CN112384196A - 油性化妆品 - Google Patents
油性化妆品 Download PDFInfo
- Publication number
- CN112384196A CN112384196A CN201980048234.4A CN201980048234A CN112384196A CN 112384196 A CN112384196 A CN 112384196A CN 201980048234 A CN201980048234 A CN 201980048234A CN 112384196 A CN112384196 A CN 112384196A
- Authority
- CN
- China
- Prior art keywords
- oil
- acid
- mass
- oily
- cosmetic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 51
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 40
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000000843 powder Substances 0.000 claims abstract description 27
- 235000000346 sugar Nutrition 0.000 claims abstract description 23
- 239000003349 gelling agent Substances 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 17
- 238000004132 cross linking Methods 0.000 claims description 14
- 229920002545 silicone oil Polymers 0.000 claims description 8
- 150000008064 anhydrides Chemical class 0.000 claims description 6
- 239000003921 oil Substances 0.000 description 53
- 235000019198 oils Nutrition 0.000 description 53
- -1 polysiloxane Polymers 0.000 description 42
- 235000014113 dietary fatty acids Nutrition 0.000 description 20
- 239000000194 fatty acid Substances 0.000 description 20
- 229930195729 fatty acid Natural products 0.000 description 20
- 239000004375 Dextrin Substances 0.000 description 19
- 229920001353 Dextrin Polymers 0.000 description 19
- 235000019425 dextrin Nutrition 0.000 description 19
- 239000000203 mixture Substances 0.000 description 17
- 229910002012 Aerosil® Inorganic materials 0.000 description 12
- 239000004166 Lanolin Substances 0.000 description 12
- 235000019388 lanolin Nutrition 0.000 description 12
- 229940039717 lanolin Drugs 0.000 description 12
- 239000004205 dimethyl polysiloxane Substances 0.000 description 11
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 11
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 11
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 10
- 239000000049 pigment Substances 0.000 description 10
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- 239000010936 titanium Substances 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 125000004432 carbon atom Chemical group C* 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 7
- 229920001577 copolymer Polymers 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 239000010445 mica Substances 0.000 description 7
- 229910052618 mica group Inorganic materials 0.000 description 7
- 238000002156 mixing Methods 0.000 description 7
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 7
- 235000012239 silicon dioxide Nutrition 0.000 description 7
- 229910052719 titanium Inorganic materials 0.000 description 7
- 238000004040 coloring Methods 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 239000000284 extract Substances 0.000 description 6
- 150000004665 fatty acids Chemical class 0.000 description 6
- 239000001993 wax Substances 0.000 description 6
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 5
- 235000021314 Palmitic acid Nutrition 0.000 description 5
- 229930006000 Sucrose Natural products 0.000 description 5
- 239000006096 absorbing agent Substances 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 5
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical class CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 description 5
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 5
- DSSYKIVIOFKYAU-OIBJUYFYSA-N (S)-camphor Chemical compound C1C[C@]2(C)C(=O)C[C@H]1C2(C)C DSSYKIVIOFKYAU-OIBJUYFYSA-N 0.000 description 4
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 description 4
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 4
- 239000004359 castor oil Substances 0.000 description 4
- 235000019438 castor oil Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000009472 formulation Methods 0.000 description 4
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 4
- 229930195733 hydrocarbon Natural products 0.000 description 4
- 150000002430 hydrocarbons Chemical class 0.000 description 4
- 230000001771 impaired effect Effects 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 239000004094 surface-active agent Substances 0.000 description 4
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- 241000521581 Millettia Species 0.000 description 3
- YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 239000010495 camellia oil Substances 0.000 description 3
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 description 3
- 125000004494 ethyl ester group Chemical group 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 150000002772 monosaccharides Chemical class 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 3
- 229920000223 polyglycerol Polymers 0.000 description 3
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 150000004671 saturated fatty acids Chemical class 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 3
- 230000008961 swelling Effects 0.000 description 3
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 3
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 3
- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 description 2
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- OBETXYAYXDNJHR-SSDOTTSWSA-M (2r)-2-ethylhexanoate Chemical compound CCCC[C@@H](CC)C([O-])=O OBETXYAYXDNJHR-SSDOTTSWSA-M 0.000 description 2
- GHOKWGTUZJEAQD-ZETCQYMHSA-N (D)-(+)-Pantothenic acid Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCC(O)=O GHOKWGTUZJEAQD-ZETCQYMHSA-N 0.000 description 2
- DGSZGZSCHSQXFV-UHFFFAOYSA-N 2,3-bis(2-ethylhexanoyloxy)propyl 2-ethylhexanoate Chemical compound CCCCC(CC)C(=O)OCC(OC(=O)C(CC)CCCC)COC(=O)C(CC)CCCC DGSZGZSCHSQXFV-UHFFFAOYSA-N 0.000 description 2
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- 235000019489 Almond oil Nutrition 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 2
- 239000005711 Benzoic acid Substances 0.000 description 2
- ZCTQGTTXIYCGGC-UHFFFAOYSA-N Benzyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OCC1=CC=CC=C1 ZCTQGTTXIYCGGC-UHFFFAOYSA-N 0.000 description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 2
- QFOHBWFCKVYLES-UHFFFAOYSA-N Butylparaben Chemical compound CCCCOC(=O)C1=CC=C(O)C=C1 QFOHBWFCKVYLES-UHFFFAOYSA-N 0.000 description 2
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 2
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- 235000019482 Palm oil Nutrition 0.000 description 2
- 235000019483 Peanut oil Nutrition 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 229910004674 SiO0.5 Inorganic materials 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 2
- 244000172533 Viola sororia Species 0.000 description 2
- 235000006886 Zingiber officinale Nutrition 0.000 description 2
- 244000273928 Zingiber officinale Species 0.000 description 2
- CFRNDJFRRKMHTL-UHFFFAOYSA-N [3-octanoyloxy-2,2-bis(octanoyloxymethyl)propyl] octanoate Chemical compound CCCCCCCC(=O)OCC(COC(=O)CCCCCCC)(COC(=O)CCCCCCC)COC(=O)CCCCCCC CFRNDJFRRKMHTL-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 125000005250 alkyl acrylate group Chemical group 0.000 description 2
- 125000002877 alkyl aryl group Chemical group 0.000 description 2
- 150000005215 alkyl ethers Chemical class 0.000 description 2
- 239000008168 almond oil Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- FKIQSOGFDBALHA-UHFFFAOYSA-L aluminum trimagnesium potassium dioxido(oxo)silane oxygen(2-) difluoride Chemical compound [O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[K+].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O FKIQSOGFDBALHA-UHFFFAOYSA-L 0.000 description 2
- UBNYRXMKIIGMKK-RMKNXTFCSA-N amiloxate Chemical compound COC1=CC=C(\C=C\C(=O)OCCC(C)C)C=C1 UBNYRXMKIIGMKK-RMKNXTFCSA-N 0.000 description 2
- 239000010775 animal oil Substances 0.000 description 2
- RWZYAGGXGHYGMB-UHFFFAOYSA-N anthranilic acid Chemical compound NC1=CC=CC=C1C(O)=O RWZYAGGXGHYGMB-UHFFFAOYSA-N 0.000 description 2
- YZXBAPSDXZZRGB-DOFZRALJSA-N arachidonic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O YZXBAPSDXZZRGB-DOFZRALJSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical compound CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 2
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- KVYGGMBOZFWZBQ-UHFFFAOYSA-N benzyl nicotinate Chemical compound C=1C=CN=CC=1C(=O)OCC1=CC=CC=C1 KVYGGMBOZFWZBQ-UHFFFAOYSA-N 0.000 description 2
- HGKOWIQVWAQWDS-UHFFFAOYSA-N bis(16-methylheptadecyl) 2-hydroxybutanedioate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)C(=O)OCCCCCCCCCCCCCCCC(C)C HGKOWIQVWAQWDS-UHFFFAOYSA-N 0.000 description 2
- 229940073609 bismuth oxychloride Drugs 0.000 description 2
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- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 2
- 229910000423 chromium oxide Inorganic materials 0.000 description 2
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- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
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- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
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- HKQYGTCOTHHOMP-UHFFFAOYSA-N formononetin Chemical compound C1=CC(OC)=CC=C1C1=COC2=CC(O)=CC=C2C1=O HKQYGTCOTHHOMP-UHFFFAOYSA-N 0.000 description 2
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- 150000004676 glycans Chemical class 0.000 description 2
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- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 2
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- FFUAGWLWBBFQJT-UHFFFAOYSA-N hexamethyldisilazane Chemical compound C[Si](C)(C)N[Si](C)(C)C FFUAGWLWBBFQJT-UHFFFAOYSA-N 0.000 description 2
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- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 description 2
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- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 description 2
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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Abstract
提供哑光感优异、稳定性良好的油性化妆品。油性化妆品,其特征在于,包含下述成分(a)~(d)。(a)交联型有机聚硅氧烷(b)无定形硅酸酐(c)具有糖骨架的油性胶凝剂(d)液态油成分(e)粉末。
Description
相关技术
本申请要求2018年 7月19日提交的日本专利申请2018-136248号的优先权,并入本文。
技术领域
本发明涉及油性化妆品,特别涉及具有哑光感、稳定性良好的油性化妆品。
背景技术
涂布了化妆品的肌肤、唇的质感大致分为赋予光泽感和哑光感的两种。这些之中,已知配合有部分交联型有机聚硅氧烷、以及固体油和/或半固体油的油性固型化妆品(参照专利文献1)。然而,对于哑光感存在改善的余地。
此外,还已知配合了交联型有机聚硅氧烷和无定形硅酸酐的油性化妆品(参照专利文献2)。然而,对于哑光感、稳定性存在改善的余地。
现有技术文献
专利文献
专利文献1:日本特开2000-281532号公报
专利文献2:日本特开2002-154918号公报。
发明内容
发明要解决的课题
本发明鉴于前述现有技术而进行,其要解决的课题在于,提供具有哑光感、稳定性良好的油性化妆品。
用于解决课题的手段
本发明人等为了解决前述的课题而进行深入研究的结果发现,通过包含特定量的(a)交联型有机聚硅氧烷、(b)无定形硅酸酐、(c)具有糖骨架的油性胶凝剂、(d)液态油成分、(e)粉末,得到哑光感优异、稳定性良好的油性化妆品,从而完成了本发明。
即,本发明所涉及的油性化妆品的特征在于,包含下述成分(a)~(e),
(a)交联型有机聚硅氧烷
(b)无定形硅酸酐
(c)具有糖骨架的油性胶凝剂
(d)液态油成分
(e)粉末。
前述油性化妆品中,(c)具有糖骨架的油性胶凝剂的配合量适合为1~15质量%。
前述油性化妆品中,(d)液态油成分中适合包含硅油和极性油成分。
本发明所涉及的唇用化妆品的特征在于,为前述油性化妆品。
发明的效果
根据本发明,能够得到具有哑光感、稳定性良好的油性化妆品。
具体实施方式
以下,针对本发明的实施方式进行详细说明。
本发明所涉及的油性化妆品的特征在于,包含下述成分(a)~(e),
(a)交联型有机聚硅氧烷
(b)无定形硅酸酐
(c)具有糖骨架的油性胶凝剂
(d)液态油成分
(e)粉末。
((a)交联型有机聚硅氧烷)
作为交联型有机聚硅氧烷,可使用在铂催化剂存在下通过(a)每1分子具有至少2个低级烯基的有机聚硅氧烷、和(b)每1分子具有至少2个与硅原子键合的氢原子的有机聚硅氧烷的加成反应与交联反应而得到的交联型有机聚硅氧烷。
此外,除此之外,还可使用以下的交联型有机聚硅氧烷。
(1)交联型有机聚硅氧烷,其在R2SiO单元、RSiO1.5单元、R3SiO0.5单元和SiO2单元之中至少包含R2SiO单元、RSiO1.5单元和R3SiO0.5单元,其中,R各自独立地表示氢原子、甲基、乙基和丙基等烷基、或苯基、和三甲基等芳基、或乙烯基等不饱和脂肪族基团等,R2SiO单元相对于RSiO1.5单元的重量比处于1~30:1的范围。
(2)交联型有机氢聚硅氧烷,其能够通过(c)有机氢聚硅氧烷、与(d)具有不饱和脂肪族基团的有机聚硅氧烷的加成而得到,(c)和(d)的氢或不饱和脂肪族基团的量分别在有机聚硅氧烷为非环状的情况下处于1~20摩尔%、在有机聚硅氧烷为环状的情况下处于1~50摩尔%的范围。
作为交联型有机聚硅氧烷,优选使用交联型烷基芳基聚硅氧烷和交联型烷基聚硅氧烷。作为交联型烷基芳基聚硅氧烷,可以举出例如具有碳原子数为1~5的烷基和碳原子数为6~10的芳基的交联型有机聚硅氧烷。作为具体例,可以举出例如甲基苯基聚硅氧烷、和乙基苯基聚硅氧烷等。
作为交联型烷基聚硅氧烷,可以举出例如具有碳原子数为1~5的烷基的交联型单烷基聚硅氧烷和交联型二烷基聚硅氧烷。作为具体例,可以举出例如交联型单甲基聚硅氧烷、交联型二甲基聚硅氧烷、交联型单乙基聚硅氧烷、交联型二乙基聚硅氧烷、和交联型甲基乙基聚硅氧烷等。
作为交联型烷基聚硅氧烷的市售品,可以举出作为二甲基聚硅氧烷与部分交联型硅酮的混合物(16重量%浓度)的Dow Corning 9041 Silicone Elastomer Blend(东レ・ダウコーニング・シリコーン株式会社制)、作为十甲基环五硅氧烷与交联型甲基聚硅氧烷的混合物(5重量%浓度)的糊状的KSG15(信越化学工业株式会社制)、作为低粘度二甲基聚硅氧烷与交联型甲基聚硅氧烷的混合物(20~30重量%浓度)的糊状的KSG16(信越化学工业株式会社制)、作为甲基苯基聚硅氧烷与交联型甲基苯基聚硅氧烷的混合物(10~20重量%浓度)的糊状的KSG18(信越化学工业株式会社制)等。这些交联型有机聚硅氧烷可使用一种或二种以上。
本发明中的交联型有机聚硅氧烷的配合量以纯成分计,优选为油性化妆品总量中的1~10质量%。此外,配合量更优选为3质量%以上。如果配合量低于1质量%,则无法得到充分的哑光感。
此外,配合量更优选为8质量%以下。如果配合量大于10质量%,有时损害涂布时的顺滑度。
((b)无定形硅酸酐)
作为无定形硅酸酐,可以举出将四氯化硅在氢氧焰中水解而得到的亲水性的无定形硅酸酐、和将前述亲水性的无定形硅酸酐的表面进行疏水化处理而得到的无定形硅酸酐。前述无定形硅酸酐可以为亲水性或经疏水化的无定形硅酸酐。作为前述疏水化处理的方法,可以举出利用三甲基氯硅烷、和六甲基二硅氮烷等的三甲基甲硅烷氧基化处理、利用二甲基二氯硅烷的甲基化处理、使用甲基氢聚硅氧烷的涂布烘烤处理、利用二甲基聚硅氧烷、金属皂等的涂布等。这些无定形硅酸酐可使用一种或二种以上。
无定形硅酸酐的平均粒径优选为0.001~0.05μm、更优选为0.001~0.02μm。如果平均粒径为前述范围内,则得到不发生粗糙的良好的使用感、和油成分不分离的良好的稳定性。该无定形微粒硅酸酐的平均粒径可通过透射型电子显微镜测定。
作为无定形硅酸酐的市售品,可以举出例如AEROSIL200(日本AEROSIL株式会社制)、AEROSIL300(日本AEROSIL株式会社制)、AEROSIL R972(日本AEROSIL株式会社制)、AEROSIL R974(日本AEROSIL株式会社制)、AEROSIL R202(日本AEROSIL株式会社制)、AEROSIL RY200(日本AEROSIL株式会社制)、タラノックス500(タルコ公司制)等。
无定形硅酸酐的配合量在油性化妆品总量中优选为0.1~10质量%。此外,配合量更优选为0.5质量%以上。如果配合量低于0.1质量%,则无法得到充分的哑光感。
此外,配合量更优选为7质量%以下。如果配合量大于5质量%,则有时损害涂布时的顺滑度。
((c)具有糖骨架的油性胶凝剂)
具有糖骨架的油性胶凝剂只要是通常能够用于化妆品的物质,则均可使用。作为具体例,可以举出例如糊精脂肪酸酯、低聚果糖脂肪酸酯、蔗糖脂肪酸酯等糖脂肪酸酯等。
用(a)成分和(b)成分增稠的化妆品具有容易分油的缺点,但通过配合本发明的具有糖骨架的油性胶凝剂,能够得到稳定性、高温稳定性优异的油性化妆品。
作为构成本发明的具有糖骨架的油性胶凝剂的糖,可以举出糖或烷基糖,可以使用单糖至多糖。作为单糖、寡糖、多糖,没有特别限制,可以举出例如葡萄糖、半乳糖、果糖、甘露糖、蔗糖、乳糖、麦芽糖、海藻糖、蜜二糖、棉子糖、低聚果糖、糊精、菊粉等。并且,优选将通过这些糖或烷基糖与脂肪酸的反应而得到的酯化合物用作油性胶凝剂。
作为脂肪酸,优选碳原子数6~32的直链或支链的饱和或不饱和脂肪酸,进一步优选碳原子数8~24的物质。作为脂肪酸,可以举出例如辛酸、癸酸、月桂酸、肉豆蔻酸、棕榈酸、硬脂酸、花生酸、山萮酸、油酸、亚油酸、亚麻酸、花生四烯酸、2-乙基己酸、异肉豆蔻酸、异棕榈酸、异硬脂酸、辛基十二烷酸等。
作为优选的具有糖骨架的脂肪酸酯的油性胶凝剂,可以举出糊精脂肪酸酯、蔗糖脂肪酸酯。
作为糊精脂肪酸酯,例如优选平均取代度为每一个单糖为2.5以上的、碳原子数6~32的直链或支链的饱和或不饱和脂肪酸与糊精的酯。
作为具体例,可以举出例如棕榈酸糊精酯、(棕榈酸/乙基己酸)糊精酯、肉豆蔻酸糊精酯、硬脂酸糊精酯、棕榈酸/硬脂酸糊精酯、油酸糊精酯、异棕榈酸糊精酯、异硬脂酸糊精酯等。
作为市售品,作为棕榈酸糊精酯,可以举出レオパールKL2、レオパールTL2(均为千叶制粉公司制),作为(棕榈酸/乙基己酸)糊精酯,可以举出レオパールTT2(千叶制粉公司制),作为肉豆蔻酸糊精酯,可以举出レオパールMKL2(千叶制粉公司制)等。
作为蔗糖脂肪酸酯,例如优选平均取代度为2.5以上的、碳原子数6~32的直链或支链的饱和或不饱和脂肪酸与蔗糖的酯。
具有糖骨架的油性胶凝剂的配合量在油性化妆品总量中优选为1~15质量%。通过将具有糖骨架的油性胶凝剂的配合量设为1~15质量%,可以得到具有哑光感、同时具有涂布时的顺滑度、高温稳定性良好的糊状的油性化妆品。此外,更优选为3质量%以上。如果配合量低于1质量%,则哑光感、稳定性差。
此外,更优选低于8质量%。如果配合量大于15质量%,则有时损害涂布时的顺滑度、形成滑腻的感触。
((d)液态油成分)
液态油成分可使用在化妆品中通常使用的液态油成分。
作为本发明中的液态油成分,优选配合硅油和极性油成分。
作为硅油,可以举出例如聚合度6以上的二甲基聚硅氧烷、苯基聚三甲基硅氧烷、二苯基聚二甲基硅氧烷、二苯基甲硅烷氧基苯基聚三甲基硅氧烷、三甲基五苯基三硅氧烷等不挥发性硅油、聚合度2~5的二甲基聚硅氧烷、十甲基环五硅氧烷、八甲基环四硅氧烷、十二甲基环六硅氧烷、甲基聚三甲基硅氧烷、二甲基聚硅氧烷、十甲基四硅氧烷、乙基三硅氧烷等挥发性硅油等。
作为极性油成分,可以举出例如三(2-乙基己酸)甘油酯、苹果酸二异硬脂基酯、二异硬脂酸甘油酯、三异硬脂酸二甘油酯、三(辛/癸)酸甘油酯、二癸酸新戊二醇酯、四(2-乙基己酸)季戊四醇酯、癸二酸二(乙基己基)酯、辛基十二烷醇、三(2-乙基己酸)三羟甲基丙烷酯、羟基硬脂酸羟基硬脂基酯、四(乙基己酸/苯甲酸)季戊四醇酯、三辛酸甘油酯、四辛酸季戊四醇酯、六羟基硬脂酸二季戊四醇酯、蓖麻油、癸二酸二异丙酯、四辛酸季戊四醇酯、三异硬脂酸三羟甲基丙烷酯等。
作为除了硅油、极性油成分之外的不挥发性液态油成分,可以举出例如烃油、天然动植物油和半合成油等。
作为烃油,可以举出氢化聚异丁烯、液体石蜡、角鲨烷、角鲨烯、重质液体异链烷烃、聚异丁烯、α-烯烃低聚物等。
作为天然动植物油和半合成油,可以举出鳄梨油、亚麻籽油、扁桃仁油、橄榄油、榧子油、肝油、杏仁油、小麦胚芽油、芝麻油、大米胚芽油、米糠油、山茶花油、红花油、中国桐油、肉桂油、鳖油、大豆油、茶籽油、山茶油、月见草油、玉米油、菜籽油、日本桐油、胚芽油、桃仁油、棕榈油、红棕榈油、棕榈仁油、蓖麻油、葵花籽油、葡萄籽油、荷荷巴油、澳洲坚果油、棉籽油、椰子油、三椰子油脂肪酸甘油酯、花生油、液态羊毛脂、还原羊毛脂、羊毛脂醇、乙酸羊毛脂、羊毛脂脂肪酸异丙酯、POE羊毛脂醇醚、POE羊毛脂醇乙酸酯、羊毛脂脂肪酸聚乙二醇酯、POE加氢羊毛脂醇醚、蛋黄油等。
作为除了挥发性硅油之外的挥发性油成分,可以举出轻质液体异链烷烃等。
液态油成分的配合量在油性化妆品总量中优选为40~90质量%。此外,更优选为50质量%以上。如果配合量低于40质量%,则润湿感不足。
此外,更优选低于80质量%。如果配合量大于90质量%,则哑光感不足。
((e)粉末)
粉末只要是一般用于化妆品的物质,则可没有特别限制地使用。
作为粉末,可以举出例如球状粉末、板状粉末、色料等。
本发明中使用的球状粉末只要是一般用于油性化妆品的物质,则可以没有特别限制地使用。
作为球状粉末,可以举出例如聚甲基丙烯酸甲酯、有机聚硅氧烷弹性体、聚苯乙烯、聚酰胺树脂(尼龙)、聚乙烯、苯乙烯与丙烯酸的共聚物、苯并胍胺树脂、聚四氟乙烯、有机硅树脂等球状树脂粉末。
本发明的粉末中,还能够配合板状粉末。板状粉末的短径与长径的比率优选相对于短径1长径为10以上。
作为板状粉末,可以举出例如云母、合成云母、滑石、绢云母、氧化铝、氧化镁、氧化锆、碳酸镁、碳酸钙、硫酸钙、氧化铬、氢氧化铬、硅酸铝、硅酸镁、硅酸铝镁、高岭土、碳化硅、硫酸钡、膨润土、蒙皂石、氮化硼等无机粉体类、N-酰基赖氨酸等有机粉体类、微粒氧化钛覆盖云母钛、微粒氧化锌覆盖云母钛、硫酸钡覆盖云母钛等复合粉体类等。
此外,本发明所涉及的化妆品中,还可配合色料。色料为了将制剂着色而配合。作为色料,可以使用颜料、珠光颜料、将它们色淀化而得到的物质等在油性化妆品中通常配合的物质。
作为色料,可以举出例如无机白色系颜料(二氧化钛、氧化锌)、无机红色系颜料(氧化铁(铁红)、钛酸铁)、无机褐色系颜料(γ-氧化铁)、无机黄色系颜料(氧化铁黄、黄土)、无机黑色系颜料(氧化铁黑、碳、低价氧化钛)、无机紫色系颜料(锰紫、钴紫)、无机绿色系颜料(氧化铬、氢氧化铬、钛酸钴)、无机蓝色系颜料(群青、普鲁士蓝)、珠光颜料(氧化钛覆盖云母、氧化钛覆盖氯氧化铋、氧化钛覆盖滑石、着色氧化钛覆盖云母、氯氧化铋、鱼鳞箔)、金属粉末颜料(铝粉末、铜粉末)、有机颜料(红色202号、红色205号、红色220号、红色228号、红色405号、橙色203号、橙色204号、黄色205号、黄色401号、蓝色404号)、锆、钡、铝色淀的有机颜料(红色3号、红色104号、红色227号、红色401号、橙色205号、黄色4号、黄色202号、绿色3号、蓝色1号)、天然色素(叶绿素、类胡萝卜素系(β-胡萝卜素)、红花素、胭脂虫红、查尔酮、姜黄素、甜菜苷、黄酮醇、黄酮、花青素、蒽醌、萘醌)、功能性颜料(氮化硼、光致变色颜料、合成氟金云母、含铁的合成氟金云母、微粒复合粉体(混合精细粉末))等。
粉末的配合量在油性化妆品总量中优选为0.1~40质量%。此外,更优选为5质量%以上、进一步优选为8质量%以上。如果配合量低于0.1质量%,则有时无法得到充分的哑光感。
此外,更优选为38质量%以下,如果为30质量%以下则在更顺滑的方面是进一步优选的。如果配合量大于40质量%,则损害涂布时的顺滑感触。
本发明所涉及的油性化妆品中,除了上述必须成分之外,在不损害本发明的效果范围,可配合通常化妆品中使用的成分、例如半固体油成分、固体油成分、表面活性剂、覆膜剂、保湿剂、紫外线吸收剂、美容成分、纤维、香料等。
作为半固体油成分,可以举出例如凡士林、四(山萮酸/苯甲酸/乙基己酸)季戊四醇酯、六羟基硬脂酸二季戊四醇酯、二聚体二亚油酸酯、澳洲坚果油聚甘油-6酯山萮酸酯、四(羟基硬脂酸/异硬脂酸)二季戊四醇酯、双二甘油多酰基己二酸酯-2等。
半固体油成分的含量优选为30质量%以下。通过配合半固体油成分,可使油性化妆品的稳定性、高温稳定性良好。
作为固体油成分,可以举出固体油脂、蜡类、固体烃、高级醇。可以例示出例如可可脂、氢化蓖麻油等固体油脂;木蜡、巴西棕榈蜡、蜂蜡、白蜂蜡、小烛树蜡、荷荷巴蜡等蜡类:聚乙烯蜡、石蜡、纯地蜡、微晶蜡等烃蜡;鲸蜡醇、硬脂醇、山萮醇、鲨肝醇等高级醇;硅酮蜡等。
固体油成分的配合量优选为10质量%以下。通过配合固体油成分,能够使油性化妆品的稳定性、高温稳定性良好。
作为非离子性表面活性剂,可以举出例如聚氧乙烯烷基醚、聚氧乙烯脂肪酸酯、聚氧乙烯多元醇脂肪酸偏酯、聚氧乙烯氢化蓖麻油衍生物等聚氧乙烯系表面活性剂、辛基多糖苷等烷基多糖苷类、聚甘油脂肪酸酯、聚甘油烷基醚等聚甘油系表面活性剂、麦芽糖醇羟基烷基醚等糖醇羟基烷基醚类、脂肪酸二乙醇酰胺等。
此外,还可配合高级脂肪酸盐类、烷基苯磺酸盐类、磷酸酯类、烷基硫酸盐类、烷基硫酸酯盐类、聚氧乙烯烷基硫酸酯盐类等阴离子性表面活性剂、氨基酸类、烷基三甲基铵盐、二烷基二甲基铵盐、烷基二甲基胺氧化物等阳离子性表面活性剂、其它表面活性剂。
作为覆膜剂,可以举出例如硅酮化普鲁兰多糖、三甲基甲硅烷氧基硅酸、二甲基氨基甲基丙烯酸酯季铵化盐、乙烯基吡咯烷酮·甲基丙烯酸-N,N-二甲基-乙基锑代乙基盐共聚物(ビニルピロリドン・メタクリル酸-N,N-ジメチル-エチルアンチニオエチル塩共重合体)、硅酮/聚醚系聚氨酯树脂、(甲基丙烯酰基氧基乙基羧基甜菜碱/甲基丙烯酰基烷基)共聚物、糊精、(乙烯基吡咯烷酮/VA)共聚物、丙烯酸烷基酯共聚物铵、聚乙烯醇、聚丙烯酸乙酯、(丙烯酸烷基酯/辛基丙烯酰胺)共聚物、(丙烯酸酯/甲基丙烯酸丙基聚三甲基硅氧烷)共聚物、聚乙酸乙烯酯、(丙烯酸烷基酯/聚二甲基硅氧烷)共聚物、聚醚接枝丙烯酰基硅酮、三甲基甲硅烷氧基硅酸、氟改性有机硅树脂等。
作为保湿剂,可以举出例如双丙甘醇、聚乙二醇、丙二醇、甘油、1,3-丁二醇、木糖醇、山梨糖醇、麦芽糖醇、硫酸软骨素、透明质酸、硫酸粘多糖、楼仁酸(カロニン酸)、缺端胶原蛋白、胆甾醇-12-羟基硬脂酸酯、乳酸钠、胆汁酸盐、dl-吡咯烷酮羧酸盐、短链可溶性胶原蛋白、二甘油(EO)PO加成物、刺梨提取物、蓍草提取物、草木犀提取物等。
作为紫外线吸收剂,可以举出例如苯甲酸系紫外线吸收剂(例如对氨基苯甲酸(以下简称为PABA)、PABA单甘油酯、N,N-二丙氧基PABA乙基酯、N,N-二乙氧基PABA乙基酯、N,N-二甲基PABA乙基酯、N,N-二甲基PABA丁基酯、N,N-二甲基PABA乙基酯等);氨茴酸系紫外线吸收剂(例如N-乙酰基氨茴酸三甲环己酯等);水杨酸系紫外线吸收剂(例如水杨酸戊酯、水杨酸基酯、水杨酸三甲环己酯、水杨酸辛酯、水杨酸苯酯、水杨酸苯甲酯、对异丙醇苯基水杨酸酯等);肉桂酸系紫外线吸收剂(例如肉桂酸辛酯、乙基-4-异丙基肉桂酸酯、甲基-2,5-二异丙基肉桂酸酯、乙基-2,4-二异丙基肉桂酸酯、甲基-2,4-二异丙基肉桂酸酯、丙基-对甲氧基肉桂酸酯、异丙基-对甲氧基肉桂酸酯、异戊基-对甲氧基肉桂酸酯、辛基-对甲氧基肉桂酸酯(2-乙基己基-对甲氧基肉桂酸酯)、2-乙氧基乙基-对甲氧基肉桂酸酯、环己基-对甲氧基肉桂酸酯、乙基-α-氰基-β-苯基肉桂酸酯、2-乙基己基-α-氰基-β-苯基肉桂酸酯、甘油单-2-乙基己酰基-二对甲氧基肉桂酸酯等);二苯甲酮系紫外线吸收剂(例如2,4-二羟基二苯甲酮、2,2'-二羟基-4-甲氧基二苯甲酮、2,2'-二羟基-4,4'-二甲氧基二苯甲酮、2,2',4,4'-四羟基二苯甲酮、2-羟基-4-甲氧基二苯甲酮、2-羟基-4-甲氧基-4'-甲基二苯甲酮、2-羟基-4-甲氧基二苯甲酮-5-磺酸盐、4-苯基二苯甲酮、2-乙基己基-4'-苯基-二苯甲酮-2-甲酸酯、2-羟基-4-正辛氧基二苯甲酮、4-羟基-3-羧基二苯甲酮等);3-(4'-甲基苯甲叉基)-d,l-樟脑、3-苯甲叉基-d,l-樟脑;2-苯基-5-甲基苯并噁唑;2,2'-羟基-5-甲基苯基苯并三唑;2-(2'-羟基-5'-叔辛基苯基)苯并三唑;2-(2'-羟基-5'-甲基苯基苯并三唑;dibenzalazine(ジベンザラジン);二茴香酰基甲烷;4-甲氧基-4'-叔丁基二苯甲酰基甲烷;5-(3,3-二甲基-2-降冰片叉基)-3-戊烷-2-酮等。
作为其它的可配合成分,可以举出例如防腐剂(尼泊金乙酯、尼泊金丁酯等);美白剂(例如胎盘提取物、虎耳草提取物、熊果苷等);血液循环促进剂(烟酸、烟酸苯甲酯、烟酸生育酚酯、烟酸β-丁氧基酯、米诺地尔或其类似物、维生素E类、γ-谷维素、烷氧基羰基吡啶N-氧化物、卡普氯铵、和乙酰胆碱或其衍生物等);各种提取物(例如姜、黄柏、黄连、紫根、桦木、枇杷、胡萝卜、芦荟、锦葵、鸢尾、葡萄、丝瓜、百合、藏红花、川芎、生姜、小连翘、芒柄花、大蒜、辣椒、陈皮、当归、牡丹、海藻等)、活化剂(例如泛醇乙基醚、烟酰胺、生物素、泛酸、蜂王浆、胆固醇衍生物等);抗脂漏剂(例如吡哆醇类、二甲噻蒽等)等。
作为本发明的油性化妆品,可以举出例如唇彩、打底用的唇底膏、顶涂口红、唇膏等唇用化妆品、眼影、粉底等。这些之中,优选为唇用化妆品。
实施例
针对本发明,以下举出实施例进一步详细描述,但本发明不以任何方式受其限定。配合量只要没有特别限制,其成分以相对于所配合的体系的质量%表示。
实施例的说明之前,针对本发明中使用的评价试验方法进行说明。
评价(1):妆容的哑光感
专门小组成员10名在唇上涂布试样,评价妆容的哑光感和涂布时的顺滑度。评价通过与标准品的比较进行。
妆容的哑光感:1(没有)←2(几乎没有)←3(标准)→4(略有)→5(有)
A:平均分为4.5分以上
B:平均分为3.5分以上且低于4.5分
C:平均分为2.5分以上且低于3.5分
D:平均分为1.5分以上且低于2.5分
E:平均分低于1.5分。
评价(2):稳定性
将试样10g加温填充于塑料罐3-100 透明(50ml)(シントー化学公司制)中,试样固化后,将塑料罐横向固定,评价在25℃或37℃下保存24小时后的稳定性(漏油的有无)。
A:完全没有发现漏油。
B:发现油成分的漏油。
C:以到达罐的上部的程度漏油。
D:以从罐的上部漏出的程度漏油。
本发明人等通过常规方法制造下表1所示的油性化妆品(唇彩),通过上述评价方法测定。结果示于表1。
(*1):部分交联型硅酮的二甲基聚硅氧烷膨润组合物;Dow Corning 9041Silicone Elastomer Blend(东レ·ダウコーニング·シリコーン株式会社制)
部分交联型硅酮:二甲基聚硅氧烷=16:84(wt/wt)
(*2)AEROSIL R972(日本AEROSIL株式会社制)。
根据表1可知,如果在包含交联型有机聚硅氧烷和无定形硅酸酐的油性化妆品中配合具有糖骨架的油性胶凝剂,则能够提高哑光感和稳定性。
此外,可知如果增加具有糖骨架的油性胶凝剂的配合量,则得到高温稳定性优异的化妆品。
接着,发明人对改变(a)交联型有机聚硅氧烷、(b)无定形硅酸酐、(e)粉末各自的配合量的情况进行评价。评价方法与上表1的方法相同。
结果示于表2~4。
由表2可知,如果不使用(a)交联型有机聚硅氧烷,则得不到作为本发明的效果的哑光感和稳定性。
由表3可知,如果加入(b)无定形硅酸酐,则感到哑光感,稳定性进一步提高。
由表4可知,通过增加(e)粉末的总量,特别是哑光感提高。
这些本发明人等的研究的结果是,本发明所涉及的油性化妆品的特征在于,包含(a)交联型有机聚硅氧烷、(b)无定形硅酸酐、(c)具有糖骨架的油性胶凝剂、(d)液态油成分、(e)粉末。
以下举出本发明所涉及的油性化妆品的配方例。本发明不因该配方例而受到任何限定,其不必说是由权利要求书确定的。
配方例1:唇彩
成分 配合量(重量%)
部分交联型硅酮膨润组合物(*1) 30.00%
二甲基甲硅烷基化二氧化硅(*2) 3.50%
棕榈酸糊精酯 5.00%
二甲基聚硅氧烷 18.50%
三(2-乙基己酸)甘油酯 15.00%
苹果酸二异硬脂基酯 7.20%
二异硬脂酸甘油酯 3.60%
聚甲基丙烯酸甲酯 10.00%
色料 7.20%。
配方例2:眼影
成分 配合量(重量%)
部分交联型硅酮膨润组合物(*1) 30.00%
二甲基甲硅烷基化二氧化硅(*2) 3.50%
棕榈酸糊精酯 5.00%
甘油三(乙基己酸)酯 16.5%
氢化聚癸烯 15.0%
云母 18.6%
氧化铁 10.5%
氧化钛 0.9%。
Claims (5)
1. 油性化妆品,其特征在于,包含下述成分(a)~(e),
(a)交联型有机聚硅氧烷 3~7质量%
(b)无定形硅酸酐
(c)具有糖骨架的油性胶凝剂
(d)液态油成分
(e)粉末 8~38质量%。
2.根据权利要求1所述的油性化妆品,其特征在于,(c)具有糖骨架的油性胶凝剂的配合量为1~15质量%。
3.根据权利要求1或2所述的油性化妆品,其特征在于,在(d)液态油成分中包含硅油和极性油成分。
4.唇用化妆品,其特征在于,为权利要求1~3中任一项所述的油性化妆品。
5.根据权利要求1所述的油性化妆品,其特征在于,(b)无定形硅酸酐的配合量为0.5~7质量%。
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- 2019-07-19 US US17/260,501 patent/US11638687B2/en active Active
- 2019-07-19 JP JP2020531393A patent/JP7401434B2/ja active Active
- 2019-07-19 CN CN201980048234.4A patent/CN112384196A/zh active Pending
- 2019-07-19 TW TW108125956A patent/TW202011925A/zh unknown
- 2019-07-19 WO PCT/JP2019/028530 patent/WO2020017650A1/ja active Application Filing
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002154918A (ja) * | 2000-11-22 | 2002-05-28 | Nippon Shikizai Inc | 油性化粧料 |
JP2009203212A (ja) * | 2008-02-29 | 2009-09-10 | Nippon Menaade Keshohin Kk | ペースト状油性化粧料組成物 |
WO2018008238A1 (ja) * | 2016-07-04 | 2018-01-11 | 信越化学工業株式会社 | 化粧料 |
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Publication number | Publication date |
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US20210299030A1 (en) | 2021-09-30 |
JP7401434B2 (ja) | 2023-12-19 |
WO2020017650A1 (ja) | 2020-01-23 |
JPWO2020017650A1 (ja) | 2021-08-02 |
TW202011925A (zh) | 2020-04-01 |
US11638687B2 (en) | 2023-05-02 |
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