CN112675087A - Plant antibacterial and bacteriostatic scalp care composition and preparation method and application thereof - Google Patents

Plant antibacterial and bacteriostatic scalp care composition and preparation method and application thereof Download PDF

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Publication number
CN112675087A
CN112675087A CN202011637585.XA CN202011637585A CN112675087A CN 112675087 A CN112675087 A CN 112675087A CN 202011637585 A CN202011637585 A CN 202011637585A CN 112675087 A CN112675087 A CN 112675087A
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bacteriostatic
parts
extract
care composition
scalp care
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周勤
黄晓颖
林诗宜
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Zhaoqing Dicai Daily Chemical Science And Technology Co ltd
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Zhaoqing Dicai Daily Chemical Science And Technology Co ltd
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Abstract

The invention relates to a plant antibacterial and bacteriostatic scalp care composition and a preparation method and application thereof. The plant antibacterial and bacteriostatic scalp care composition comprises an extract of milfoil, an extract of pomegranate bark and an extract of magnolia bark. The plant antibacterial and bacteriostatic scalp care composition provided by the invention has good scalp care and bacteriostatic effects through the synergistic cooperation of the three plant components, is harmless to the scalp, and can avoid negative effects on the environment.

Description

Plant antibacterial and bacteriostatic scalp care composition and preparation method and application thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a plant antibacterial and bacteriostatic scalp care composition, and a preparation method and application thereof.
Background
Compared with human beings, microorganisms are the original residents on the earth, exist in the atmosphere, water, soil and various extreme environments, and are also planted on the skin and the cavity surface of the human body in a large quantity. Humans are harmoniously present with microorganisms and humans are not able or suitable to survive in a completely sterile environment. Pathogenic microorganisms require a certain virulence, quantity and a proper invasive route to cause infection in the body. The antibacterial function is to reduce the breeding and propagation of pathogenic microorganisms on the surface of the article to the greatest extent, so that the quantity of the pathogenic microorganisms does not cause body infection, and the surface of the article does not become an infection medium.
Along with the development of society, people pay more and more attention to health, the antibacterial consciousness is also strengthened continuously, products with antibacterial and bacteriostatic functions are more and more concerned, particularly various daily necessities closely related to the life of people, but many antibacterial and bacteriostatic agents are on the market, the antibacterial agents are generally divided into inorganic antibacterial agents, organic antibacterial agents and natural antibacterial agents, and the antibacterial agents of daily necessities with antibacterial functions sold in the market at present are generally inorganic antibacterial agents and organic antibacterial agents. The inorganic antibacterial agent is basically metal ions, and metals such as mercury, cadmium, lead and the like have antibacterial capacity but are harmful to human bodies; copper, nickel, lead and other ions have colors, which affect the appearance of the product, and zinc has certain antibacterial property, but the antibacterial strength of zinc is only 1/1000 of silver ions. The main varieties of organic antibacterial agents are vanillin or ethyl vanillin compounds, but the safety of organic antibacterial agents is still under study. The use of natural plant antimicrobial ingredients in combination with personal care products has a beneficial factor in both consumer health and acceptability. The scalp is the thinnest skin on the surface of a human body, sebum secretion is vigorous, various bacteria reproduction is increased, and the organic and inorganic antibacterial bacteriostats on the market are harmful to the scalp to a greater or lesser extent, so that the antibacterial and bacteriostatic capability of the scalp needs to be improved by the natural harmless antibacterial bacteriostat. Patent CN108403541A discloses a plant-derived bacteriostatic shampoo with bacteriostatic effect, but the research on this aspect is still less.
Therefore, the development of a plant type bacteriostatic care product with a good bacteriostatic effect and no harm has important research significance and application prospect.
Disclosure of Invention
The invention aims to overcome the defect or deficiency that organic and inorganic antibacterial bacteriostatic agents have certain damage to scalp in the prior art, and provides a plant antibacterial and bacteriostatic scalp care composition. The plant antibacterial and bacteriostatic scalp care composition provided by the invention has good scalp care and bacteriostatic effects through the synergistic cooperation of the three plant components, is harmless to the scalp, and can avoid negative effects on the environment.
The invention also aims to provide a preparation method of the plant antibacterial and bacteriostatic scalp care composition.
The invention also aims to provide application of the plant antibacterial and bacteriostatic scalp care composition in preparing scalp care products.
The invention also aims to provide a shampoo product.
In order to achieve the purpose, the invention adopts the following technical scheme:
a plant antibacterial and bacteriostatic scalp care composition comprises the following components in parts by weight:
0.01 to 5.0 parts of an extract of milfoil,
0.01 to 10.0 parts of pomegranate bark extract,
0.01-10.0 parts of magnolia bark extract.
Achillea millefolium (also called yarrow, millefolium, etc.) is the whole plant of Achillea millefolium or Achillea millefolium of Compositae. The flower and leaf are rich in flavonoid glycoside compounds such as apigenin-7-D-glucoside and luteolin-7-D-glucoside. The leaves also contain milfoil, podophyllol and north water soda. The flower contains myristic acid, palmitic acid, hexacosanoic acid, linoleic acid, oleic acid, hexacosanol, triacontane, sitosterol and stigmasterol; the leaves contain polyacetylene compounds such as tridecane 1,3, 5-triene-7, 9, 11-triyne, 3- (2-thiocyclopenta) propynal, etc., and the lactone compounds include terpenoids such as milfoil lactone, deacetyl matricin, etc. Research shows that the milfoil extract has antibacterial property and has inhibitory effect on Staphylococcus aureus, Pseudomonas aeruginosa, Escherichia coli, Bacillus subtilis, etc. Has effects in promoting proliferation of epidermal keratinocyte, restoring elasticity of skin fibrous tissue, balancing skin, and promoting metabolism of skin cells.
The extract of yarrow is commercially available.
Pomegranate is Laurentia punica Praeparata, which is Laurentia pungens of Laurentia in Punicaceae. Pomegranate rind contains rich substances, and when contacting with mucosa, wound surface, etc., it can precipitate or coagulate local protein to form compact protective layer on the surface, which is helpful for healing local wound surface or protecting local part from stimulation. Comparing the in-vitro bactericidal power of 400 traditional Chinese medicines on typhoid bacillus, vibrio cholerae, staphylococcus and the like, the pomegranate bark has the strongest effect of inhibiting the typhoid bacillus. In addition, in vitro experiments prove that the bacillus subtilis has an inhibiting effect on various bacteria such as tubercle bacillus, escherichia coli, proteus vulgaris, pseudomonas aeruginosa and the like.
The pomegranate rind extract is commercially available.
Cortex Magnolia officinalis contains lignan compounds such as magnolol (magnolol), honokiol (honokiol), honokiol (obovatol), etc. Magnolol has remarkable antibacterial activity on gram-positive bacteria, acid-resistant bacteria and filamentous fungi, has more remarkable antibacterial effect on streptococcus mutans, has strongest inhibition effect on staphylococcus, also has special and lasting muscle relaxation effect and strong antibacterial effect, and can inhibit platelet aggregation. Is mainly used as antibacterial and antifungal drugs in clinic. The honokiol has broad-spectrum antibacterial effect, and researches show that the honokiol has strong antibacterial activity on gram-positive bacteria and gram-negative bacteria, has stable antibacterial property, and is not easy to be damaged by heat, acid and alkali. For example, Escherichia coli (Escherichia coli), Staphylococcus aureus (Staphylococcus aureus), Candida albicans (Candida albicans), Aspergillus brazilis (Aspergillus brazilians), and the like.
Magnolia bark extract is commercially available.
The plant antibacterial and bacteriostatic scalp care composition provided by the invention has good scalp care and bacteriostatic effects through the synergistic cooperation of the three plant components, is harmless to the scalp, and can avoid negative effects on the environment.
Preferably, the plant antibacterial and bacteriostatic scalp care composition comprises the following components in parts by weight:
0.5 to 2.0 parts of an extract of milfoil,
1.0-5.0 parts of pomegranate bark extract,
2.0-7.0 parts of magnolia bark extract.
More preferably, the plant antibacterial and bacteriostatic scalp care composition comprises the following components in parts by weight:
1.0 part of an extract of milfoil,
3.5 parts of an extract of the pomegranate bark,
5.5 parts of magnolia bark extract.
The preparation method of the plant antibacterial and bacteriostatic scalp care composition comprises the following steps: mixing the milfoil extract, the pomegranate bark extract and the magnolia bark extract to obtain the plant antibacterial and bacteriostatic scalp care composition.
The application method of the plant antibacterial and bacteriostatic scalp care composition comprises the following steps: the plant antibacterial and bacteriostatic scalp care composition (or the diluent thereof) can be directly sprayed on the scalp in a small amount and can be absorbed by the scalp after being massaged for a moment; the plant antibacterial and bacteriostatic scalp care composition can also be directly added into a hair washing and caring product for daily hair washing and caring.
The application of the plant antibacterial and bacteriostatic scalp care composition in preparing scalp care products is also within the protection scope of the invention.
Preferably, the addition amount of the plant antibacterial and bacteriostatic scalp care composition in the hair washing and caring product is 1.0-30.0%.
A shampoo product comprises the following components in parts by mass:
Figure BDA0002877063050000041
preferably, the shampoo product comprises the following components in parts by mass:
Figure DEST_PATH_IMAGE001
preferably, the anionic surfactant is one or more of ammonium laureth sulfate, sodium laureth sulfate, ammonium laureth sulfate or sodium methyl cocoyl taurate.
Preferably, the amphoteric surfactant is one or more of cocamidopropyl betaine, cocamidopropyl hydroxysultaine, sodium lauroamphoacetate or sodium cocamidopropionate.
Preferably, the hair conditioner is one or more of polydimethylsiloxane, amino-terminated polydimethylsiloxane or dimethiconol.
Preferably, the thickener is one or more of sodium chloride, cocamide MEA, cocamide methyl MEA or cocamide DEA.
Preferably, the pearling agent is one or two of ethylene glycol distearate or ethylene glycol stearate.
Preferably, the cationic conditioner is one or more of guar hydroxypropyl trimethyl ammonium chloride, polyquaternium-10, polyquaternium-7, polyquaternium-80 or dipalmitoyloxyethyl hydroxyethyl methyl ammonium methyl sulfate.
Preferably, the chelating agent is one or more of disodium EDTA, tetrasodium glutamate diacetate, or hydroxyethyldiphosphonic acid.
Preferably, the pH value regulator is one or more of citric acid, sodium citrate or sodium hydroxide.
Preferably, the essence is one or more of orange flower essence, rose flower essence or juicy peach essence.
Specifically, the shampoo product comprises the following components in parts by mass:
Figure BDA0002877063050000051
compared with the prior art, the invention has the following beneficial effects:
the plant antibacterial and bacteriostatic scalp care composition provided by the invention has good scalp care and bacteriostatic effects through the synergistic cooperation of the three plant components, is harmless to the scalp, and can avoid negative effects on the environment.
Detailed Description
The invention is further illustrated by the following examples. These examples are intended to illustrate the invention and are not intended to limit the scope of the invention. Experimental procedures without specific conditions noted in the examples below, generally according to conditions conventional in the art or as suggested by the manufacturer; the raw materials, reagents and the like used are, unless otherwise specified, those commercially available from the conventional markets and the like. Any insubstantial changes and substitutions made by those skilled in the art based on the present invention are intended to be covered by the claims.
The raw materials selected in the examples and comparative examples of the invention are as follows:
yarrow extract: yarrow extract, walnuts, wayotis, inc;
pomegranate rind extract: gan zhou baizhentang biotechnology limited, pomegranate rind extract;
cortex Magnolia officinalis extract: zhenghe (Guangzhou) Biotechnology Ltd, Magnolia officinalis extract.
Examples 1 to 9
This example provides a series of shampoo compositions having the formula shown in Table 1.
Table 1 formulas (mass fraction%) of shampoo products provided in examples 1 to 5
Figure BDA0002877063050000061
Table 2 formula (mass fraction%) of shampoo products provided in examples 1, 6 to 9
Figure BDA0002877063050000062
The plant antibacterial and bacteriostatic scalp care composition 1# is prepared by the following method: mixing Achillea millefolium L.extract 1 part, pericarpium Granati extract 3.5 parts and cortex Magnolia officinalis extract 5.5 parts.
The plant antibacterial and bacteriostatic scalp care composition No. 2 is prepared by the following method: mixing 0.5 part of milfoil extract, 5.0 parts of pericarpium Granati extract and 2.0 parts of cortex Magnolia officinalis extract.
The plant antibacterial and bacteriostatic scalp care composition No. 3 is prepared by the following method: mixing 2.0 parts of milfoil extract, 1.0 part of pericarpium Granati extract and 7.0 parts of cortex Magnolia officinalis extract.
The plant antibacterial and bacteriostatic scalp care composition No. 4 is prepared by the following method: mixing 0.01 part of milfoil extract, 10.0 parts of pericarpium Granati extract and 0.01 part of cortex Magnolia officinalis extract.
The plant antibacterial and bacteriostatic scalp care composition No. 5 is prepared by the following method: mixing 5.0 parts of milfoil extract, 0.01 part of pomegranate bark extract and 10.0 parts of cortex Magnolia officinalis bark extract.
The plant antibacterial and bacteriostatic scalp care composition 1-3 is similar to the preparation method of the plant antibacterial and bacteriostatic scalp care composition 1#, and the difference is that: the plant antibacterial and bacteriostatic scalp care composition 1# comprises the yarrow extract, the pomegranate bark extract and the magnolia bark extract which are sequentially replaced by the same amount of deionized water, and the composition 1-3 is obtained.
Comparative examples 1 to 4
This comparative example provides a series of shampoo products having the formula shown in table 3.
Table 3 shampoo products provided in comparative examples 1 to 3 (% by mass)
Components Comparative example 1 Comparative example 2 Comparative example 3
Composition 1 15 / /
Composition 2 / 15 /
Composition 3 / / 15
The rest components Balance of Balance of Balance of
In each of the examples and comparative examples, the remaining components included: 11.0% of ammonium laureth sulfate, 8.0% of ammonium laureth sulfate, 5.0% of cocamidopropyl betaine, 4.0% of polydimethylsiloxane, 1.2% of cocamide MEA, 1.5% of ethylene glycol distearate, 0.2% of guar hydroxypropyltrimonium chloride, 100.2% of polyquaternium, 0.3% of sodium chloride, 0.1% of disodium EDTA, 0.05% of citric acid, 0.5% of essence (orange flower fragrance), and the balance of water, based on the total amount of the formulations of the examples and comparative examples.
Comparative example 4 is a difen hair treatment shampoo.
The preparation method of the shampoo products of the examples and comparative examples 1 to 3 is as follows: heating water to 80-85 ℃ in a water bath kettle, keeping the temperature constant, adding guar hydroxypropyl trimethyl ammonium chloride, polyquaternary ammonium salt-10, EDTA disodium and citric acid which are dispersed by water in advance, then adding laureth ammonium sulfate, lauryl ammonium sulfate and cocamidopropyl betaine, adding cocamide MEA and ethylene glycol distearate after the guar hydroxypropyl trimethyl ammonium chloride, polyquaternary ammonium salt-10, EDTA disodium and citric acid are completely dissolved, keeping the temperature constant for 20 minutes, cooling to below 45 ℃, adding the rest polydimethylsiloxane, sodium chloride and essence, finally adding the plant antibacterial scalp care composition (or composition), and continuously stirring for 15 minutes.
Performance testing
The shampoo products of the examples and the comparative examples are tested for bacteriostatic effect according to GB 15979-2002 bacteriostatic test.
Table 4 shows the test results.
TABLE 4 results of Performance test of each example and comparative example
Figure BDA0002877063050000081
As can be seen from table 4, the shampoo products of the embodiments of the present invention all have a good bacteriostatic effect, and when the mass fraction of the plant antibacterial scalp care composition in the shampoo is 15.0% (example 1), the bacteriostatic value reaches an ideal value, so as to achieve an ideal antibacterial and bacteriostatic effect, while the composition selected in the shampoo products lacks a certain component, so that the synergistic effect is weak (for example, comparative examples 1 to 3), and the products without the added bacteriostatic component in the market (for example, comparative example 4) have a poor bacteriostatic effect. The components of the plant antibacterial and bacteriostatic scalp care composition 1# have optimal mutual synergistic effect, so that the scalp is healthier, and the optimal ideal state of antibacterial and bacteriostatic is achieved.
It will be appreciated by those of ordinary skill in the art that the examples provided herein are intended to assist the reader in understanding the principles of the invention and are to be construed as being without limitation to such specifically recited examples and embodiments. Those skilled in the art can make various other specific changes and combinations based on the teachings of the present invention without departing from the spirit of the invention, and these changes and combinations are within the scope of the invention.

Claims (10)

1. A plant antibacterial and bacteriostatic scalp care composition is characterized by comprising the following components in parts by weight:
0.01 to 5.0 parts of an extract of milfoil,
0.01 to 10.0 parts of pomegranate bark extract,
0.01-10.0 parts of magnolia bark extract.
2. The plant antibacterial and bacteriostatic scalp care composition according to claim 1, which is characterized by comprising the following components in parts by weight:
0.5 to 2.0 parts of an extract of milfoil,
1.0-5.0 parts of pomegranate bark extract,
2.0-7.0 parts of magnolia bark extract.
3. The plant antibacterial and bacteriostatic scalp care composition according to claim 2, which is characterized by comprising the following components in parts by weight:
1.0 part of an extract of milfoil,
3.5 parts of an extract of the pomegranate bark,
5.5 parts of magnolia bark extract.
4. A method for preparing a plant antibacterial and bacteriostatic scalp care composition according to any one of claims 1 to 3, which comprises the following steps: mixing the milfoil extract, the pomegranate bark extract and the magnolia bark extract to obtain the plant antibacterial and bacteriostatic scalp care composition.
5. Use of the plant antibacterial and bacteriostatic scalp care composition according to any one of claims 1 to 3 in the preparation of hair washing and caring products.
6. The application of claim 5, wherein the plant antibacterial and bacteriostatic scalp care composition is added in the cosmetic or the washing care product in an amount of 1.0-30.0%.
7. A shampoo product is characterized by comprising the following components in parts by mass:
Figure FDA0002877063040000011
Figure FDA0002877063040000021
the balance of water.
8. The shampoo product according to claim 7, characterized by comprising the following components in parts by mass:
Figure FDA0002877063040000022
the balance of water.
9. The shampoo product of claim 7, wherein the anionic surfactant is one or more of ammonium laureth sulfate, sodium laureth sulfate, ammonium laureth sulfate, and sodium methylcocoyl taurate;
the amphoteric surfactant is one or more of cocamidopropyl betaine, cocamidopropyl hydroxysultaine, sodium lauroamphoacetate or sodium cocamidopropionate;
the hair conditioner is one or more of polydimethylsiloxane, amino-terminated polydimethylsiloxane or dimethiconol;
the thickening agent is one or more of sodium chloride, cocamide MEA, cocamide methyl MEA or cocamide DEA;
the pearling agent is one or two of ethylene glycol distearate or ethylene glycol stearate;
the cationic conditioner is one or more of guar hydroxypropyl trimethyl ammonium chloride, polyquaternium-10, polyquaternium-7, polyquaternium-80 or dipalmitoyloxyethyl hydroxyethyl methyl ammonium methyl sulfate.
10. The shampoo product of claim 7 wherein the chelating agent is one or more of disodium EDTA, tetrasodium glutamate diacetate, or ethylene diphosphate;
the pH value regulator is one or more of citric acid, sodium citrate or sodium hydroxide;
the essence is one or more of orange flower essence, rose flower essence or juicy peach essence.
CN202011637585.XA 2020-12-31 2020-12-31 Plant antibacterial and bacteriostatic scalp care composition and preparation method and application thereof Pending CN112675087A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102743363A (en) * 2011-04-20 2012-10-24 上海莱博生物科技有限公司 Product for treating skin diseases caused by Malassezia
CN109646352A (en) * 2019-01-10 2019-04-19 澳宝化妆品（惠州）有限公司 A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract
CN109846771A (en) * 2018-07-05 2019-06-07 上海珈凯生物科技有限公司 A kind of composition of plant extracts and preparation method thereof with acne-removing
CN110522665A (en) * 2019-09-17 2019-12-03 上海珈凯生物科技有限公司 A kind of scalp care compositions and its preparation and the application in scalp care product
CN112043641A (en) * 2020-09-24 2020-12-08 广州美物生物科技有限公司 Facial mask and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102743363A (en) * 2011-04-20 2012-10-24 上海莱博生物科技有限公司 Product for treating skin diseases caused by Malassezia
CN109846771A (en) * 2018-07-05 2019-06-07 上海珈凯生物科技有限公司 A kind of composition of plant extracts and preparation method thereof with acne-removing
CN109646352A (en) * 2019-01-10 2019-04-19 澳宝化妆品（惠州）有限公司 A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract
CN110522665A (en) * 2019-09-17 2019-12-03 上海珈凯生物科技有限公司 A kind of scalp care compositions and its preparation and the application in scalp care product
CN112043641A (en) * 2020-09-24 2020-12-08 广州美物生物科技有限公司 Facial mask and preparation method thereof

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Application publication date: 20210420