CN112402326A - Tianxiangju hydrolat and preparation method thereof - Google Patents

Tianxiangju hydrolat and preparation method thereof Download PDF

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Publication number
CN112402326A
CN112402326A CN202011508301.7A CN202011508301A CN112402326A CN 112402326 A CN112402326 A CN 112402326A CN 202011508301 A CN202011508301 A CN 202011508301A CN 112402326 A CN112402326 A CN 112402326A
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CN
China
Prior art keywords
extract
chrysanthemum
extraction device
essence
indicum
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Application number
CN202011508301.7A
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Chinese (zh)
Inventor
许心青
陈绩峰
方定国
刘辉
赵晓辉
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Nanjing Tianxiangju Biotechnology Co ltd
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Nanjing Tianxiangju Biotechnology Co ltd
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Priority to CN202011508301.7A priority Critical patent/CN112402326A/en
Publication of CN112402326A publication Critical patent/CN112402326A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/282—Artemisia, e.g. wormwood or sagebrush
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/287—Chrysanthemum, e.g. daisy
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/35—Caprifoliaceae (Honeysuckle family)
    • A61K36/355—Lonicera (honeysuckle)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/62—Nymphaeaceae (Water-lily family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00—Drugs for disorders of the senses
    • A61P27/02—Ophthalmic agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00—Drugs for disorders of the senses
    • A61P27/02—Ophthalmic agents
    • A61P27/10—Ophthalmic agents for accommodation disorders, e.g. myopia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P27/00—Drugs for disorders of the senses
    • A61P27/02—Ophthalmic agents
    • A61P27/12—Ophthalmic agents for cataracts
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P37/00—Drugs for immunological or allergic disorders
    • A61P37/08—Antiallergic agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/008—Preparations for oily skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Abstract

The invention relates to the technical field of biological extraction, and discloses a preparation method of a pure dew of osbeckia chinensis, which comprises the following materials in parts by mass: 60-100% of a chrysanthemum extract essence and 0-40% of an auxiliary plant extract essence; the method comprises the following specific steps: washing fresh leaves and flowers of Dendranthema indicum with water, and air drying. And (3) extraction: cutting fresh leaves and flowers of Dendranthema indicum, extracting in a first extraction device to obtain an extract A, mixing and cutting auxiliary plants, and extracting in a second extraction device to obtain an extract B; and (3) distillation: distilling the extract liquid A and the extract liquid B under reduced pressure respectively to obtain a chrysanthemum indicum extract essence and an auxiliary plant extract essence; preparation: mixing the obtained chrysanthemum indicum extract essence and the auxiliary plant extract essence according to the mass preparation proportion. The invention can increase the resistance and repair function of skin epidermis, has the effects of resisting inflammation, inhibiting bacteria, reducing swelling, healing and removing oily skin, and has the aim of delaying skin aging.

Description

Tianxiangju hydrolat and preparation method thereof
Technical Field
The invention relates to the technical field of biological extraction, and particularly relates to a pure natural chrysanthemum juice and a preparation method thereof.
Background
The chrysanthemum indicum native place North America has more than 30 years of history when being introduced into China, and is a new cultivated variety bred through multi-generation breeding. Chemical analysis and pharmacological tests show that: the herba Dendranthematis indici is rich in nutrients and bioactive substances such as protein, amino acids, flavonoids, polyphenols, polysaccharides, carotene, vitamin C, vitamin E, SOD (superoxide dismutase), etc. Has great economic value and scientific research value.
At present, the utilization value and the functional utility of the chrysanthemum are further developed. The invention provides a novel technology and a method for preparing the chrysanthemum indicum hydrolat.
Disclosure of Invention
The invention provides an innovative technology and a method for preparing the chrysanthemum indicum hydrolat, and aims to solve the problems in the background technology.
The invention provides a preparation method of a pure dew of osbeckia chinensis, which comprises the following materials by mass: 60-100% of a chrysanthemum extract essence and 0-40% of an auxiliary plant extract essence;
wherein the auxiliary plant hydrolat comprises one or more of honeysuckle, wormwood, wild chrysanthemum flower, groundsel, lophatherum gracile and lotus leaf which are mixed and extracted according to the mass ratio;
the method comprises the following specific steps:
step 1, extraction: collecting fresh leaves and fresh auxiliary plants of the Dendranthema indicum, chopping the fresh leaves and flowers of the Dendranthema indicum, putting the chopped leaves and flowers into a first extraction device, adding an extracting agent to extract active ingredients in the Dendranthema indicum to obtain an extract A, mixing, chopping the auxiliary plants, putting the chopped auxiliary plants into a second extraction device, adding mixed active ingredients extracted by the extracting agent to obtain an extract B;
step 2, distillation: respectively carrying out reduced pressure distillation on the extract liquor A and the extract liquor B obtained in the step 1 to obtain a chrysanthemum indicum extract essence and an auxiliary plant extract essence;
step 3, preparation: the obtained chrysanthemum indicum extract essence and the auxiliary plant extract essence are uniformly mixed according to the mass preparation proportion, bottled and sealed.
Further, in step 1, the first extraction device and the second extraction device adopt one of a rotating cone column extraction device, a carbon dioxide supercritical extraction device, a microwave extraction device and an ultrasonic extraction device.
Further, in the step 2, the temperature of the reduced pressure distillation is 90 ℃, and the pressure is 0.08-0.09 MPa.
The senecio cineraria provided by the invention purely contains multiple antibacterial, detumescent and mosquito-repellent components such as eugenol, protocatechuic acid, dibutyl phthalate and the like, and linoleic acid and other components beneficial to the skin, can increase the resistance of the skin epidermis, has the effects of resisting inflammation, inhibiting bacteria, detumescent, healing and removing greasy skin, endows the skin with elasticity, promotes skin metabolism, strengthens the cleanness and softness of the facial skin, and achieves the purpose of delaying aging; the osbeckia chinensis dew can also remove oily dirt, age cutin and shrink pores, is very suitable for people with oily skin and large blackheads, and enables the skin to return to youth. It also has effects in treating skin allergy, skin ulcer, presbyopia, cataract, and muscae volitantes.
Detailed Description
The invention is further illustrated by the following examples.
Example 1
The invention provides a preparation method of a pure dew of chrysanthemum indicum, which is characterized in that the pure dew is prepared from the following materials in parts by mass: 100% of chrysanthemum extract essence and 0% of auxiliary plant extract essence;
the method comprises the following specific steps:
step 1, extraction: collecting fresh leaves and flowers of the Dendranthema indicum, chopping the leaves and flowers, putting the cut leaves and flowers into extraction equipment, adding an extracting agent into the extraction equipment to extract active ingredients in the leaves and flowers of the Dendranthema indicum to obtain an extract liquid;
step 2, distillation: carrying out reduced pressure distillation on the extract liquor obtained in the step 1 to obtain the chrysanthemum indicum extract essence,
namely the pure natural chrysanthemum juice;
step 3, preparation: bottling the obtained pure dew of flos Dendranthematis indici, and sealing.
In the step 1, the extraction equipment is one of rotating cone column extraction equipment, carbon dioxide supercritical extraction equipment, microwave extraction equipment and ultrasonic extraction equipment.
In step 2, the temperature of the reduced pressure distillation was 90 ℃ and the pressure was 0.09 MPa.
Example 2
The invention provides a preparation method of a pure dew of osbeckia chinensis, which comprises the following materials by mass: 60% of chrysanthemum extract and 40% of auxiliary plant extract;
wherein the auxiliary plant hydrolat comprises extraction essence obtained by uniformly mixing and extracting one or more of honeysuckle, wormwood, wild chrysanthemum flower, chrysanthemum morifolium, chrysanthemum foetida, chrysanthemum morifolium, groundsel, lophatherum gracile and lotus leaf according to a mass ratio;
the method comprises the following specific steps:
step 1, extraction: collecting fresh leaves and flowers of Dendranthema indicum and fresh auxiliary plants, chopping the leaves and flowers of Dendranthema indicum, placing the chopped leaves and flowers in a first extraction device, adding an extracting agent to extract active ingredients in the leaves and flowers of Dendranthema indicum to obtain an extract A, mixing, chopping the auxiliary plants, placing the chopped auxiliary plants in a second extraction device, adding a mixed active ingredient extracted by the extracting agent to obtain an extract B;
step 2, distillation: respectively carrying out reduced pressure distillation on the extract liquor A and the extract liquor B obtained in the step 1 to obtain a chrysanthemum indicum extract essence and an auxiliary plant extract essence;
step 3, preparation: the obtained chrysanthemum indicum extract essence and the auxiliary plant extract essence are uniformly mixed according to the mass preparation proportion, bottled and sealed.
In step 1, the first extraction device and the second extraction device adopt one of a rotating cone column extraction device, a carbon dioxide supercritical extraction device, a microwave extraction device and an ultrasonic extraction device.
In step 2, the temperature of the reduced pressure distillation was 90 ℃ and the pressure was 0.085 MPa.
Example 3
The invention provides a preparation method of a pure dew of chrysanthemum indicum, which is characterized in that the pure dew is prepared from the following materials in parts by mass: 80% of chrysanthemum extract essence and 20% of auxiliary plant extract essence;
wherein the auxiliary plant hydrolat comprises one or more of honeysuckle, wormwood, wild chrysanthemum flower, chrysanthemum bud, chrysanthemum flower, groundsel, lophatherum gracile and lotus leaf which are mixed and extracted according to the mass ratio;
the method comprises the following specific steps:
step 1, extraction: collecting fresh leaves and flowers of Dendranthema indicum and fresh auxiliary plants, chopping the leaves and flowers, placing in a first extraction device, adding an extracting agent to extract active ingredients in the leaves and flowers to obtain an extract A, mixing, chopping the auxiliary plants, placing in a second extraction device, adding a mixed active ingredient extracted by the extracting agent to obtain an extract B;
step 2, distillation: respectively carrying out reduced pressure distillation on the extract liquor A and the extract liquor B obtained in the step 1 to obtain a chrysanthemum indicum extract essence and an auxiliary plant extract essence;
step 3, preparation: the obtained chrysanthemum indicum extract essence and the auxiliary plant extract essence are uniformly mixed according to the mass preparation proportion, bottled and sealed.
In step 1, the first extraction device and the second extraction device adopt one of a rotating cone column extraction device, a carbon dioxide supercritical extraction device, a microwave extraction device and an ultrasonic extraction device.
In step 2, the temperature of the reduced pressure distillation was 90 ℃ and the pressure was 0.09 MPa.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (3)

1. A preparation method of a pure dew of chrysanthemum is characterized in that the raw materials are prepared according to the mass proportion: 60-100% of a chrysanthemum extract essence and 0-40% of an auxiliary plant extract essence;
wherein the auxiliary plant hydrolat comprises extraction essence obtained by uniformly mixing and extracting one or more of honeysuckle, wormwood, wild chrysanthemum, chrysanthemum morifolium, chrysanthemum foetida, chrysanthemum morifolium, senecio scandens, lophatherum gracile and lotus leaves according to a mass ratio; the method comprises the following specific steps:
step 1, extraction: collecting fresh leaves and flowers of Dendranthema indicum and fresh auxiliary plants, chopping the leaves and leaves of Dendranthema indicum, placing in a first extraction device, adding an extractant to extract active ingredients in the leaves and flowers of Dendranthema indicum to obtain an extract A, mixing, chopping the auxiliary plants, placing in a second extraction device, adding the active ingredients extracted by the extractant to obtain an extract B;
step 2, distillation: respectively carrying out reduced pressure distillation on the extract liquor A and the extract liquor B obtained in the step 1 to obtain a chrysanthemum indicum extract essence and an auxiliary plant extract essence;
step 3, preparation: the obtained chrysanthemum indicum extract essence and the auxiliary plant extract essence are uniformly mixed according to the mass preparation proportion, bottled and sealed.
2. The method for preparing the senecio cineraria hydrolat according to claim 1, wherein in step 1, the first extraction device and the second extraction device are one of a rotating cone column extraction device, a carbon dioxide supercritical extraction device, a microwave extraction device and an ultrasonic extraction device.
3. The method for preparing senecio cineraria hydrolat according to claim 1, wherein in step 2, the temperature of the reduced pressure distillation is 90 ℃ and the pressure is 0.08 to 0.09 MPa.
CN202011508301.7A 2020-12-18 2020-12-18 Tianxiangju hydrolat and preparation method thereof Pending CN112402326A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022255282A1 (en) * 2021-05-31 2022-12-08 国立大学法人大阪大学 Dynamic visual acuity-enhancing composition

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104651056A (en) * 2015-03-12 2015-05-27 安吉依思味食品有限公司 Method for preparing tea tree flower essential oil
CN111134085A (en) * 2020-02-09 2020-05-12 董锦铭 Snowflake pork breeding method and fermentation bed pigsty for breeding

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104651056A (en) * 2015-03-12 2015-05-27 安吉依思味食品有限公司 Method for preparing tea tree flower essential oil
CN111134085A (en) * 2020-02-09 2020-05-12 董锦铭 Snowflake pork breeding method and fermentation bed pigsty for breeding

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022255282A1 (en) * 2021-05-31 2022-12-08 国立大学法人大阪大学 Dynamic visual acuity-enhancing composition

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Application publication date: 20210226