CN112715572A - Air disinfectant for livestock and poultry houses or vegetable greenhouses - Google Patents
Air disinfectant for livestock and poultry houses or vegetable greenhouses Download PDFInfo
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- CN112715572A CN112715572A CN202110001294.XA CN202110001294A CN112715572A CN 112715572 A CN112715572 A CN 112715572A CN 202110001294 A CN202110001294 A CN 202110001294A CN 112715572 A CN112715572 A CN 112715572A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/12—Antidiarrhoeals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P15/00—Drugs for genital or sexual disorders; Contraceptives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P15/00—Drugs for genital or sexual disorders; Contraceptives
- A61P15/14—Drugs for genital or sexual disorders; Contraceptives for lactation disorders, e.g. galactorrhoea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
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- Life Sciences & Earth Sciences (AREA)
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- Veterinary Medicine (AREA)
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- Endocrinology (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Inorganic Chemistry (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Gynecology & Obstetrics (AREA)
- Toxicology (AREA)
- Epidemiology (AREA)
- Pregnancy & Childbirth (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses an air disinfectant for livestock and poultry houses or vegetable greenhouses, which comprises the following raw materials in parts by weight: 4-16 parts of montmorillonite, 8-10 parts of zeolite powder, 10-15 parts of an acidic solution, 20-30 parts of a sucrose solution with the mass fraction of 30-40%, 20-30 parts of a liquid stable chlorine dioxide aqueous solution with the mass fraction of 3-5%, 4-8 parts of a stabilizer and 2-4 parts of a slow release agent. The invention discloses a preparation method of the air disinfectant for livestock and poultry houses or vegetable greenhouses, which comprises the following steps: adding montmorillonite and zeolite powder into an acid solution for soaking, taking out, washing, drying, placing in a sucrose solution for soaking, sealing for hydrothermal reaction, and then placing in a nitrogen atmosphere for calcining to obtain an activated adsorbent; adding the activated adsorbent into a liquid stable chlorine dioxide aqueous solution, uniformly mixing, carrying out suction filtration, adding the stabilizer, uniformly mixing, grinding, adding the slow release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
Description
Technical Field
The invention relates to the technical field of disinfectants, in particular to an air disinfectant for livestock and poultry houses or vegetable greenhouses.
Background
The existing disinfectants mainly comprise: traditional halogen type disinfectants, phenolic disinfectants, alcohol type disinfectants, oxidant type disinfectants and surfactant type disinfectants. Wherein the traditional halogen disinfectant comprises the following components: 1. the chlorine preparation has strong bactericidal effect on bacteria, spores, viruses and fungi, but has short duration of drug effect, difficult long-term storage of the drugs, strong irritation and corrosiveness, and serious damage to the environment after long-term use; 2. the bromine preparation has almost the same bactericidal effect as the chlorine preparation, has good algae removal performance and high price; 3. iodine preparation belongs to a middle-effect disinfectant, and dilute solution thereof has low toxicity and no corrosiveness, but is unstable, needs to be prepared at present and is generally used for disinfecting hands and surgical skin.
The phenol disinfectant has low pH value, is easily influenced by alkaline organic substances, pollutes the environment, has pungent smell (irritability to a mucous membrane system of an organism), has smell detention property, has strong toxicity to people and livestock, is generally only used for disinfecting livestock and poultry empty houses, is not suitable for disinfecting during breeding, and has poor sterilizing effect.
Alcohol disinfectants are volatile, have little irritation to skin and mucous membrane, and are commonly used for disinfecting hands, skin and the like. The oxidant disinfectant is mainly used for environmental disinfection, such as disinfection of livestock and poultry houses, feeding troughs, tools, vehicles, floors and walls, has a good sterilization effect especially in a low-temperature environment, is selected as a good disinfectant of a refrigeration house, does not leave residual toxicity on articles after disinfection, but has unstable chemical properties, is ready to use, and has strong oxidizing property, so that skin mucosa and corrosive articles can be stimulated and damaged in high concentration, and the oxidant disinfectant can powerfully damage eyes, respiratory mucosa and environment of human and animals after long-term use.
The surfactant disinfectant has the characteristics of stability, small side effect and the like, but has no effect on non-membrane viruses (such as foot-and-mouth disease viruses and vesicular disease viruses), belongs to a low-efficiency disinfectant, and cannot be used for disinfection when epidemic diseases are epidemic.
Good ventilation must be maintained during intensive cultivation and planting, but air circulation improves the environment and increases the risk of entry of horizontally transmitted viruses. The existing disinfection products have the defects of short disinfection time, single type of killed bacteria and viruses, incapability of durably and effectively killing the bacteria and viruses and difficulty in controlling the biological prevention and control effect of viral pathogenic substances horizontally spread in the air.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides an air disinfectant for livestock and poultry houses or vegetable greenhouses.
The invention provides an air disinfectant for livestock and poultry houses or vegetable greenhouses, which comprises the following raw materials in parts by weight: 4-16 parts of montmorillonite, 8-10 parts of zeolite powder, 10-15 parts of an acid solution with the pH value of 2-3, 20-30 parts of a sucrose solution with the mass fraction of 30-40%, 20-30 parts of a liquid stable chlorine dioxide aqueous solution with the mass fraction of 3-5%, 4-8 parts of a stabilizer and 2-4 parts of a slow release agent.
Preferably, the liquid stable aqueous chlorine dioxide solution is prepared by the following process: adding sodium carbonate decahydrate into deionized water for dissolving, adding hydrogen peroxide solution under the condition of stirring in the dark, adding deionized water for stirring, and then filling chlorine dioxide to obtain the product.
Specifically, the liquid stable chlorine dioxide aqueous solution is prepared by adopting the following process: 286g of sodium carbonate decahydrate is added into 250mL of deionized water to be dissolved, 150mL of hydrogen peroxide solution with the mass fraction of 30% is added under the condition of stirring in the dark, 500mL of deionized water is added to be stirred for 10min, the pH value is 9-10, and then chlorine dioxide is filled in to obtain the sodium carbonate decahydrate.
Preferably, the acidic solution is one of hydrochloric acid, sulfuric acid, oxalic acid and citric acid.
Preferably, the stabilizer comprises: sodium pyrophosphate, magnesium sulfate and sodium silicate.
Preferably, the mass ratio of sodium pyrophosphate to magnesium sulfate to sodium silicate is 4-18: 8-12: 2-6.
Preferably, the sustained release agent is citric acid and/or ferric chloride.
Preferably, the sustained release agent is prepared by mixing citric acid and ferric trichloride according to a mass ratio of 1-2: 2.5-4.5.
Preferably, the blue absorbing amount of the air disinfectant for the livestock and poultry house or the vegetable greenhouse is more than or equal to 20g/100 g.
Preferably, the ammonia absorption amount of the air disinfectant for the livestock and poultry house or the vegetable greenhouse is more than or equal to 60mmol/100 g.
The preparation method of the air disinfectant for the livestock and poultry house or the vegetable greenhouse, provided by the invention, comprises the following steps of:
s1, adding montmorillonite and zeolite powder into an acid solution, soaking for 2-4h, taking out, washing until a washing solution is neutral, drying, placing in a sucrose solution, soaking for 10-12h, then sealing, and carrying out hydrothermal reaction for 2-4h at the temperature of 180-450 ℃ in a nitrogen atmosphere for calcination to obtain an activated adsorbent;
s2, adding the activated adsorbent into the liquid stable chlorine dioxide aqueous solution, uniformly mixing, carrying out suction filtration, adding the stabilizer, uniformly mixing, grinding, adding the slow release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
Preferably, in S1, the calcination time in the nitrogen atmosphere is 1-2 h.
Preferably, in S2, the grinding time is 1-2h, and the grinding pressure is 3-5 MPa.
In the invention S1, montmorillonite and zeolite powder are soaked in an acidic solution to remove impurities in the montmorillonite and zeolite powder and enlarge the pores, and then the montmorillonite and zeolite powder are soaked in a sucrose solution to ensure that sucrose molecules are fully adsorbed into the pores of the montmorillonite and zeolite powder, and then the sucrose molecules are converted into active carbon particles by adopting a hydrothermal reaction under a high-pressure and high-heat environment and are embedded in the pores of the montmorillonite and zeolite powder, so that the montmorillonite and zeolite powder have rich macroporous, mesoporous and microporous structures and are beneficial to adsorbing substances, and then the montmorillonite and zeolite powder is calcined in a nitrogen atmosphere to further remove the oxyhydrogen element in the montmorillonite and zeolite powder; s2, adding the activated adsorbent into the liquid stable chlorine dioxide aqueous solution, mixing to make the chlorine dioxide molecules fully enter the pores of the activated adsorbent, and then mutually matching the stabilizing agent and the slow-release agent to obtain light gray to light brown uniform powder, namely the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The invention has the following beneficial effects:
1. long-acting slow release and sustained action: under the forced saturation and water absorption states, the release of the oxidizing substances can be maintained for more than 7 days, so that harmful microorganisms in the environment can be continuously purified;
2. oxidizing harmful microorganisms, reducing diseases: can effectively oxidize harmful microorganisms such as bacteria, viruses, fungi and the like, and obviously reduce the occurrence of phenomena such as mammitis, hoof diseases, diarrhea and the like of animals; the magnesium salt contained in the umbilical cord has good astringency and anti-allergic effects, accelerates the drying and falling of the young umbilical cord, and is beneficial to the healing of windows such as castration, tail shearing and the like;
3. strong moisture absorption and drying environment: the breeding and propagation of harmful microorganisms in the environment are reduced, the sliding of animals to falling injury is reduced, and the protective effect on pregnancy, mammals and newborn young children is particularly good;
4. eliminating peculiar smell and purifying the environment: harmful gases such as ammonia gas, hydrogen sulfide and the like in the house are strongly adsorbed and degraded, are not easily influenced by organic matters and human factors, really realize effective environmental improvement, have excellent adsorption and ion exchange functions, can adsorb and fix heavy metal ions in the environment and reduce environmental pollution;
5. non-toxic, harmless, safe and environment-friendly: the invention adopts natural silicon-aluminum-hydrochloric acid compound, which is non-toxic, harmless, non-irritant, non-corrosive to equipment, and has no adverse effect on livestock, poultry and human bodies even if the compound is eaten or inhaled.
Detailed Description
The technical solution of the present invention will be described in detail below with reference to specific examples.
Example 1
A preparation method of an air disinfectant for livestock and poultry houses or vegetable greenhouses comprises the following steps:
s1, adding 4kg of montmorillonite and 10kg of zeolite powder into 10kg of hydrochloric acid with the pH value of 2-3, soaking for 4h, taking out and washing until the washing liquid is neutral, drying, soaking in 20kg of sucrose solution with the mass fraction of 40% for 10h, sealing to perform hydrothermal reaction for 4h at the hydrothermal reaction temperature of 180 ℃, and then calcining for 2h in nitrogen atmosphere at the calcining temperature of 400 ℃ to obtain an activated adsorbent;
s2, adding 30kg of liquid stable chlorine dioxide aqueous solution with the mass fraction of 3% into the activated adsorbent, uniformly mixing, carrying out suction filtration, adding 8kg of stabilizer, uniformly mixing, grinding at 3MPa for 2 hours, and then adding 2kg of slow-release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The stabilizer is prepared from sodium pyrophosphate, magnesium sulfate and sodium silicate according to a mass ratio of 2: 6: 1. The sustained release agent is prepared from citric acid and ferric trichloride according to the mass ratio of 2: 2.5.
Example 2
A preparation method of an air disinfectant for livestock and poultry houses or vegetable greenhouses comprises the following steps:
s1, adding 16kg of montmorillonite and 8kg of zeolite powder into 15kg of hydrochloric acid with the pH value of 2-3, soaking for 2h, taking out and washing until the washing liquid is neutral, drying, soaking in 30kg of sucrose solution with the mass fraction of 30% for 12h, sealing to perform hydrothermal reaction for 2h at the hydrothermal reaction temperature of 200 ℃, and then calcining in a nitrogen atmosphere for 1h at the calcining temperature of 450 ℃ to obtain an activated adsorbent;
s2, adding 20kg of liquid stable chlorine dioxide aqueous solution with the mass fraction of 5% into the activated adsorbent, uniformly mixing, carrying out suction filtration, adding 4kg of stabilizing agent, uniformly mixing, grinding at 5MPa for 1 hour, and then adding 4kg of slow-release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The stabilizer is prepared from sodium pyrophosphate, magnesium sulfate and sodium silicate according to a mass ratio of 9: 4: 3, and (3). The sustained release agent is prepared from citric acid and ferric trichloride according to a mass ratio of 1: 4.5.
Example 3
A preparation method of an air disinfectant for livestock and poultry houses or vegetable greenhouses comprises the following steps:
s1, adding 6kg of montmorillonite and 9.5kg of zeolite powder into 12kg of hydrochloric acid with the pH value of 2-3, soaking for 3.5h, taking out, washing until the washing liquid is neutral, drying, soaking in 22kg of sucrose solution with the mass fraction of 37% for 10.5h, sealing, carrying out hydrothermal reaction for 3.5h at the temperature of 185 ℃, and then calcining for 1.7h in nitrogen atmosphere at the temperature of 410 ℃ to obtain an activated adsorbent;
s2, adding 28kg of liquid stable chlorine dioxide aqueous solution with the mass fraction of 3.5% into the activated adsorbent, uniformly mixing, carrying out suction filtration, adding 7kg of stabilizer, uniformly mixing, grinding at 3.5Mpa for 1.7h, adding 2.5kg of slow-release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The stabilizer is prepared from sodium pyrophosphate, magnesium sulfate and sodium silicate according to a mass ratio of 6: 11: 3, and (3). The sustained release agent is prepared from citric acid and ferric trichloride according to the mass ratio of 1.7: 3, and (3).
Example 4
A preparation method of an air disinfectant for livestock and poultry houses or vegetable greenhouses comprises the following steps:
s1, adding 14kg of montmorillonite and 8.5kg of zeolite powder into 14kg of hydrochloric acid with the pH value of 2-3, soaking for 2.5h, taking out, washing until the washing liquid is neutral, drying, soaking in 28kg of sucrose solution with the mass fraction of 33% for 11.5h, sealing, carrying out hydrothermal reaction for 2.5h at the temperature of 195 ℃, and then calcining in a nitrogen atmosphere for 1.3h at the temperature of 430 ℃ to obtain an activated adsorbent;
s2, adding 22kg of liquid stable chlorine dioxide aqueous solution with the mass fraction of 4.5% into the activated adsorbent, uniformly mixing, carrying out suction filtration, adding 5kg of stabilizer, uniformly mixing, grinding at 4.5Mpa for 1.3h, adding 3.5kg of slow-release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The stabilizer is prepared from sodium pyrophosphate, magnesium sulfate and sodium silicate according to a mass ratio of 14: 9: 5. The sustained release agent is prepared from citric acid and ferric trichloride according to the mass ratio of 1.3: 4.
Example 5
A preparation method of an air disinfectant for livestock and poultry houses or vegetable greenhouses comprises the following steps:
s1, adding 10kg of montmorillonite and 9kg of zeolite powder into 13kg of hydrochloric acid with the pH value of 2-3, soaking for 3h, taking out and washing until the washing liquid is neutral, drying, soaking in 25kg of sucrose solution with the mass fraction of 35% for 11h, then sealing to carry out hydrothermal reaction for 3h, wherein the hydrothermal reaction temperature is 190 ℃, and then placing in a nitrogen atmosphere to calcine for 1.5h, and the calcining temperature is 420 ℃, so as to obtain the activated adsorbent;
s2, adding 25kg of liquid stable chlorine dioxide aqueous solution with the mass fraction of 4% into the activated adsorbent, uniformly mixing, carrying out suction filtration, adding 6kg of stabilizer, uniformly mixing, grinding at 4MPa for 1.5h, and then adding 3kg of slow-release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
The stabilizer is prepared from sodium pyrophosphate, magnesium sulfate and sodium silicate according to a mass ratio of 5: 5: 2. The sustained release agent is prepared from citric acid and ferric trichloride according to the mass ratio of 3: 7.
The air disinfectant obtained in the example 3-5 is subjected to an adsorption test, and the blue absorption amount is more than or equal to 20g/100g, and the ammonia absorption amount is more than or equal to 60mmol/100 g.
The invention can be continuously and continuously released for more than 7 days in use, and the low-concentration chlorine dioxide gas can rapidly kill pathogenic microorganisms in the air without dead angles, and the data shows that the low-concentration chlorine dioxide gas has no three-cause effect on people and animals (chlorine dioxide gas subacute inhalation toxicity research, by the disease control center of Guangdong province), has no residue, is an ideal air purification disinfectant, can realize continuous and uninterrupted disinfection, and improves the biological safety grade of planting/breeding farms to the maximum extent.
The specific use method is as follows:
the application scheme of the pig farm is as follows:
poultry farm application scheme:
the above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (10)
1. An air disinfectant for livestock and poultry houses or vegetable greenhouses is characterized by comprising the following raw materials in parts by weight: 4-16 parts of montmorillonite, 8-10 parts of zeolite powder, 10-15 parts of an acid solution with the pH value of 2-3, 20-30 parts of a sucrose solution with the mass fraction of 30-40%, 20-30 parts of a liquid stable chlorine dioxide aqueous solution with the mass fraction of 3-5%, 4-8 parts of a stabilizer and 2-4 parts of a slow release agent.
2. An air disinfectant for livestock and poultry houses or vegetable greenhouses according to claim 1, wherein the liquid stable aqueous solution of chlorine dioxide is prepared by the following process: adding sodium carbonate decahydrate into deionized water for dissolving, adding hydrogen peroxide solution under the condition of stirring in the dark, adding deionized water for stirring, and then filling chlorine dioxide to obtain the product.
3. The air disinfectant for livestock and poultry houses or vegetable greenhouses according to claim 1, wherein the acidic solution is one of hydrochloric acid, sulfuric acid, oxalic acid and citric acid.
4. An air disinfectant for livestock and poultry houses or vegetable greenhouses according to claim 1, wherein the stabilizer comprises: sodium pyrophosphate, magnesium sulfate and sodium silicate.
5. The air disinfectant for livestock and poultry houses or vegetable greenhouses as claimed in claim 3, wherein the mass ratio of sodium pyrophosphate to magnesium sulfate to sodium silicate is 4-18: 8-12: 2-6.
6. The air disinfectant for livestock and poultry houses or vegetable greenhouses as claimed in claim 1, wherein the slow release agent is citric acid and/or ferric chloride.
7. The air disinfectant for livestock and poultry houses or vegetable greenhouses as claimed in claim 6, wherein the slow release agent is prepared from citric acid and ferric trichloride in a mass ratio of 1-2: 2.5-4.5.
8. A method for preparing an air disinfectant for livestock and poultry houses or vegetable greenhouses as claimed in any of claims 1 to 7, comprising the steps of:
s1, adding montmorillonite and zeolite powder into an acid solution, soaking for 2-4h, taking out, washing until a washing solution is neutral, drying, placing in a sucrose solution, soaking for 10-12h, then sealing, and carrying out hydrothermal reaction for 2-4h at the temperature of 180-450 ℃ in a nitrogen atmosphere for calcination to obtain an activated adsorbent;
s2, adding the activated adsorbent into the liquid stable chlorine dioxide aqueous solution, uniformly mixing, carrying out suction filtration, adding the stabilizer, uniformly mixing, grinding, adding the slow release agent, and mixing to obtain the air disinfectant for livestock and poultry houses or vegetable greenhouses.
9. The method for preparing an air disinfectant for livestock and poultry houses or vegetable greenhouses according to claim 8, wherein the calcination time in the nitrogen atmosphere in S1 is 1-2 h.
10. The method for preparing an air disinfectant for livestock and poultry houses or vegetable greenhouses according to claim 8, wherein in S2, the grinding time is 1-2h, and the grinding pressure is 3-5 MPa.
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| CN202110001294.XA CN112715572A (en) | 2021-01-04 | 2021-01-04 | Air disinfectant for livestock and poultry houses or vegetable greenhouses |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1293540A (en) * | 1999-02-26 | 2001-05-02 | 崔永成 | Weak acidic disinfectant |
| CN1454837A (en) * | 2003-04-22 | 2003-11-12 | 贵州大学 | Method of preparing stable chloride dioxide |
| WO2007138058A1 (en) * | 2006-05-30 | 2007-12-06 | Solvay (Société Anonyme) | Product and process for treating water bodies, sediments and soils |
| CN105080615A (en) * | 2015-07-29 | 2015-11-25 | 安徽科浦环保科技有限公司 | Adsorption catalyst capable of removing formaldehyde quickly and preparing method thereof |
| CN105536825A (en) * | 2016-01-09 | 2016-05-04 | 深圳市康风环境科技发展有限公司 | Catalyst for air sterilization, disinfection and purification and preparation method thereof |
| CN106861607A (en) * | 2017-03-17 | 2017-06-20 | 武汉理工大学 | A kind of preparation method of the modified carbon/montmorillonite Composite sorbing material of organic-inorganic |
| CN107467065A (en) * | 2017-08-23 | 2017-12-15 | 广西大学 | A kind of preparation method of long-acting slow release type solid chlorine dioxide air purifying preparation |
-
2021
- 2021-01-04 CN CN202110001294.XA patent/CN112715572A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1293540A (en) * | 1999-02-26 | 2001-05-02 | 崔永成 | Weak acidic disinfectant |
| CN1454837A (en) * | 2003-04-22 | 2003-11-12 | 贵州大学 | Method of preparing stable chloride dioxide |
| WO2007138058A1 (en) * | 2006-05-30 | 2007-12-06 | Solvay (Société Anonyme) | Product and process for treating water bodies, sediments and soils |
| CN105080615A (en) * | 2015-07-29 | 2015-11-25 | 安徽科浦环保科技有限公司 | Adsorption catalyst capable of removing formaldehyde quickly and preparing method thereof |
| CN105536825A (en) * | 2016-01-09 | 2016-05-04 | 深圳市康风环境科技发展有限公司 | Catalyst for air sterilization, disinfection and purification and preparation method thereof |
| CN106861607A (en) * | 2017-03-17 | 2017-06-20 | 武汉理工大学 | A kind of preparation method of the modified carbon/montmorillonite Composite sorbing material of organic-inorganic |
| CN107467065A (en) * | 2017-08-23 | 2017-12-15 | 广西大学 | A kind of preparation method of long-acting slow release type solid chlorine dioxide air purifying preparation |
Non-Patent Citations (2)
| Title |
|---|
| 郑书忠主编: "《水处理药剂及其应用》", 31 March 2003, 中国石化出版社 * |
| 闫碧莹: "天然蒙脱石钠化工艺研究", 《质量与市场》 * |
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