CN111592025A - 一种菊花状微米碳酸钙的制备方法 - Google Patents
一种菊花状微米碳酸钙的制备方法 Download PDFInfo
- Publication number
- CN111592025A CN111592025A CN202010393300.6A CN202010393300A CN111592025A CN 111592025 A CN111592025 A CN 111592025A CN 202010393300 A CN202010393300 A CN 202010393300A CN 111592025 A CN111592025 A CN 111592025A
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- Prior art keywords
- calcium carbonate
- chrysanthemum
- micron calcium
- preparing
- shaped micron
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 103
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 51
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000004530 micro-emulsion Substances 0.000 claims abstract description 21
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 20
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 18
- 239000003921 oil Substances 0.000 claims abstract description 10
- 239000002244 precipitate Substances 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 9
- 239000004094 surface-active agent Substances 0.000 claims abstract description 8
- 230000032683 aging Effects 0.000 claims abstract description 7
- 239000004064 cosurfactant Substances 0.000 claims abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims abstract description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical group [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 14
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- 239000001110 calcium chloride Substances 0.000 claims description 12
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 12
- 238000005303 weighing Methods 0.000 claims description 10
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical group CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000004579 marble Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 4
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical group [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 4
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims description 2
- 235000007516 Chrysanthemum Nutrition 0.000 abstract description 4
- 239000006185 dispersion Substances 0.000 abstract description 3
- 244000189548 Chrysanthemum x morifolium Species 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 12
- 239000005060 rubber Substances 0.000 description 6
- 229910021532 Calcite Inorganic materials 0.000 description 5
- 239000004033 plastic Substances 0.000 description 5
- 229920003023 plastic Polymers 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 241000723353 Chrysanthemum Species 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000001276 controlling effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- 238000001878 scanning electron micrograph Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000875 corresponding effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 239000002070 nanowire Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/184—Preparation of calcium carbonate by carbonation of solutions based on non-aqueous solvents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
- C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
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CN202010393300.6A CN111592025B (zh) | 2020-05-11 | 2020-05-11 | 一种菊花状微米碳酸钙的制备方法 |
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CN202010393300.6A CN111592025B (zh) | 2020-05-11 | 2020-05-11 | 一种菊花状微米碳酸钙的制备方法 |
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CN111592025A true CN111592025A (zh) | 2020-08-28 |
CN111592025B CN111592025B (zh) | 2023-03-21 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113912099A (zh) * | 2021-11-23 | 2022-01-11 | 新乡学院 | 一种载药用多层碳酸钙空心微球及其制备方法和应用 |
CN113955788A (zh) * | 2021-10-20 | 2022-01-21 | 兰州交通大学 | 一种通过调节反相微乳液体系中S/CoS的比值制备不同形貌碳酸钙颗粒的方法 |
CN114455620A (zh) * | 2022-01-11 | 2022-05-10 | 兰州交通大学 | 一种方形与簇状共生一体的微米级碳酸钙的制备方法 |
CN114455621A (zh) * | 2022-01-11 | 2022-05-10 | 兰州交通大学 | 一种针状碳酸钙的制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102583481A (zh) * | 2012-01-18 | 2012-07-18 | 兰州交通大学 | 反相微乳法制备不同粒径球形纳米碳酸钙粒子的方法 |
-
2020
- 2020-05-11 CN CN202010393300.6A patent/CN111592025B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102583481A (zh) * | 2012-01-18 | 2012-07-18 | 兰州交通大学 | 反相微乳法制备不同粒径球形纳米碳酸钙粒子的方法 |
Non-Patent Citations (1)
Title |
---|
YANG DING等: ""Controllable synthesis of all the anhydrous CaCO3 polymorphs with various morphologies in CaCl2-NH3-CO2 aqueous system"", 《POWDER TECHNOLOGY》 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113955788A (zh) * | 2021-10-20 | 2022-01-21 | 兰州交通大学 | 一种通过调节反相微乳液体系中S/CoS的比值制备不同形貌碳酸钙颗粒的方法 |
CN113955788B (zh) * | 2021-10-20 | 2023-03-21 | 兰州交通大学 | 一种通过调节反相微乳液体系中S/CoS的比值制备不同形貌碳酸钙颗粒的方法 |
CN113912099A (zh) * | 2021-11-23 | 2022-01-11 | 新乡学院 | 一种载药用多层碳酸钙空心微球及其制备方法和应用 |
CN113912099B (zh) * | 2021-11-23 | 2023-07-07 | 新乡学院 | 一种载药用多层碳酸钙空心微球及其制备方法和应用 |
CN114455620A (zh) * | 2022-01-11 | 2022-05-10 | 兰州交通大学 | 一种方形与簇状共生一体的微米级碳酸钙的制备方法 |
CN114455621A (zh) * | 2022-01-11 | 2022-05-10 | 兰州交通大学 | 一种针状碳酸钙的制备方法 |
CN114455620B (zh) * | 2022-01-11 | 2023-10-27 | 兰州交通大学 | 一种方形与簇状共生一体的微米级碳酸钙的制备方法 |
CN114455621B (zh) * | 2022-01-11 | 2023-10-27 | 兰州交通大学 | 一种针状碳酸钙的制备方法 |
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CN111592025B (zh) | 2023-03-21 |
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Effective date of registration: 20240418 Address after: 541208 Jinshan Industrial Zone, Tanxia Town, Lingchuan County, Guilin City, Guangxi Zhuang Autonomous Region Patentee after: GUILIN JINSHAN CHEMICAL INDUSTRIAL Co.,Ltd. Country or region after: China Address before: 730070 No. 118 Anning West Road, Anning District, Gansu, Lanzhou Patentee before: Lanzhou Jiaotong University Country or region before: China Patentee before: HEZHOU University |