CN112611814A - 一种干血片中1,5-脱水葡萄糖醇的测定方法 - Google Patents
一种干血片中1,5-脱水葡萄糖醇的测定方法 Download PDFInfo
- Publication number
- CN112611814A CN112611814A CN202011365068.1A CN202011365068A CN112611814A CN 112611814 A CN112611814 A CN 112611814A CN 202011365068 A CN202011365068 A CN 202011365068A CN 112611814 A CN112611814 A CN 112611814A
- Authority
- CN
- China
- Prior art keywords
- anhydroglucitol
- acetonitrile
- mobile phase
- dried blood
- blood
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/30—Control of physical parameters of the fluid carrier of temperature
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/062—Preparation extracting sample from raw material
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
- G01N2030/324—Control of physical parameters of the fluid carrier of pressure or speed speed, flow rate
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202011365068.1A CN112611814B (zh) | 2020-11-27 | 2020-11-27 | 一种干血片中1,5-脱水葡萄糖醇的测定方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202011365068.1A CN112611814B (zh) | 2020-11-27 | 2020-11-27 | 一种干血片中1,5-脱水葡萄糖醇的测定方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN112611814A true CN112611814A (zh) | 2021-04-06 |
CN112611814B CN112611814B (zh) | 2021-07-27 |
Family
ID=75229744
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202011365068.1A Active CN112611814B (zh) | 2020-11-27 | 2020-11-27 | 一种干血片中1,5-脱水葡萄糖醇的测定方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN112611814B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113203805A (zh) * | 2021-04-21 | 2021-08-03 | 深圳市第二人民医院(深圳市转化医学研究院) | 同时测定血液中葡萄糖、果糖和1,5-脱氧葡萄糖醇的液相色谱串联质谱方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS646756A (en) * | 1987-06-29 | 1989-01-11 | Nippon Kayaku Kk | Quantification of 1,5-anhydroglucitol |
CN1180378A (zh) * | 1996-02-20 | 1998-04-29 | 协和发酵工业株式会社 | 用于定量测定1,5-失水葡糖醇的方法 |
CN101446582A (zh) * | 2008-10-30 | 2009-06-03 | 上海市徐汇区中心医院 | 1,5-脱水葡萄糖醇检测试剂盒及检测方法 |
CN110146580A (zh) * | 2019-06-03 | 2019-08-20 | 桂林电子科技大学 | 一种基于柿单宁复合纳米材料检测l,5-脱水葡萄糖醇的方法 |
-
2020
- 2020-11-27 CN CN202011365068.1A patent/CN112611814B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS646756A (en) * | 1987-06-29 | 1989-01-11 | Nippon Kayaku Kk | Quantification of 1,5-anhydroglucitol |
CN1180378A (zh) * | 1996-02-20 | 1998-04-29 | 协和发酵工业株式会社 | 用于定量测定1,5-失水葡糖醇的方法 |
CN101446582A (zh) * | 2008-10-30 | 2009-06-03 | 上海市徐汇区中心医院 | 1,5-脱水葡萄糖醇检测试剂盒及检测方法 |
CN110146580A (zh) * | 2019-06-03 | 2019-08-20 | 桂林电子科技大学 | 一种基于柿单宁复合纳米材料检测l,5-脱水葡萄糖醇的方法 |
Non-Patent Citations (3)
Title |
---|
TOSHIMITSU NIWA 等: "Quantification of Serum 1,5-Anhydroglucitolin Uremic and Diabetic Patients by Liquid Chromatography/Mass Spectrometry", 《CUNICAL CHEMISTR》 * |
李昕等: "全酶法测定血浆1,5-脱水葡萄糖醇在全自动生化分析仪上的应用 ", 《天津医科大学学报》 * |
瞿纯 等: "血浆1,5-脱水葡萄糖醇的UPLC-TQMS定量方法研究", 《转化医学杂志》 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113203805A (zh) * | 2021-04-21 | 2021-08-03 | 深圳市第二人民医院(深圳市转化医学研究院) | 同时测定血液中葡萄糖、果糖和1,5-脱氧葡萄糖醇的液相色谱串联质谱方法 |
CN113203805B (zh) * | 2021-04-21 | 2022-08-30 | 深圳市第二人民医院(深圳市转化医学研究院) | 同时测定血液中葡萄糖、果糖和1,5-脱氧葡萄糖醇的液相色谱串联质谱方法 |
Also Published As
Publication number | Publication date |
---|---|
CN112611814B (zh) | 2021-07-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Bolner et al. | Plasma and urinary HPLC-ED determination of the ratio of 8-OHdG/2-dG in Parkinson's disease | |
Cheng et al. | High-performance liquid chromatographic analysis with electrochemical detection of biogenic amines using microbore columns | |
JP2019082481A (ja) | 質量分析による逆トリヨードサイロニンの検出法 | |
Soldin et al. | Simultaneous liquid-chromatographic analysis for 4-hydroxy-3-methoxymandelic acid and 4-hydroxy-3-methoxyphenylacetic acid in urine. | |
US20150212055A1 (en) | Sensitive Method for Measuring Cis-Diol Containing Compounds in Plasma Using 2D-LC-MS/MS | |
CN113777209B (zh) | 尿液中挥发性污染物暴露与效应标志物同步检测及应用 | |
WO2014152502A1 (en) | Method for determining derivatized analytes in a separated biological fluid | |
CN109738539A (zh) | 液相色谱串联质谱测定样品极长链脂肪酸的方法及试剂盒 | |
Chou et al. | High performance liquid chromatography with fluorimetric detection for the determination of total homocysteine in human plasma: method and clinical applications | |
Wang et al. | A simple method for the analysis by MS/MS of underivatized amino acids on dry blood spots from newborn screening | |
CN112611814B (zh) | 一种干血片中1,5-脱水葡萄糖醇的测定方法 | |
KR101321034B1 (ko) | 생체 시료 내 다환 방향족 탄화수소 대사체 분석 방법 | |
CN113406235A (zh) | 一种基于uplc-ms/ms检测色氨酸及其代谢物的试剂盒和方法 | |
CN112782295A (zh) | 一种在线测定尿液中邻苯二甲酸酯代谢物含量的方法与应用 | |
Liao et al. | Quantitative detection of N7‐(2‐hydroxyethyl) guanine adducts in DNA using high‐performance liquid chromatography/electrospray ionization tandem mass spectrometry | |
US20130037709A1 (en) | Method for Clinically Monitoring Niacin and Niacin Metabolites in Serum or Plasma | |
Min et al. | Rapid and sensitive determination of diacetylpolyamines in human fingernail by ultraperformance liquid chromatography coupled with electrospray ionization tandem mass spectrometry | |
CN113917008A (zh) | 质谱检测尿液中代谢物水平的产品在制备用于早期评估肠道息肉和结直肠癌产品中的应用 | |
Becerra et al. | Miniaturized imprinted solid phase extraction to the selective analysis of Coenzyme Q10 in urine | |
Namera et al. | Monolithic spin column: a new extraction device for analysis of drugs in urine and serum by GC/MS and HPLC/MS | |
CN114624338A (zh) | 利用液相色谱-串联质谱定量分析生物样本中游离氨基酸的方法 | |
Kawaguchi et al. | New analyser for the determination of urinary vanillylmandelic acid, homovanillic acid and creatinine | |
KR100330860B1 (ko) | 호모시스테인의 혈중 농도의 분석 방법 | |
CN116858978B (zh) | 一种同时检测门冬胰岛素和德谷胰岛素的方法及其血浆样品处理方法 | |
CN113341023B (zh) | 一种基于液质联用的血清二氨基庚二酸的检测试剂盒及检测方法与应用 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20221110 Address after: 116001 No. 1 (- 4), Floor 4, No. 11A, Yuguang Street, Zhongshan District, Dalian, Liaoning Patentee after: Dalian Boyuan Medical Technology Co.,Ltd. Address before: 3 / F, No. 300-8, jinlongsi Road, Ganjingzi District, Dalian City, Liaoning Province, 116033 Patentee before: Dalian Runsheng Kangtai Medical Laboratory Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230519 Address after: No. 906, Building 57A-9, Tongqing Street, Xigang District, Dalian City, Liaoning Province, 116011 Patentee after: Dalian Boyuan Medical Laboratory Co.,Ltd. Address before: 116001 No. 1 (- 4), Floor 4, No. 11A, Yuguang Street, Zhongshan District, Dalian, Liaoning Patentee before: Dalian Boyuan Medical Technology Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230918 Address after: No. 908, Building 57A-9, Tongqing Street, Xigang District, Dalian City, Liaoning Province, 116011 Patentee after: Dalian Boyuan Medical Technology Co.,Ltd. Address before: No. 906, Building 57A-9, Tongqing Street, Xigang District, Dalian City, Liaoning Province, 116011 Patentee before: Dalian Boyuan Medical Laboratory Co.,Ltd. |