CN111956532A - Facial cleaning mask for refining pores and brightening skin color and preparation method thereof - Google Patents
Facial cleaning mask for refining pores and brightening skin color and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of cosmetics, in particular to a facial cleaning mask for refining pores and brightening skin color and a preparation method thereof. The product has smooth skin feel, no stickiness, moistening, no tightness and good cleaning capability, is rich in mineral substances and humus, can inhibit sebum oxidation, weaken the stimulation and decomposition of oxygen free radicals to elastin, accelerate the repair of tissue cells, and has obvious effects of refining pores and brightening skin color; also has antiinflammatory, antibacterial, and acne inhibiting effects. The preparation method adopts a wrapping technology, adopts an oil-in-water emulsion system, combines the strong cleaning effect, the antibacterial, anti-inflammatory and antioxidant effects of clay and the moistening of an oil phase system, and ensures that the facial cleaning mask not only has a good cleaning effect, but also has other skin care effects.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a facial cleaning mask for refining pores and brightening skin and a preparation method thereof.
Background
The facial mask is a skin care product which is relatively popular among Asian consumers and comprises a patch type and an application type. Mud masks are one type of facial masks that are being applied and have recently been sought after by consumers. The mud film is applied by uniformly applying on face for about 2-3mm, standing for about 15min, and washing. Due to the adsorption of mud, mud films are mainly used to remove facial dirt. The clay film sold in the market mainly adopts kaolin as a main component, and the main effect is cleaning effect. Some mud films incorporate surfactants with strong detergency to enhance cleaning efficacy, but may be irritating to the skin.
The Chinese patent with the patent number of CN 111407690A discloses a moisturizing mud film which is composed of components such as wax, a skin feel regulator, vegetable oil, a humectant, a preservative, an emulsifier, kaolin, water and the like. The mud film has good skin feeling, but poor cleaning performance and single efficacy.
According to the search, Chinese patent with patent number CN 110478282A discloses a multifunctional cleaning mud film, and the mud matrix adopts Wudalianchi volcanic mud which contains various mineral substances and has the skin care effects of moisturizing, wrinkle removal, tightening and the like. However, the components of the detergent contain sodium glutamate, which is a common washing and decontaminating component and can cause irritation when staying on the skin for a long time; in addition, the mud film using method comprises the following steps: coating the mud film matrix on the surface of skin, and cleaning after coating; or the content phase of the mud film forming ball is uniformly mixed with the mud film substrate, and the mixture is coated on the surface of skin to form a film, and is cleaned and removed, and is used step by step, so that the operation time is prolonged, and the use is inconvenient.
Disclosure of Invention
One of the purposes of the invention is to provide a facial cleansing mask for refining pores and brightening skin color, which is a mud mask, has good cleansing effect and other skin care effects, and is safe and mild, convenient to use and good in use experience.
The second purpose of the invention is to provide a preparation method of a facial cleansing mask for refining pores and brightening skin color aiming at the defects of the prior art.
In order to achieve one of the purposes, the invention adopts the following technical scheme:
the facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the clay is one or two of Australian Haierwood clay and Hokkaido Ardisia clay.
Preferably, the stabilizer is one or a combination of more than two of xanthan gum, carbomer, carnauba wax and palm wax or stearyl alcohol.
Preferably, the humectant is one or a combination of more than two of glycerin, propylene glycol or butanediol.
Preferably, the oil is one or a composition of more than two of Indian rattan seed oil, propylene glycol dinonyl ester and hydrogenated sunflower seed oil.
Preferably, the emulsifier is a composition of span-60 and tween-60;
the preservative is a composition of honokiol and hexylene glycol.
In order to achieve the second purpose, the invention adopts the following technical scheme:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water and clay in a formula amount into an emulsifying pot, stirring at room temperature, adding a stabilizer and a humectant in a formula amount, stirring and heating, and shearing and homogenizing to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the grease and the emulsifier with the formula ratio into an oil phase pot, stirring and heating to completely dissolve the grease and the emulsifier, thus obtaining the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot in the step one, mixing with the formula A, heating, shearing, homogenizing, vacuumizing, and stirring at constant temperature to prepare a formula B;
step four, preparing a facial cleaning mud film: and (4) cooling the formula B prepared in the step three, adding a preservative in the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the technical scheme, in the first step, water and clay in a formula amount are added into an emulsifying pot, stirred at room temperature for 3-8 min, then added with a stabilizer and a humectant in a formula amount, stirred and heated to reach 80-85 ℃, and then sheared and homogenized at a high speed for 2-5 min to completely dissolve the stabilizer, so that the formula A is prepared.
In the technical scheme, in the second step, the grease and the emulsifier with the formula amount are added into an oil phase pot, stirred and heated to 75-80 ℃ to be completely dissolved, and the oil phase formula is prepared.
In the technical scheme, in the third step, the oil phase formula prepared in the second step is added into the emulsifying pot in the first step to be mixed with the formula A, the mixture is heated to 78-82 ℃, then is subjected to high-speed shearing and homogenization for 2-5 min, then is vacuumized, and is stirred at constant temperature for 15-25 min to prepare the formula B.
In the technical scheme, the shearing and homogenizing speed in the first step and the third step is 2000 r/min-3000 r/min;
the stirring speed in the first step to the fourth step is 30 r/min-100 r/min;
the vacuum degree in the third step is-0.02 MPa-0.04 MPa.
Compared with the prior art, the invention has the beneficial effects that:
(1) the facial cleaning mask for refining pores and brightening skin color provided by the invention has the advantages that the mud matrix is the Australian Haierwood clay and the Hokkaido Ardisia clay, the two clays are the montmorillonite, the water solution of the montmorillonite has high osmotic pressure, and when the montmorillonite is applied to the surface of the skin, the montmorillonite not only can adsorb grease and dirt on the surface of the skin, but also can suck out dirt dissolved and loosened in the pores. Wherein, the Australia sea wood clay is rich in humus, and the content of the humus is greatly higher than that of kaolin, Canadian bentonite, volcanic ash, sea mud and the like. The humus is a macromolecular colloid mixture formed by decomposing organic matters in soil by microorganisms, and comprises humins, humic acid and fulvic acid, and the two are called humic acid. The humic acid contains biological original stimulants, can promote the immune response of macrophages, improve the immune function of organisms, and stimulate mitochondrial respiration, thereby accelerating tissue cell repair. When the humic acid is externally applied to the skin, the humic acid can resist bacteria and inflammation, inhibit the generation of a large amount of free radicals caused by inflammation, enhance the functional activity of the skin and play a role in promoting wound healing when the content of the humic acid is extremely low. Wherein, the Arctic clay of Hokkaido is produced in Arctic area of Laminaria japonica of North Japan, is rich in various minerals such as calcium, magnesium, iron, silicon, manganese, etc., and the minerals mainly exist in the form of oxides and salts thereof, so the clay has strong ion exchange capacity and buffering capacity. After the minerals are dispersed in water, various divalent or trivalent metal cations can be dissociated, and oxygen radical anions and peroxy radical anions generated by skin can be neutralized, so that the mineral has an antioxidant effect. Therefore, the facial cleaning mask disclosed by the invention has a good facial cleaning effect, and can be used for resisting bacteria, inflammation and oxidation and further delaying skin aging.
(2) The facial cleaning mask for refining pores and brightening skin color provided by the invention adopts an oil-in-water emulsion, wherein the Indian gamboge seed oil in the oil is rich in natural VE and polyunsaturated oleic acid and can deeply nourish the skin, the propylene glycol dipelargonate has good lubricity and spreadability, and the hydrogenated sunflower seed oil is moistened and not greasy; the prepared mud film has smooth skin feeling, good ductility and moist, clean and bright skin after use and is not tight by scientifically proportioning the three oils.
(3) The facial cleansing mask for refining pores and brightening skin color provided by the invention adopts honokiol and hexanediol as the preservatives, so that the synergy can be realized. Wherein, the honokiol is a polyphenol compound extracted from plants, has antibacterial and anti-inflammatory effects, and has obvious acne removing effect.
(4) According to the preparation method of the facial cleaning mask for refining pores and brightening skin color, a wrapping technology is applied, an oil-in-water emulsification system is adopted, oil and an emulsifier are wrapped in water and clay, and the strong cleaning effect, the antibacterial, anti-inflammatory and antioxidant effects and the moistening of an oil phase system of the clay are combined, so that the facial cleaning mask not only has a good cleaning effect, but also has other skin care effects, and is safe, mild, convenient to use and good in use experience. And the preparation method has the characteristics of simple process, low production cost and suitability for large-scale production.
Drawings
Fig. 1 is a diagram of pore refining effect in experimental tests.
Fig. 2 is a result graph of the acne inhibition rate of the evaluation of the acne treatment effect in the experimental test.
Detailed Description
In order to make the technical problems, technical solutions and advantageous effects solved by the present invention more apparent, the present invention is further described in detail below with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water, Australian Haiermu clay and Hokkaido Ardisia clay into an emulsifying pot according to the formula, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula, stirring and heating to 82 ℃, and shearing at high speed for homogenizing for 3min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Example 2.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water, Australian Haiermu clay and Hokkaido Ardisia clay into an emulsifying pot according to the formula, stirring at room temperature for 3min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula, stirring and heating to 80 ℃, and shearing at high speed for homogenizing for 5min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, Indian gamboge seed oil, hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot, stirring and heating to 75 ℃ to completely dissolve the components, thus obtaining the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 78 ℃, then shearing at a high speed and homogenizing for 5min, then vacuumizing, and stirring at a constant temperature for 15min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2000 r/minn;
in the embodiment, the stirring speed in the first step to the fourth step is 30 r/min;
in this example, the vacuum degree in the third step was-0.02 MPa.
Example 3.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water, Australian Haiermu clay and Hokkaido Ardisia clay into an emulsifying pot according to the formula, stirring at room temperature for 8min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula, stirring and heating to 85 ℃, and shearing at high speed for homogenizing for 2min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, Indian gamboge seed oil, hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot, stirring and heating to 80 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 82 ℃, then shearing at a high speed and homogenizing for 2min, then vacuumizing, and stirring at a constant temperature for 25min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 3000 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 100 r/min;
in this example, the vacuum degree in step three was 0.04 MPa.
Example 4.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
wherein the clay is one or two of Australian Halloysitum roseum clay and Hokkaido Ardisia clay.
Wherein the stabilizer is one or more of xanthan gum, carbomer, carnauba wax or stearyl alcohol.
Wherein the humectant is one or a composition of more than two of glycerol, propylene glycol or butanediol.
Wherein the oil and fat is one or more of Indian turnbuckle seed oil, propylene glycol dinonyl ester, and hydrogenated sunflower seed oil.
Wherein the emulsifier is a composition of span-60 and tween-60;
wherein the antiseptic is a composition of honokiol and hexanediol.
The preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water and clay in a formula amount into an emulsifying pot, stirring at room temperature for 3-8 min, adding a stabilizer and a humectant in the formula amount, stirring and heating to reach the temperature of 80-85 ℃, and then shearing at a high speed and homogenizing for 2-5 min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the grease and the emulsifier with the formula ratio into an oil phase pot, stirring and heating to 75-80 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing the oil phase formula with the formula A, heating to 78-82 ℃, then shearing at a high speed and homogenizing for 2-5 min, then vacuumizing, and stirring at a constant temperature for 15-25 min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (4) cooling the formula B prepared in the step three, adding a preservative in the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
Wherein, the shearing and homogenizing speed in the first step and the third step is 2000 r/min-3000 r/min;
wherein the stirring speed in the first step to the fourth step is 30 r/min-100 r/min;
wherein the vacuum degree in the third step is-0.02 MPa-0.04 MPa.
Comparative example 1.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water, Australian Haiermu clay and Hokkaido Ardisia clay into an emulsifying pot according to the formula, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula, stirring and heating to 82 ℃, and shearing at high speed for homogenizing for 3min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Comparative example 2.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water, Australian Haiermu clay and Hokkaido Ardisia clay into an emulsifying pot according to the formula, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula, stirring and heating to 82 ℃, and shearing at high speed for homogenizing for 3min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Comparative example 3.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water and kaolin into an emulsifying pot according to the formula, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerin and butanediol according to the formula, stirring and heating to 82 ℃, and shearing at high speed and homogenizing for 3min to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Comparative example 4.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water and Australian Haerful wood clay into an emulsifying pot according to the formula amount, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerol and butanediol according to the formula amount, stirring and heating to 82 ℃, and shearing at high speed for homogenizing for 3min to completely dissolve a stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Comparative example 5.
A facial cleansing mask for refining pores and brightening skin color comprises the following raw materials in percentage by weight:
the preparation method of the facial cleansing mask for refining pores and brightening skin color comprises the following steps:
step one, preparing a formula A: adding water and Arisaema heterophyllum Clay in formula amount into emulsifying pot, stirring at room temperature for 5min, adding xanthan gum, carnauba wax, glycerol and butanediol in formula amount, stirring and heating to 82 deg.C, and high-speed shearing and homogenizing for 3min to dissolve stabilizer completely to obtain formula A;
step two, preparing an oil phase formula: adding the propylene glycol azelaic acid ester, the Indian gamboge seed oil, the hydrogenated sunflower seed oil, span-60 and tween-60 into an oil phase pot according to the formula amount, stirring and heating to 78 ℃, and completely dissolving to obtain the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot prepared in the step one, mixing with the formula A, heating to 80 ℃, then shearing at a high speed and homogenizing for 3min, then vacuumizing, and stirring at a constant temperature for 20min to prepare a formula B;
step four, preparing a facial cleaning mud film: and (3) cooling the formula B prepared in the step (three), adding hexanediol and honokiol according to the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
In the embodiment, the shearing and homogenizing speed in the first step and the third step is 2500 r/min;
in the embodiment, the stirring speed in the first step to the fourth step is 60 r/min;
in this example, the vacuum degree in step three was-0.03 MPa.
Experimental testing
First, stability test
The facial cleansing masks obtained in examples 1 to 3 and comparative examples 1 to 5 above were subjected to a stability test according to a method common in the cosmetics industry, and the results are shown in table 1.
Table 1 stability test table of facial cleansing mask of examples 1 to 3 and comparative examples 1 to 5
As can be seen from the stability test results of table 1 above, the facial cleansing masks prepared in examples 1 to 3 of the present invention and comparative examples 1 to 5 were good in heat resistance, cold resistance and cycle test stability.
Second, product efficacy evaluation
(one) evaluation of feeling of use and cleaning ability
The facial cleansing masks prepared in examples 1 to 3 and comparative examples 1, 3, 4 and 5 were evaluated for use experience and cleansing ability, and the use experience included spreadability, moisturizing ability and washability, and the above indices were scored by 10 points, and a high score indicated good spreadability (or high moisturizing ability, easy washability and good cleansing ability). The above index evaluation was scored by 20 volunteers, and the results were averaged as shown in Table 2.
Table 2 evaluation results table of feeling of use and cleaning ability
The results from table 2 show that all the products have better spreadability, with comparative example 1 having the best spreadability and comparative example 3 having the relatively worst spreadability, mainly because the body is smoother and easier to push away with only 13 parts of clay added to comparative example 1 (australian hallwood clay and north seaway alpine clay). The mud base of comparative example 3 was kaolin, which was more sticky and less likely to be pushed off than both clays used in the present invention. In addition, the moisturizing effect of the comparative example 1 and the examples 1 to 3 on the skin is better, the moisturizing effect of the comparative example 5 on the skin is general, the moisturizing degree of the comparative example 3 is poorer, and the phenomenon of skin tightness occurs, mainly because the mud matrix of the comparative example 3 is kaolin, and the moisturizing performance is poor compared with the Australian Haier wood clay and the Hokkaido clay. All the products of the above examples and comparative examples can be washed off conveniently and do not remain easily after use. Except for comparative examples 1 and 4, all other groups of products have good cleaning effect on facial dirt and meet the basic requirements of mud films.
According to table 2, further comparison shows that: 1. the clay matrix with the same addition amount has the viscosity of kaolin, Arisado clay, Australian Haier wood clay; 2. the total amount of the two kinds of clay is low, the cleaning capability is weak, and the addition amount needs more than 20 parts; 3. the kaolin has a single structure, strong water absorption and poor water retention capacity, and is easy to cause discomfort such as skin tightness or irritation; 4. the mud film prepared by singly adopting Australia Haierwood clay or Norway Arisaema clay as the mud matrix has better comprehensive evaluation experience feeling than the effect of simultaneously using the Australia Haierwood clay and the Norway Arisaema clay. The Australian Haiermu clay is rich in organic humus and has strong water absorption and retention capacity, and the Nordo Atka clay is rich in mineral substances, loose and porous in microstructure; the two are compatible to prepare the mud film, so that the mud film has strong cleaning capability and good water retention capability, and can not cause skin tightness and discomfort.
(II) evaluation of pore refining Effect and skin lightening Effect
The facial cleansing masks prepared in examples 1 to 3 and comparative example 3 were used for 30 days by 60 subjects of 20 to 45 years old, and the above products were comparatively analyzed for skin-pore-refining and skin-lightening effects. Wherein, the skin of the face of the subject has no physiological and pathological abnormal conditions such as damage, allergy, red swelling and the like, but the T area has a more obvious pore enlargement phenomenon, the subject is divided into 4 groups, and each group comprises 15 persons. Each group uses a sample to be tested once every 5 days, and the using method comprises the steps of uniformly coating 8-10g of the product on the face with the thickness of 2-3mm, standing for 15 minutes, washing with clear water, and wiping to dry.
Pore detection: calculating pore areas of the sample before and after 0, 5, 10, 15, 25 and 30 days respectively by using an image analyzer, and analyzing by using data before and after the sample to improve pore size enlarging effect and make the pore visible area μm2It is shown that the larger the improvement rate is, the more obvious the effect of improving the pore size of the tested sample is, and the specific test result is shown in figure 1.
The results in figure 1 show that the products of examples 1-3 have a skin pore improvement of around 16-20% over 30 days of use, whereas the product of comparative example 3 has a skin pore improvement of around 8%, wherein the mud base of comparative example 3 is kaolin. The facial cleansing mask of the present invention was able to improve the problem of large pores in the skin by using the Australian Haier wood clay and the Nordheim clay. The Australian Haierwood clay and the Hokkaido Ardisia clay in the mud membrane can remove dirt deep in the skin surface layer and pores through adsorption, and on the other hand, positive charge mineral substances rich in the clay can neutralize oxygen free radicals, so that oxidation of the clay to grease in the pores is avoided, and the phenomenon that the pores are large due to blockage and stimulation of grease oxidation products to the pores is prevented.
Skin brightness detection: the skin brightness was measured by a German CK skin tester, GL200 probe, before the application of the sample, after 5 days, 10 days, 15 days, 25 days and 30 days of the application of the sample, and the skin brightness change rate was calculated from the skin brightness change rate before the application of the sample, and the test results are shown in Table 3.
TABLE 3 skin Brightness Change Rate
The results in table 3 show that the facial cleansing masks prepared in examples 1-3 can significantly improve skin brightness after 30 days of use, and the overall improvement rate is about 9%, which is about 2 times that of the product in comparative example 3. The facial cleaning mask has the functions of moistening, stimulating the synthesis of skin elastin, inhibiting the activity of free radicals, weakening the decomposition of protein, improving the plumpness and brightness of the skin, promoting the metabolism of cells and accelerating the renewal due to the addition of the Australian Haiermu clay and the Hokkaido Ardisia clay.
(III) evaluation of acne-removing Effect
The facial cleansing masks obtained in example 1 and comparative example 2 were used with a commercially available acne cream for 4 days by 30 subjects, and the acne removing effects of the above products were analyzed and compared. The test subjects were divided into 3 groups of ten people each using one sample to be tested, and the products prepared in example 1 and comparative example 2 were applied by uniformly applying 8-10g of the product on the face with a thickness of 2-3mm, left to stand for 15 minutes, washed with clear water, and wiped dry. The application method of the commercially available acne-removing cream is to take a proper amount of sample and spot-coat the sample on the position where acne grows. The number of anterior pox-spots and the number of posterior pox-spots per product were recorded, and the inhibition rate of pox-spots was calculated as shown in FIG. 2.
The results of fig. 2 show that the facial cleansing mud film prepared by the invention has a certain acne suppression effect. After 4 days of use, the acne suppression rate of the product in the example 1 is more than 40%, the acne suppression rate of the product in the comparative example 2 is more than 25%, and the acne suppression rate of the commercial acne cream is about 70%. Compared with the products sold in the market, the product prepared by the invention has the acne removing effect which is not as good as that of the acne removing cream sold in the market, but has good cleaning effect and skin brightening effect on the skin.
Therefore, the facial cleaning mask disclosed by the invention adopts two kinds of clay (Australian Haierwood clay and Norway Arisaema clay) as the composite mud substrate, so that the prepared product is smooth in skin feel, not sticky, moist, not tight and good in cleaning capacity, is rich in minerals and humus, can inhibit sebum oxidation, weaken the stimulation and decomposition of oxygen radicals on elastin, accelerate the repair of tissue cells, and has obvious effects of refining pores and brightening skin color; in addition, the facial cleaning mask disclosed by the invention can also be anti-inflammatory and bacteriostatic, and has a certain inhibition effect on acnes.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
2. The facial cleansing mask for pore refinement and skin tone enhancement according to claim 1, wherein: the stabilizer is one or more of xanthan gum, carbomer, carnauba wax, palm wax or stearyl alcohol.
3. The facial cleansing mask for pore refinement and skin tone enhancement according to claim 1, wherein: the humectant is one or a composition of more than two of glycerin, propylene glycol or butanediol.
4. The facial cleansing mask for pore refinement and skin tone enhancement according to claim 1, wherein: the oil is one or more of Indian turnbuckle seed oil, propylene glycol dinonyl ester, and hydrogenated sunflower seed oil.
5. The facial cleansing mask for pore refinement and skin tone enhancement according to claim 1, wherein: the emulsifier is a composition of span-60 and tween-60;
the preservative is a composition of honokiol and hexylene glycol.
6. A method of preparing a facial cleansing mask for refining pores and lightening skin color according to any one of claims 1 to 5, wherein: it comprises the following steps:
step one, preparing a formula A: adding water and clay in a formula amount into an emulsifying pot, stirring at room temperature, adding a stabilizer and a humectant in a formula amount, stirring and heating, and shearing and homogenizing to completely dissolve the stabilizer to obtain a formula A;
step two, preparing an oil phase formula: adding the grease and the emulsifier with the formula ratio into an oil phase pot, stirring and heating to completely dissolve the grease and the emulsifier, thus obtaining the oil phase formula;
step three, preparing a formula B: adding the oil phase formula prepared in the step two into the emulsifying pot in the step one, mixing with the formula A, heating, shearing, homogenizing, vacuumizing, and stirring at constant temperature to prepare a formula B;
step four, preparing a facial cleaning mud film: and (4) cooling the formula B prepared in the step three, adding a preservative in the formula amount, and uniformly stirring and mixing to obtain the facial cleaning mask for refining pores and brightening skin.
7. The method for preparing a facial cleansing mask for refining pores and lightening skin color according to claim 6, wherein the method comprises the following steps: in the first step, the water and the clay with the formula amount are added into an emulsifying pot, stirred for 3-8 min at room temperature, then added with the stabilizer and the humectant with the formula amount, stirred and heated to enable the temperature to reach 80-85 ℃, and then sheared and homogenized at high speed for 2-5 min to enable the stabilizer to be completely dissolved, thus obtaining the formula A.
8. The method for preparing a facial cleansing mask for refining pores and lightening skin color according to claim 6, wherein the method comprises the following steps: and in the second step, adding the grease and the emulsifier with the formula amount into an oil phase pot, stirring and heating to 75-80 ℃, and completely dissolving to obtain the oil phase formula.
9. The method for preparing a facial cleansing mask for refining pores and lightening skin color according to claim 6, wherein the method comprises the following steps: and in the third step, adding the oil phase formula prepared in the second step into the emulsifying pot in the first step, mixing the oil phase formula with the formula A, heating to 78-82 ℃, shearing at a high speed, homogenizing for 2-5 min, vacuumizing, and stirring at a constant temperature for 15-25 min to obtain the formula B.
10. The method for preparing a facial cleansing mask for refining pores and lightening skin color according to claim 6, wherein the method comprises the following steps: the shearing and homogenizing speed in the first step and the third step is 2000 r/min-3000 r/min;
the stirring speed in the first step to the fourth step is 30 r/min-100 r/min;
the vacuum degree in the third step is-0.02 MPa-0.04 MPa.
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