CN112618387A - Scalp care solution rich in oxygen and preparation method thereof - Google Patents
Scalp care solution rich in oxygen and preparation method thereof Download PDFInfo
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- CN112618387A CN112618387A CN202011078535.2A CN202011078535A CN112618387A CN 112618387 A CN112618387 A CN 112618387A CN 202011078535 A CN202011078535 A CN 202011078535A CN 112618387 A CN112618387 A CN 112618387A
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an oxygen-rich scalp care solution and a preparation method thereof, and the oxygen-rich scalp care solution comprises the following components in percentage by weight: 0.1-10% of tropaeolum majus extract, 0.1-10% of rehmannia glutinosa extract, 0.1-10% of swertia japonica extract, 0.1-10% of watercress leaf/stem extract, 0.1-10% of cocoa extract, 2.0-10.0% of humectant, 0.1-0.6% of preservative, 0.2-10.0% of skin conditioner, 0.05-0.3% of essence and the balance of oxygen-enriched water with the oxygen concentration of 20-1000 ppm. The scalp care solution rich in oxygen can be directly applied to scalp skin, can promote absorption of the surface layer of the scalp skin, can bring more oxygen, and has the effects of moisturizing the scalp, controlling oil, nourishing the scalp, strengthening hair roots, reducing hair loss and enhancing scalp respiration.
Description
Technical Field
The invention belongs to the field of scalp care products, and particularly relates to an oxygen-rich scalp care solution and a preparation method thereof.
Background
Oxygen is a key substance for human metabolism and is the first requirement of human life activities. Physiological studies have shown that oxygen enters the lungs through human breath, then passes through a thin alveolar membrane to reach the blood, and combines with hemoglobin in the red blood cells in the blood, and hemoglobin is a train for transporting oxygen and sends oxygen to the tissues of various parts of the body along the blood circulation track of the human body. At the cellular level, the supply of oxygen is a condition that ensures that the skin cells produce the required metabolic energy, thereby ensuring normal growth of skin and hair.
The oxygen-enriched water has the strong effects of activating human cells, delaying senescence and removing harmful substances in cell membranes or blood vessels, and people slowly begin to use the oxygen-enriched water to protect the skin in recent years. Oxygen-enriched water has been reported in cosmetics, but there are technical obstacles to practical use:
on one hand, the solubility of oxygen in pure water is only 8ppm under normal pressure, and oxygen-enriched water needs to pass through special equipment and technology, and oxygen components are added in the production process, so that the oxygen content in the water reaches 20 ppm. However, in the conventional oxygen-enriched water production process, oxygen is bubbled into water, and the oxygen produced by the process cannot be stabilized in water for a long time and is easy to volatilize.
On the other hand, oxygen has poor diffusion ability and solubility, and oxygen entering the scalp skin through air is present only on the surface of the scalp and hardly diffuses to the vicinity of hair follicles in the bottom layer of the scalp. While the utilization of oxygen by cells is often achieved through the blood circulation: oxygen in the blood is reversibly bound to hemoglobin to form oxygenated hemoglobin, and upon reaching the vicinity of the cells, oxygen is separated from the hemoglobin, penetrates the capillary wall through a concentration gradient into the extracellular environment, and is subsequently captured and utilized by the cells. The upper skin layer is at a reduced supply of molecular oxygen with increasing depth, while capillaries are present only in the dermal papilla layer and below, and numerous cells in the epidermis are at or below the critical oxygen partial pressure because they are dormant due to insufficient oxygen and energy availability.
Scalp plays an important role in hair health as a root of hair, and thus scalp care is increasingly receiving attention. Researches on scalp care solution similar products sold in the market find that most of similar products sold in the market take traditional Chinese medicine components as effective components and are used as products for growing hair, growing hair and the like. Related researches or reports on scalp care by an oxygenation mode are not found in the prior art.
Disclosure of Invention
The present invention has been made to solve the above-mentioned problems, and an object of the present invention is to provide an oxygen-rich scalp care solution and a method for preparing the same.
In a first aspect of the present invention, there is provided an oxygen-enriched scalp care solution comprising, in weight percent: herba Ecliptae extract 0.1-10%, rehmanniae radix extract 0.1-10%, swertia japonica Makino extract 0.1-10%, Phaseolus vulgaris leaf/stem extract 0.1-10%, cacao extract 0.1-10%, and oxygen-rich water with oxygen concentration of 20-1000ppm as the rest.
Preferably, in the oxygen-enriched water, oxygen exists in the form of oxygen clathrate hydrate or micro-nano bubbles. Preferably the oxygen concentration is 20-100ppm, most preferably 50 ppm.
The oxygen-enriched water used in the present invention is oxygen-enriched water produced by Nippon pharmaceutical sciences hope corporation or oxygen-enriched water produced by domestic static spiral cutters. The japanese medical science hopes that oxygen in oxygen-enriched water manufactured by japan ltd exists in the form of oxygen clathrate hydrate, that oxygen stably exists even under shaking and heating, and that it does not react with cosmetic ingredients when applied to cosmetics. When the oxygen-enriched water is prepared by adopting a static spiral cutter, micro-nano cutting and refining of gas and liquid can be realized, and oxygen is cut into micro-nano-scale small bubbles which can stably exist in water.
Preferably, the oxygen-enriched scalp care solution provided by the invention further comprises: the moisturizing agent, the preservative and the essence comprise the following raw materials in percentage by weight:
humectant 2.0-10.0%
0.1 to 0.6 percent of preservative
0.05 to 0.3 percent of essence
Preferably, the oxygen-enriched scalp care solution of the present invention comprises, in weight percent: 2-5% of tropaeolum majus extract, 2-5% of rehmannia glutinosa extract, 1-5% of swertia japonica extract, 1-5% of watercress leaf/stem extract, 1-5% of cocoa extract, 2.0-10.0% of humectant, 0.1-0.6% of preservative, 0.05-0.3% of essence and the balance of water with the oxygen concentration of 20-100 ppm.
More preferably, it comprises, in weight percent: 3-5% of tropaeolum majus extract, 3-5% of rehmannia glutinosa extract, 2-5% of swertia japonica extract, 2-5% of watercress leaf/stem extract, 2-5% of cocoa extract, 3.0-10.0% of humectant, 0.2-0.6% of preservative, 0.05-0.3% of essence and the balance of water with oxygen concentration of 50 ppm.
Preferably, the moisturizer is selected from butylene glycol, propylene glycol, glycerin, sorbitol, polyethylene glycols, isoprene glycol, etc. to supplement skin moisture and lock moisture.
The antiseptic can be selected from phenoxyethanol, ethylhexyl glycerol, p-hydroxyacetophenone, methylisothiazolinone, iodopropynyl butylcarbamate, methylparaben, propylparaben, etc., preferably phenoxyethanol and chlorphenesin.
In a second aspect of the present invention, there is provided a method for preparing the scalp care solution containing oxygen, comprising the steps of: mixing oxygen-enriched water and humectant, stirring, heating to 80-85 deg.C, cooling to 43-45 deg.C, adding herba Ecliptae extract, rehmanniae radix extract, swertia Japonica Makino extract, folium Pimpinellae Candolleanae/stem extract, cacao extract, antiseptic, skin conditioner and essence, stirring, filtering, and discharging to obtain the scalp care solution containing oxygen.
The invention has the beneficial effects that:
firstly, the invention adopts oxygen-enriched water with oxygen concentration of 20-1000ppm as solvent, oxygen exists in the form of oxygen clathrate hydrate or micro-nano bubbles, can be stably dissolved in water, and oxygen stably exists even under shaking and heating conditions, and does not react with cosmetic ingredients when being applied to shampoo.
Secondly, the eclipta alba extract which is rich in arabinogalactan is added, so that the content of a cell oxygen carrier, namely cytoglobulin, can be increased, the effect of conveying oxygen in blood vessels into capillary vessels is facilitated, the oxygenation effect of the deep layer of the skin is enhanced, and the problems of scalp aging, easy hair falling and the like are solved.
Thirdly, the invention adds the rehmannia glutinosa extract, the swertia japonica extract, the bean cotyledon/stem extract and the cocoa extract as skin conditioners, and has the advantages of natural plant sources and safe components; on the other hand, components which do not cause irritation to the scalp are not generated during the use, so that the scalp care solution rich in oxygen is higher in safety.
In a word, the scalp care solution prepared from the oxygen-enriched water with the oxygen content of more than 20ppm is directly smeared on the scalp and absorbed by the surface layer of the scalp skin, so that more oxygen can be brought to the surface layer of the scalp; the eclipta alba extract is rich in arabinogalactan, can improve the content of cell oxygen carrier-cytoglobulin, helps oxygen in blood vessels to be conveyed into capillary vessels, enhances the oxygenation effect of the deep scalp, and the oxygen-enriched water and the eclipta alba extract supplement each other to bring more oxygen to the skin, so that the cell activity is improved, and the scalp becomes full of vitality after long-term use. And adding rehmanniae radix extract, swertia japonica Makino extract, folium seu cacumen Musae/stem extract, and cacao extract to accelerate skin blood circulation, promote hair papilla growth and development, and reduce hair follicle withering, thereby increasing hair amount and improving fine and soft hair quality.
Drawings
Fig. 1 is a diagram illustrating the scoring of four shampoo use feelings of four volunteers.
Detailed Description
In order to more clearly illustrate the invention, the invention is further described below in connection with preferred embodiments. It is to be understood by persons skilled in the art that the following detailed description is illustrative and not restrictive, and is not to be taken as limiting the scope of the invention.
Example 1 and comparative examples 1 to 3
The compositions and proportions of the scalp care solutions of example 1 and comparative examples 1 to 3 are shown in table 1 below:
TABLE 1 compositions and proportions of scalp care solutions of example 1 and comparative examples 1-3
The preparation method of the four shampoos is the same as follows:
mixing water and humectant, stirring, heating to 80-85 deg.C, cooling to 43-45 deg.C, adding herba Ecliptae extract, rehmanniae radix extract, swertia Japonica extract, folium Pimpinellae Candolleanae/stem extract, cacao extract, antiseptic and essence, stirring, filtering, and discharging to obtain scalp care solution.
The four formulations shown in table 1 were filled into finished products, and the dissolved oxygen amounts in the scalp care solutions were measured by the Clark dissolved oxygen electrode method and were 83ppm, 81ppm, 4ppm, and 4ppm, respectively.
Comparison of effects
(1) Transcutaneous partial oxygen pressure test
Test subjects: 40 volunteers in the same area and age range of 25-50 years are selected, averagely divided into 4 groups, and 10 individuals in each group are subjected to a percutaneous oxygen partial pressure test by using the scalp care solutions of example 1 and comparative examples 1-3.
The test method comprises the following steps: transcutaneous measurement of oxygen partial pressure (tcpO) of skin2). Initial skin parameters were measured, and treated and untreated skin parameters were measured after 1.5, 3, 4.5 and 6 hours.
Application area: scalp (the middle of the vertex).
Testing an instrument: a radimite TCM 4 transcutaneous monitor.
And (3) test results: the oxygen partial pressure tests for example 1-comparative example 3 are shown in table 2 below:
TABLE 2 partial pressure of oxygen through skin test results for scalp care solutions of example 1 and comparative examples 1 to 3
As can be seen from the results in Table 2, the scalp care liquids of example 1 and comparative example 1, which contained water and tropaeolum majus extract with an oxygen concentration of 50ppm, were applied to the scalp, and the percutaneous oxygen partial pressure increase ratio was high, and the oxygen content in the scalp skin was high. Comparative examples 2 and 3 of scalp care solutions containing no water, tropaeolum extract having an oxygen concentration of 50ppm hardly increased the transdermal oxygen partial pressure.
2. Contrast in usage experience
40 volunteers in the same area and age range of 25-50 years are selected, the volunteers are averagely divided into 4 groups, 10 individuals in each group are selected, and the scalp care solutions in the embodiment 1 and the comparative examples 1-3 are respectively used for self evaluation of the hair and scalp states after being continuously used for 3 months. Four volunteers scored the use experience of four shampoo styles, and the test results are shown in fig. 1:
example 1 shows a significant improvement in the reduction of hair loss, hair growth rate, and overall skin health. It is demonstrated that the oxygen-rich scalp care solution is effective in improving hair health, hair growth and strength.
In conclusion, the oxygen-rich scalp care solution provided by the invention has the advantages that volunteers feel good in the whole using process, and under the condition that other components are the same and the using amount is the same, the scalp health and hair growth can be improved, and the oxygen-rich scalp care solution is suitable for recovering hair loss, thin and soft hair and hair injury of people at present.
Claims (8)
1. An oxygen-rich scalp care solution is characterized by comprising the following raw material components in percentage by weight: herba Ecliptae extract 0.1-10%, rehmanniae radix extract 0.1-10%, swertia japonica Makino extract 0.1-10%, Phaseolus vulgaris leaf/stem extract 0.1-10%, cacao extract 0.1-10%, and oxygen-rich water with oxygen concentration of 20-1000ppm as the rest.
2. The oxygen-enriched scalp care solution according to claim 1 further comprising: humectant 2.0-10.0%, antiseptic 0.1-0.6% and essence 0.05-0.3%.
3. An oxygen-enriched scalp care solution according to claim 2, characterized in that it comprises, in percentages by weight: 2-5% of tropaeolum majus extract, 2-5% of rehmannia glutinosa extract, 1-5% of swertia japonica extract, 1-5% of watercress leaf/stem extract, 1-5% of cocoa extract, 2.0-10.0% of humectant, 0.1-0.6% of preservative, 0.05-0.3% of essence and the balance of oxygen-enriched water with the oxygen concentration of 20-1000 ppm.
4. The oxygen-enriched shampoo as claimed in claim 1 wherein the oxygen is present in the form of oxygen clathrate hydrate or micro-nano bubbles in the oxygen-enriched water, and the concentration of the oxygen is 20-100 ppm.
5. The oxygen-enriched shampoo as claimed in claim 4 wherein the oxygen concentration in the oxygen-enriched water is 50 ppm.
6. An oxygen-enriched scalp care solution according to claim 2 wherein the moisturizer is selected from one or more of glycerol, 1, 3-propanediol, 1, 3-butanediol, dipropylene glycol, 1, 2-pentanediol, 1, 2-hexanediol, betaine, trehalose, xylitol and panthenol.
7. An oxygen-enriched scalp care solution according to claim 2 wherein the preservatives are selected from one or more of phenoxyethanol, methylisothiazolinone, iodopropynyl butylcarbamate, methylparaben, propylparaben, chlorphenesin.
8. A method of preparing an oxygen-enriched scalp care solution according to any of claims 1 to 7 comprising the steps of: mixing oxygen-enriched water and humectant, stirring, heating to 80-85 deg.C, cooling to 43-45 deg.C, adding herba Ecliptae extract, rehmanniae radix extract, swertia Japonica Makino extract, folium Pimpinellae Candolleanae/stem extract, cacao extract, antiseptic, skin conditioner and essence, stirring, filtering, and discharging to obtain the scalp care solution containing oxygen.
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