CN111991330A - Pearl brightening and refreshing toothpaste and preparation method thereof - Google Patents
Pearl brightening and refreshing toothpaste and preparation method thereof Download PDFInfo
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- CN111991330A CN111991330A CN202011007083.9A CN202011007083A CN111991330A CN 111991330 A CN111991330 A CN 111991330A CN 202011007083 A CN202011007083 A CN 202011007083A CN 111991330 A CN111991330 A CN 111991330A
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- pearl
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- 239000000606 toothpaste Substances 0.000 title claims abstract description 65
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 64
- 238000002360 preparation method Methods 0.000 title claims description 14
- 238000005282 brightening Methods 0.000 title description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 34
- 239000000843 powder Substances 0.000 claims abstract description 34
- 230000002087 whitening effect Effects 0.000 claims abstract description 29
- FENRSEGZMITUEF-ATTCVCFYSA-E [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] FENRSEGZMITUEF-ATTCVCFYSA-E 0.000 claims abstract description 25
- 229940083982 sodium phytate Drugs 0.000 claims abstract description 25
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims abstract description 20
- 239000000419 plant extract Substances 0.000 claims abstract description 20
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 17
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims abstract description 17
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 17
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims abstract description 17
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 17
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 17
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229960004029 silicic acid Drugs 0.000 claims abstract description 17
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 17
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 17
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 17
- 239000011780 sodium chloride Substances 0.000 claims abstract description 17
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims abstract description 17
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims abstract description 17
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims abstract description 17
- 239000000600 sorbitol Substances 0.000 claims abstract description 17
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000230 xanthan gum Substances 0.000 claims abstract description 17
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 17
- 229940082509 xanthan gum Drugs 0.000 claims abstract description 17
- 235000010493 xanthan gum Nutrition 0.000 claims abstract description 17
- ABBQHOQBGMUPJH-UHFFFAOYSA-M Sodium salicylate Chemical compound [Na+].OC1=CC=CC=C1C([O-])=O ABBQHOQBGMUPJH-UHFFFAOYSA-M 0.000 claims abstract description 16
- 239000008213 purified water Substances 0.000 claims abstract description 14
- 108700004121 sarkosyl Proteins 0.000 claims abstract description 11
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims abstract description 11
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940085605 saccharin sodium Drugs 0.000 claims abstract description 7
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims abstract description 4
- 239000000686 essence Substances 0.000 claims abstract description 4
- 229960003885 sodium benzoate Drugs 0.000 claims abstract description 4
- 239000006072 paste Substances 0.000 claims description 42
- 238000004898 kneading Methods 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 21
- 238000000227 grinding Methods 0.000 claims description 18
- 230000032683 aging Effects 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 10
- 235000013599 spices Nutrition 0.000 claims description 9
- 230000000694 effects Effects 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 4
- 229940105902 mint extract Drugs 0.000 claims description 4
- 238000003860 storage Methods 0.000 claims description 4
- 235000007297 Gaultheria procumbens Nutrition 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 230000002431 foraging effect Effects 0.000 claims description 3
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 claims description 3
- 238000005086 pumping Methods 0.000 claims description 3
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 claims 3
- 241000333569 Pyrola minor Species 0.000 claims 1
- 238000004140 cleaning Methods 0.000 abstract description 11
- 208000002064 Dental Plaque Diseases 0.000 abstract description 8
- 241000196324 Embryophyta Species 0.000 abstract description 5
- 239000006260 foam Substances 0.000 abstract description 4
- 239000000779 smoke Substances 0.000 abstract description 4
- 241001122767 Theaceae Species 0.000 abstract 1
- WINXNKPZLFISPD-UHFFFAOYSA-M Saccharin sodium Chemical compound [Na+].C1=CC=C2C(=O)[N-]S(=O)(=O)C2=C1 WINXNKPZLFISPD-UHFFFAOYSA-M 0.000 description 6
- 244000269722 Thea sinensis Species 0.000 description 4
- 241000736246 Pyrola Species 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- 235000003325 Ilex Nutrition 0.000 description 1
- 241000209035 Ilex Species 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 241001085205 Prenanthella exigua Species 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 239000000551 dentifrice Substances 0.000 description 1
- 210000004268 dentin Anatomy 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000003670 easy-to-clean Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000002200 mouth mucosa Anatomy 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- PESXGULMKCKJCC-UHFFFAOYSA-M sodium;4-methoxycarbonylphenolate Chemical compound [Na+].COC(=O)C1=CC=C([O-])C=C1 PESXGULMKCKJCC-UHFFFAOYSA-M 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000011232 storage material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
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- Birds (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Zoology (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses pearl whitening fresh toothpaste, which comprises sorbitol, aluminum hydroxide, purified water, hydrated silica, sodium lauryl sulfate, essence, cellulose gum, xanthan gum, sodium lauroyl sarcosinate, saccharin sodium, sodium benzoate, sodium hydroxybenzoate, tetrasodium pyrophosphate, sodium chloride, natural plant extracts, sodium bicarbonate, sodium phytate and pearl powder; sodium bicarbonate, sodium phytate, pearl powder and the like are added into the formula of the toothpaste, the natural plant stain removing sodium phytate helps to improve exogenous color plates such as smoke stains and tea stains, reduce dental plaque and whiten teeth, and the pearl powder in the formula also helps to clean teeth stains and play a role in reducing dental plaque when a user uses the toothpaste; the toothpaste, which is kneaded, ground and aged, generates dense foam that penetrates between teeth, thus providing deep cleaning of the user's teeth and more effective cleaning of dental stains.
Description
Technical Field
The invention belongs to the technical field of daily toothpaste, and particularly relates to pearl whitening fresh toothpaste; in particular to a preparation method of the pearl whitening refreshing toothpaste.
Background
The toothpaste is a cleaning article commonly used in daily life, is a dentifrice, is generally in a gel shape, can be usually smeared on a toothbrush for cleaning teeth, keeps the beauty and brightness of the teeth, has a long history, and with the continuous development of scientific technology, the continuous improvement and perfection of manufacturing technology and equipment, various types of toothpaste are appeared one after another, the quality and the grade of products are continuously improved, and as far as 2019, the variety of the toothpaste is changed from single cleaning type toothpaste, the toothpaste is developed into hundreds of multifunctional toothpastes with complete varieties and various functions, thereby meeting the requirements of different consumption levels.
The definition of the chinese toothpaste industry association is: the toothpaste is used together with the toothbrush for cleaning teeth and protecting oral hygiene, and is a daily necessity for protecting human body safety. Can remove pellicle and plaque from tooth surface without damaging enamel and dentin; has good function of cleaning the oral cavity and the periphery thereof; no toxicity and no stimulation to oral mucosa; has comfortable fragrance and taste, and has cool and fresh feeling after use; easy to use, and is extruded into uniform, bright and soft strips; the cleaning agent is easy to clean from the oral cavity, teeth and toothbrush; the storage agent has good chemical and physical stability, and ensures that each index meets the standard requirement in the storage period; has reasonable cost performance. The toothpaste formula and the production and preparation method in the prior art are single, and when exogenous stains such as smoke stains, tea stains and the like on teeth of a user are more, the cleaning effect of the conventional toothpaste on the teeth is limited, so that a pearl whitening fresh toothpaste and a preparation method thereof are provided.
Disclosure of Invention
The invention aims to provide pearl bright white fresh toothpaste and a preparation method thereof, wherein sodium bicarbonate, sodium phytate, pearl powder and the like are added into a formula of the toothpaste, and effective paste kneading, grinding and aging processes are set in the preparation method, natural plant stain-removing sodium phytate helps to improve exogenous color plates such as smoke stains and tea stains, reduce dental plaque and whiten teeth, and the pearl powder in the formula also helps to clean dental stains and plays a role in reducing dental plaque in the process of using the toothpaste by a user; the toothpaste, which is kneaded, ground and aged, generates dense foam that penetrates deeply between teeth, thus deeply cleaning the teeth of a user to more effectively clean the stains on the teeth, thereby solving the problems of the background art as described above.
In order to achieve the purpose, the invention adopts the following technical scheme: the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 15-20 parts of sorbitol, 2-5 parts of aluminum hydroxide, 80-100 parts of purified water, 15-20 parts of hydrated silica, 0.2-0.4 part of sodium lauryl sulfate, 0.5-1 part of essence, 3-5 parts of cellulose gum, 0.4-0.6 part of xanthan gum, 0.2-0.4 part of sodium lauroyl sarcosinate, 0.2-0.3 part of saccharin sodium, 0.1-0.2 part of sodium benzoate, 0.1-0.3 part of sodium hydroxybenzoate, 0.1-0.4 part of tetrasodium pyrophosphate, 1-5 parts of sodium chloride, 3-5 parts of natural plant extract, 5-9 parts of sodium bicarbonate, 2-3 parts of sodium phytate and 10-15 parts of pearl powder.
Preferably, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 15 parts of sorbitol, 2 parts of aluminum hydroxide, 80 parts of purified water, 15 parts of hydrated silica, 0.2 part of sodium lauryl sulfate, 0.5 part of essence, 3 parts of cellulose gum, 0.4 part of xanthan gum, 0.2 part of sodium lauroyl sarcosinate, 0.2 part of sodium saccharin, 0.1 part of sodium benzoate, 0.1 part of sodium hydroxybenzoate, 0.1 part of tetrasodium pyrophosphate, 1 part of sodium chloride, 3 parts of a natural plant extract, 5 parts of sodium bicarbonate, 2 parts of sodium phytate and 10 parts of pearl powder.
Preferably, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 20 parts of sorbitol, 5 parts of aluminum hydroxide, 100 parts of purified water, 20 parts of hydrated silica, 0.4 part of sodium lauryl sulfate, 1 part of essence, 5 parts of cellulose gum, 0.6 part of xanthan gum, 0.4 part of sodium lauroyl sarcosine, 0.3 part of sodium saccharin, 0.2 part of sodium benzoate, 0.3 part of sodium hydroxybenzoate, 0.4 part of tetrasodium pyrophosphate, 5 parts of sodium chloride, 5 parts of a natural plant extract, 9 parts of sodium bicarbonate, 3 parts of sodium phytate and 15 parts of pearl powder.
Preferably, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 18 parts of sorbitol, 3 parts of aluminum hydroxide, 90 parts of water, 17 parts of hydrated silica, 0.3 part of sodium lauryl sulfate, 0.75 part of essence, 4 parts of cellulose gum, 0.5 part of xanthan gum, 0.3 part of sodium lauroyl sarcosine, 0.25 part of sodium saccharin, 0.15 part of sodium benzoate, 0.2 part of sodium hydroxybenzoate, 0.3 part of tetrasodium pyrophosphate, 3 parts of sodium chloride, 4 parts of natural plant extract, 7 parts of sodium bicarbonate, 2.5 parts of sodium phytate and 12.5 parts of pearl powder.
Preferably, the natural plant extract is a mixture of 3-5 parts of wintergreen extract and 3-5 parts of mint extract.
The invention also provides a preparation method of the pearl whitening fresh toothpaste, which comprises the following steps:
s1, weighing, metering, preparing and feeding materials, weighing and feeding sorbitol, aluminum hydroxide, hydrated silica, sodium lauryl sulfate, essence, cellulose gum, xanthan gum, sodium lauroyl sarcosinate, saccharin sodium, sodium benzoate, sodium hydroxybenzoate, tetrasodium pyrophosphate, sodium chloride, natural plant extracts, sodium bicarbonate, sodium phytate, pearl powder and the like according to the mass part process formula of the pearl whitening fresh toothpaste, putting the weighed materials into a pre-dissolving pot or a pre-mixing pot, dissolving the materials uniformly by purified water, and finally feeding the spices and solid powder in the formula;
s2, mixing and making paste, taking the full input of the spice and the solid powder in the formula as a limit, stirring and mixing with a scraper and homogenizing and stirring and mixing after all the materials in the formula are input until the powder, the spice and other formulas are stirred to be in a homogeneous paste state;
s3, kneading the paste, transferring the final mixture stirred in the step S2 to a paste kneading machine for vacuum kneading, wherein the kneading effect of the paste can fully mix the toothpaste;
s4, carrying out vacuum grinding, keeping the kneaded paste in a vacuum environment, and grinding the kneaded paste by using a grinder until the fineness of the ground paste reaches the fineness standard of the corresponding process;
and S5, storing and aging, namely pumping the fully ground toothpaste body into a paste body storage pot for aging, naturally cooling the materials to normal temperature, fully expanding the materials to form a homogeneous adhesive body, and improving the elasticity of the materials.
Preferably, in steps S3 and S4, bubbles are generated in the paste during kneading and grinding, and the degree of vacuum of the paste during kneading and grinding is-0.090 Mpa to-0.096 Mpa.
Preferably, in step S5, the aging time of the paste is at least 120 minutes; in steps S3, S4 and S5, the paste temperature and the ambient temperature during kneading, grinding and aging of the toothpaste are at most 45 ℃.
Compared with the prior art, the invention has the technical effects and advantages that: by adding sodium bicarbonate, sodium phytate, pearl powder and the like into the formula of the toothpaste and setting effective paste kneading, grinding and aging processes in the preparation method, the natural plant stain-removing sodium phytate helps to improve exogenous color plates such as smoke stains and tea stains, reduce dental plaque and whiten teeth, and the pearl powder in the formula also helps to clean tooth stains and play a role in reducing dental plaque in the process of using the toothpaste by a user; the toothpaste, which is kneaded, ground and aged, generates dense foam that penetrates between teeth, thus providing deep cleaning of the user's teeth and more effective cleaning of dental stains.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. The specific embodiments described herein are merely illustrative of the invention and do not delimit the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The pearl whitening refreshing toothpaste comprises the following components in parts by weight: 15 parts of sorbitol, 2 parts of aluminum hydroxide, 80 parts of purified water, 15 parts of hydrated silica, 0.2 part of sodium lauryl sulfate, 0.5 part of essence, 3 parts of cellulose gum, 0.4 part of xanthan gum, 0.2 part of sodium lauroyl sarcosinate, 0.2 part of sodium saccharin, 0.1 part of sodium benzoate, 0.1 part of sodium hydroxybenzoate, 0.1 part of tetrasodium pyrophosphate, 1 part of sodium chloride, 3 parts of a natural plant extract, 5 parts of sodium bicarbonate, 2 parts of sodium phytate and 10 parts of pearl powder.
The natural plant extract is a mixture of 3-5 parts of wintergreen extract and 3-5 parts of mint extract.
The invention also provides a preparation method of the pearl whitening fresh toothpaste, which comprises the following steps:
s1, weighing, metering, preparing and feeding materials, weighing and feeding sorbitol, aluminum hydroxide, hydrated silica, sodium lauryl sulfate, essence, cellulose gum, xanthan gum, sodium lauroyl sarcosinate, saccharin sodium, sodium benzoate, sodium hydroxybenzoate, tetrasodium pyrophosphate, sodium chloride, natural plant extracts, sodium bicarbonate, sodium phytate, pearl powder and the like according to the mass part process formula of the pearl whitening fresh toothpaste, putting the weighed materials into a pre-dissolving pot or a pre-mixing pot, dissolving the materials uniformly by purified water, and finally feeding the spices and solid powder in the formula;
s2, mixing and making paste, taking the full input of the spice and the solid powder in the formula as a limit, stirring and mixing with a scraper and homogenizing and stirring and mixing after all the materials in the formula are input until the powder, the spice and other formulas are stirred to be in a homogeneous paste state;
s3, kneading the paste, transferring the final mixture stirred in the step S2 to a paste kneading machine for vacuum kneading, wherein the kneading effect of the paste can fully mix the toothpaste;
s4, carrying out vacuum grinding, keeping the kneaded paste in a vacuum environment, and grinding the kneaded paste by using a grinder until the fineness of the ground paste reaches the fineness standard of the corresponding process;
and S5, storing and aging, namely pumping the fully ground toothpaste body into a paste body storage pot for aging, naturally cooling the materials to normal temperature, fully expanding the materials to form a homogeneous adhesive body, and improving the elasticity of the materials.
In steps S3 and S4, bubbles are generated in the paste during kneading and grinding, and the vacuum degree of the paste during kneading and grinding is-0.090 MPa to-0.096 MPa.
In step S5, the aging time of the paste is at least 120 minutes; in steps S3, S4 and S5, the paste temperature and the ambient temperature during kneading, grinding and aging of the toothpaste are at most 45 ℃.
Example 2
Different from the embodiment 1, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 20 parts of sorbitol, 5 parts of aluminum hydroxide, 100 parts of purified water, 20 parts of hydrated silica, 0.4 part of sodium lauryl sulfate, 1 part of essence, 5 parts of cellulose gum, 0.6 part of xanthan gum, 0.4 part of sodium lauroyl sarcosine, 0.3 part of sodium saccharin, 0.2 part of sodium benzoate, 0.3 part of sodium hydroxybenzoate, 0.4 part of tetrasodium pyrophosphate, 5 parts of sodium chloride, 5 parts of a natural plant extract, 9 parts of sodium bicarbonate, 3 parts of sodium phytate and 15 parts of pearl powder.
Example 3
Different from the embodiment 1, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 18 parts of sorbitol, 3 parts of aluminum hydroxide, 90 parts of water, 17 parts of hydrated silica, 0.3 part of sodium lauryl sulfate, 0.75 part of essence, 4 parts of cellulose gum, 0.5 part of xanthan gum, 0.3 part of sodium lauroyl sarcosine, 0.25 part of sodium saccharin, 0.15 part of sodium benzoate, 0.2 part of sodium hydroxybenzoate, 0.3 part of tetrasodium pyrophosphate, 3 parts of sodium chloride, 4 parts of natural plant extract, 7 parts of sodium bicarbonate, 2.5 parts of sodium phytate and 12.5 parts of pearl powder.
Example 4
Different from the embodiment 1, the formula of the pearl whitening refreshing toothpaste comprises the following components in parts by weight: 17 parts of sorbitol, 4 parts of aluminum hydroxide, 85 parts of purified water, 16 parts of hydrated silica, 0.25 part of sodium lauryl sulfate, 0.6 part of essence, 3.5 parts of cellulose gum, 0.45 part of xanthan gum, 0.25 part of sodium lauroyl sarcosinate, 0.25 part of saccharin sodium, 0.15 part of sodium benzoate, 0.25 part of sodium hydroxybenzoate, 0.2 part of tetrasodium pyrophosphate, 2 parts of sodium chloride, 3.5 parts of natural plant extract, 8 parts of sodium bicarbonate, 2.5 parts of sodium phytate and 14 parts of pearl powder.
The specific formulation data for the four groups of examples of the invention are given in the following table:
| example 1 | Example 2 | Example 3 | Example 4 | |
| Sorbitol | 15 portions of | 20 portions of | 18 portions of | 17 portions of |
| Aluminum hydroxide | 2 portions of | 5 portions of | 3 portions of | 4 portions of |
| Purified water | 80 portions | 100 portions of | 90 portions of | 85 portions of |
| Hydrated silica | 15 portions of | 20 portions of | 17 portions of | 16 portions of |
| Sodium lauryl sulfate | 0.2 part | 0.4 portion of | 0.3 part | 0.25 part |
| Essence | 0.5 portion | 1 part of | 0.75 portion | 0.6 part |
| Cellulose gum | 3 portions of | 5 portions of | 4 portions of | 3.5 parts of |
| Xanthan gum | 0.4 portion of | 0.6 part | 0.5 portion | 0.45 part |
| Sodium lauroyl sarcosinate | 0.2 part | 0.4 portion of | 0.3 part | 0.25 part |
| Saccharin sodium salt | 0.2 part | 0.3 part | 0.25 part | 0.25 part |
| Sodium benzoate | 0.1 part | 0.2 part | 0.15 part | 0.15 part |
| Sodium methyl hydroxybenzoate | 0.1 part | 0.3 part | 0.2 part | 0.25 part |
| Tetrasodium pyrophosphate | 0.1 part | 0.4 portion of | 0.3 part | 0.2 part |
| Sodium chloride | 1 part of | 5 portions of | 3 portions of | 2 portions of |
| Natural plant extract | 3 portions of | 5 portions of | 4 portions of | 3.5 parts of |
| Sodium bicarbonate | 5 portions of | 9 portions of | 7 portions of | 8 portions of |
| Sodium phytate | 2 portions of | 3 portions of | 2.5 parts of | 2.5 parts of |
| Pearl powder | 10 portions of | 15 portions of | 12.5 portions | 14 portions of |
In conclusion, the sodium bicarbonate, the sodium phytate, the pearl powder and the like are added into the formula of the toothpaste, and effective paste kneading, grinding and aging processes are set in the preparation method, the natural plant sodium phytate capable of removing stains helps to improve exogenous color plates such as tobacco stains and tea stains, reduce dental plaque and whiten teeth, and the pearl powder in the formula also helps to clean the stains and play a role in reducing the dental plaque in the process of using the toothpaste by a user; the toothpaste which is kneaded, ground and aged has dense foam which can penetrate into the teeth, so that the teeth of a user can be cleaned deeply, and the dirt on the teeth can be cleaned more effectively;
the natural plants of the ilex extract and the mint extract added in the formula can achieve the effects of refreshing breath and refreshing mind and body in the process of using the toothpaste by a user.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.
Claims (8)
1. The pearl whitening and refreshing toothpaste is characterized in that: the formula of the pearl whitening fresh toothpaste comprises the following components in parts by mass: 15-20 parts of sorbitol, 2-5 parts of aluminum hydroxide, 80-100 parts of purified water, 15-20 parts of hydrated silica, 0.2-0.4 part of sodium lauryl sulfate, 0.5-1 part of essence, 3-5 parts of cellulose gum, 0.4-0.6 part of xanthan gum, 0.2-0.4 part of sodium lauroyl sarcosinate, 0.2-0.3 part of saccharin sodium, 0.1-0.2 part of sodium benzoate, 0.1-0.3 part of sodium hydroxybenzoate, 0.1-0.4 part of tetrasodium pyrophosphate, 1-5 parts of sodium chloride, 3-5 parts of natural plant extract, 5-9 parts of sodium bicarbonate, 2-3 parts of sodium phytate and 10-15 parts of pearl powder.
2. The pearl whitening refreshing toothpaste according to claim 1, wherein: the formula of the pearl whitening fresh toothpaste comprises the following components in parts by mass: 15 parts of sorbitol, 2 parts of aluminum hydroxide, 80 parts of purified water, 15 parts of hydrated silica, 0.2 part of sodium lauryl sulfate, 0.5 part of essence, 3 parts of cellulose gum, 0.4 part of xanthan gum, 0.2 part of sodium lauroyl sarcosinate, 0.2 part of sodium saccharin, 0.1 part of sodium benzoate, 0.1 part of sodium hydroxybenzoate, 0.1 part of tetrasodium pyrophosphate, 1 part of sodium chloride, 3 parts of a natural plant extract, 5 parts of sodium bicarbonate, 2 parts of sodium phytate and 10 parts of pearl powder.
3. The pearl whitening refreshing toothpaste according to claim 1, wherein: the formula of the pearl whitening fresh toothpaste comprises the following components in parts by mass: 20 parts of sorbitol, 5 parts of aluminum hydroxide, 100 parts of purified water, 20 parts of hydrated silica, 0.4 part of sodium lauryl sulfate, 1 part of essence, 5 parts of cellulose gum, 0.6 part of xanthan gum, 0.4 part of sodium lauroyl sarcosine, 0.3 part of sodium saccharin, 0.2 part of sodium benzoate, 0.3 part of sodium hydroxybenzoate, 0.4 part of tetrasodium pyrophosphate, 5 parts of sodium chloride, 5 parts of a natural plant extract, 9 parts of sodium bicarbonate, 3 parts of sodium phytate and 15 parts of pearl powder.
4. The pearl whitening refreshing toothpaste according to claim 1, wherein: the formula of the pearl whitening fresh toothpaste comprises the following components in parts by mass: 18 parts of sorbitol, 3 parts of aluminum hydroxide, 90 parts of water, 17 parts of hydrated silica, 0.3 part of sodium lauryl sulfate, 0.75 part of essence, 4 parts of cellulose gum, 0.5 part of xanthan gum, 0.3 part of sodium lauroyl sarcosine, 0.25 part of sodium saccharin, 0.15 part of sodium benzoate, 0.2 part of sodium hydroxybenzoate, 0.3 part of tetrasodium pyrophosphate, 3 parts of sodium chloride, 4 parts of natural plant extract, 7 parts of sodium bicarbonate, 2.5 parts of sodium phytate and 12.5 parts of pearl powder.
5. The pearl whitening refreshing toothpaste according to claim 1, wherein: the natural plant extract is a mixture of 3-5 parts of wintergreen extract and 3-5 parts of mint extract.
6. The preparation method of the pearl whitening refreshing toothpaste as claimed in claim 1, which is characterized by comprising the following steps:
s1, weighing, metering, preparing and feeding materials, weighing and feeding sorbitol, aluminum hydroxide, hydrated silica, sodium lauryl sulfate, essence, cellulose gum, xanthan gum, sodium lauroyl sarcosinate, saccharin sodium, sodium benzoate, sodium hydroxybenzoate, tetrasodium pyrophosphate, sodium chloride, natural plant extracts, sodium bicarbonate, sodium phytate, pearl powder and the like according to the mass part process formula of the pearl whitening fresh toothpaste, putting the weighed materials into a pre-dissolving pot or a pre-mixing pot, dissolving the materials uniformly by purified water, and finally feeding the spices and solid powder in the formula;
s2, mixing and making paste, taking the full input of the spice and the solid powder in the formula as a limit, stirring and mixing with a scraper and homogenizing and stirring and mixing after all the materials in the formula are input until the powder, the spice and other formulas are stirred to be in a homogeneous paste state;
s3, kneading the paste, transferring the final mixture stirred in the step S2 to a paste kneading machine for vacuum kneading, wherein the kneading effect of the paste can fully mix the toothpaste;
s4, carrying out vacuum grinding, keeping the kneaded paste in a vacuum environment, and grinding the kneaded paste by using a grinder until the fineness of the ground paste reaches the fineness standard of the corresponding process;
and S5, storing and aging, namely pumping the fully ground toothpaste body into a paste body storage pot for aging, naturally cooling the materials to normal temperature, fully expanding the materials to form a homogeneous adhesive body, and improving the elasticity of the materials.
7. The preparation method of the pearl whitening refreshing toothpaste according to claim 6, which is characterized in that: in steps S3 and S4, bubbles are generated in the paste during kneading and grinding, and the vacuum degree of the paste during kneading and grinding is-0.090 MPa to-0.096 MPa.
8. The preparation method of the pearl whitening refreshing toothpaste according to claim 6, which is characterized in that: in step S5, the aging time of the paste is at least 120 minutes; in steps S3, S4 and S5, the paste temperature and the ambient temperature during kneading, grinding and aging of the toothpaste are at most 45 ℃.
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