CN107163651A - A kind of durable nanometer assistant agent oil colour of anti-mildew and preparation method - Google Patents

A kind of durable nanometer assistant agent oil colour of anti-mildew and preparation method Download PDF

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Publication number
CN107163651A
CN107163651A CN201710232509.2A CN201710232509A CN107163651A CN 107163651 A CN107163651 A CN 107163651A CN 201710232509 A CN201710232509 A CN 201710232509A CN 107163651 A CN107163651 A CN 107163651A
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China
Prior art keywords
nano
oil
oil colour
colour
mildew
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Pending
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CN201710232509.2A
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Chinese (zh)
Inventor
李小福
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SUZHOU BINGXIN STATIONERY Co Ltd
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SUZHOU BINGXIN STATIONERY Co Ltd
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Priority to CN201710232509.2A priority Critical patent/CN107163651A/en
Publication of CN107163651A publication Critical patent/CN107163651A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/06—Artists' paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
    • C09D191/005—Drying oils
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2237—Oxides; Hydroxides of metals of titanium
    • C08K2003/2241—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2262—Oxides; Hydroxides of metals of manganese
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2296—Oxides; Hydroxides of metals of zinc
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/24—Acids; Salts thereof
    • C08K3/26—Carbonates; Bicarbonates
    • C08K2003/265—Calcium, strontium or barium carbonate
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend

Abstract

The present invention discloses a kind of durable nanometer assistant agent oil colour of anti-mildew and preparation method, and its raw materials by weight includes following components：30~50% dry vegetable oils, 20~40% colorants, 5~20% nano-calcium carbonates, 1~7% nano zine oxide, 1~7% nano titanium oxide, 0.5~2% plant cellulose, 0.5~2% beeswax, 0.5~2% manganese dioxide, the oil colour of the present invention has preferable Antimould power after paintings have been done, and paintings are not easy mouldy in wet condition.

Description

A kind of durable nanometer assistant agent oil colour of anti-mildew and preparation method
Technical field
The present invention relates to pigment art, the durable nanometer assistant agent oil colour of particularly a kind of anti-mildew and preparation method.
Background technology
Oil painting is to use drip-dry vegetable oil（Linseed oil, poppy seed oil, walnut oil etc.）Filling colour, in painting canvas flax One made on cloth, cardboard or plank, which draws, to plant.The diluent used when drawing a picture is volatile turpentine oil and dryness Linseed oil etc..Pigment accompanying by picture has stronger hardness, and after picture is dried, gloss can be kept for a long time.By pigment Covering power and transparent performance more fully hereinafter show rendered object, rich color, match volume is strong.Oil painting is the main of Western painting One of picture kind.
Generally, oil colour is relatively easy to preserve, and mold-resistant material will not be added in oil colour, but in the actual guarantor of oil painting During depositing, the environment of humidity is run into, still there is Signs of Mould.In addition, paintings receive the ultraviolet in the external world in long-time Also the problem of pigment fades is easily caused after irradiation.
Therefore, the mouldy and problem for being difficult to overcome when always being paintings collection of fading of paintings, is badly in need of a kind of at present Later anti-mildew and the durable oil colour of color can have been done in paintings.
The content of the invention
In paintings later anti-mildew and the durable oil colour of color have been done it is an object of the invention to provide a kind of.
To reach above-mentioned purpose, the technical solution adopted by the present invention is：
A kind of durable nanometer assistant agent oil colour of anti-mildew, its raw materials by weight includes following components：30~50% is dry Property vegetable oil, 20~40% colorants, 5~20% nano-calcium carbonates, 1~7% nano zine oxide, 1~7% nano titanium oxide, 0.5~ 2% plant cellulose, 0.5~2% beeswax, 0.5~2% manganese dioxide.
Preferably, its raw materials by weight includes following components：35~45% dry vegetable oils, 30~40% colors Material, 10~20% nano-calcium carbonates, 1~5% nano zine oxide, 1~5% nano titanium oxide, 1~2% plant cellulose, 1~2% Beeswax, 0.5~1% manganese dioxide.
It is further preferred that its raw materials by weight includes following components：40% dry vegetable oil, 34% colorant, 15% nano-calcium carbonate, 4% nano zine oxide, 4% nano titanium oxide, 1% plant cellulose, 1% beeswax, 1% manganese dioxide.
Preferably, the dry vegetable oil is one kind in linseed oil, sunflower oil or walnut oil.
Preferably, the plant cellulose is derived from cotton seeds epidermis.
A kind of preparation method of the durable nanometer assistant agent oil colour of above-mentioned anti-mildew, comprises the following steps：Step one：Will Beeswax and plant cellulose are dissolved in dry vegetable oil；Step 2：Colorant and nano titanium oxide are added in agitator tank and mixed Close 30~60min of stirring；Step 3：Nano-calcium carbonate, nano zine oxide and titanium dioxide are added into the agitator tank of step 2 again Manganese continues to mix 30~60min；Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix Stir 30~60min；Step 5：The mixture stirred in step 4 is added in grinder, 20~40min of grinding is made Oil colour.
Because above-mentioned technical proposal is used, the present invention has following advantages compared with prior art：
1st, oil colour of the invention has preferable Antimould power after paintings have been done, and paintings are not easy in wet condition It is mouldy.
2nd, because nano titanium oxide is covered in the surface of colorant, it is possible to increase the uvioresistant of oil colour of the invention Line ability, increases the durability degree of pigment.
Embodiment
With reference to embodiment, the invention will be further described：
Embodiment 1：Oil colour is made using following steps：
Step one：0.5kg beeswaxs and 0.5kg plant celluloses are dissolved in 30kg linseed oil；
Step 2：40kg colorants and 3.5kg nano titanium oxides are added in agitator tank and mix 30min；
Step 3：20kg nano-calcium carbonates, 5kg nano zine oxides and 3.5kg titanium dioxides are added into the agitator tank of step 2 again Manganese continues to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 2 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 20~40min of grinding.
Embodiment 2：Oil colour is made using following steps：
Step one：2kg beeswaxs and 1.5kg plant celluloses are dissolved in 35kg linseed oil；
Step 2：30kg colorants and 5kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：18kg nano-calcium carbonates, 7kg nano zine oxides and 1.5kg titanium dioxides are added into the agitator tank of step 2 again Manganese continues to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Embodiment 3：Oil colour is made using following steps：
Step one：1kg beeswaxs and 1kg plant celluloses are dissolved in 40kg sunflower oils；
Step 2：34kg colorants and 4kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：15kg nano-calcium carbonates, 4kg nano zine oxides and 1kg manganese dioxide are added into the agitator tank of step 2 again Continue to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Embodiment 4：Oil colour is made using following steps：
Step one：1.5kg beeswaxs and 2kg plant celluloses are dissolved in 40kg sunflower oils；
Step 2：40kg colorants and 1kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：13kg nano-calcium carbonates, 1kg nano zine oxides and 1.5kg titanium dioxides are added into the agitator tank of step 2 again Manganese continues to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Embodiment 5：Oil colour is made using following steps：
Step one：2kg beeswaxs and 1kg plant celluloses are dissolved in dry vegetable oil；
Step 2：20kg colorants and 5kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：20kg nano-calcium carbonates, 5kg nano zine oxides and 2kg manganese dioxide are added into the agitator tank of step 2 again Continue to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Embodiment 6：Oil colour is made using following steps：
Step one：2kg beeswaxs and 2kg plant celluloses are dissolved in 50kg walnut oils；
Step 2：25kg colorants and 7kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：Added again into the agitator tank of step 2 5kg nano-calcium carbonates, 7kg nano zine oxides and 2kg manganese dioxide after It is continuous to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Comparative example 1：Oil colour is made using following steps：
Step one：During 1kg beeswaxs and 1kg plant celluloses are dissolved in 40kg sunflower oils；
Step 2：38kg colorants and 4kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：Added again into the agitator tank of step 2,15kg nano-calcium carbonates and 1kg manganese dioxide continue to mix 30 ~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Comparative example 2：Oil colour is made using following steps：
Step one：1kg beeswaxs and 1kg plant celluloses are dissolved in 40kg walnut oils；
Step 2：Be stirred for adding in tank 38kg colorants, 15kg nano-calcium carbonates, 4kg nano zine oxides and 1kg manganese dioxide after It is continuous to mix 30~60min；
Step 3：The solution added again into the agitator tank of step 2 in step one continues to mix 30~60min；
Step 4：The mixture stirred in step 3 is added in grinder, oil colour is made in 10~40min of grinding.
Comparative example 3：Oil colour is made using following steps：
Step one：1kg beeswaxs are dissolved in dry vegetable oil；
Step 2：35kg colorants and 4kg nano titanium oxides are added 30~60min is mixed in agitator tank；
Step 3：15kg nano-calcium carbonates, 4kg nano zine oxides and 1kg manganese dioxide are added into the agitator tank of step 2 again Continue to mix 30~60min；
Step 4：The solution added again into the agitator tank of step 3 in step one continues to mix 30~60min；
Step 5：The mixture stirred in step 4 is added in grinder, oil colour is made in 10~40min of grinding.
Above-mentioned plant cellulose is using the plant cellulose extracted in cotton seeds epidermis using organic solvent, cotton The use of the moderate suitable oil colour of cellulose length in seed coat.
Above-mentioned colorant is using conventional oil painting colorant, and by the agitator tank in above-described embodiment and comparative example and grinding Machine is the conventional equipment in existing oil colour production and operated with conventional parameter.
The oil colour of the oil colour of the embodiment of the present invention and comparative example is uniformly coated on etc. on big drawing paper, it is to be painted Paper is parched naturally, then drawing paper is placed in the environment of 30 DEG C of temperature, humidity 70%, without sunlight irradiation, from drawing paper surface after 4 weeks Remove part pigment and detect its bacteria containing amount, as a result such as following table：
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Comparative example 1 Comparative example 2 Comparative example 3
Bacteria containing amount（CFU/g） 1300 900 1300 1900 1400 1100 4600 1400 1400
The oil colour of the oil colour of the embodiment of the present invention and comparative example is uniformly coated on etc. on big drawing paper, treat drawing paper from So parch, then drawing paper is placed under direct sunlight environment be exposed to the sun, its aberration is detected after 4 weeks, as a result such as following table：
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Comparative example 1 Comparative example 2 Comparative example 3
Aberration 0.12 0.08 0.09 0.15 0.09 0.07 0.09 0.19 0.11
The above embodiments merely illustrate the technical concept and features of the present invention, and its object is to allow person skilled in the art's energy Solution present disclosure much of that is simultaneously implemented according to this, and it is not intended to limit the scope of the present invention.It is all spiritual according to the present invention The equivalent change or modification that essence is made, should all be included within the scope of the present invention.

Claims (6)

1. a kind of durable nanometer assistant agent oil colour of anti-mildew, it is characterised in that：Its raw materials by weight includes following Component：30~50% dry vegetable oils, 20~40% colorants, 5~20% nano-calcium carbonates, 1~7% nano zine oxide, 1~7% nanometer Titanium dioxide, 0.5~2% plant cellulose, 0.5~2% beeswax, 0.5~2% manganese dioxide.
2. a kind of durable nanometer assistant agent oil colour of anti-mildew according to claim 1, it is characterised in that：Its raw material is pressed Percentage by weight includes following components：35~45% dry vegetable oils, 30~40% colorants, 10~20% nano-calcium carbonates, 1~5% Nano zine oxide, 1~5% nano titanium oxide, 1~2% plant cellulose, 1~2% beeswax, 0.5~1% manganese dioxide.
3. a kind of durable nanometer assistant agent oil colour of anti-mildew according to claim 2, it is characterised in that：Its raw material is pressed Percentage by weight includes following components：40% dry vegetable oil, 34% colorant, 15% nano-calcium carbonate, 4% nano zine oxide, 4% are received Rice titanium dioxide, 1% plant cellulose, 1% beeswax, 1% manganese dioxide.
4. a kind of durable nanometer assistant agent oil colour of anti-mildew according to claim 1, it is characterised in that：The dryness is planted Thing oil is one kind in linseed oil, sunflower oil or walnut oil.
5. a kind of durable nanometer assistant agent oil colour of anti-mildew according to claim 1, it is characterised in that：The plant is fine Dimension element is derived from cotton seeds epidermis.
6. a kind of a kind of preparation method of the durable nanometer assistant agent oil colour of anti-mildew described in any one of claim 1-5, its It is characterised by, comprises the following steps：Step one：Beeswax and plant cellulose are dissolved in dry vegetable oil；Step 2：By color Material adds with nano titanium oxide and 30~60min is mixed in agitator tank；Step 3：Added again into the agitator tank of step 2 Nano-calcium carbonate, nano zine oxide and manganese dioxide continue to mix 30~60min；Step 4：Again to the stirring of step 3 The solution added in tank in step one continues to mix 30~60min；Step 5：By the mixture stirred in step 4 Add in grinder, oil colour is made in 20~40min of grinding.
CN201710232509.2A 2017-04-11 2017-04-11 A kind of durable nanometer assistant agent oil colour of anti-mildew and preparation method Pending CN107163651A (en)

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Cited By (4)

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Publication number Priority date Publication date Assignee Title
CN109082150A (en) * 2018-07-10 2018-12-25 苏州德加画材科技有限公司 A kind of drawing gouache color and preparation method thereof
CN109096917A (en) * 2018-07-10 2018-12-28 贝碧欧美术颜料(昆山)有限公司 A kind of no cobalt oil colour and preparation method thereof
CN109135572A (en) * 2018-05-31 2019-01-04 苏州西玛家具股份有限公司 A kind of Precerving liquid for furniture panel
CN115491060A (en) * 2022-08-12 2022-12-20 苏州冰心文化用品有限公司 Preparation method of nano-adjuvant oil painting pigment with high mildew resistance

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109135572A (en) * 2018-05-31 2019-01-04 苏州西玛家具股份有限公司 A kind of Precerving liquid for furniture panel
CN109082150A (en) * 2018-07-10 2018-12-25 苏州德加画材科技有限公司 A kind of drawing gouache color and preparation method thereof
CN109096917A (en) * 2018-07-10 2018-12-28 贝碧欧美术颜料(昆山)有限公司 A kind of no cobalt oil colour and preparation method thereof
CN115491060A (en) * 2022-08-12 2022-12-20 苏州冰心文化用品有限公司 Preparation method of nano-adjuvant oil painting pigment with high mildew resistance

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Application publication date: 20170915

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