CN109535834A - A kind of preparation method of novelty painting and calligraphy prepared Chinese ink - Google Patents
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink Download PDFInfo
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- CN109535834A CN109535834A CN201811246338.XA CN201811246338A CN109535834A CN 109535834 A CN109535834 A CN 109535834A CN 201811246338 A CN201811246338 A CN 201811246338A CN 109535834 A CN109535834 A CN 109535834A
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- 238000010422 painting Methods 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- 239000006229 carbon black Substances 0.000 claims abstract description 38
- 239000000049 pigment Substances 0.000 claims abstract description 38
- 239000003381 stabilizer Substances 0.000 claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000008234 soft water Substances 0.000 claims abstract description 30
- 239000003112 inhibitor Substances 0.000 claims abstract description 29
- 239000000080 wetting agent Substances 0.000 claims abstract description 29
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 28
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 28
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 28
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 28
- 239000002270 dispersing agent Substances 0.000 claims abstract description 28
- 239000003205 fragrance Substances 0.000 claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 19
- 239000007787 solid Substances 0.000 claims abstract description 18
- 230000005484 gravity Effects 0.000 claims abstract description 14
- 239000006185 dispersion Substances 0.000 claims abstract description 12
- 238000000227 grinding Methods 0.000 claims abstract description 9
- 239000002002 slurry Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims description 18
- KGRVJHAUYBGFFP-UHFFFAOYSA-N 2,2'-Methylenebis(4-methyl-6-tert-butylphenol) Chemical compound CC(C)(C)C1=CC(C)=CC(CC=2C(=C(C=C(C)C=2)C(C)(C)C)O)=C1O KGRVJHAUYBGFFP-UHFFFAOYSA-N 0.000 claims description 15
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 claims description 15
- 230000010148 water-pollination Effects 0.000 claims description 12
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical class [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 claims description 9
- -1 2- ethylhexyl Chemical group 0.000 claims description 8
- IHBCFWWEZXPPLG-UHFFFAOYSA-N [Ca].[Zn] Chemical group [Ca].[Zn] IHBCFWWEZXPPLG-UHFFFAOYSA-N 0.000 claims description 7
- 239000004283 Sodium sorbate Substances 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 6
- LROWVYNUWKVTCU-STWYSWDKSA-M sodium sorbate Chemical group [Na+].C\C=C\C=C\C([O-])=O LROWVYNUWKVTCU-STWYSWDKSA-M 0.000 claims description 6
- 235000019250 sodium sorbate Nutrition 0.000 claims description 6
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 4
- 239000003610 charcoal Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 2
- SNRUBQQJIBEYMU-NJFSPNSNSA-N dodecane Chemical group CCCCCCCCCCC[14CH3] SNRUBQQJIBEYMU-NJFSPNSNSA-N 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 11
- 235000007164 Oryza sativa Nutrition 0.000 abstract description 7
- 235000009566 rice Nutrition 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 3
- 240000007594 Oryza sativa Species 0.000 abstract 1
- 241001465754 Metazoa Species 0.000 description 6
- 241000209094 Oryza Species 0.000 description 6
- 239000003292 glue Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 108010082495 Dietary Plant Proteins Proteins 0.000 description 5
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical group OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 5
- 230000002708 enhancing effect Effects 0.000 description 5
- 229920003002 synthetic resin Polymers 0.000 description 5
- 239000000057 synthetic resin Substances 0.000 description 5
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
- 239000000549 coloured material Substances 0.000 description 4
- 239000012895 dilution Substances 0.000 description 4
- 238000010790 dilution Methods 0.000 description 4
- 238000005457 optimization Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000003643 water by type Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014103 egg white Nutrition 0.000 description 1
- 210000000969 egg white Anatomy 0.000 description 1
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 229940075582 sorbic acid Drugs 0.000 description 1
- 235000010199 sorbic acid Nutrition 0.000 description 1
- 239000004334 sorbic acid Substances 0.000 description 1
- WSWCOQWTEOXDQX-MQQKCMAXSA-N sorbic acid group Chemical group C(\C=C\C=C\C)(=O)O WSWCOQWTEOXDQX-MQQKCMAXSA-N 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
- C09D11/17—Writing inks characterised by colouring agents
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps: A, weighs raw material；B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into agitator tank, stirs 20~40min, form slurry；C, it puts into grinder again, after grinding 30~50min；D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and be gradually added into remaining soft water, be tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product.Novel painting and calligraphy prepared Chinese ink obtained by the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, it is not easy to which corruption mildew matter has good brightness and fastness；Solid content is high, and viscosity is low；Fineness is small, and dispersion effect is good；Specific gravity is reasonable, and tension is larger, is not in exudation flash phenomenon on rice paper.
Description
Technical field
The present invention relates to field of stationery, and in particular to a kind of preparation method of novelty painting and calligraphy prepared Chinese ink.
Background technique
Prepared Chinese ink is the peculiar traditional product in China, has long history in thousand, Chinese calligraphy, painting be unable to do without prepared Chinese ink.But
Prepared Chinese ink production technology, product are not but timely updated and are developed.The brand prepared Chinese ink sold on domestic market, substantially
On be all traditional production technology and raw material, be out of step with the times development need, and especially high-grade quality prepared Chinese ink market is all by one
Occupied by a little foreign brand names.
Because domestic brand prepared Chinese ink production primary raw material still rests on oil smoke, animal/vegetable protein glue composition, so that prepared Chinese ink
Store unstable with climate change, when writing, is not smooth, paints on rice paper and is easy exudation flash, using can go out often
Existing rotten mildew matter.
Based on the above situation, the invention proposes a kind of preparation methods of novel painting and calligraphy prepared Chinese ink can effectively solve above ask
Topic.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of novel painting and calligraphy prepared Chinese ink.Novel painting and calligraphy prepared Chinese ink of the invention
Preparation method, primary raw material selects the water soluble acrylic acid organic synthetic resin for improving low molecular weight to make the bonding of prepared Chinese ink
Material solves the problems, such as that existing prepared Chinese ink is easy rotten mildew matter, while enhancing prepared Chinese ink instead of original animal/vegetable protein glue
Brightness and fastness；It is made up of selected raw material, and optimization formula, both adjusts and change solid content, it is solid increasing prepared Chinese ink
The consistency of prepared Chinese ink, high-solid-content and low-viscosity, legibility, full, stream when prepared Chinese ink being made to write, paint are reduced while content
Smooth and brightness is good；Selection hydrophily high-carbon black pigment powder is coloured material, substantially increases font degree of blackness, and colour saturation is high；
It is made up of selected raw material, and optimization formula, improves the surface tension and specific gravity of prepared Chinese ink, keep prepared Chinese ink sufficiently dilute in drawing
It releases in the case where watering down, is not in exudation flash phenomenon on rice paper；Novel painting and calligraphy prepared Chinese ink of the invention is bright, painting and calligraphy stream
Freely, frost resistance is good, corrosion resistant become, easily mount it is auspicious, burnt, dense, wet, light, gently have it is good.
The present invention is achieved through the following technical solutions:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, weigh water-based acrylic resin 15~18% in terms of percentage composition, dispersing agent 3~5%, wetting agent 4~
5%, high-carbon black pigment 20~22%, stabilizer 15~20%, antioxidant 3~5%, mould inhibitor 1~2%, fragrance 1~2%,
Soft water 21~38%；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um.
The preparation method of novel painting and calligraphy prepared Chinese ink of the invention, primary raw material are selected and improve aqueous the third of low molecular weight
Olefin(e) acid organic synthetic resin makees the binding material of prepared Chinese ink, instead of original animal/vegetable protein glue, solves existing prepared Chinese ink and is easy corruption
The problem of matter of going mouldy, while enhancing the brightness and fastness of prepared Chinese ink；It is made up of selected raw material, and optimization formula, both adjusted
Solid content is changed, the consistency of prepared Chinese ink is reduced while increasing prepared Chinese ink solid content, high-solid-content and low-viscosity makes prepared Chinese ink
Legibility, full, smooth and brightness are good when writing, painting；Selection hydrophily high-carbon black pigment powder is coloured material, greatly
Font degree of blackness is improved greatly, and colour saturation is high；It is made up of selected raw material, and optimization formula, improves the surface tension of prepared Chinese ink
It in the case where making prepared Chinese ink sufficiently dilution waters down in drawing is not in exudation flash phenomenon on rice paper with specific gravity.
As a preferred embodiment, step A are as follows: weigh water-based acrylic resin 17%, the dispersing agent in terms of percentage composition
3.5%, wetting agent 4.5%, high-carbon black pigment 21%, stabilizer 17%, antioxidant 3.5%, mould inhibitor 1.4%, fragrance
1.6%, soft water 30.5%.
As a preferred embodiment, step A are as follows: weigh the water-based acrylic resin 17.5% in terms of percentage composition, disperse
Agent 3.8%, wetting agent 4.6%, high-carbon black pigment 21.5%, stabilizer 18.5%, antioxidant 4.5%, mould inhibitor 1.8%, perfume
Expect 1.7%, soft water 26.1%.
The water-based acrylic resin selects this field conventional products.As a preferred embodiment, described aqueous third
The number-average molecular weight of olefin(e) acid resin is 1500~3000g/mol.
The water soluble acrylic acid organic synthetic resin of low molecular weight makees the binding material of prepared Chinese ink, instead of original animals and plants egg
White glue solves the problems, such as that existing prepared Chinese ink is easy rotten mildew matter, while enhancing the brightness and fastness of prepared Chinese ink.
The dispersing agent selects this field conventional products.As a preferred embodiment, the dispersing agent is dodecane
Base sodium sulphate.
Prepared Chinese ink each component dispersion of the invention in this way is more uniform, and the holding time is longer, is not in precipitating etc..
The wetting agent selects this field conventional products.As a preferred embodiment, the wetting agent is bis- (2-
Ethylhexyl) Disodium sulfosuccinate.
Bis- (2- ethylhexyl) Disodium sulfosuccinates belong to one of anionic surfactant, select bis- (2- second
Base hexyl) Disodium sulfosuccinate can make the wet smoothness of prepared Chinese ink.
The high-carbon black pigment selects this field conventional products.As a preferred embodiment, the high-carbon black pigment
For hydrophily high-carbon black pigment.
Hydrophily high-carbon black pigment improves prepared Chinese ink tinctorial strength of the invention, and blackness light is gorgeous, legibility.
The stabilizer selects this field conventional products.As a preferred embodiment, the stabilizer is multiple for calcium zinc
Close stabilizer.
The antioxidant selects this field conventional products.As a preferred embodiment, the antioxidant is antioxidant
1010 and antioxidant 2246 mixture, and antioxidant 1010 and antioxidant 2246 mass ratio are 1:1.2~1.6.
Antioxidant 1010 and antioxidant 2246 are used cooperatively, and rational proportion, and it is long-term to be more advantageous to prepared Chinese ink for prepared Chinese ink after addition
Storage.
The mould inhibitor selects this field conventional products.As a preferred embodiment, the mould inhibitor is sorbic acid
Sodium.
Prevent rotten mould modification effect more preferable in this way.
Compared with prior art, the present invention have the following advantages that and the utility model has the advantages that
1, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, primary raw material are selected and improve the aqueous of low molecular weight
Acrylic acid organic synthetic resin makees the binding material of prepared Chinese ink, instead of original animal/vegetable protein glue, solves existing prepared Chinese ink and is easy
The problem of corruption mildew matter, while enhancing the brightness and fastness of prepared Chinese ink.
2, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, adjustment change solid content, are increasing prepared Chinese ink solid content
While reduce the consistency of prepared Chinese ink, high-solid-content and low-viscosity, write prepared Chinese ink, drawing when legibility, it is full, smooth and
Brightness is good.
3, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, selection hydrophily high-carbon black pigment powder are coloured material, greatly
Font degree of blackness is improved greatly, and colour saturation is high.
4, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, improves the surface tension and specific gravity of prepared Chinese ink, prepared Chinese ink is made to exist
It is not in exudation flash phenomenon on rice paper in the case that sufficiently dilution waters down when drawing.
Specific embodiment
The present invention is described in further detail below with reference to embodiment, embodiments of the present invention are not limited thereto.
Test method described in following embodiments or test method are unless otherwise specified conventional method；The examination
Agent and material are obtained from routine business approach, or prepare in conventional manner unless otherwise specified.
Embodiment 1:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, weigh water-based acrylic resin 15~18% in terms of percentage composition, dispersing agent 3~5%, wetting agent 4~
5%, high-carbon black pigment 20~22%, stabilizer 15~20%, antioxidant 3~5%, mould inhibitor 1~2%, fragrance 1~2%,
Soft water 21~38%；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um.
Embodiment 2:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, weigh water-based acrylic resin 15~18% in terms of percentage composition, dispersing agent 3~5%, wetting agent 4~
5%, high-carbon black pigment 20~22%, stabilizer 15~20%, antioxidant 3~5%, mould inhibitor 1~2%, fragrance 1~2%,
Soft water 21~38%；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um；
The number-average molecular weight of the water-based acrylic resin is 1500~3000g/mol；
The dispersing agent is lauryl sodium sulfate；
The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；
The high-carbon black pigment is hydrophily high-carbon black pigment；
The stabilizer is calcium-zinc composite stabilizing agent；
The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246, and antioxidant 1010 and antioxidant 2246
Mass ratio is 1:1.2~1.6；
The mould inhibitor is sodium sorbate.
Embodiment 3:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, water-based acrylic resin 15%, dispersing agent 3%, wetting agent 4%, the high pigment charcoal in terms of percentage composition are weighed
Black 20%, stabilizer 15%, antioxidant 3%, mould inhibitor 1%, fragrance 1%, surplus are soft water；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um；
The number-average molecular weight of the water-based acrylic resin is 1500~3000g/mol；
The dispersing agent is lauryl sodium sulfate；
The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；
The high-carbon black pigment is hydrophily high-carbon black pigment；
The stabilizer is calcium-zinc composite stabilizing agent；
The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246, and antioxidant 1010 and antioxidant 2246
Mass ratio is 1:1.2；
The mould inhibitor is sodium sorbate.
Embodiment 4:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, water-based acrylic resin 18%, dispersing agent 5%, wetting agent 5%, the high pigment charcoal in terms of percentage composition are weighed
Black 22%, stabilizer 20%, antioxidant 5%, mould inhibitor 2%, fragrance 2%, surplus are soft water；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um；
The number-average molecular weight of the water-based acrylic resin is 1500~3000g/mol；
The dispersing agent is lauryl sodium sulfate；
The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；
The high-carbon black pigment is hydrophily high-carbon black pigment；
The stabilizer is calcium-zinc composite stabilizing agent；
The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246, and antioxidant 1010 and antioxidant 2246
Mass ratio is 1:1.6；
The mould inhibitor is sodium sorbate.
Embodiment 5:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, water-based acrylic resin 17%, dispersing agent 3.5%, wetting agent 4.5%, the high color in terms of percentage composition are weighed
Plain carbon black 21%, stabilizer 17%, antioxidant 3.5%, mould inhibitor 1.4%, fragrance 1.6%, surplus are soft water；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um；
The number-average molecular weight of the water-based acrylic resin is 1500~3000g/mol；
The dispersing agent is lauryl sodium sulfate；
The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；
The high-carbon black pigment is hydrophily high-carbon black pigment；
The stabilizer is calcium-zinc composite stabilizing agent；
The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246, and antioxidant 1010 and antioxidant 2246
Mass ratio is 1:1.4；
The mould inhibitor is sodium sorbate.
Embodiment 6:
A kind of preparation method of novelty painting and calligraphy prepared Chinese ink, includes the following steps:
A, water-based acrylic resin 17.5%, dispersing agent 3.8%, wetting agent 4.6%, the height in terms of percentage composition are weighed
Colour carbon black 21.5%, stabilizer 18.5%, antioxidant 4.5%, mould inhibitor 1.8%, fragrance 1.7%, surplus are soft water；
B, it by the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, puts into
In agitator tank, 20~40min is stirred, forms slurry；
C, it puts into grinder again, after grinding 30~50min；
D, it puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and gradually
Remaining soft water is added, is tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
E, after the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to
1.1g/ml and tension are more than or equal to 50 dynes, fineness≤5um；
The number-average molecular weight of the water-based acrylic resin is 1500~3000g/mol；
The dispersing agent is lauryl sodium sulfate；
The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；
The high-carbon black pigment is hydrophily high-carbon black pigment；
The stabilizer is calcium-zinc composite stabilizing agent；
The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246, and antioxidant 1010 and antioxidant 2246
Mass ratio is 1:1.5；
The mould inhibitor is sodium sorbate.
Novel painting and calligraphy prepared Chinese ink obtained by embodiment 3-6 is tested, the results are shown in Table 1.
As can be seen from the above table, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention has the advantage that of the invention new
Novel painting and calligraphy prepared Chinese ink solid content obtained by the preparation method of clever painting and calligraphy prepared Chinese ink is high, and viscosity is low；Fineness is small, and dispersion effect is good；
Specific gravity is reasonable, and tension is larger, make prepared Chinese ink drawing when sufficiently dilution water down in the case where, be not in exudation hair on rice paper
Side phenomenon, it is burnt, dense, wet, light, gently have it is good.
Compared with prior art, the present invention have the following advantages that and the utility model has the advantages that
1, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, primary raw material are selected and improve the aqueous of low molecular weight
Acrylic acid organic synthetic resin makees the binding material of prepared Chinese ink, instead of original animal/vegetable protein glue, solves existing prepared Chinese ink and is easy
The problem of corruption mildew matter, while enhancing the brightness and fastness of prepared Chinese ink.
2, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, adjustment change solid content, are increasing prepared Chinese ink solid content
While reduce the consistency of prepared Chinese ink, high-solid-content and low-viscosity, write prepared Chinese ink, drawing when legibility, it is full, smooth and
Brightness is good.
3, the preparation method of novel painting and calligraphy prepared Chinese ink of the invention, selection hydrophily high-carbon black pigment powder are coloured material, greatly
Font degree of blackness is improved greatly, and colour saturation is high.
The preparation method of novel painting and calligraphy prepared Chinese ink of the invention, improves the surface tension and specific gravity of prepared Chinese ink, is drawing prepared Chinese ink
It is not in exudation flash phenomenon on rice paper in the case that sufficiently dilution waters down when picture.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, all
Any simple modification to the above embodiments, equivalent variations according to the technical essence of the invention, each fall within guarantor of the invention
Within the scope of shield.
Claims (5)
1. a kind of preparation method of novelty painting and calligraphy prepared Chinese ink, characterized by the following steps:
Weigh water-based acrylic resin 15~18%, dispersing agent 3~5%, wetting agent 4~5%, the high pigment charcoal in terms of percentage composition
Black 20~22%, stabilizer 15~20%, antioxidant 3~5%, mould inhibitor 1~2%, fragrance 1~2%, surplus are soft water；
By the 50% of weighed water-based acrylic resin, high-carbon black pigment, dispersing agent, wetting agent and soft water, agitator tank is put into
In, 20~40min is stirred, slurry is formed；
It puts into grinder again, after grinding 30~50min；
It puts into dispersion tank again, continues to stir, and stabilizer, antioxidant, mould inhibitor and fragrance is added, and be gradually added into residue
Soft water, be tested for the property while stirring, otherwise the performance indicator until reaching setting is discarded；
After the performance indicator for reaching setting, after 120 meshes, and it is filling at product；
The performance indicator of the setting are as follows: viscosity 40 ± 2 seconds, solid content are more than or equal to 38 ± 2%, specific gravity and are more than or equal to 1.1g/ml
It is more than or equal to 50 dynes with tension, fineness≤5um.
2. the preparation method of novelty painting and calligraphy prepared Chinese ink according to claim 1, it is characterised in that: step A are as follows: weigh with percentage
Water-based acrylic resin 17%, dispersing agent 3.5%, wetting agent 4.5%, high-carbon black pigment 21%, the stabilizer 17%, antioxygen of content meter
Agent 3.5%, mould inhibitor 1.4%, fragrance 1.6%, soft water 30.5%.
3. the preparation method of novelty painting and calligraphy prepared Chinese ink according to claim 1, it is characterised in that: step A are as follows: weigh with percentage
Water-based acrylic resin 17.5%, dispersing agent 3.8%, wetting agent 4.6%, the high-carbon black pigment 21.5%, stabilizer of content meter
18.5%, antioxidant 4.5%, mould inhibitor 1.8%, fragrance 1.7%, soft water 26.1%.
4. the preparation method of novelty painting and calligraphy prepared Chinese ink according to claim 1, it is characterised in that: the water-based acrylic resin
Number-average molecular weight be 1500~3000g/mol.
5. the preparation method of novelty painting and calligraphy prepared Chinese ink according to claim 1, it is characterised in that: the dispersing agent is dodecane
Base sodium sulphate；The wetting agent is bis- (2- ethylhexyl) Disodium sulfosuccinates；The high-carbon black pigment is the high color of hydrophily
Plain carbon black；The stabilizer is calcium-zinc composite stabilizing agent；The antioxidant is the mixture of antioxidant 1010 and antioxidant 2246,
And antioxidant 1010 and antioxidant 2246 mass ratio are 1:1.2~1.6；The mould inhibitor is sodium sorbate.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112063223A (en) * | 2020-09-04 | 2020-12-11 | 华协书画院有限公司 | Method for extracting special carbon black for ink from black rock |
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| CN105176170A (en) * | 2015-10-30 | 2015-12-23 | 河北青竹画材科技有限公司 | Water-based acrylic painting pigment and preparation method thereof |
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| CN106280827A (en) * | 2016-08-31 | 2017-01-04 | 惠州市固德尔合成材料有限公司 | A kind of high glaze water lustering oil and preparation method thereof |
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| CN1644638A (en) * | 2004-12-08 | 2005-07-27 | 贵州博士化工有限公司 | Composite aqueous ink |
| CN105176170A (en) * | 2015-10-30 | 2015-12-23 | 河北青竹画材科技有限公司 | Water-based acrylic painting pigment and preparation method thereof |
| CN105802337A (en) * | 2016-03-24 | 2016-07-27 | 陕西科技大学 | Ink based on synthetic macromolecule polymer and preparing method thereof |
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