CN112063223A - Method for extracting special carbon black for ink from black rock - Google Patents

Method for extracting special carbon black for ink from black rock Download PDF

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Publication number
CN112063223A
CN112063223A CN202010920257.4A CN202010920257A CN112063223A CN 112063223 A CN112063223 A CN 112063223A CN 202010920257 A CN202010920257 A CN 202010920257A CN 112063223 A CN112063223 A CN 112063223A
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CN
China
Prior art keywords
ink
black
carbon black
component
materials
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010920257.4A
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Chinese (zh)
Inventor
刘广文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huaxie Calligraphy And Painting Institute Co ltd
Original Assignee
Huaxie Calligraphy And Painting Institute Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huaxie Calligraphy And Painting Institute Co ltd filed Critical Huaxie Calligraphy And Painting Institute Co ltd
Priority to CN202010920257.4A priority Critical patent/CN112063223A/en
Publication of CN112063223A publication Critical patent/CN112063223A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/04—Carbon
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)

Abstract

The invention provides a method for extracting special carbon black for ink from black rocks, and relates to the field of ink. According to the invention, a black shale is subjected to dry purification of mineral black elements, extracted melanin, modified solid powder desalination by a scientific and technological nano technology, penetrant, colorant and adsorbent are added, the extracted element materials are softened by high-speed high-temperature equipment, and then a special high-carbon black semi-finished product for ink can be obtained; the product is widely used in printing ink, coating, plastic color master batch, offset printing ink and product characteristics, and the product is the medium and high pigment furnace carbon black with good dispersibility: stable hue, high brightness, etc.

Description

Method for extracting special carbon black for ink from black rock
Technical Field
The invention relates to the field of ink, in particular to a method for extracting special carbon black for ink from black rocks.
Background
The ink is an important material for printing packaging materials, is a sticky fluid substance with certain color, and can be used for expressing patterns and characters on a printing material through printing.
However, the prior art for extracting the carbon black special for the ink from the black rocks is not perfect, so that a method for extracting the carbon black special for the ink from the black rocks is needed.
Disclosure of Invention
The invention aims to provide a method for extracting carbon black special for ink from black rocks, so as to solve the technical problem.
In order to solve the technical problems, the invention adopts the following technical scheme: the method for extracting the carbon black special for the ink from the black rock comprises the following components:
a first component:
mineral high carbon black semi-finished product: 30-300 g;
mineral ink: 30-300 g;
direct black mineral: 30-300 g;
a second component:
petroleum black: 50-500 g;
melanin: 50-500 g;
titanium melanin: 50-500 g;
and (3) third component:
and (3) corrosion inhibitor: 5.5-15 g;
antistatic agent: 4.9-10.8 g;
oil refers to transforming agent: 16.3-23.1 g;
the ink comprises the following process flow steps:
s1: taking the first component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s2: taking the second component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s3: taking a third component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s4: taking three standby materials, unwinding in a vacuum pressurization reaction kettle, starting a heating system to heat to 100 ℃, opening a high-speed dispersion system, dispersing at a high speed for 15-25 minutes, opening the pressurization system to pressurize to 6 air pressures, continuing to disperse, pressurizing while dispersing, then opening the vacuum system to continue dispersing for 15 minutes, stopping heating, opening a water cooling system to cool to 25 ℃ at normal temperature, not opening the reaction kettle, continuing to cool for 4 hours, taking out the materials, placing in a sealed oak for two periods of cooling, taking out and subpackaging, and obtaining the special carbon black for the printing ink.
The invention has the beneficial effects that:
according to the invention, a black shale is subjected to dry purification of mineral black elements, extracted melanin, modified solid powder desalination by a scientific and technological nano technology, penetrant, colorant and adsorbent are added, the extracted element materials are softened by high-speed high-temperature equipment, and then a special high-carbon black semi-finished product for ink can be obtained;
the product is widely used in printing ink, coating, plastic color master batch, offset printing ink and product characteristics, and the product is the medium and high pigment furnace carbon black with good dispersibility: stable hue, high brightness, etc.
Detailed Description
The present invention will be further described with reference to specific embodiments for the purpose of facilitating an understanding of technical means, characteristics of creation, objectives and functions realized by the present invention, but the following embodiments are only preferred embodiments of the present invention, and are not intended to be exhaustive. Based on the embodiments in the implementation, other embodiments obtained by those skilled in the art without any creative efforts belong to the protection scope of the present invention.
Specific embodiments of the present invention are described below.
Example 1
A method for extracting carbon black special for ink from black rocks comprises the following components,
a first component:
mineral high carbon black semi-finished product: 30-300 g;
mineral ink: 30-300 g;
direct black mineral: 30-300 g;
a second component:
petroleum black: 50-500 g;
melanin: 50-500 g;
titanium melanin: 50-500 g;
and (3) third component:
and (3) corrosion inhibitor: 5.5-15 g;
antistatic agent: 4.9-10.8 g;
oil refers to transforming agent: 16.3-23.1 g;
the ink comprises the following steps:
s1: taking the first component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s2: taking the second component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s3: taking a third component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s4: taking three standby materials, unwinding in a vacuum pressurization reaction kettle, starting a heating system to heat to 100 ℃, opening a high-speed dispersion system, dispersing at a high speed for 15-25 minutes, opening the pressurization system to pressurize to 6 air pressures, continuing to disperse, pressurizing while dispersing, then opening the vacuum system to continue dispersing for 15 minutes, stopping heating, opening a water cooling system to cool to 25 ℃ at normal temperature, not opening the reaction kettle, continuing to cool for 4 hours, taking out the materials, placing in a sealed oak for two periods of cooling, taking out and subpackaging, and obtaining the special carbon black for the printing ink.
The invention relates to a black shale, which is prepared by purifying mineral black elements by a dry method, extracting melanin, desalting modified solid powder by a scientific and technological nano technology, adding penetrant, colorant and adsorbent, softening the extracted element materials by high-speed high-temperature equipment to obtain a special high-carbon black semi-finished product for ink;
the product is widely used in printing ink, coating, plastic color master batch, offset printing ink and product characteristics, and the product is the medium and high pigment furnace carbon black with good dispersibility: stable hue, high brightness, etc.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (1)

1. The method for extracting the carbon black special for the ink from the black rock comprises the following components:
a first component:
mineral high carbon black semi-finished product: 30-300 g;
mineral ink: 30-300 g;
direct black mineral: 30-300 g;
a second component:
petroleum black: 50-500 g;
melanin: 50-500 g;
titanium melanin: 50-500 g;
and (3) third component:
and (3) corrosion inhibitor: 5.5-15 g;
antistatic agent: 4.9-10.8 g;
oil refers to transforming agent: 16.3-23.1 g;
the ink comprises the following process flow steps:
s1: taking the first component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s2: taking the second component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s3: taking a third component, and uniformly stirring the three materials by a high-speed stirrer for later use;
s4: taking three standby materials, unwinding in a vacuum pressurization reaction kettle, starting a heating system to heat to 100 ℃, opening a high-speed dispersion system, dispersing at a high speed for 15-25 minutes, opening the pressurization system to pressurize to 6 air pressures, continuing to disperse, pressurizing while dispersing, then opening the vacuum system to continue dispersing for 15 minutes, stopping heating, opening a water cooling system to cool to 25 ℃ at normal temperature, not opening the reaction kettle, continuing to cool for 4 hours, taking out the materials, placing in a sealed oak for two periods of cooling, taking out and subpackaging, and obtaining the special carbon black for the printing ink.
CN202010920257.4A 2020-09-04 2020-09-04 Method for extracting special carbon black for ink from black rock Pending CN112063223A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010920257.4A CN112063223A (en) 2020-09-04 2020-09-04 Method for extracting special carbon black for ink from black rock

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010920257.4A CN112063223A (en) 2020-09-04 2020-09-04 Method for extracting special carbon black for ink from black rock

Publications (1)

Publication Number Publication Date
CN112063223A true CN112063223A (en) 2020-12-11

Family

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CN202010920257.4A Pending CN112063223A (en) 2020-09-04 2020-09-04 Method for extracting special carbon black for ink from black rock

Country Status (1)

Country Link
CN (1) CN112063223A (en)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070109377A1 (en) * 2005-10-31 2007-05-17 Seiko Epson Corporation Ink set containing at least three black ink compositions
JP2008163063A (en) * 2006-12-27 2008-07-17 Toyo Ink Mfg Co Ltd Printing ink composition
CN101481108A (en) * 2009-02-23 2009-07-15 上海焦化化工发展商社 Method for producing easy to disperse black carbon
CN103013224A (en) * 2012-12-27 2013-04-03 茂名阪田油墨有限公司 Planographic printing ink containing high-concentration kaolin and preparation method thereof
CN103849036A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Color master batch capable of coloring polyethylene with carbon black
CN108624128A (en) * 2018-06-08 2018-10-09 奥莱鑫科技股份有限公司 A kind of environment-friendly type freezes off black ink and its production technology
CN109535834A (en) * 2018-10-24 2019-03-29 嘉兴凯兴达新材料科技有限公司 A kind of preparation method of novelty painting and calligraphy prepared Chinese ink
CN110564207A (en) * 2019-08-22 2019-12-13 苏州市贝特利高分子材料股份有限公司 butanone wiping resistant black ink for insulation intaglio printing on film material
CN110964377A (en) * 2019-11-20 2020-04-07 华协书画院有限公司 Ink with good mineral bonding effect extracted from silica and preparation method thereof

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070109377A1 (en) * 2005-10-31 2007-05-17 Seiko Epson Corporation Ink set containing at least three black ink compositions
JP2008163063A (en) * 2006-12-27 2008-07-17 Toyo Ink Mfg Co Ltd Printing ink composition
CN101481108A (en) * 2009-02-23 2009-07-15 上海焦化化工发展商社 Method for producing easy to disperse black carbon
CN103849036A (en) * 2012-12-04 2014-06-11 青岛三利中德美水设备有限公司 Color master batch capable of coloring polyethylene with carbon black
CN103013224A (en) * 2012-12-27 2013-04-03 茂名阪田油墨有限公司 Planographic printing ink containing high-concentration kaolin and preparation method thereof
CN108624128A (en) * 2018-06-08 2018-10-09 奥莱鑫科技股份有限公司 A kind of environment-friendly type freezes off black ink and its production technology
CN109535834A (en) * 2018-10-24 2019-03-29 嘉兴凯兴达新材料科技有限公司 A kind of preparation method of novelty painting and calligraphy prepared Chinese ink
CN110564207A (en) * 2019-08-22 2019-12-13 苏州市贝特利高分子材料股份有限公司 butanone wiping resistant black ink for insulation intaglio printing on film material
CN110964377A (en) * 2019-11-20 2020-04-07 华协书画院有限公司 Ink with good mineral bonding effect extracted from silica and preparation method thereof

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Application publication date: 20201211