CN111575084B - 一种合成抗水型长寿命真空泵油及其制备方法 - Google Patents
一种合成抗水型长寿命真空泵油及其制备方法 Download PDFInfo
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/047—Thioderivatives not containing metallic elements
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/049—Phosphite
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/02—Unspecified siloxanes; Silicones
Abstract
Description
项目 | 低粘度烷基萘 | 高粘度烷基萘 | PAOs | 己二酸酯 | 多元醇酯 |
100℃运动黏度,mm<sub>2</sub>/s | 4.7 | 12.4 | 5.8 | 5.3 | 4.3 |
旋转氧弹实验(150℃,621kPa,水,铜)/min | 195 | 180 | 17 | 70 | - |
差式扫描热分析(180℃,3.45MPa)/min | 60+ | 60+ | 2.5 | 5.0 | 60+ |
氧化腐蚀试验后总酸值(以氢氧化钾计)/(mg·g<sup>-1</sup>) | 0.092 | 0.089 | - | 7.1 | 1.3 |
项目 | 低粘度烷基萘 | 高粘度烷基萘 | PAOs | 合成酯 | 烷基苯 | Ⅰ类基础油 |
100℃运动黏度,mm<sub>2</sub>/s | 4.7 | 12.4 | 5.5 | 5.2 | 4.2 | 4.0 |
苯胺点,℃ | 32 | 90 | 119 | 20 | 77.8 | 100 |
项目 | 低粘度烷基萘 | 高粘度烷基萘 | 己二酸酯 | 多元醇酯 |
100℃运动黏度,mm<sub>2</sub>/s | 4.7 | 12.4 | 5.3 | 4.3 |
水解后总酸值增加值(以氢氧化钾计)mg/g | 0.02 | 0.02 | 0.16 | 0.20 |
样品成分 | 原料名称 | 含量(kg) | 生产商 |
天然气合成油 | GTL430 | 60 | SHELL |
烷基萘基础油 | Synesstic 12 | 25 | ExxonMobil |
疏水剂 | 聚异丁烯 | 10 | DAELIM |
油性剂1 | 聚酯 | 1.2 | CRODA |
油性剂2 | 脂肪酸酯 | 1.8 | CRODA |
抗氧剂 | 烷基化二苯胺 | 4 | BASF |
极压抗磨剂 | 亚磷酸三(二叔丁基苯基)酯 | 0.5 | BASF |
腐蚀抑制剂 | 苯并三氮唑及其衍生物 | 0.2 | Vanderbilt |
防锈剂 | 有机胺 | 0.005 | BASF |
游离水捕捉剂 | 非离子型表面活性剂 | 0.1 | DOW |
破乳剂 | 环氧乙烷环氧丙烷共聚物 | 0.1 | Lubrizol |
消泡剂 | 高分子有机硅氧烷 | 0.05 | Lubrizol |
样品成分 | 原料名称 | 含量(kg) | 生产商 |
天然气合成油 | GTL420 | 25 | SHELL |
烷基萘基础油 | Synesstic 12 | 60 | ExxonMobil |
疏水剂 | 聚异丁烯 | 5 | DAELIM |
油性剂 | 聚酯 | 1 | CRODA |
抗氧剂 | 高分子苯酚 | 1 | BASF |
极压抗磨剂1 | 丁基三苯基硫代磷酸酯 | 1 | BASF |
极压抗磨剂2 | 三苯基亚磷酸酯 | 2 | BASF |
腐蚀抑制剂 | 苯并三氮唑及其衍生物 | 0.005 | Vanderbilt |
防锈剂 | 有机胺 | 0.2 | BASF |
游离水捕捉剂 | 非离子型表面活性剂 | 0.5 | DOW |
破乳剂 | 环氧乙烷环氧丙烷共聚物 | 0.03 | Lubrizol |
消泡剂 | 高分子有机硅氧烷 | 0.01 | Lubrizol |
样品成分 | 原料名称 | 含量(kg) | 生产商 |
天然气合成油 | GTL430 | 44.585 | SHELL |
烷基萘基础油 | NA-LUBE KR-015 | 45 | KING |
疏水剂 | 聚异丁烯 | 5 | DAELIM |
油性剂 | 聚酯 | 1 | Italmatch |
抗氧剂1 | 辛基丁基二苯胺 | 0.5 | BASF |
抗氧剂2 | 二叔丁基苯酚 | 0.5 | BASF |
极压抗磨剂 | 丁基三苯基硫代磷酸酯 | 3 | BASF |
腐蚀抑制剂 | 烷基化苯三唑 | 0.005 | Vanderbilt |
防锈剂 | 十二烯基丁二酸 | 0.2 | Vanderbilt |
游离水捕捉剂 | 烷基酚聚氧乙烯醚 | 0.1 | DOW |
破乳剂 | 环氧乙烷环氧丙烷共聚物 | 0.1 | Lubrizol |
消泡剂 | 高分子有机硅氧烷 | 0.01 | Lubrizol |
样品成分 | 原料名称 | 含量(kg) | 生产商 |
天然气合成油 | GTL420 | 26.25 | SHELL |
烷基萘基础油 | NA-LUBE KR-023 | 60 | KING |
疏水剂 | 聚异丁烯 | 7.5 | DAELIM |
油性剂 | 脂肪酸酯 | 2 | CRODA |
抗氧剂1 | 二异辛基二苯胺 | 1 | BASF |
抗氧剂2 | 液态高分子苯酚 | 1 | BASF |
极压抗磨剂 | 三苯基亚磷酸酯 | 1.5 | BASF |
腐蚀抑制剂 | 烷基化苯三唑 | 0.1 | Vanderbilt |
防锈剂 | 磷酸胺混合液 | 0.1 | Vanderbilt |
游离水捕捉剂 | 烷基酚聚氧乙烯醚 | 0.5 | DOW |
破乳剂 | 环氧乙烷环氧丙烷共聚物 | 0.03 | Lubrizol |
消泡剂 | 高分子有机硅氧烷 | 0.02 | Lubrizol |
样品成分 | 原料名称 | 含量(kg) | 生产商 |
天然气合成油 | GTL430 | 56.945 | SHELL |
烷基萘基础油 | NA-LUBE KR-023 | 25 | KING |
疏水剂 | 聚异丁烯 | 10 | DAELIM |
油性剂 | 脂肪酸酯 | 3 | CRODA |
抗氧剂1 | 辛基丁基二苯胺 | 2 | BASF |
抗氧剂2 | 液态高分子苯酚 | 2 | BASF |
极压抗磨剂 | 丁基三苯基硫代磷酸酯 | 0.5 | BASF |
腐蚀抑制剂 | 烷基化苯三唑 | 0.2 | Vanderbilt |
防锈剂 | 异构壬基苯氧基乙酸 | 0.005 | Vanderbilt |
游离水捕捉剂 | 烷基酚聚氧乙烯醚 | 0.25 | DOW |
破乳剂 | 环氧乙烷环氧丙烷共聚物 | 0.05 | Lubrizol |
消泡剂 | 高分子有机硅氧烷 | 0.05 | Lubrizol |
序号 | 性能指标 | 方法依据 |
1 | 运动黏度,40℃ | GB/T 265-88 |
2 | 闪点,℃ | GB/T 3536-2008 |
3 | 蒸发损失,120℃,3h | 参考NOACK蒸发损失SH/T0059-1996 |
4 | 蒸发损失,200℃,3h | 参考NOACK蒸发损失SH/T0059-1996 |
5 | 抗乳化,82℃,40-37-3ml | GB/T 7305-2003 |
6 | 总酸值(以氢氧化钾计)/(mg·g<sup>-1</sup>) | GB/T 7304-2014 |
7 | 水解安定性 | ASTM D2619 |
8 | 空气释放性能,50℃,min | SH/T 0308-2004 |
9 | 泡沫倾向性/泡沫稳定性 | GB/T 12579-2002 |
10 | 旋转氧弹,(150℃,621kPa,水,铜)min | SH/T 0193-2008 |
11 | 差式扫描热分析(180℃,3.45MPa),min | PDSC |
12 | 氧化腐蚀试验后总酸值(以氢氧化钾计)/(mg·g<sup>-1</sup>) | GB/T 7304-2014电位滴定 |
13 | 铜片腐蚀,100℃,3h | GB/T 5096-2017 |
14 | 液相锈蚀,24h | GB/T 11143-2008 |
Claims (7)
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