CN111944618A - 一种银离子抑菌除螨洗衣凝珠 - Google Patents

一种银离子抑菌除螨洗衣凝珠 Download PDF

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CN111944618A
CN111944618A CN202010916233.1A CN202010916233A CN111944618A CN 111944618 A CN111944618 A CN 111944618A CN 202010916233 A CN202010916233 A CN 202010916233A CN 111944618 A CN111944618 A CN 111944618A
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silver ion
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江华初
张武功
陈鑫隆
黄惠先
林学智
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Private Customized Guangzhou Technology Co ltd
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Abstract

本发明公开了一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：月桂醇聚醚硫酸酯钠5‑10％、C14‑16烯烃磺酸钠8‑12％、椰油酰胺丙基甜菜碱3‑10％、甘油2‑5％、丙二醇5‑20％、甲基异噻唑啉酮0.001‑0.009％、三乙醇胺0.5‑5％、冬青提取物0.5‑5％、香茅提取物0.5‑5％、银离子溶液0.1‑5％、香精0.3‑3％、余量为水。本发明清洁去污能力、除螨能力、广谱杀菌抑菌效果均优于现有技术且对人体安全性较高。

Description

一种银离子抑菌除螨洗衣凝珠
技术领域
本发明涉及洗衣产品技术领域，尤其涉及一种银离子抑菌除螨洗衣凝珠。
背景技术
衣服是人们生活的必需要素，俗话说人靠衣装，衣服除了穿上好看之外，衣服的清洁也是人们日常生活非常关注的问题。随着现代人们生活质量的提高，洗衣用的化工品也在不断提升，从最早用的洗衣用化工品为肥皂、洗衣粉，但肥皂块状难溶解，以及洗衣粉在使用时也经常出现在水中溶解不充分，又由于碱性较强，局部溶解不均匀部分会对衣物造成损伤，且对皮肤刺激性较强，容易伤害手部皮肤。因此，现如今分散性更好的洗衣液逐渐在市场占有率越来越大，洗衣液良好的分散性使得洗衣液能够均匀的洗涤衣物，同时也易冲洗，解决了表面活性剂沉积问题。然而随着社会的发展进步，人们生活节奏的逐渐改变，方便、便捷成为了人们新的喜好。于是，有了洗衣凝珠的诞生。
随着人们健康意识的不断提高，虽然洗衣用的化工品的剂型在不断改变，但是人们对洗涤剂的要求不单单局限在洗干净衣服，衣服是皮肤直接接触的日用品，每天都难免会沾染皮肤分泌的汗液、皮屑以及会沾染其他细小病毒细菌等有害污染物。螨虫通常分为尘螨、粉螨、革螨、恙螨等几大类，是一种肉眼不易看见的微型害虫，在皮肤里面吸取营养成分，刺激毛细血管以及细胞组织，引向皮肤恶化。轻者会引起皮肤瘙痒、小丘疹等，严重会导致过敏性皮炎和痤疮。市面上也越来越多的洗衣产品有抑菌除螨作用，市面上用于洗衣用品的杀菌剂大多数为醛类、酸类抗菌剂(甲醛、苯甲酸)和氯制剂(次氯酸钠、84消毒液、次氯酸钙、漂白粉、漂粉净、优氯净)，这些抗菌剂清洁去污能力、除螨能力、广谱杀菌抑菌效果以及对人体皮肤致敏性方面都不尽人意，有待提高。
发明内容
针对现有技术的不足，本发明所解决的技术问题是如何提高抑菌剂产品清洁去污能力、除螨能力、广谱杀菌抑菌效果且对人体安全性较高。
为解决上述技术问题，本发明采用的技术方案是一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠5-10％，
C14-16烯烃磺酸钠8-12％，
椰油酰胺丙基甜菜碱3-10％，
甘油2-5％，
丙二醇5-20％，
甲基异噻唑啉酮0.001-0.009％，
三乙醇胺0.5-5％，
冬青提取物0.5-5％，
香茅提取物0.5-5％，
银离子溶液0.1-5％，
香精0.3-3％，
余量为水。
优选地，一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠6-8％，
C14-16烯烃磺酸钠9-10％，
椰油酰胺丙基甜菜碱4-8％，
甘油3-4％，
丙二醇8-15％，
甲基异噻唑啉酮0.004-0.007％，
三乙醇胺1-3％，
冬青提取物2-4％，
香茅提取物2-4％，
银离子溶液2-3％，
香精0.5-1.5％，
余量为水。
与现有技术相比，本发明清洁去污能力、除螨能力、广谱杀菌抑菌效果均优于现有技术且对人体安全性较高。
具体实施方式
下面结合实施例对本发明的具体实施方式作进一步的说明，但不是对本发明的限定。
实施例1：
一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠5％，
C14-16烯烃磺酸钠12％，
椰油酰胺丙基甜菜碱3％，
甘油2％，
丙二醇5％，
甲基异噻唑啉酮0.009％，
三乙醇胺0.5％，
冬青提取物5％，
香茅提取物0.5％，
银离子溶液5％，
香精0.3％，
余量为水。
实施例2：
一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠6％，
C14-16烯烃磺酸钠10％，
椰油酰胺丙基甜菜碱8％，
甘油4％，
丙二醇15％，
甲基异噻唑啉酮0.005％，
三乙醇胺2％，
冬青提取物4％，
香茅提取物4％，
银离子溶液3％，
香精1％，
余量为水。
实施例3：
一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠10％，
C14-16烯烃磺酸钠8％，
椰油酰胺丙基甜菜碱10％，
甘油5％，
丙二醇20％，
甲基异噻唑啉酮0.001％，
三乙醇胺5％，
冬青提取物0.5％，
香茅提取物5％，
银离子溶液0.1％，
香精3％，
余量为水。
实施例4：
一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠6％，
C14-16烯烃磺酸钠10％，
椰油酰胺丙基甜菜碱4％，
甘油4％，
丙二醇8％，
甲基异噻唑啉酮0.007％，
三乙醇胺1％，
冬青提取物4％，
香茅提取物2％，
银离子溶液3％，
香精0.5％，
余量为水。
实施例5：
一种银离子抑菌除螨洗衣凝珠，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠8％，
C14-16烯烃磺酸钠9％，
椰油酰胺丙基甜菜碱8％，
甘油3％，
丙二醇15％，
甲基异噻唑啉酮0.004％，
三乙醇胺3％，
冬青提取物2％，
香茅提取物4％，
银离子溶液2％，
香精1.5％，
余量为水。
为了更好地说明本发明的有益效果，进行以下功效评价测试：
(1)去污力测试：
本发明产品的去污力测试参照GB/T13174-2008《衣物用洗涤剂去污力及循环洗涤性能的测定》进行，选用实施例1-3制得的本发明产品和某三款市售抑菌除螨洗衣凝珠进行对比，实验结果表明，实施例1-3本发明产品以及某三款市售抑菌除螨洗衣凝珠对炭黑油污布、皮脂污布去污值与标准洗衣液去污值的比值如表1所示：
表1本发明产品和某三款市售洗衣液去污力测试结果
Figure BDA0002665115500000081
Figure BDA0002665115500000091
表1的数据表明，本实施例1-3制备的本发明产品具有更强的去污力。
(2)螨虫去除率测试：
以规格为10cm×10cm的棉布为试样，将试样棉布在太阳下暴晒10h，然后分别采用医用定量取螨器在人面颊、额部等部位取螨虫，采用牙签将含有螨虫的皮脂分泌物从取螨器上取出，并刮刀试样棉布上，加1-2滴甘油在皮脂分泌物上，涂匀，在显微镜下观察并分别计数，每个试样棉布上活螨虫数量均在100-105之间，然后分别将实施例1-3与市售例1-3制得的洗衣凝珠按1:20体积比兑水后，分别将试样棉布放入，浸泡20min，然后揉搓10min，然后取出，自然晾干后，对处理后的各组试样棉布存留的螨虫进行测试，并分别计数，计算螨虫去除率，对比:
表2
Figure BDA0002665115500000092
Figure BDA0002665115500000101
由表2可以看出，本发明的除螨效果明显优于市售产品。
(3)抗菌性测试：
依据《消毒技术规范》(2002年版)2.1.11.3.3的检验依据和分析方法，选择实例1-3及市售产品做了以下测试,得到以下测试结果表3
表3：
Figure BDA0002665115500000102
结论：依照试验结果表3，本发明产品对大肠埃希氏菌、金黄色葡萄球菌和白色念珠菌的杀菌率均达到90％以上，明显高出市售产品对应值，产品具有较强的抗菌作用，能有效杀灭大肠埃希氏菌、金黄色葡萄球菌和白色念珠菌的。
(4)持续抗菌性测试：
依据《消毒技术规范》(2002年版)2.1.11.3.3的检验依据和分析方法，选择实例1-3及市售产品进行测试，得到以下测试结果表4。
表4：
Figure BDA0002665115500000111
结论：依照试验结果表4，本发明产品对大肠埃希氏菌、金黄色葡萄球菌和白色念珠菌的杀菌率均达到90％以上，明显高出市售产品对应值，产品具有较强的抗菌作用，能持续48小时有效杀灭大肠埃希氏菌、金黄色葡萄球菌和白色念珠菌的。
(5)毒理性测试：
依据《消毒技术规范》2002年版，第二部分2.3.1的检验依据和分析方法。
受试物质：本发明产品为受试样品，称取5g样品，加入灭菌水定容至20mL，混匀。
实验动物：动物种属品系：SPF级KM小鼠。
试验环境：环境温度22-25℃，相对湿度40-70％。
试验步骤：实验前，实验动物禁食过夜，不限制饮水。试验时，称量动物体重，随机分组，一次给予受试样品经口染毒，每只小鼠灌胃量为0.2mL/10g体重，剂量为5000mg/kg·BW，染毒后禁食3-4h。染毒后对每只动物进行单独全面的记录，观察实验动物的中毒表现和死亡情况，其后每天进行一次仔细检查，于给药D0、D7和D14称量体重。观察期限为14d。观察结束后，处死动物进行大体解剖学检查。
试验结果，表7：
Figure BDA0002665115500000131
注：14天观察期内所有受试动物未见明显中毒症状及死亡。
结论：在本次试验条件下，受试物对SPF级KM小鼠急性经口毒性LD50＞5000mg/kg·BW，属于实际无毒。
通过上述功效评价项目测试，可以知道，本发明相比于现有技术，其清洁去污能力、除螨能力、广谱杀菌抑菌效果均优于现有技术且对人体安全性较高。
以上结合实施例对本发明的实施方式做出了详细说明，但本发明不局限于所描述的实施方式。对于本领域技术人员而言，在不脱离本发明的原理和精神的情况下，对这些实施方式进行各种变化、修改、替换和变型仍落入本发明的保护范围内。

Claims (2)

1.一种银离子抑菌除螨洗衣凝珠，其特征在于，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠5-10％，
C14-16烯烃磺酸钠8-12％，
椰油酰胺丙基甜菜碱3-10％，
甘油2-5％，
丙二醇5-20％，
甲基异噻唑啉酮0.001-0.009％，
三乙醇胺0.5-5％，
冬青提取物0.5-5％，
香茅提取物0.5-5％，
银离子溶液0.1-5％，
香精0.3-3％，
余量为水。
2.根据权利要求1所述的银离子抑菌除螨洗衣凝珠，其特征在于，按质量百分比包括以下组分：
月桂醇聚醚硫酸酯钠6-8％，
C14-16烯烃磺酸钠9-10％，
椰油酰胺丙基甜菜碱4-8％，
甘油3-4％，
丙二醇8-15％，
甲基异噻唑啉酮0.004-0.007％，
三乙醇胺1-3％，
冬青提取物2-4％，
香茅提取物2-4％，
银离子溶液2-3％，
香精0.5-1.5％，
余量为水。
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112375631A (zh) * 2020-11-24 2021-02-19 云南超越日化有限公司 一种抗菌抑菌洗衣液及其制备方法
CN112625812A (zh) * 2021-01-04 2021-04-09 合创博远(北京)科技有限公司 一种抑菌除螨洗衣液及其制备方法
CN112791206A (zh) * 2021-03-29 2021-05-14 许卓辉 一种首穿免洗的内裤生产工艺流程

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112375631A (zh) * 2020-11-24 2021-02-19 云南超越日化有限公司 一种抗菌抑菌洗衣液及其制备方法
CN112375631B (zh) * 2020-11-24 2021-11-09 云南超越日化有限公司 一种抗菌抑菌洗衣液及其制备方法
CN112625812A (zh) * 2021-01-04 2021-04-09 合创博远(北京)科技有限公司 一种抑菌除螨洗衣液及其制备方法
CN112791206A (zh) * 2021-03-29 2021-05-14 许卓辉 一种首穿免洗的内裤生产工艺流程

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