CN105802337A - Ink based on synthetic macromolecule polymer and preparing method thereof - Google Patents
Ink based on synthetic macromolecule polymer and preparing method thereof Download PDFInfo
- Publication number
- CN105802337A CN105802337A CN201610170792.6A CN201610170792A CN105802337A CN 105802337 A CN105802337 A CN 105802337A CN 201610170792 A CN201610170792 A CN 201610170792A CN 105802337 A CN105802337 A CN 105802337A
- Authority
- CN
- China
- Prior art keywords
- chinese ink
- prepared chinese
- synthesising macromolecule
- macromolecule copolymer
- ink
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002521 macromolecule Polymers 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title abstract description 7
- 229920000642 polymer Polymers 0.000 title abstract 5
- 239000000976 ink Substances 0.000 claims abstract description 45
- 239000002270 dispersing agent Substances 0.000 claims abstract description 28
- 238000003756 stirring Methods 0.000 claims abstract description 25
- 239000006229 carbon black Substances 0.000 claims abstract description 18
- 239000010692 aromatic oil Substances 0.000 claims abstract description 17
- 239000004094 surface-active agent Substances 0.000 claims abstract description 16
- 239000000080 wetting agent Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 42
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical group OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 18
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 claims description 9
- 238000013019 agitation Methods 0.000 claims description 7
- 239000003292 glue Substances 0.000 abstract description 5
- 239000006185 dispersion Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000000855 fermentation Methods 0.000 abstract description 2
- 230000004151 fermentation Effects 0.000 abstract description 2
- 239000005416 organic matter Substances 0.000 abstract description 2
- 239000002639 bone cement Substances 0.000 abstract 2
- 230000001580 bacterial effect Effects 0.000 abstract 1
- 238000000354 decomposition reaction Methods 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000005562 fading Methods 0.000 abstract 1
- 235000019241 carbon black Nutrition 0.000 description 15
- 230000002159 abnormal effect Effects 0.000 description 9
- 235000013399 edible fruits Nutrition 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 239000002304 perfume Substances 0.000 description 9
- 230000035943 smell Effects 0.000 description 9
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
- C09D11/17—Writing inks characterised by colouring agents
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention relates to an ink based on a synthetic macromolecule polymer and a preparing method thereof. Inks sold currently in the market are mostly prepared from animal glue and bone glue and contain bacterial in air to cause fermentation and decomposition of organic matter in the inks, and therefore the inks smell bad. The ink based on the synthetic macromolecule polymer is prepared according to the steps of uniformly mixing and stirring high-fineness carbon black, a dispersing agent and a wetting agent, and conducting standing for use; adding the synthetic macromolecule polymer to water while stirring for dissolution to be used; adding a surface active agent after uniform mixing and stirring, and then adding concentrated aromatic oil, so that the ink is obtained after uniform stirring. The adopted synthetic macromolecule polymer has high dispersity and adhesiveness, and can improve the wettability and lubricity of the ink and make the ink absorbed by paper easily without blotting after being matched with the dispersing agent, the wetting agent and the surface active agent; the problem that inks smell bad when animal glue and bone glue are used is solved; furthermore, the ink is not prone to color fading or dispersion, and writing effect is good.
Description
Technical field
The present invention relates to a kind of prepared Chinese ink, be specifically related to a kind of prepared Chinese ink based on synthesising macromolecule copolymer and preparation method thereof.
Background technology
Prepared Chinese ink is a kind of product that people are commonly used in study and writing process, and consumption is very big.The prepared Chinese ink sold in the market is various in style, but many with animal glue, osseocolla for primary raw material, uses middle meeting to distribute unpleasant taste.This is because the antibacterial in air is dropped on wherein, the organic matter fermentation in prepared Chinese ink is made to rot.So needing adding preservative agent and spice, and due to the degraded of natural polymer, its serviceability can be reduced.
Summary of the invention
It is an object of the invention to provide a kind of prepared Chinese ink based on synthesising macromolecule copolymer and preparation method thereof, solve prior art and select animal glue, osseocolla to cause smelly problem, and improve its wettability and lubricity.
The technical solution adopted in the present invention is:
Prepared Chinese ink based on synthesising macromolecule copolymer, it is characterised in that:
Comprise the component of following mass percent:
High fineness white carbon black 8-18%；
Dispersant 5-10%；
Wetting agent 3-6%；
Synthesising macromolecule copolymer 6-9%；
Surfactant 1-4%；
Concentration aromatic oil 0.02-0.1%；
Surplus is water；
Described synthesising macromolecule copolymer structural formula is:
Wherein, m > 70.
Described dispersant structure formula is:
Wherein, n=2-13.
Described wetting agent is selected from ethylene glycol, propylene glycol, glycerol.
Described surfactant is selected from NPE, SAS.
Preparation method based on the prepared Chinese ink of synthesising macromolecule copolymer, it is characterised in that:
Comprise the following steps:
Step one: by high fineness white carbon black, dispersant, wetting agent stirring and evenly mixing, set aside for use；
Step 2: under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving；
Step 3: the mixture obtained in step 2 is poured in the solution of step one gained, stir；
Step 4: surfactant adds the solution obtained in step 3, is subsequently adding concentration aromatic oil, stirs and obtains prepared Chinese ink；
Described synthesising macromolecule copolymer structural formula is:
Wherein, m > 70.
Described dispersant structure formula is:
Wherein, n=2-13.
Described wetting agent is selected from ethylene glycol, propylene glycol, glycerol.
Described surfactant is selected from NPE, SAS.
The invention have the advantages that
The synthesising macromolecule copolymer that the present invention selects, there is good dispersibility and cohesive, dispersant can improve the suspension of high fineness white carbon black, wetting agent can make prepared Chinese ink sprawl uniformly, surfactant has the performances such as decontamination, moistening, emulsifying, dispersion, cohesion, improve wettability and the lubricity of prepared Chinese ink after cooperation, make prepared Chinese ink be prone to paper and not fall into oblivion；Avoiding the problem selecting animal glue, osseocolla smelly, and not fugitive color, not easily dizzy open, writing effect is good.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention will be described in detail.
The prepared Chinese ink based on synthesising macromolecule copolymer that the present invention relates to, comprises the component of following mass percent:
High fineness white carbon black 8-18%；
Dispersant 5-10%；
Wetting agent 3-6%；
Synthesising macromolecule copolymer 6-9%；
Surfactant 1-4%；
Concentration aromatic oil 0.02-0.1%；
Surplus is water.
Described synthesising macromolecule copolymer structural formula is as follows, or the mixture of following structure:
Wherein, m > 70.
Described dispersant structure formula is as follows, or the mixture of following structure:
Wherein, n=2-13.
Described wetting agent is one or more in ethylene glycol, propylene glycol, glycerol.
Described surfactant is one or more in NPE, SAS.
In above-mentioned formula, high fineness white carbon black is as coloring agent, synthesising macromolecule copolymer can as binding agent, dispersant can improve the suspension of high fineness white carbon black, wetting agent can make prepared Chinese ink sprawl uniformly, surfactant has the performances such as decontamination, moistening, emulsifying, dispersion, cohesion, and concentration aromatic oil is the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of synthetic, increases prepared Chinese ink fragrance.
The preparation method of the above-mentioned prepared Chinese ink based on synthesising macromolecule copolymer, comprises the following steps:
Step one: by high fineness white carbon black, dispersant, wetting agent stirring and evenly mixing, set aside for use；
Step 2: under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving；
Step 3: the mixture obtained in step 2 is poured in the solution of step one gained, stir；
Step 4: surfactant adds the solution obtained in step 3, is subsequently adding concentration aromatic oil, stirs and obtains prepared Chinese ink.
Described synthesising macromolecule copolymer structural formula is as follows, or the mixture of following structure:
Wherein, m > 70.
Described dispersant structure formula is as follows, or the mixture of following structure:
Wherein, n=2-13.
Described wetting agent is one or more in ethylene glycol, propylene glycol, glycerol.
Described surfactant is one or more in NPE, SAS.
Embodiment 1:
8 parts high fineness white carbon blacks, 5 parts of dispersants, 4 parts of glycerol, 7 parts of synthesising macromolecule copolymers, 2 parts of NPEs, the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of 0.03 part of synthetic, 73.97 parts of water.
Dispersant structure is as follows:
Synthesising macromolecule copolymer structural formula is as follows:
The method preparing above-mentioned prepared Chinese ink, comprises the steps
1) by high fineness white carbon black, dispersant, glycerol stirring and evenly mixing, set aside for use.
2) under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving.
3) by step 2) in the mixture that obtains pour step 1 into) in the solution of gained, stir.
4) NPE is added step 3) in the solution that obtains, be subsequently adding the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of synthetic, stir and obtain the prepared Chinese ink of the present invention.
Embodiment 2:
10 parts high fineness white carbon blacks, 8 parts of dispersants, 6 parts of glycerol, 8 parts of synthesising macromolecule copolymers, 2 parts of NPEs, the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of 0.08 part of synthetic, 65.92 parts of water.
Dispersant structure is as follows:
Synthesising macromolecule copolymer structural formula is as follows:
The method preparing above-mentioned prepared Chinese ink, comprises the steps
1) by high fineness white carbon black, dispersant, glycerol stirring and evenly mixing, set aside for use.
2) under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving.
3) by step 2) in the mixture that obtains pour step 1 into) in the solution of gained, stir.
4) NPE is added step 3) in the solution that obtains, be subsequently adding the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of synthetic, stir and obtain the prepared Chinese ink of the present invention.
Embodiment 3:
10 parts high fineness white carbon blacks, 8 parts of dispersants, 6 parts of glycerol, 8 parts of synthesising macromolecule copolymers, 2 parts of NPEs, the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of 0.1 part of synthetic, 65.9 parts of water.
Dispersant structure is as follows:
Synthesising macromolecule copolymer structural formula is as follows:
The method preparing above-mentioned prepared Chinese ink, comprises the steps
1) by high fineness white carbon black, dispersant, glycerol stirring and evenly mixing, set aside for use.
2) under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving.
3) by step 2) in the mixture that obtains pour step 1 into) in the solution of gained, stir.
4) NPE is added step 3) in the solution that obtains, be subsequently adding the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of synthetic, stir and obtain the prepared Chinese ink of the present invention.
Embodiment 4:
9 parts high fineness white carbon blacks, 7 parts of dispersants, 6 parts of glycerol, 7 parts of synthesising macromolecule copolymers, 2 parts of NPEs, the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of 0.1 part of synthetic, 68.9 parts of water.
Dispersant structure is as follows:
Synthesising macromolecule copolymer structural formula is as follows:
The method preparing above-mentioned prepared Chinese ink, comprises the steps
1) by high fineness white carbon black, dispersant, glycerol stirring and evenly mixing, set aside for use.
2) under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving.
3) by step 2) in the mixture that obtains pour step 1 into) in the solution of gained, stir.
4) NPE is added step 3) in the solution that obtains, be subsequently adding the concentration aromatic oil imitating fruit and natural perfume material abnormal smells from the patient of synthetic, stir and obtain the prepared Chinese ink of the present invention.
Present disclosure is not limited to cited by embodiment, and the conversion of any equivalence that technical solution of the present invention is taked by those of ordinary skill in the art by reading description of the present invention, the claim being the present invention is contained.
Claims (8)
1. based on the prepared Chinese ink of synthesising macromolecule copolymer, it is characterised in that:
Comprise the component of following mass percent:
High fineness white carbon black 8-18%；
Dispersant 5-10%；
Wetting agent 3-6%；
Synthesising macromolecule copolymer 6-9%；
Surfactant 1-4%；
Concentration aromatic oil 0.02-0.1%；
Surplus is water；
Described synthesising macromolecule copolymer structural formula is:
Wherein, m > 70.
2. the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 1, it is characterised in that:
Described dispersant structure formula is:
Wherein, n=2-13.
3. the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 1, it is characterised in that:
Described wetting agent is selected from ethylene glycol, propylene glycol, glycerol.
4. the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 1, it is characterised in that:
Described surfactant is selected from NPE, SAS.
5. based on the preparation method of the prepared Chinese ink of synthesising macromolecule copolymer, it is characterised in that:
Comprise the following steps:
Step one: by high fineness white carbon black, dispersant, wetting agent stirring and evenly mixing, set aside for use；
Step 2: under agitation synthesising macromolecule copolymer is added to the water, stand-by after dissolving；
Step 3: the mixture obtained in step 2 is poured in the solution of step one gained, stir；
Step 4: surfactant adds the solution obtained in step 3, is subsequently adding concentration aromatic oil, stirs and obtains prepared Chinese ink；
Described synthesising macromolecule copolymer structural formula is:
Wherein, m > 70.
6. the preparation method of the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 5, it is characterised in that:
Described dispersant structure formula is:
Wherein, n=2-13.
7. the preparation method of the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 5, it is characterised in that:
Described wetting agent is selected from ethylene glycol, propylene glycol, glycerol.
8. the preparation method of the prepared Chinese ink based on synthesising macromolecule copolymer according to claim 5, it is characterised in that:
Described surfactant is selected from NPE, SAS.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610170792.6A CN105802337B (en) | 2016-03-24 | 2016-03-24 | Prepared Chinese ink based on synthesising macromolecule copolymer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610170792.6A CN105802337B (en) | 2016-03-24 | 2016-03-24 | Prepared Chinese ink based on synthesising macromolecule copolymer and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105802337A true CN105802337A (en) | 2016-07-27 |
| CN105802337B CN105802337B (en) | 2017-11-07 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610170792.6A Expired - Fee Related CN105802337B (en) | 2016-03-24 | 2016-03-24 | Prepared Chinese ink based on synthesising macromolecule copolymer and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105802337B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106634199A (en) * | 2016-12-11 | 2017-05-10 | 钦州学院 | Negative-ion-release ink and preparation method thereof |
| CN109401436A (en) * | 2018-10-24 | 2019-03-01 | 蒋加寿 | A kind of novelty painting and calligraphy prepared Chinese ink |
| CN109535834A (en) * | 2018-10-24 | 2019-03-29 | 嘉兴凯兴达新材料科技有限公司 | A kind of preparation method of novelty painting and calligraphy prepared Chinese ink |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803945A (en) * | 2005-12-29 | 2006-07-19 | 大连思创信息材料有限公司 | Black pigment ink for ink-jet printer and method for preparing the same |
| CN103232761A (en) * | 2013-04-24 | 2013-08-07 | 李莉 | High-stability neutral ink |
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
-
2016
- 2016-03-24 CN CN201610170792.6A patent/CN105802337B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1803945A (en) * | 2005-12-29 | 2006-07-19 | 大连思创信息材料有限公司 | Black pigment ink for ink-jet printer and method for preparing the same |
| CN103232761A (en) * | 2013-04-24 | 2013-08-07 | 李莉 | High-stability neutral ink |
| CN104212236A (en) * | 2014-08-20 | 2014-12-17 | 中山艺展装饰工程有限公司 | Fragrant ink with refreshing effect |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106634199A (en) * | 2016-12-11 | 2017-05-10 | 钦州学院 | Negative-ion-release ink and preparation method thereof |
| CN109401436A (en) * | 2018-10-24 | 2019-03-01 | 蒋加寿 | A kind of novelty painting and calligraphy prepared Chinese ink |
| CN109535834A (en) * | 2018-10-24 | 2019-03-29 | 嘉兴凯兴达新材料科技有限公司 | A kind of preparation method of novelty painting and calligraphy prepared Chinese ink |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105802337B (en) | 2017-11-07 |
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Granted publication date: 20171107 |
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