CN110964377A - Ink with good mineral bonding effect extracted from silica and preparation method thereof - Google Patents

Abstract

The invention discloses ink with a good bonding effect of minerals extracted from silica and a preparation method thereof, and relates to the technical field of ink stick preparation. The adhesive comprises, by weight, 1-8 parts of an anionic active agent, 1-8 parts of a nonionic active agent, 2-6 parts of a solid gum surfactant, 1-2 parts of an animal gum, 2-3 parts of a vegetable gum, 10-15 parts of a thickening agent, 10-15 parts of a dispersing agent, 15-25 parts of deionized water, 30-32 parts of a silica, 5-8 parts of a stabilizing agent, 2-3 parts of an aromatic agent and the balance of soft water. The prepared ink is non-toxic and harmless, has high pasting effect, strong permeability and high bonding strength, and not only has good appearance, but also cannot delaminate and decolor.

Description

Ink with good mineral bonding effect extracted from silica and preparation method thereof

Technical Field

The invention relates to the technical field of ink stick preparation, in particular to ink with a good bonding effect of minerals extracted from silica and a preparation method thereof.

Background

The ink is generally called as black liquid or solid, Chinese seems to have a preference for black, and the calligraphy and painting arts in two thousand years are not said, and the pottery which is more than four thousand years ago is also the oriental-specific full black pottery which is used besides the ink color on the colored pottery. The inscriptions on the carapace bone are written first and then engraved with ink, the inscriptions on the West Qin text are written with pen on bamboo slips, wooden slips and coarse silk, however, the ink used in the middle and old age period is different from the one used in the eastern Han and the later, some are natural ore graphite, and some are silicon graphite fired by charcoal.

The traditional black ink formula is prepared from organic matters, and the main materials are as follows: silica stone, bone glue, glycerol, urea, compound copper amino acid, Turkey red oil, grade A silicone oil, direct black, ethylene glycol, polyvinyl alcohol and gelatin.

Chinese patent No. CN201811246338.X discloses a preparation method of novel ink for painting and calligraphy, which comprises the following steps: A. weighing raw materials; B. putting 50% of the weighed water-based acrylic resin, high-pigment silica, dispersing agent, wetting agent and soft water into a stirring tank, and stirring for 20-40 min to form slurry; C. then putting the mixture into a grinding machine, and grinding for 30-50 min; D. putting into a dispersion tank, continuously stirring, adding the stabilizer, the antioxidant, the mildew preventive and the spice, gradually adding the rest soft water, and performing performance test while stirring until reaching the set performance index, or discarding; E. and after the set performance index is reached, sieving by a 120-mesh sieve, and filling into a product. The novel calligraphy and painting ink prepared by the preparation method of the novel calligraphy and painting ink is not easy to rot and deteriorate, and has good brightness and fastness; high solid content and low viscosity; the fineness is small, and the dispersion effect is good; reasonable proportion, large tension and no burr seepage on the rice paper.

Chinese patent No. CN201710329989.4 discloses an ink with high glossiness, which is prepared from the following raw materials in parts by weight: 10-15 parts of a coloring agent, 10-15 parts of Arabic gum, 10-15 parts of a graphene dispersion liquid, 1-3 parts of lignosulfonate, 2-5 parts of borax, 2-5 parts of fatty alcohol-polyoxyethylene ether, 0.05-0.2 part of an aromatic and 15-25 parts of deionized water. The prepared ink has high writing attachment fastness, brightness, elegance, suitability for both writing and painting, easy drying of ink marks, easy rubbing and mounting and certain antibacterial capability. However, the ink produced by the two methods has poor pasting effect, is easy to delaminate and decolor, and is inconvenient to store.

An effective solution to the problems in the related art has not been proposed yet.

Disclosure of Invention

The invention provides ink with good bonding effect of minerals extracted from silica and a preparation method thereof, aiming at solving the technical problems in the prior art.

In order to solve the technical problems, the invention is realized by the following technical scheme:

the invention provides ink with a good mineral bonding effect extracted from silica, which comprises, by weight, 1-8 parts of an anionic active agent, 1-8 parts of a nonionic active agent, 2-6 parts of a solid gum surfactant, 1-2 parts of animal gum, 2-3 parts of vegetable gum, 10-15 parts of a thickening agent, 10-15 parts of a dispersing agent, 15-25 parts of deionized water, 30-32 parts of silica, 5-8 parts of a stabilizing agent, 2-3 parts of an aromatic and the balance of soft water.

Further, silica is a main mineral body, and the silica powder is a main material.

Further, the thickening agent is one of peach gum, Arabic gum and guar gum, and the thickening agent is food grade.

Further, the stabilizer is food grade, and the aromatic is one or more of clove, sandalwood or agastache.

The preparation method of the ink with good bonding effect of the minerals extracted from the silica comprises the following steps:

s1, primary processing:

(1) 1-8 parts of anionic active agent, 1-8 parts of nonionic active agent, 2-6 parts of solid gum surfactant, 1-2 parts of animal gum and 2-3 parts of vegetable gum are prepared by entering the materials into special chemical equipment according to a batching procedure;

(2) pouring the prepared solid powder into a prepared storage box;

(3) turning on a prepared storage switch, operating an equipment production line, turning on a gas switch, and adjusting the radiation degree of a spray gun;

(4) performing balanced antistatic treatment;

s2, reprocessing: pouring the materials to be ground into a grinder according to the parts by weight, and grinding the materials to be ground until the particle size is 5-6 microns;

s3, (1) adding a part of water according to the prescription amount into a container, adding a bonding material under stirring, heating to 90-95 ℃, and swelling to form sol;

(2) adding the rest of the prescribed amount of water and silica stone into the obtained sol in sequence for grinding to obtain grinding liquid ink;

(3) sieving the obtained grinding fluid, and adding the rest materials such as aromatic agent and the like under stirring at 90-95 ℃ to obtain a mixed solution;

(4) and (3) adjusting the pH of the obtained mixed solution to 8-9 by using a pH regulator, sieving, standing, and finally bottling to obtain the ecological environment-friendly ink.

By the method, the prepared ink with good bonding effect of the minerals extracted from the silica is as follows: the ink powder material prepared from the anionic active agent, the nonionic active agent, the solid gum surfactant, the animal gum and the vegetable gum according to a certain weight ratio is non-toxic and harmless, has high pasting effect, strong permeability and large bonding force, and not only has good appearance but also can not delaminate and decolor.

Detailed Description

Example 1:

an ink with good binding effect of minerals extracted from silica and a preparation method thereof comprise the following steps:

s1, primary processing:

(1) 1 part of anionic active agent, 1 part of nonionic active agent, 2 parts of solid gum surfactant, 1 part of animal gum and 2 parts of vegetable gum are put into special chemical equipment according to the burdening procedure to prepare;

(2) pouring the prepared solid powder into a prepared storage box;

(3) turning on a prepared storage switch, operating an equipment production line, turning on a gas switch, and adjusting the radiation degree of a spray gun;

(4) performing balanced antistatic treatment;

s2, reprocessing: pouring the materials to be ground into a grinder according to the parts by weight, and grinding the materials until the particle size is 5 microns;

s3, (1) adding a part of water according to the prescription amount into a container, adding the binder under stirring, heating to 90 ℃, and swelling to form sol;

(2) adding the rest of the prescribed amount of water and silica stone into the obtained sol in sequence for grinding to obtain grinding fluid;

(3) sieving the obtained grinding fluid, adding rest materials such as aromatic agent under stirring at 90 deg.C to obtain mixed solution;

(4) and (3) adjusting the pH of the obtained mixed solution to 8 by using a pH regulator, sieving, standing, and finally bottling to obtain the ecological environment-friendly ink.

Example 2:

an ink with good binding effect of minerals extracted from silica and a preparation method thereof comprise the following steps:

s1, primary processing:

(1) 4 parts of anionic active agent, 4 parts of nonionic active agent, 4 parts of solid gum surfactant, 1 part of animal gum and 2 parts of vegetable gum are put into special chemical equipment according to the burdening procedure to prepare;

(2) pouring the prepared solid powder into a prepared storage box;

(3) turning on a prepared storage switch, operating an equipment production line, turning on a gas switch, and adjusting the radiation degree of a spray gun;

(4) performing balanced antistatic treatment;

s2, reprocessing: pouring the materials to be ground into a grinder according to the parts by weight, and grinding the materials until the particle size is 6 microns;

s3, (1) adding a part of water according to the prescription amount into a container, adding the binder under stirring, heating to 93 ℃, and swelling to form sol;

(2) adding the rest of the prescribed amount of water and silica stone into the obtained sol in sequence for grinding to obtain grinding liquid ink;

(3) sieving the obtained grinding fluid, adding rest materials such as aromatic agent under stirring at 93 deg.C to obtain mixed solution;

(4) and (3) adjusting the pH of the obtained mixed solution to 8 by using a pH regulator, sieving, standing, and finally bottling to obtain the ecological environment-friendly ink.

Example 3:

an ink with good binding effect of minerals extracted from silica and a preparation method thereof comprise the following steps:

s1, primary processing:

(1) 8 parts of anionic active agent, 8 parts of nonionic active agent, 6 parts of solid gum surfactant, 2 parts of animal gum and 3 parts of vegetable gum are put into special chemical equipment according to the burdening procedure to prepare inorganic nano solid powder;

(2) pouring the prepared solid powder into a prepared storage box;

(3) turning on a prepared storage switch, operating an equipment production line, turning on a gas switch, and adjusting the radiation degree of a spray gun;

(4) performing balanced antistatic treatment;

s2, reprocessing: pouring the materials to be ground into a grinder according to the parts by weight, and grinding the materials until the particle size is 6 microns;

s3, (1) adding a part of water according to the prescription amount into a container, adding the binder under stirring, heating to 95 ℃, and swelling to form sol;

(2) adding the rest of the prescribed amount of water and silica stone into the obtained sol in sequence for grinding to obtain grinding liquid ink;

(3) sieving the obtained grinding fluid, adding rest materials such as aromatic agent under stirring at 95 deg.C to obtain mixed solution;

(4) and (3) adjusting the pH of the obtained mixed solution to 9 by using a pH regulator, sieving, standing, and finally bottling to obtain the ecological environment-friendly ink.

The prepared ink with good bonding effect of minerals extracted from the silica is as follows: the ink powder material prepared from the anionic active agent, the nonionic active agent, the solid gum surfactant, the animal gum and the vegetable gum according to a certain weight ratio is non-toxic and harmless, has high pasting effect, strong permeability and large bonding force, and not only has good appearance but also can not delaminate and decolor.

The results of the ink of the present invention compared to a certain brand of ink on the market are shown in the following table:

the above description is only exemplary of the present invention, and the present invention is not limited thereto, and any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (5)

1. The ink with good mineral bonding effect extracted from the silica is characterized by comprising, by weight, 1-8 parts of an anionic active agent, 1-8 parts of a nonionic active agent, 2-6 parts of a solid gum surfactant, 1-2 parts of an animal gum, 2-3 parts of a vegetable gum, 10-15 parts of a thickening agent, 10-15 parts of a dispersing agent, 15-25 parts of deionized water, 30-32 parts of the silica, 5-8 parts of a stabilizing agent, 2-3 parts of an aromatic and the balance of soft water.

2. The ink as claimed in claim 1, wherein the silica is a main mineral and the silica powder is a main material.

3. The ink as claimed in claim 1, wherein the thickener is one of peach gum, gum arabic and guar gum, and the thickener is food grade.

4. The ink as claimed in claim 1, wherein the stabilizer is food grade, and the aromatic agent is one or more selected from clove, sandalwood and agastache rugosa.

5. A method of making an ink having a good binding effect of a silica-extracted mineral according to any one of claims 1 to 4, comprising the steps of:

s1, primary processing:

(1) 1-8 parts of anionic active agent, 1-8 parts of nonionic active agent, 2-6 parts of solid gum surfactant, 1-2 parts of animal gum and 2-3 parts of vegetable gum are prepared by entering the materials into special chemical equipment according to a batching procedure;

(2) pouring the prepared solid powder into a prepared storage box;

(3) turning on a prepared storage switch, operating an equipment production line, turning on a gas switch, and adjusting the radiation degree of a spray gun;

(4) performing balanced antistatic treatment;

s2, reprocessing: pouring the materials to be ground into a grinder according to the parts by weight, and grinding the materials to be ground until the particle size is 5-6 microns;

s3, (1) adding a part of water according to the prescription amount into a container, adding a bonding material under stirring, heating to 90-95 ℃, and swelling to form sol;

(2) adding the rest of the prescribed amount of water and silica stone into the obtained sol in sequence for grinding to obtain grinding liquid ink;

(3) sieving the obtained grinding fluid, and adding the rest materials such as aromatic agent and the like under stirring at 90-95 ℃ to obtain a mixed solution;

(4) and (3) adjusting the pH of the obtained mixed solution to 8-9 by using a pH regulator, sieving, standing, and finally bottling to obtain the ecological environment-friendly ink.