showed significant differences (p < 0.05).
TABLE 4
P < 0.05 compared to control group
In the experimental period, the example group and the blank control group have no adverse reaction, and each subject completes the evaluation of the experimental test.
4 conclusion
The composition disclosed by the invention is proved to be capable of obviously increasing skin oil content through experimental observation, and also capable of increasing skin moisture and improving skin elasticity along with the increase of the using time.
Claims (3)
1. The makeup removing composition consists of a medically acceptable external-use medicine auxiliary material and effective components, wherein the effective components are water extracts of the following raw material medicines in percentage by weight: 23-30% of saponaria gleditsiae, 16-22% of camellia seeds, 16-22% of soapberry skin, 9-12% of melaleuca alternifolia, 9-12% of lophatherum gracile, 9-12% of astragalus membranaceus and 5-8% of glycyrrhiza glabra; the makeup removing composition comprises 1-20 wt% of active ingredients.
2. The makeup removing composition for moisturizing, controlling oil and nourishing skin according to claim 1, wherein the effective components are water extracts of the following plants in percentage by weight: 26% of saponaria gleditsiae, 19% of camellia seeds, 19% of soapberry skin, 10% of melaleuca alternifolia, 10% of lophatherum gracile, 10% of astragalus membranaceus and 6% of glycyrrhiza glabra.
3. The makeup removing composition for moisturizing, controlling oil and nourishing skin according to claims 1 and 2, characterized in that the aqueous extract is prepared by the following method:
adding 8-12 times of water into the raw material medicines, soaking for 30-45 minutes, extracting for 2 times by refluxing, extracting for 1.5-3 hours each time, filtering, combining filtrates, and concentrating to obtain a concentrated solution containing 1g of the raw material medicines per milliliter; or,
adding 6-10 times of water into the raw material medicines, soaking for 30-45 minutes, extracting for 2 times by refluxing, extracting for 1.5-2 hours each time, filtering, combining filtrates, concentrating to a proper amount, adding ethanol, standing overnight, filtering, and steaming into thick paste by water bath at 100 ℃.
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