CN112656699A - Cosmetic repairing water and preparation method thereof - Google Patents

Cosmetic repairing water and preparation method thereof Download PDF

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CN112656699A
CN112656699A CN201910975397.9A CN201910975397A CN112656699A CN 112656699 A CN112656699 A CN 112656699A CN 201910975397 A CN201910975397 A CN 201910975397A CN 112656699 A CN112656699 A CN 112656699A
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extract
water
solution
skin
supernatant
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康山峰
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Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to a cosmetic repairing water and a preparation method thereof, wherein the repairing water comprises the following components in percentage by weight: 74% of water, 3.1-3.7% of glycerin, 1.2-1.8% of propylene glycol, 1.85-2.35% of cactus extract, 0.8-1.3% of ethylhexyl glycerin, 1.75-2.3% of witch hazel extract, 2.9-3.2% of safflower extract, 0.7-1.2% of dipotassium glycyrrhizinate, 4.8-5.25% of allantoin, 1.75-2.15% of sodium hyaluronate, 2.85-3.25% of lavender oil and 1.9-2.1% of disodium EDTA. The invention has remarkable curative effects of repairing deep skin and sterilizing, has treatment effect on contact dermatitis, seborrheic dermatitis, pruritus and neurodermatitis, deeply supplements various nutrient components of the skin and enhances the natural water retention capacity of the skin.

Description

Cosmetic repairing water and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to a cosmetic repairing water and a preparation method thereof.
Background
The cactus is light in taste and cold in nature, has the effects of promoting qi and blood circulation, clearing away heat and toxic materials, relieving swelling and pain, invigorating spleen, relieving diarrhea, tranquilizing mind and promoting urination, and can be orally taken and externally used for treating various diseases. The radix et caulis Opuntiae Dillenii is mainly used for treating furuncle and toxic swelling, and can also be used for treating stomachache, abdominal pain due to mass, acute dysentery, intestinal hemorrhoid, hemorrhage, asthma, etc., and the radix et caulis Opuntiae Dillenii extract is the extract of root and stem of Opuntia Dillenii of Cactaceae, and has effects of reducing weight, lowering blood sugar, inhibiting bacteria, and relieving inflammation.
With the aging, the skin condition gradually becomes loose and the appearance of color spots is observed during the division of cell tissues in the human skin, and according to analysis, the appearance of the skin loose and wrinkles is mainly reflected in water shortage, and the color spots and skin dull luster are mainly reflected in the loss of self-repairing ability of cells or the reduction of self-repairing ability. At present, modern young women are relatively poor in skin state due to staying up at night and various bad tastes, pockmarks and color spots on the surface of the modern young women are relatively obvious, and the traditional skin repair product is a big vacancy.
Disclosure of Invention
The invention provides a cosmetic repair water and a preparation method thereof based on the technical problems that the skin cannot be effectively repaired and the water and moisture can not be supplemented.
The invention provides a technical scheme of cosmetic repairing water, which comprises the following components in percentage by weight: 74% of water, 3.1-3.7% of glycerin, 1.2-1.8% of propylene glycol, 1.85-2.35% of cactus extract, 0.8-1.3% of ethylhexyl glycerin, 1.75-2.3% of witch hazel extract, 2.9-3.2% of safflower extract, 0.7-1.2% of dipotassium glycyrrhizinate, 4.8-5.25% of allantoin, 1.75-2.15% of sodium hyaluronate, 2.85-3.25% of lavender oil and 1.9-2.1% of disodium EDTA.
Preferably, the 74% water may be one of distilled water or purified water, and the standards of the components in the 74% water are as follows: the content of ignition slag is less than or equal to 0.01 percent, the content of manganese is less than or equal to 0.00001 percent, the content of iron is less than or equal to 0.0004 percent, the content of chlorine is less than or equal to 0.0005 percent, the content of reduced potassium permanganate substances is less than or equal to 0.0002 percent, the content of nitric acid and nitrite is less than or equal to 0.0003 percent, and the content of ammonium is less.
Preferably, the glycerin may be replaced with one of glycerin, olive oil or aloe vera gel, wherein the content of the glycerin is constant by weight percentage.
Another technical problem to be solved by the present invention is to provide a method for preparing a cosmetic repair water, comprising the following steps:
step one, cleaning and disinfecting. And step two, heating and mixing. And step three, cooling and dissolving. And step four, cooling and stirring. And step five, preserving heat and dissolving. And step six, discharging. And seventhly, performing quality sampling inspection. And step eight, filling and packaging.
In step one, the production equipment and the tools are first cleaned and sterilized to make the production equipment and the operation space in a sterile state.
In the second step, water, glycerol and propylene glycol are sequentially added into a clean container, then the temperature is slowly increased to 80-85 ℃, the temperature increase time is controlled within 30min, and after the temperature increase time is controlled to be within 5min, mechanical stirring is adopted for 30min to be in a uniform state.
In the third step, cactus extract, ethylhexyl glycerol, Hamamelis virginiana extract and Carthami flos extract are sequentially added into a container, and then cooled to 60-70 deg.C, and stirred for 30min to dissolve.
In the fourth step, when the temperature in the container is reduced to 55 ℃, the dipotassium glycyrrhizinate, the allantoin, the sodium hyaluronate and the lavender oil are added, and the mixture is stirred for 45min until the mixture is uniformly mixed.
In the fifth step, when the temperature is reduced to 50 ℃, the disodium EDTA is added, and the mixture is stirred for 30 minutes until the mixture is uniformly mixed.
And in the sixth step, naturally cooling to the room temperature state, and then discharging.
And seventhly, sampling and inspecting the product, and entering the next process after the quality detection data meet the standard.
In step eight, the product is subjected to canning and packaging operations and then transferred to a finished product warehouse for storage.
The beneficial effects of the invention are as follows:
1. the repair water provided by the invention has remarkable curative effects of repairing deep skin and sterilizing, has a treatment effect on contact dermatitis, seborrheic dermatitis, pruritus and neurodermatitis, deeply supplements various nutrient components of the skin, makes moisture stay in the skin for a long time, enhances the natural water retention capacity of the skin, keeps the skin in a tender state for a long time, contains efficient whitening and moisturizing factors, locks the moisture, maintains the health and whitening of the skin, prevents blackheads and acnes, and has good effects of quickly presenting fine, smooth and compact states of the skin.
2. The cactus extract has obvious growth promoting effect on human skin fibroblasts cultured in vitro, the effect is superior to AHA, the anti-aging effect on human fibroblasts is achieved, the aging process of cells can be delayed, the cactus extract provides continuous and lasting moisture for the skin for 24 hours, the cactus extract has super-strong moisture-retaining components, moisture is retained in the skin for a long time, the natural moisture-retaining capacity of the skin is enhanced, the skin is kept in a moisture-tender state for a long time, and meanwhile, the cactus extract contains efficient whitening and moisture-retaining factors, locks the moisture, maintains the health and whitening of the skin, is very suitable for being applied to beauty cosmetics, and has good application value and prospect.
3. The safflower extract has the functions of promoting blood circulation, resisting inflammation, resisting oxidation and the like, plays the effects of whitening, preventing sunburn and resisting aging by improving skin blood circulation, promoting skin metabolism, eliminating free radicals, inhibiting melanin deposition, accelerating freckle removal and decoloration, absorbing ultraviolet rays and the like, has the treatment effect on contact dermatitis, seborrheic dermatitis, pruritus and neurodermatitis, and deeply supplements various nutritional ingredients of skin, thereby having good repairing effect.
Detailed Description
The following will clearly and completely describe the technical solutions in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments.
Example one
The cosmetic repairing water comprises the following components in percentage by weight: 74% of water, 3.1-3.7% of glycerin, 1.2-1.8% of propylene glycol, 1.85-2.35% of cactus extract, 0.8-1.3% of ethylhexyl glycerin, 1.75-2.3% of witch hazel extract, 2.9-3.2% of safflower extract, 0.7-1.2% of dipotassium glycyrrhizinate, 4.8-5.25% of allantoin, 1.75-2.15% of sodium hyaluronate, 2.85-3.25% of lavender oil and 1.9-2.1% of disodium EDTA.
The 74% water may be one of distilled water or purified water, and the respective criteria for the composition in the 74% water are: the content of ignition slag is less than or equal to 0.01 percent, the content of manganese is less than or equal to 0.00001 percent, the content of iron is less than or equal to 0.0004 percent, the content of chlorine is less than or equal to 0.0005 percent, the content of reduced potassium permanganate substances is less than or equal to 0.0002 percent, the content of nitric acid and nitrite is less than or equal to 0.0003 percent, and the content of ammonium is less.
The glycerol can be replaced by one of glycerol, olive oil or aloe gel, wherein the content of the glycerol in percentage by weight is unchanged.
The preparation process of the cactus extract mainly comprises the following steps:
firstly, taking 500g of new cactus, removing thorns, washing and chopping, adding 400mL of 95% ethanol solution, fully shaking, leaching the solution for 40h, taking supernatant, storing the supernatant in a refrigerator at 5 ℃, and storing residual bottom residues for later use.
And secondly, adding 250mL of 95% ethanol solution into the bottom slag, fully oscillating, and leaching the solution for 15 hours.
And thirdly, taking the supernatant, combining the supernatant with the first supernatant, carrying out suction filtration, putting the filtrate into a separating funnel, adding 100mL of petroleum ether, fully shaking, standing for 10min, taking the lower layer liquid, then carrying out reduced pressure concentration, carrying out freeze drying on the concentrated liquid, and then obtaining the cactus extract.
The preparation process of the Hamamelis virginiana extract mainly comprises the following steps:
firstly, weighing 500 parts of Hamamelis virginiana raw material, crushing and grinding the Hamamelis virginiana raw material into powder by using a ball mill, and screening the powder by using a 800-mesh screen for later use.
And secondly, putting the screened raw materials into an extractor, adding 500 parts of distilled water into the extractor, uniformly stirring, adding boric acid, extracting for 1-2h at 60-70 ℃, filtering by adopting a 80-mesh screen, and taking supernatant.
Thirdly, adding citric acid into the supernatant to adjust the pH value to be between 4 and 5.5, then extracting at room temperature for 20 to 24 hours, and then adding hydrochloric acid to adjust the pH value to be between 3.5 and 3.8.
Fourthly, heating the solution in water bath to 75-85 ℃, then preserving the heat for 30-35min, filtering by adopting a 50-mesh screen to obtain a precipitate, then adding 65-70% ethanol solution by volume fraction into the precipitate, and carrying out ultrasonic extraction for 2h at 70-75 ℃.
Fifthly, after the solution is cooled to the room temperature state, filtering the solution by adopting a 50-mesh screen to obtain filter residue and supernatant, and concentrating and drying the supernatant to obtain the powdery hamamelis virginiana extract.
The preparation process of the safflower extract mainly comprises the following steps:
firstly, taking 500g of high-quality safflower raw material, cleaning, drying, putting into a ball mill after drying, grinding into powder, and screening by adopting a 80-mesh screen.
And secondly, transferring the screened safflower powder into an extractor, adding 4-6 times of ethanol water, heating and refluxing for extraction for 40-50min at the constant temperature of 45 ℃ to obtain a reflux extracting solution and reflux extracting residues.
Thirdly, adding 2-3 times of ethanol water solution into the reflux extraction residue, soaking for 5-8h, and performing ultrasonic treatment for 50-60min to obtain an ultrasonic extraction solution and ultrasonic extraction residue.
And fourthly, combining the ultrasonic wave extracting solution and the reflux extracting solution, and performing reduced pressure evaporation and concentration to obtain the safflower extract, wherein the volume of the safflower extract is 12-15% of the original volume.
The mass concentration of the ethanol water solution is 60-70%.
Another technical problem to be solved by the present invention is to provide a method for preparing a cosmetic repair water, comprising the following steps:
step one, cleaning and disinfecting. And step two, heating and mixing. And step three, cooling and dissolving. And step four, cooling and stirring. And step five, preserving heat and dissolving. And step six, discharging. And seventhly, performing quality sampling inspection. And step eight, filling and packaging.
In step one, the production equipment and the tools are first cleaned and sterilized to make the production equipment and the operation space in a sterile state.
In the second step, water, glycerol and propylene glycol are sequentially added into a clean container, then the temperature is slowly increased to 80-85 ℃, the temperature increase time is controlled within 30min, and after the temperature increase time is controlled to be within 5min, mechanical stirring is adopted for 30min to be in a uniform state.
In the third step, cactus extract, ethylhexyl glycerol, Hamamelis virginiana extract and Carthami flos extract are sequentially added into a container, and then cooled to 60-70 deg.C, and stirred for 30min to dissolve.
In the fourth step, when the temperature in the container is reduced to 55 ℃, the dipotassium glycyrrhizinate, the allantoin, the sodium hyaluronate and the lavender oil are added, and the mixture is stirred for 45min until the mixture is uniformly mixed.
In the fifth step, when the temperature is reduced to 50 ℃, the disodium EDTA is added, and the mixture is stirred for 30 minutes until the mixture is uniformly mixed.
And in the sixth step, naturally cooling to the room temperature state, and then discharging.
And seventhly, sampling and inspecting the product, and entering the next process after the quality detection data meet the standard.
In step eight, the product is subjected to canning and packaging operations and then transferred to a finished product warehouse for storage.
Example two
The cosmetic repairing water comprises the following components in percentage by weight: 74% of water, 3.5% of glycerol, 1.5% of propylene glycol, 2% of cactus extract, 1% of ethylhexyl glycerol, 2% of witch hazel extract, 3% of safflower extract, 1% of dipotassium glycyrrhizinate, 5% of allantoin, 2% of sodium hyaluronate, 3% of lavender oil and 2% of EDTA disodium.
Another technical problem to be solved by the present invention is to provide a method for preparing a cosmetic repair water, comprising the following steps:
step one, cleaning and disinfecting. And step two, heating and mixing. And step three, cooling and dissolving. And step four, cooling and stirring. And step five, preserving heat and dissolving. And step six, discharging. And seventhly, performing quality sampling inspection. And step eight, filling and packaging.
In step one, the production equipment and the tools are first cleaned and sterilized to make the production equipment and the operation space in a sterile state.
In the second step, water, glycerol and propylene glycol are sequentially added into a clean container, then the temperature is slowly increased to 80-85 ℃, the temperature increase time is controlled within 30min, and after the temperature increase time is controlled to be within 5min, mechanical stirring is adopted for 30min to be in a uniform state.
In the third step, cactus extract, ethylhexyl glycerol, Hamamelis virginiana extract and Carthami flos extract are sequentially added into a container, and then cooled to 60-70 deg.C, and stirred for 30min to dissolve.
In the fourth step, when the temperature in the container is reduced to 55 ℃, the dipotassium glycyrrhizinate, the allantoin, the sodium hyaluronate and the lavender oil are added, and the mixture is stirred for 45min until the mixture is uniformly mixed.
In the fifth step, when the temperature is reduced to 50 ℃, the disodium EDTA is added, and the mixture is stirred for 30 minutes until the mixture is uniformly mixed.
And in the sixth step, naturally cooling to the room temperature state, and then discharging.
And seventhly, sampling and inspecting the product, and entering the next process after the quality detection data meet the standard.
In step eight, the product is subjected to canning and packaging operations and then transferred to a finished product warehouse for storage.
EXAMPLE III
The cosmetic repairing water comprises the following components in percentage by weight: 74% of water, 3.7% of glycerin, 1.8% of propylene glycol, 2.35% of cactus extract, 1.3% of ethylhexyl glycerin, 2.3% of witch hazel extract, 3.2% of safflower extract, 1.2% of dipotassium glycyrrhizinate, 5.25% of allantoin, 2.15% of sodium hyaluronate, 3.25% of lavender oil and 2.1% of EDTA disodium.
Another technical problem to be solved by the present invention is to provide a method for preparing a cosmetic repair water, comprising the following steps:
step one, cleaning and disinfecting. And step two, heating and mixing. And step three, cooling and dissolving. And step four, cooling and stirring. And step five, preserving heat and dissolving. And step six, discharging. And seventhly, performing quality sampling inspection. And step eight, filling and packaging.
In step one, the production equipment and the tools are first cleaned and sterilized to make the production equipment and the operation space in a sterile state.
In the second step, water, glycerol and propylene glycol are sequentially added into a clean container, then the temperature is slowly increased to 80-85 ℃, the temperature increase time is controlled within 30min, and after the temperature increase time is controlled to be within 5min, mechanical stirring is adopted for 30min to be in a uniform state.
In the third step, cactus extract, ethylhexyl glycerol, Hamamelis virginiana extract and Carthami flos extract are sequentially added into a container, and then cooled to 60-70 deg.C, and stirred for 30min to dissolve.
In the fourth step, when the temperature in the container is reduced to 55 ℃, the dipotassium glycyrrhizinate, the allantoin, the sodium hyaluronate and the lavender oil are added, and the mixture is stirred for 45min until the mixture is uniformly mixed.
In the fifth step, when the temperature is reduced to 50 ℃, the disodium EDTA is added, and the mixture is stirred for 30 minutes until the mixture is uniformly mixed.
And in the sixth step, naturally cooling to the room temperature state, and then discharging.
And seventhly, sampling and inspecting the product, and entering the next process after the quality detection data meet the standard.
In step eight, the product is subjected to canning and packaging operations and then transferred to a finished product warehouse for storage.
Examples of the experiments
1. Multiple skin irritation test
The test is divided into three groups, the products in the first to third examples are used for carrying out the test in sequence, three healthy and non-skin disease new Zealand white rabbits are obtained, each rabbit adopts the same operation, the weight is 2.1kg-2.2kg, two sides of the spine are sheared into 2.5cm and 2.5cm respectively, 0.2g of cactus extract is directly smeared on the skin on one side, the other side is used for comparison, the cactus extract is smeared once a day and is continuously applied for 14 days (shearing hairs if necessary), the skin reaction is observed and recorded every day, after the test is finished, the local skin is taken for pathological histological examination, the test result shows that the stimulation index of the product on the skin of the rabbits is 11.0, the average value of pathological integral is 2.0, and the product is non-irritant.
2. Skin allergy test
Guinea pigs were used, and 3 trials were set up: the test result shows that the tested animals have no symptoms such as erythema, edema and the like in 24 hours and 48 hours, and have higher safety and no skin allergy compared with the positive control group.
3. Guinea pig skin phototoxicity experiment
A albino male guinea pig with the weight of 300g-50g and the irradiation dose of 10J/cm, the intensity of 1692mW +/cm, the irradiation time of 60s, a hair removal area selected 18h-24h before an animal test, UVA point light source irradiation on the test area after medicine application for 30min, skin reaction observed at 1h, 24h, 48h and 72h after the test is finished, a positive control group coated with a positive control substance of 0.05% -MOP on the hair removal area, and the test result shows that the skin of the guinea pig is subjected to UV irradiation treatment without skin phototoxicity.
4. Human body patch experiment
The test subject is selected from volunteers, 25 persons, 4 men and 21 women, the age distribution is 22-58 years, a closed spot sticking test method is adopted, the test subject is removed after 2 hours, skin reactions are observed in spot sticking tests for 24 hours, 48 hours and 72 hours, the results are recorded according to the skin reaction grading standard in GB7919-87 of cosmetic safety evaluation program and method, the test results show that the spot sticking to the human body does not have any side effect on the skin of the human body, none of the 25 persons shows positive, and the test subject does not cause obvious adverse reaction on the human body according to the GB7919-87 standard of the cosmetic safety evaluation program and method.
In conclusion, the cactus is changed from the fields of food and medicine to the field of cosmetics, the application range of the cactus is widened, new vitality is also brought to the cosmetic industry, the cactus belongs to a natural additive, no toxic or side effect exists, the development trend of 'component naturalization' and 'returning to nature' of cosmetics is conformed, the cactus extract has an obvious growth promoting effect on human skin fibroblasts cultured in vitro, the effect is superior to AHA, the anti-aging effect is realized on human fibroblasts, the cell aging process can be delayed, the cactus extract provides 24 hours of uninterrupted and lasting moisture for the skin, the cactus in the cactus extract has an ultra-strong moisture-retaining component, the moisture is retained in the skin for a long time, the natural moisture-retaining capacity of the skin is enhanced, the moisture-tenderness state of the skin is maintained for a long time, and the chemical components such as amino acid, superoxide dismutase (SOD) and polysaccharide which are rich in the cactus are active components having the skin, and the abundant vitamin C contained in the skin whitening cream has the capacity of eliminating and inhibiting free radicals, contains efficient whitening and moisturizing factors, locks moisture, maintains the health and whitening of the skin, is very suitable for being applied to beauty cosmetics, and has good application value and prospect.
The beneficial effects of the invention are as follows: the repair water provided by the invention has remarkable curative effects of repairing deep skin and sterilizing, has a treatment effect on contact dermatitis, seborrheic dermatitis, pruritus and neurodermatitis, deeply supplements various nutrient components of the skin, makes moisture stay in the skin for a long time, enhances the natural water retention capacity of the skin, keeps the skin in a tender state for a long time, contains efficient whitening and moisturizing factors, locks the moisture, maintains the health and whitening of the skin, prevents blackheads and acnes, and has good effects of quickly presenting fine, smooth and compact states of the skin.
The cactus extract has obvious growth promoting effect on human skin fibroblasts cultured in vitro, the effect is superior to AHA, the anti-aging effect on human fibroblasts is achieved, the aging process of cells can be delayed, the cactus extract provides continuous and lasting moisture for the skin for 24 hours, the cactus extract has super-strong moisture-retaining components, moisture is retained in the skin for a long time, the natural moisture-retaining capacity of the skin is enhanced, the skin is kept in a moisture-tender state for a long time, and meanwhile, the cactus extract contains efficient whitening and moisture-retaining factors, locks the moisture, maintains the health and whitening of the skin, is very suitable for being applied to beauty cosmetics, and has good application value and prospect.
The safflower extract has the functions of promoting blood circulation, resisting inflammation, resisting oxidation and the like, plays the effects of whitening, preventing sunburn and resisting aging by improving skin blood circulation, promoting skin metabolism, eliminating free radicals, inhibiting melanin deposition, accelerating freckle removal and decoloration, absorbing ultraviolet rays and the like, has the treatment effect on contact dermatitis, seborrheic dermatitis, pruritus and neurodermatitis, and deeply supplements various nutritional ingredients of skin, thereby having good repairing effect.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (8)

1. The cosmetic repairing water is characterized by comprising the following components in percentage by weight: 74% of water, 3.1-3.7% of glycerin, 1.2-1.8% of propylene glycol, 1.85-2.35% of cactus extract, 0.8-1.3% of ethylhexyl glycerin, 1.75-2.3% of witch hazel extract, 2.9-3.2% of safflower extract, 0.7-1.2% of dipotassium glycyrrhizinate, 4.8-5.25% of allantoin, 1.75-2.15% of sodium hyaluronate, 2.85-3.25% of lavender oil and 1.9-2.1% of disodium EDTA.
2. The cosmetic repair water according to claim 1, wherein: the 74% water may be one of distilled water or purified water, and the standards of the components in the 74% water are as follows: the content of ignition slag is less than or equal to 0.01 percent, the content of manganese is less than or equal to 0.00001 percent, the content of iron is less than or equal to 0.0004 percent, the content of chlorine is less than or equal to 0.0005 percent, the content of reduced potassium permanganate substances is less than or equal to 0.0002 percent, the content of nitric acid and nitrite is less than or equal to 0.0003 percent, and the content of ammonium is less.
3. The cosmetic repair water according to claim 1, wherein: the glycerol can be replaced by one of glycerol, olive oil or aloe gel, wherein the content of the glycerol in percentage by weight is unchanged.
4. The cosmetic repair water according to claim 1, wherein: the preparation process of the cactus extract mainly comprises the following steps:
firstly, taking 500g of new cactus, removing and cleaning the thorns, chopping the cactus, adding 400mL of 95% ethanol solution, fully shaking the cactus, leaching the solution for 40 hours, taking supernatant, storing the supernatant in a refrigerator at the temperature of 5 ℃, and storing residual bottom residues for later use;
secondly, adding 250mL of 95% ethanol solution into the bottom slag, fully oscillating, and leaching the solution for 15 hours;
and thirdly, taking the supernatant, combining the supernatant with the first supernatant, carrying out suction filtration, putting the filtrate into a separating funnel, adding 100mL of petroleum ether, fully shaking, standing for 10min, taking the lower layer liquid, then carrying out reduced pressure concentration, carrying out freeze drying on the concentrated liquid, and then obtaining the cactus extract.
5. The cosmetic repair water according to claim 1, wherein: the preparation process of the hamamelis virginiana extract mainly comprises the following steps:
firstly, weighing 500 parts of Hamamelis virginiana raw material, crushing and grinding the Hamamelis virginiana raw material into powder by using a ball mill, and screening the powder by using a 800-mesh screen for later use;
secondly, putting the screened raw materials into an extractor, adding 500 parts of distilled water into the extractor, uniformly stirring, adding boric acid, extracting for 1-2h at 60-70 ℃, filtering by adopting a 80-mesh screen, and taking supernatant;
thirdly, adding citric acid into the supernatant to adjust the pH value to be between 4 and 5.5, then extracting at room temperature for 20 to 24 hours, and then adding hydrochloric acid to adjust the pH value to be between 3.5 and 3.8;
fourthly, heating the solution in water bath to 75-85 ℃, then preserving the heat for 30-35min, filtering by adopting a 50-mesh screen to obtain a precipitate, then adding 65-70% ethanol solution by volume fraction into the precipitate, and carrying out ultrasonic extraction for 2h at 70-75 ℃;
fifthly, after the solution is cooled to the room temperature state, filtering the solution by adopting a 50-mesh screen to obtain filter residue and supernatant, and concentrating and drying the supernatant to obtain the powdery hamamelis virginiana extract.
6. The cosmetic repair water according to claim 1, wherein: the preparation process of the safflower extract mainly comprises the following steps:
firstly, taking 500g of high-quality safflower raw material, cleaning, drying, putting the cleaned high-quality safflower raw material into a ball mill, grinding the safflower raw material into powder, and screening the powder by adopting a 80-mesh screen;
secondly, transferring the screened safflower powder into an extractor, then adding 4-6 times of ethanol water, heating and refluxing for extraction for 40-50min at the constant temperature of 45 ℃ to obtain a reflux extracting solution and reflux extracting residues;
thirdly, adding 2-3 times of ethanol water solution into the reflux extraction residue, soaking for 5-8h, and performing ultrasonic treatment for 50-60min to obtain an ultrasonic extraction solution and ultrasonic extraction residue;
and fourthly, combining the ultrasonic wave extracting solution and the reflux extracting solution, and performing reduced pressure evaporation and concentration to obtain the safflower extract, wherein the volume of the safflower extract is 12-15% of the original volume.
7. The process for preparing a safflower extract according to claim 6, wherein: the mass concentration of the ethanol water solution is 60-70%.
8. The preparation method of the cosmetic repairing water is characterized by comprising the following steps:
step one, cleaning and disinfecting; step two, heating and mixing; step three, cooling and dissolving; step four, cooling and stirring; step five, heat preservation and dissolution are carried out; step six, discharging; step seven, quality sampling inspection; step eight, filling and packaging;
in the first step, firstly, cleaning and disinfecting treatment is carried out on production equipment and tools to ensure that the production equipment and the operation space are in a sterile state;
in the second step, water, glycerol and propylene glycol are sequentially added into a clean container, then the temperature is slowly increased to 80-85 ℃, the temperature increase time is controlled within 30min, and after the temperature increase time is controlled within 5min, mechanical stirring is adopted for 30min to be in a uniform state;
in the third step, cactus extract, ethylhexyl glycerol, Hamamelis virginiana extract and Carthami flos extract are sequentially added into a container, then cooled to 60-70 deg.C, and stirred for 30min to dissolve;
in the fourth step, when the temperature in the container is reduced to 55 ℃, adding dipotassium glycyrrhizinate, allantoin, sodium hyaluronate and lavender oil, and stirring for 45min to mix uniformly;
in the fifth step, when the temperature is reduced to 50 ℃, EDTA disodium is added, and the mixture is stirred for 30 minutes until the mixture is uniformly mixed;
naturally cooling to a room temperature state, and discharging;
in the seventh step, sampling inspection is carried out on the product, and the next procedure is carried out after the quality detection data meets the standard;
in step eight, the product is subjected to canning and packaging operations and then transferred to a finished product warehouse for storage.
CN201910975397.9A 2019-10-15 2019-10-15 Cosmetic repairing water and preparation method thereof Pending CN112656699A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115844797A (en) * 2022-12-29 2023-03-28 福建片仔癀化妆品有限公司 Preparation method of moisturizing lotion based on aloe vera gel

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115844797A (en) * 2022-12-29 2023-03-28 福建片仔癀化妆品有限公司 Preparation method of moisturizing lotion based on aloe vera gel

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Application publication date: 20210416