CN109251585A - A kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance and preparation method thereof - Google Patents
A kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance and preparation method thereof Download PDFInfo
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- CN109251585A CN109251585A CN201810856704.7A CN201810856704A CN109251585A CN 109251585 A CN109251585 A CN 109251585A CN 201810856704 A CN201810856704 A CN 201810856704A CN 109251585 A CN109251585 A CN 109251585A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of dry company's degree, anti-stick dirty performance and the strong water-based inks of heat resistance and preparation method thereof, including following composition by weight: 45-60 parts of prepolymer, 10-30 parts of solvent, 25-55 parts of environmental-friendly pigment, 40-55 parts of adhesion promoter, 45-65 parts of monomer reactivity agent, solvent includes following composition by weight: 5-16 parts of terpinol, 3-9 parts of diethylene glycol ether acetate, 2-6 parts of phosphoric acid propane diamine, environmental-friendly pigment include following composition by weight: 16-25 parts of titanium dioxide, 25-42 parts of lead-free glass powder, 22-30 parts of silane coupling agent；The following steps are included: S1: weighing proportion, S2: mixing environmental-friendly pigment, S3: production prepolymer, S4: production adhesion promoter, S5: production monomer reactivity agent, S6: addition solvent.Inventive formulation is more scientific and reasonable, water-based ink can be made quickly to dry, and has centainly stain, and glutinous viscosity is relatively low, is also equipped with the characteristic of heat resisting, application range is than wide.
Description
Technical field
The present invention relates to a kind of water-based ink production field, specially a kind of dry company degree, anti-stick dirty performance and heat resistance
Strong water-based ink.
The present invention relates to a kind of water-based ink preparation method field, specially a kind of dry company degree, anti-stick dirty performance and resistance to
The preparation method of hot strong water-based ink.
Background technique
Water-based ink is mainly formed by water-soluble resin, organic pigment, solvent and related auxiliaries through abrasive machining,
Water-based ink requires stringent packages printing to produce especially suitable for sanitary conditions such as cigarette, wine, food, beverage, drug, toys for children
Product disclose a kind of scraped water of flexible version printing in Chinese invention patent application prospectus CN102558961B
Property ink and preparation method thereof, change the production procedure of water-based ink to shorten preparation time and production process, but it is prepared
Water-based ink there is no characteristic, be unable to high temperature resistant, preventing stick dirty is very poor, and dry speed is very slow.
Summary of the invention
The purpose of the present invention is to provide a kind of dry company's degree, anti-stick dirty performance and the strong water-based inks and its system of heat resistance
Preparation Method, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme: a kind of drying company degree, anti-stick dirty performance and heat resistance
Strong water-based ink, including following composition by weight: 45-60 parts of prepolymer, 10-30 parts of solvent, 25-55 parts of environmental-friendly pigment, attachment
40-55 parts of power promotor, 45-65 parts of monomer reactivity agent；
Solvent includes following composition by weight: 5-16 parts of terpinol, 3-9 parts of diethylene glycol ether acetate, phosphoric acid propane diamine 2-6
Part；
Environmental-friendly pigment includes following composition by weight: 16-25 parts of titanium dioxide, 25-42 parts of lead-free glass powder, silane coupling agent 22-30
Part.
Preferably, the prepolymer is polyester acrylate, urethane acrylate, epoxy acrylate, polyethers propylene
One or more of acid esters and unsaturated polyester (UP).
Preferably, the polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate with not
Saturated polyester mass ratio is 1.1:1.5:2.1:3.1:4.
Preferably, the adhesion promoter is methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate
One or more of monomer and acrylic acid dicyclopentadiene ester monomer.
Preferably, the methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers and acrylic acid are double
Cyclopentadiene ester monomer mass ratio is 1.7:2:2.5:3.1.
Preferably, the monomer reactivity agent is acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl
One or more of ester.
Preferably, the mass ratio of the acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester is
0.5:1:2.1.
A kind of preparation method of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, comprising the following steps:
S1: proportion is weighed, required raw material is weighed, is taken according to a certain percentage, and is stored；
S2: mixing the raw material of environmental-friendly pigment, and load weighted silane coupling agent and lead-free glass powder are put into closed mixing plant
Middle tentatively to be stirred, mixing time 1-5h, the temperature of mixing plant is controlled at 30-65 degrees Celsius, then through cooling, filtering,
After drying and grinding, modified lead-free glass powder is obtained, modified lead-free glass powder is mixed with titanium valve, by adequately stirring
It is mixed to get environmental-friendly pigment；
S3: production prepolymer, by polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate with not
One or more of saturated polyester is mixed, mixing time 0.5-2h, stands after stirring sufficiently；
S4: production adhesion promoter, by methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers with
One or more of acrylic acid dicyclopentadiene ester monomer is mixed, mixing time 0.5-1h, stands after stirring sufficiently；
S5: production monomer reactivity agent, by one in acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester
Kind or it is several according to mass ratio be 0.5:1:2.1 mixed；
S6: addition solvent mixes environmental-friendly pigment, prepolymer, adhesion promoter and monomer reactivity agent, then to mixing
Solvent mixing is added in solution, is again stirring for 0.1-0.5h, is stood 1-2h, is completed.
Compared with prior art, the beneficial effects of the present invention are: formula and preparation method of the invention is simple, therefore can
Production cost is reduced, formula is more scientific and reasonable, water-based ink can be made quickly to dry, and have certain bear dirty
Property, glutinous viscosity is relatively low, is also equipped with the characteristic of heat resisting, application range is than wide.
Detailed description of the invention
Fig. 1 is preparation method flow chart of the invention.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment one
The present invention provides a kind of technical solution: a kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, including with
Lower composition by weight: 45-60 parts of prepolymer, 10-30 parts of solvent, 25-55 parts of environmental-friendly pigment, 40-55 parts of adhesion promoter, monomer
45-65 parts of activating agent；
Wherein, solvent includes following composition by weight: 5-16 parts of terpinol, 3-9 parts of diethylene glycol ether acetate, phosphoric acid propane diamine
2-6 parts；
Environmental-friendly pigment includes following composition by weight: 16-25 parts of titanium dioxide, 25-42 parts of lead-free glass powder, silane coupling agent 22-30
Part, prepolymer is polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate and unsaturated polyester (UP)
One or more of, adhesion promoter is methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers
One or more of with acrylic acid dicyclopentadiene ester monomer, monomer reactivity agent is acryloyl morpholine, two propylene of tripropylene glycol
One or more of acid esters and hexanediyl ester.
A kind of preparation method of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, comprising the following steps:
S1: proportion is weighed, required raw material is weighed, is taken according to a certain percentage, and is stored；
S2: mixing the raw material of environmental-friendly pigment, and load weighted silane coupling agent and lead-free glass powder are put into closed mixing plant
Middle tentatively to be stirred, mixing time 1-5h, the temperature of mixing plant is controlled at 30-65 degrees Celsius, then through cooling, filtering,
After drying and grinding, modified lead-free glass powder is obtained, modified lead-free glass powder is mixed with titanium valve, by adequately stirring
It is mixed to get environmental-friendly pigment；
S3: production prepolymer, by polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate with not
One or more of saturated polyester is mixed, mixing time 0.5-2h, stands after stirring sufficiently；
S4: production adhesion promoter, by methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers with
One or more of acrylic acid dicyclopentadiene ester monomer is mixed, mixing time 0.5-1h, stands after stirring sufficiently；
S5: production monomer reactivity agent, by one in acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester
Kind or it is several according to mass ratio be 0.5:1:2.1 mixed；
S6: addition solvent mixes environmental-friendly pigment, prepolymer, adhesion promoter and monomer reactivity agent, then to mixing
Solvent mixing is added in solution, is again stirring for 0.1-0.5h, is stood 1-2h, is completed.
Embodiment two
The present invention provides a kind of technical solution: a kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, including with
Lower composition by weight: 20-30 parts of prepolymer, 30-50 parts of solvent, 10-25 parts of environmental-friendly pigment, 20-35 parts of adhesion promoter, monomer
15-30 parts of activating agent；
Solvent includes following composition by weight: 15-20 parts of terpinol, 10-15 parts of diethylene glycol ether acetate, phosphoric acid propane diamine
20-30 parts；
Environmental-friendly pigment includes following composition by weight: 3-4 parts of titanium dioxide, 5-15 parts of lead-free glass powder, 10-20 parts of silane coupling agent,
Prepolymer is in polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate and unsaturated polyester (UP)
One or more, adhesion promoter are methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers and third
One or more of olefin(e) acid dicyclopentadiene ester monomer, monomer reactivity agent are acryloyl morpholine, tripropylene glycol diacrylate
One or more of with hexanediyl ester.
A kind of preparation method of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, comprising the following steps:
S1: proportion is weighed, required raw material is weighed, is taken according to a certain percentage, and is stored；
S2: mixing the raw material of environmental-friendly pigment, and load weighted silane coupling agent and lead-free glass powder are put into closed mixing plant
Middle tentatively to be stirred, mixing time 1-5h, the temperature of mixing plant is controlled at 70-80 degrees Celsius, then through cooling, filtering,
After drying and grinding, modified lead-free glass powder is obtained, modified lead-free glass powder is mixed with titanium valve, by adequately stirring
It is mixed to get environmental-friendly pigment；
S3: production prepolymer, by polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate with not
One or more of saturated polyester is mixed, mixing time 0.5-2h, stands after stirring sufficiently；
S4: production adhesion promoter, by methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers with
One or more of acrylic acid dicyclopentadiene ester monomer is mixed, mixing time 0.5-1h, stands after stirring sufficiently；
S5: production monomer reactivity agent, by one in acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester
Kind or it is several according to mass ratio be 1:2.1:4.3 mixed；
S6: addition solvent mixes environmental-friendly pigment, prepolymer, adhesion promoter and monomer reactivity agent, then to mixing
Solvent mixing is added in solution, is again stirring for 0.1-0.5h, is stood 1-2h, is completed.
By comparing experiment to above-mentioned two groups of embodiments, it can be derived that every group of embodiment can prepare aqueous oil
Ink, the water-based ink function that wherein prepared by embodiment one best, of the invention formula and simple production process, therefore can reduce
Production cost, formula is more scientific and reasonable, water-based ink can be made quickly to dry, and has centainly stain, sticks
Viscosity is relatively low, is also equipped with the characteristic of heat resisting, application range is than wide.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance, which is characterized in that including following weight group
Part: 45-60 parts of prepolymer, 10-30 parts of solvent, 25-55 parts of environmental-friendly pigment, 40-55 parts of adhesion promoter, monomer reactivity agent
45-65 parts；
Solvent includes following composition by weight: 5-16 parts of terpinol, 3-9 parts of diethylene glycol ether acetate, phosphoric acid propane diamine 2-6
Part；
Environmental-friendly pigment includes following composition by weight: 16-25 parts of titanium dioxide, 25-42 parts of lead-free glass powder, silane coupling agent 22-30
Part.
2. a kind of dry company's degree according to claim 1, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the prepolymer is polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate and unsaturation
One or more of polyester.
3. a kind of dry company's degree according to claim 2, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate and unsaturated polyester (UP) quality
Than for 1.1:1.5:2.1:3.1:4.
4. a kind of dry company's degree according to claim 1, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the adhesion promoter is methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers and acrylic acid
One or more of dicyclopentadiene ester monomer.
5. a kind of dry company's degree according to claim 4, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers and acrylic acid dicyclopentadienyl ester list
Body mass ratio is 1.7:2:2.5:3.1.
6. a kind of dry company's degree according to claim 1, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the monomer reactivity agent be one of acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester or
It is several.
7. a kind of dry company's degree according to claim 6, anti-stick dirty performance and the strong water-based ink of heat resistance, feature exist
In: the mass ratio of the acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester is 0.5:1:2.1.
8. the preparation method of a kind of dry company's degree as described in claim 1, anti-stick dirty performance and the strong water-based ink of heat resistance,
Characterized by comprising the following steps:
S1: proportion is weighed, required raw material is weighed, is taken according to a certain percentage, and is stored；
S2: mixing the raw material of environmental-friendly pigment, and load weighted silane coupling agent and lead-free glass powder are put into closed mixing plant
Middle tentatively to be stirred, mixing time 1-5h, the temperature of mixing plant is controlled at 30-65 degrees Celsius, then through cooling, filtering,
After drying and grinding, modified lead-free glass powder is obtained, modified lead-free glass powder is mixed with titanium valve, by adequately stirring
It is mixed to get environmental-friendly pigment；
S3: production prepolymer, by polyester acrylate, urethane acrylate, epoxy acrylate, polyether acrylate with not
One or more of saturated polyester is mixed, mixing time 0.5-2h, stands after stirring sufficiently；
S4: production adhesion promoter, by methylpropanoic acid phosphate ester monomer, silane coupling agent, phosphorus methacrylate monomers with
One or more of acrylic acid dicyclopentadiene ester monomer is mixed, mixing time 0.5-1h, stands after stirring sufficiently；
S5: production monomer reactivity agent, by one in acryloyl morpholine, tripropylene glycol diacrylate and hexanediyl ester
Kind or it is several according to mass ratio be 0.5:1:2.1 mixed；
S6: addition solvent mixes environmental-friendly pigment, prepolymer, adhesion promoter and monomer reactivity agent, then to mixing
Solvent mixing is added in solution, is again stirring for 0.1-0.5h, is stood 1-2h, is completed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810856704.7A CN109251585A (en) | 2018-07-31 | 2018-07-31 | A kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810856704.7A CN109251585A (en) | 2018-07-31 | 2018-07-31 | A kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance and preparation method thereof |
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| Publication Number | Publication Date |
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| CN109251585A true CN109251585A (en) | 2019-01-22 |
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| CN201810856704.7A Pending CN109251585A (en) | 2018-07-31 | 2018-07-31 | A kind of dry company's degree, anti-stick dirty performance and the strong water-based ink of heat resistance and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109880436A (en) * | 2019-03-28 | 2019-06-14 | 郑州知淘信息科技有限责任公司 | A kind of plastic film flexographic printing water-based ink |
| CN109943144A (en) * | 2019-03-28 | 2019-06-28 | 郑州知淘信息科技有限责任公司 | A kind of preparation method of plastic film flexographic printing water-based ink |
| CN115595015A (en) * | 2022-07-05 | 2023-01-13 | 佛山市儒林化工有限公司（Cn） | High-temperature-resistant ultra-bright extra-white ink and preparation method thereof |
-
2018
- 2018-07-31 CN CN201810856704.7A patent/CN109251585A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109880436A (en) * | 2019-03-28 | 2019-06-14 | 郑州知淘信息科技有限责任公司 | A kind of plastic film flexographic printing water-based ink |
| CN109943144A (en) * | 2019-03-28 | 2019-06-28 | 郑州知淘信息科技有限责任公司 | A kind of preparation method of plastic film flexographic printing water-based ink |
| CN115595015A (en) * | 2022-07-05 | 2023-01-13 | 佛山市儒林化工有限公司（Cn） | High-temperature-resistant ultra-bright extra-white ink and preparation method thereof |
| CN115595015B (en) * | 2022-07-05 | 2023-11-14 | 佛山市儒林化工有限公司 | High-temperature-resistant super-bright extra-white ink and preparation method thereof |
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Application publication date: 20190122 |